Crystallography Open Database

Information card for entry 7702918

Preview

Coordinates	7702918.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C140 H161 Gd6 N13 Na2 O70
Calculated formula	C138 H127 Gd6 N13 Na2 O55
Title of publication	Synthesis, structures and magnetic properties of a family of nitrate-bridged octanuclear [Na2Ln6] (Ln = Dy, Tb, Gd, Sm) complexes.
Authors of publication	She, Shixiong; Chen, Yanmei; Zaworotko, Michael J.; Liu, Wei; Cao, Yanyuan; Wu, Jian; Li, Yahong
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	29
Pages of publication	10433 - 10438
a	28.6753 ± 0.0015 Å
b	19.3572 ± 0.001 Å
c	30.6841 ± 0.0016 Å
α	90°
β	104.296 ± 0.003°
γ	90°
Cell volume	16504.5 ± 1.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0695
Residual factor for significantly intense reflections	0.0511
Weighted residual factors for significantly intense reflections	0.1532
Weighted residual factors for all reflections included in the refinement	0.1663
Goodness-of-fit parameter for all reflections included in the refinement	1.061
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
244809 (current)	2019-11-29	cif/ Adding structures of 7702916, 7702917, 7702918, 7702919 via cif-deposit CGI script.	7702918.cif