Crystallography Open Database

Information card for entry 7702996

Preview

Coordinates	7702996.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C35.5 H66 Co N4 O7.5 S2 Si2
Calculated formula	C35.5 H66 Co N4 O7.5 S2 Si2
Title of publication	Structural, magnetic and spectral properties of tetrahedral cobalt(ii) silanethiolates: a variety of structures and manifestation of field-induced slow magnetic relaxation.
Authors of publication	Kowalkowska-Zedler, D; Dołęga, A; Nedelko, N.; Łyszczek, R; Aleshkevych, P.; Demchenko, I.; Łuczak, J; Slawska-Waniewska, A; Pladzyk, A.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	3
Pages of publication	697 - 710
a	9.556 ± 0.009 Å
b	13.484 ± 0.007 Å
c	20.611 ± 0.014 Å
α	99.29 ± 0.05°
β	101.1 ± 0.06°
γ	108.21 ± 0.06°
Cell volume	2405 ± 3 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0863
Residual factor for significantly intense reflections	0.0664
Weighted residual factors for significantly intense reflections	0.1629
Weighted residual factors for all reflections included in the refinement	0.1766
Goodness-of-fit parameter for all reflections included in the refinement	1.054
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
247747 (current)	2020-02-04	cif/ Updating files of 7702994, 7702995, 7702996, 7702997, 7702998 Original log message: Adding full bibliography for 7702994--7702998.cif.	7702996.cif
245365	2019-12-19	cif/ Adding structures of 7702994, 7702995, 7702996, 7702997, 7702998 via cif-deposit CGI script.	7702996.cif