Crystallography Open Database

Information card for entry 7250292

Preview

Coordinates	7250292.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H19 Cl3 O8
Calculated formula	C12 H19 Cl3 O8
Title of publication	Intermittent Ultrasound‑Assisted Anti‑Solvent Crystallization for Sucralose Production with Ultra-low Aspect Ratio and Larger Crystal Size
Authors of publication	Zhou, Dongyu; Li, Yongshang; Jie, Huimig; Lei, Jiayan; Chen, Zi'ang; Chen, Xiao-Ping; Cui, Can; Luo, Huadong; Chen, Jingjing; Li, Hao-Hong; Zheng, Huidong
Journal of publication	CrystEngComm
Year of publication	2025
a	7.3167 ± 0.0006 Å
b	12.0459 ± 0.001 Å
c	18.1855 ± 0.0015 Å
α	90°
β	90°
γ	90°
Cell volume	1602.8 ± 0.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0864
Residual factor for significantly intense reflections	0.0671
Weighted residual factors for significantly intense reflections	0.1591
Weighted residual factors for all reflections included in the refinement	0.1833
Goodness-of-fit parameter for all reflections included in the refinement	1.12
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
299357 (current)	2025-04-23	cif/ Adding structures of 7250292, 7250293, 7250294, 7250295 via cif-deposit CGI script.	7250292.cif