Crystallography Open Database

Information card for entry 7702969

Preview

Coordinates	7702969.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C49 H58 Ge O2 P2 Si
Calculated formula	C45 H48 Ge O P2 Si
Title of publication	Avenue to phosphaalkenes from Ph<sub>3</sub>GePCO.
Authors of publication	Szkop, Kevin M.; Jupp, Andrew R.; Razumkov, Hlib; Stephan, Douglas W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	3
Pages of publication	885 - 890
a	12.244 ± 0.009 Å
b	13.196 ± 0.009 Å
c	16.49 ± 0.012 Å
α	109.25 ± 0.03°
β	93.811 ± 0.019°
γ	105.368 ± 0.013°
Cell volume	2391 ± 3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1211
Residual factor for significantly intense reflections	0.0555
Weighted residual factors for significantly intense reflections	0.1058
Weighted residual factors for all reflections included in the refinement	0.1201
Goodness-of-fit parameter for all reflections included in the refinement	0.937
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
247744 (current)	2020-02-04	cif/ Updating files of 7702969, 7702970 Original log message: Adding full bibliography for 7702969--7702970.cif.	7702969.cif
245233	2019-12-17	cif/ Adding structures of 7702969, 7702970 via cif-deposit CGI script.	7702969.cif