#------------------------------------------------------------------------------ #$Date: 2020-08-13 04:55:43 +0300 (Thu, 13 Aug 2020) $ #$Revision: 255284 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/51/7705140.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7705140 loop_ _publ_author_name 'Gimeno, Maria Concepcion' 'Johnson, Alice' 'Marzo, Isabel' _publ_section_title ; Heterobimetallic propargyl gold complexes with \p-bound copper or silver with enhanced anticancer activity ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D0DT02113J _journal_year 2020 _chemical_formula_moiety 'C66 H56 Au2 Cu2 N6 P2, 4(C H2 Cl2), 2(H2 O), 2(N O3)' _chemical_formula_sum 'C70 H68 Au2 Cl8 Cu2 N8 O8 P2' _chemical_formula_weight 2015.961 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_Int_Tables_number 2 _audit_creation_date 2020-07-10 _audit_creation_method ; Olex2 1.3-dev (compiled 2020.05.13 svn.r35546bd3 for OlexSys, GUI svn.r5830) ; _audit_update_record ; 2020-07-29 deposited with the CCDC. 2020-08-10 downloaded from the CCDC. ; _cell_angle_alpha 72.656(1) _cell_angle_beta 76.336(1) _cell_angle_gamma 83.163(1) _cell_formula_units_Z 1 _cell_length_a 10.6521(6) _cell_length_b 11.9337(7) _cell_length_c 15.9069(9) _cell_measurement_reflns_used 9932 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 26.44 _cell_measurement_theta_min 2.14 _cell_volume 1872.92(19) _computing_cell_refinement SMART _computing_data_collection SMART _computing_data_reduction SMART _computing_molecular_graphics 'Olex2 1.3-dev (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3-dev (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)' _computing_structure_solution SHELXS _diffrn_ambient_temperature 100.15 _diffrn_detector_area_resol_mean 8.26 _diffrn_measured_fraction_theta_full 0.9968 _diffrn_measured_fraction_theta_max 0.9005 _diffrn_measurement_device_type 'SMART APEX CCD' _diffrn_measurement_method 'w rotations with narrow frames' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0206 _diffrn_reflns_av_unetI/netI 0.0245 _diffrn_reflns_Laue_measured_fraction_full 0.9968 _diffrn_reflns_Laue_measured_fraction_max 0.9005 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 22593 _diffrn_reflns_point_group_measured_fraction_full 0.9968 _diffrn_reflns_point_group_measured_fraction_max 0.9005 _diffrn_reflns_theta_full 25.2417 _diffrn_reflns_theta_max 28.68 _diffrn_reflns_theta_min 1.79 _exptl_absorpt_coefficient_mu 4.852 _exptl_absorpt_correction_T_max 0.4437 _exptl_absorpt_correction_T_min 0.329 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.787 _exptl_crystal_description prism _exptl_crystal_F_000 989.639 _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.24 _exptl_crystal_size_min 0.2 _refine_diff_density_max 2.2178 _refine_diff_density_min -0.7914 _refine_diff_density_rms 0.1087 _refine_ls_d_res_high 0.7406 _refine_ls_d_res_low 11.3754 _refine_ls_goodness_of_fit_ref 1.0513 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_constraints 66 _refine_ls_number_parameters 538 _refine_ls_number_reflns 8705 _refine_ls_number_restraints 655 _refine_ls_restrained_S_all 1.0115 _refine_ls_R_factor_all 0.0255 _refine_ls_R_factor_gt 0.0224 _refine_ls_shift/su_max 0.0010 _refine_ls_shift/su_mean 0.0000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0332P)^2^+0.9440P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0556 _refine_ls_wR_factor_ref 0.0572 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 14 _reflns_limit_h_min -13 _reflns_limit_k_max 15 _reflns_limit_k_min -14 _reflns_limit_l_max 21 _reflns_limit_l_min 0 _reflns_number_gt 8111 _reflns_number_total 8705 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL con291_0m in P-1 CELL 0.71073 10.6521 11.9337 15.9069 72.656 76.336 83.163 ZERR 1 0.0006 0.0007 0.0009 0.001 0.001 0.001 LATT 1 SFAC C H Au Cl Cu N O P UNIT 70 68 2 8 2 8 8 2 DFIX_1 1.25 N1 O1 N1 O3 DFIX_1 1.24 N1 O2 RIGU_1 N1 O1 O2 O3 RIGU_2 N1 O1 O2 O3 DFIX_2 1.24 N1 O2 SIMU 0.04 0.08 1 SADI_NITR 0.04 O1 O2 O2 O3 O3 O1 SADI_NITR N1 O1 N1 O2 N1 O3 DFIX_2 1.25 N1 O1 N1 O3 FLAT_NITR N1 O1 O2 O3 SADI 0.04 H35b Cl4 H35d Cl4A SADI C35 Cl4 C35A Cl4A SADI 0.04 Cl3 Cl4 Cl3A Cl4A SADI C35 H35b C35A H35d SADI 0.04 H35b Cl3 H35d Cl3A SADI C35 Cl3 C35A Cl3A SADI 0.04 H35a Cl3 H35c Cl3A SADI 0.04 H35a Cl4 H35c Cl4A SADI C35 H35a C35A H35c SADI 0.04 H35a H35b H35c H35d L.S. 20 PLAN 7 SIZE 0.3 0.24 0.2 TEMP -173 CONF LIST 4 BOND MORE -1 BOND $H fmap 2 acta OMIT 0 0 1 OMIT 1 0 0 OMIT -2 2 2 WGHT 0.033194 0.944039 FVAR 0.094984 0.4234 REM REM REM > REM REM > REM > REM REM Au1 3 0.65454 0.88950 0.66965 11.00000 0.01852 0.01832 0.01914 = -0.00378 -0.00149 -0.00323 Cu1 5 0.81546 1.07253 0.46256 11.00000 0.02447 0.01667 0.01789 = -0.00570 -0.00233 -0.00581 P1 8 0.48974 0.83216 0.79044 11.00000 0.01892 0.01916 0.02005 = -0.00581 -0.00120 -0.00308 N1 6 0.65704 1.17925 0.49022 11.00000 0.02690 0.02032 0.02084 = -0.00585 -0.00504 -0.00363 N2 6 0.90404 1.20423 0.50553 11.00000 0.02259 0.02070 0.01912 = -0.00749 -0.00199 -0.00270 N3 6 0.92719 1.15310 0.34302 11.00000 0.02577 0.01689 0.01837 = -0.00426 -0.00491 -0.00304 C1 1 0.79591 0.91724 0.55898 11.00000 0.02454 0.01867 0.02195 = -0.00438 -0.00551 -0.00508 C2 1 0.88586 0.90559 0.49670 11.00000 0.02338 0.01580 0.02159 = -0.00522 -0.00455 -0.00574 C3 1 0.99416 0.84987 0.44319 11.00000 0.02695 0.02291 0.01993 = -0.00931 -0.00377 -0.00370 AFIX 23 H3a 2 1.03240 0.90983 0.38769 11.00000 -1.20000 H3b 2 0.96062 0.78871 0.42504 11.00000 -1.20000 AFIX 0 C4 1 0.54191 1.17832 0.46954 11.00000 0.03521 0.02423 0.03071 = -0.00993 -0.01352 -0.00416 AFIX 43 H4 2 0.53184 1.12254 0.44002 11.00000 -1.20000 AFIX 0 C5 1 0.43757 1.25373 0.48874 11.00000 0.03554 0.02939 0.04594 = -0.01510 -0.02250 0.00352 AFIX 43 H5 2 0.35727 1.24885 0.47415 11.00000 -1.20000 AFIX 0 C6 1 0.45337 1.33652 0.52980 11.00000 0.03705 0.02726 0.04173 = -0.01501 -0.01892 0.01120 AFIX 43 H6 2 0.38390 1.39039 0.54353 11.00000 -1.20000 AFIX 0 C7 1 0.57140 1.34018 0.55072 11.00000 0.03412 0.02525 0.02874 = -0.01177 -0.01245 0.00219 AFIX 43 H7 2 0.58445 1.39775 0.57771 11.00000 -1.20000 AFIX 0 C8 1 0.67068 1.25885 0.53190 11.00000 0.02955 0.02058 0.01904 = -0.00449 -0.00568 -0.00470 C9 1 0.79420 1.24957 0.56423 11.00000 0.02525 0.02889 0.02375 = -0.01393 -0.00356 -0.00172 AFIX 23 H9a 2 0.78331 1.19657 0.62633 11.00000 -1.20000 H9b 2 0.81296 1.32811 0.56581 11.00000 -1.20000 AFIX 0 C10 1 0.95164 1.29425 0.42116 11.00000 0.02996 0.01736 0.02303 = -0.00679 -0.00381 -0.00548 AFIX 23 H10a 2 0.88335 1.35763 0.41071 11.00000 -1.20000 H10b 2 1.02755 1.32919 0.42737 11.00000 -1.20000 AFIX 0 C11 1 0.98955 1.24602 0.34070 11.00000 0.02495 0.01684 0.02026 = -0.00239 -0.00734 -0.00197 C12 1 1.08278 1.29892 0.26577 11.00000 0.02368 0.02175 0.02306 = 0.00125 -0.00660 -0.00501 AFIX 43 H12 2 1.12453 1.36527 0.26520 11.00000 -1.20000 AFIX 0 C13 1 1.11373 1.25404 0.19260 11.00000 0.02240 0.03072 0.01831 = -0.00041 -0.00175 0.00105 AFIX 43 H13 2 1.17738 1.28856 0.14115 11.00000 -1.20000 AFIX 0 C14 1 1.04994 1.15696 0.19540 11.00000 0.02875 0.02815 0.01946 = -0.00808 -0.00505 0.00520 AFIX 43 H14 2 1.07002 1.12391 0.14606 11.00000 -1.20000 AFIX 0 C15 1 0.95737 1.10978 0.27085 11.00000 0.02906 0.02251 0.02041 = -0.00543 -0.00825 0.00160 C16 1 0.54040 0.78955 0.89733 11.00000 0.01756 0.02711 0.02094 = -0.00721 -0.00048 -0.00206 C17 1 0.54950 0.67363 0.94910 11.00000 0.02489 0.02428 0.02698 = -0.00756 -0.00386 -0.00395 AFIX 43 H17 2 0.52068 0.61293 0.93202 11.00000 -1.20000 AFIX 0 C18 1 0.60093 0.64624 1.02615 11.00000 0.03172 0.02608 0.02690 = -0.00514 -0.00449 0.00112 AFIX 43 H18 2 0.60647 0.56682 1.06151 11.00000 -1.20000 AFIX 0 C19 1 0.64381 0.73333 1.05151 11.00000 0.02336 0.03861 0.02225 = -0.01077 -0.00526 -0.00075 AFIX 43 H19 2 0.67978 0.71408 1.10363 11.00000 -1.20000 AFIX 0 C20 1 0.63398 0.84911 1.00033 11.00000 0.03699 0.03454 0.03211 = -0.01481 -0.01025 -0.00885 AFIX 43 H20 2 0.66243 0.90952 1.01793 11.00000 -1.20000 AFIX 0 C21 1 0.58305 0.87753 0.92375 11.00000 0.03620 0.02356 0.03077 = -0.00676 -0.00853 -0.00580 AFIX 43 H21 2 0.57706 0.95720 0.88899 11.00000 -1.20000 AFIX 0 C22 1 0.35702 0.94105 0.80093 11.00000 0.01714 0.02770 0.03013 = -0.01359 -0.00480 -0.00243 C23 1 0.35077 1.03949 0.72853 11.00000 0.02102 0.02436 0.03658 = -0.00988 -0.00623 -0.00286 AFIX 43 H23 2 0.41317 1.04746 0.67374 11.00000 -1.20000 AFIX 0 C24 1 0.25265 1.12701 0.73615 11.00000 0.02644 0.02556 0.05637 = -0.01380 -0.01334 0.00002 AFIX 43 H24 2 0.24794 1.19425 0.68643 11.00000 -1.20000 AFIX 0 C25 1 0.16274 1.11558 0.81594 11.00000 0.02330 0.03962 0.06211 = -0.03156 -0.01246 0.00655 AFIX 43 H25 2 0.09681 1.17561 0.82136 11.00000 -1.20000 AFIX 0 C26 1 0.16804 1.01748 0.88786 11.00000 0.02379 0.05805 0.04310 = -0.03033 -0.00149 0.00280 AFIX 43 H26 2 0.10500 1.00983 0.94232 11.00000 -1.20000 AFIX 0 C27 1 0.26502 0.92959 0.88130 11.00000 0.02297 0.04165 0.03157 = -0.01631 -0.00506 -0.00052 AFIX 43 H27 2 0.26863 0.86227 0.93113 11.00000 -1.20000 AFIX 0 C28 1 0.42675 0.70281 0.78044 11.00000 0.03433 0.02292 0.01675 = -0.00380 -0.00448 -0.00809 C29 1 0.29586 0.68361 0.80069 11.00000 0.03418 0.02520 0.05340 = -0.00302 -0.02351 -0.00433 AFIX 43 H29 2 0.23416 0.73521 0.82620 11.00000 -1.20000 AFIX 0 C30 1 0.25627 0.58724 0.78296 11.00000 0.06204 0.02865 0.07943 = 0.00515 -0.05067 -0.01528 AFIX 43 H30 2 0.16656 0.57448 0.79561 11.00000 -1.20000 AFIX 0 C31 1 0.34307 0.51119 0.74801 11.00000 0.11002 0.02567 0.03323 = -0.00004 -0.03415 -0.02437 AFIX 43 H31 2 0.31402 0.44671 0.73563 11.00000 -1.20000 AFIX 0 C32 1 0.47369 0.52813 0.73060 11.00000 0.10283 0.03322 0.03370 = -0.01860 0.02124 -0.02752 AFIX 43 H32 2 0.53491 0.47375 0.70806 11.00000 -1.20000 AFIX 0 C33 1 0.51560 0.62442 0.74597 11.00000 0.05611 0.03032 0.04022 = -0.01786 0.02064 -0.01756 AFIX 43 H33 2 0.60547 0.63673 0.73284 11.00000 -1.20000 AFIX 0 C34 1 0.68193 1.23756 0.82334 11.00000 0.02721 0.04130 0.06879 = -0.02908 -0.01108 0.00075 AFIX 23 H34a 2 0.72087 1.31031 0.78145 11.00000 -1.20000 H34b 2 0.63350 1.25630 0.87920 11.00000 -1.20000 AFIX 0 PART 1 C35 1 0.91378 0.43110 0.91890 21.00000 0.05444 0.02260 0.02861 = 0.00631 -0.01726 -0.00590 AFIX 23 H35a 2 0.94676 0.43148 0.85519 21.00000 -1.20000 H35b 2 0.92059 0.51105 0.92339 21.00000 -1.20000 AFIX 0 PART 0 Cl1 4 0.57338 1.19097 0.77369 11.00000 0.03425 0.03556 0.02948 = -0.01125 -0.00182 -0.00708 Cl2 4 0.80557 1.13083 0.84927 11.00000 0.04210 0.04176 0.09447 = -0.01384 -0.02716 0.00057 PART 1 Cl3 4 0.74876 0.39507 0.95233 21.00000 0.03296 0.04254 0.05709 = -0.02283 -0.00862 -0.00349 Cl4 4 1.00865 0.33119 0.98586 21.00000 0.06506 0.06090 0.06137 = -0.00250 -0.04162 0.00091 AFIX 6 O1B 7 0.76489 0.54109 0.58526 10.80000 0.03566 0.04828 0.08023 = -0.03040 -0.01723 0.00003 H1Ba 2 0.81127 0.50012 0.62332 10.80000 -1.50000 H1Bb 2 0.82090 0.56666 0.53522 10.80000 -1.50000 AFIX 0 PART 2 C35A 1 0.93966 0.42347 0.90295 -21.00000 0.02764 0.05698 0.03137 = -0.00758 -0.00579 -0.00261 H35c 2 0.97638 0.40734 0.84492 -21.00000 0.05674 H35d 2 0.96502 0.49928 0.90675 -21.00000 0.06810 Cl3A 4 0.76994 0.42587 0.92918 -21.00000 0.02976 0.04361 0.05235 = -0.02177 -0.00881 0.00370 Cl4A 4 1.00465 0.31075 0.98359 -21.00000 0.03989 0.07192 0.03650 = 0.00226 -0.01172 0.01437 AFIX 6 O6 7 0.79273 0.55012 0.53803 10.20000 0.06254 0.05004 0.11263 = -0.02781 -0.05936 0.01320 H6a 2 0.82558 0.56710 0.48046 10.20000 -1.50000 H6b 2 0.84817 0.49863 0.56246 10.20000 -1.50000 AFIX 0 RESI NITR 1 PART 1 N1 6 1.03159 1.40626 0.66752 10.80000 0.06100 0.01650 0.04258 = -0.00280 -0.02431 -0.01040 O1 7 1.12120 1.40023 0.70510 10.80000 0.07454 0.06054 0.08268 = -0.03092 -0.05024 0.01405 O2 7 1.05228 1.40419 0.58721 10.80000 0.08397 0.04373 0.04558 = -0.01863 -0.01344 -0.01815 O3 7 0.91712 1.41893 0.70832 10.80000 0.06575 0.04943 0.03983 = -0.00532 -0.01782 -0.01757 RESI NITR 2 PART 2 N1 6 0.96858 1.41028 0.68882 10.20000 0.05702 0.06956 0.07605 = -0.02889 -0.02585 0.00247 O1 7 1.05266 1.40937 0.73204 10.20000 0.04505 0.09589 0.06663 = -0.03213 -0.01185 -0.00405 O2 7 0.85679 1.44541 0.71606 10.20000 0.05701 0.02484 0.07242 = -0.00743 -0.02126 -0.00904 O3 7 1.00270 1.40164 0.60924 10.20000 0.09137 0.07863 0.07896 = -0.03465 -0.02313 -0.00673 HKLF 4 END Q1 1 0.666667 0.888889 0.611111 11 0.05 2.22 Q2 1 0.638889 0.888889 0.722222 11 0.05 2.2 Q3 1 0.722222 0.888889 0.666667 11 0.05 1.11 Q4 1 0.638889 0.977778 0.648148 11 0.05 1.07 Q5 1 0.638889 0.822222 0.685185 11 0.05 1 Q6 1 0.916667 1.044444 0.277778 11 0.05 0.95 Q7 1 0.833333 1.066667 0.407407 11 0.05 0.71 REM The information below was added by Olex2. REM REM R1 = 0.0224 for 8111 Fo > 4sig(Fo) and 0.0255 for all 8705 data REM 538 parameters refined using 655 restraints REM Highest difference peak 2.2178, deepest hole -0.7914 REM Mean Shift 0.0000, Max Shift 0.0010. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0255 REM R1_gt = 0.0224 REM wR_ref = 0.0572 REM GOOF = 1.0513 REM Shift_max = 0.0010 REM Shift_mean = 0.0000 REM Reflections_all = 8705 REM Reflections_gt = 8111 REM Parameters = 538 REM Hole = -0.7914 REM Peak = 2.2178 REM Flack = n/a ; _cod_data_source_file d0dt02113j2.cif _cod_data_source_block con291_0m _cod_database_code 7705140 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All O(H,H) groups 2. Restrained distances N1_1-O1_1 = N1_1-O3_1 1.25 with sigma of 0.02 N1_1-O2_1 1.24 with sigma of 0.02 N1_2-O2_2 1.24 with sigma of 0.02 N1_2-O1_2 = N1_2-O3_2 1.25 with sigma of 0.02 O1_1-O2_1 \\sim O2_1-O3_1 \\sim O3_1-O1_1 O1_2-O2_2 \\sim O2_2-O3_2 \\sim O3_2-O1_2 with sigma of 0.04 N1_1-O1_1 \\sim N1_1-O2_1 \\sim N1_1-O3_1 N1_2-O1_2 \\sim N1_2-O2_2 \\sim N1_2-O3_2 with sigma of 0.02 H35b-Cl4 \\sim H35d-Cl4A with sigma of 0.04 C35-Cl4 \\sim C35A-Cl4A with sigma of 0.02 Cl3-Cl4 \\sim Cl3A-Cl4A with sigma of 0.04 C35-H35b \\sim C35A-H35d with sigma of 0.02 H35b-Cl3 \\sim H35d-Cl3A with sigma of 0.04 C35-Cl3 \\sim C35A-Cl3A with sigma of 0.02 H35a-Cl3 \\sim H35c-Cl3A with sigma of 0.04 H35a-Cl4 \\sim H35c-Cl4A with sigma of 0.04 C35-H35a \\sim C35A-H35c with sigma of 0.02 H35a-H35b \\sim H35c-H35d with sigma of 0.04 3. Restrained planarity N1_1, O1_1, O2_1, O3_1 N1_2, O1_2, O2_2, O3_2 with sigma of 0.1 4. Uiso/Uaniso restraints and constraints All non-hydrogen atoms have similar U: within 1A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 1A 5. Rigid body (RIGU) restrains N1_1, O1_1, O2_1, O3_1 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 N1_2, O1_2, O2_2, O3_2 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 6. Others Sof(C35A)=Sof(H35c)=Sof(H35d)=Sof(Cl3A)=Sof(Cl4A)=1-FVAR(1) Sof(C35)=Sof(H35a)=Sof(H35b)=Sof(Cl3)=Sof(Cl4)=FVAR(1) Fixed Sof: O1B(0.8) H1Ba(0.8) H1Bb(0.8) O6(0.2) H6a(0.2) H6b(0.2) N1(0.8) O1(0.8) O2(0.8) O3(0.8) N1(0.2) O1(0.2) O2(0.2) O3(0.2) 7.a Free rotating group: O1B(H1Ba,H1Bb), O6(H6a,H6b) 7.b Secondary CH2 refined with riding coordinates: C3(H3a,H3b), C9(H9a,H9b), C10(H10a,H10b), C34(H34a,H34b), C35(H35a,H35b) 7.c Aromatic/amide H refined with riding coordinates: C4(H4), C5(H5), C6(H6), C7(H7), C12(H12), C13(H13), C14(H14), C17(H17), C18(H18), C19(H19), C20(H20), C21(H21), C23(H23), C24(H24), C25(H25), C26(H26), C27(H27), C29(H29), C30(H30), C31(H31), C32(H32), C33(H33) ; _iucr_refine_fcf_details ; data_con291_0m_CCDC1 _computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_Int_Tables_number 2 _cell_length_a 10.6521(6) _cell_length_b 11.9337(7) _cell_length_c 15.9069(9) _cell_angle_alpha 72.656(1) _cell_angle_beta 76.336(1) _cell_angle_gamma 83.163(1) _cell_volume 1872.92(19) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -13 -4 1 1949.990 1929.760 94.216 13.800 o -13 -3 1 1510.150 1566.190 86.457 17.857 o -13 -3 2 601.201 594.332 34.409 95.699 o -13 -3 3 19.060 25.806 27.159 270.672 o -13 -2 1 1133.800 1155.230 55.636 36.605 o -13 -2 2 1899.780 1941.400 68.692 19.435 o -13 -2 3 587.938 620.284 36.332 90.007 o -13 -1 1 158.638 178.478 34.086 152.262 o -13 -1 2 1692.190 1731.470 91.445 15.576 o -13 -1 3 1184.650 1170.930 58.583 33.754 o -13 0 1 787.813 807.067 70.385 32.074 o -13 0 2 653.211 653.204 50.335 56.689 o -13 0 3 684.656 679.412 48.736 58.078 o -13 1 1 1619.570 1505.230 98.649 14.680 o -13 1 2 258.238 130.793 50.987 71.895 o -13 2 1 2629.890 2834.220 133.010 7.263 o -13 3 1 2188.140 2511.670 114.167 9.769 o -12 -6 1 1944.930 2001.800 96.432 13.325 o -12 -5 1 1827.590 1839.970 89.782 15.217 o -12 -5 2 1620.540 1526.290 84.240 18.036 o -12 -5 3 361.883 336.959 50.987 66.826 o -12 -5 4 1132.650 1151.780 54.555 37.445 o -12 -4 1 232.863 236.093 41.011 104.548 o -12 -4 2 2222.480 2344.510 57.825 18.450 o -12 -4 3 2195.650 2168.820 112.519 10.265 o -12 -4 4 24.913 -7.346 22.637 388.400 o -12 -3 1 284.132 245.328 24.974 213.624 o -12 -3 2 1273.780 1291.720 46.079 39.960 o -12 -3 3 1926.510 2058.370 60.359 20.982 o -12 -3 4 792.973 851.916 68.034 33.517 o -12 -3 5 172.531 185.825 71.493 38.631 o -12 -2 1 1405.690 1492.510 46.611 35.418 o -12 -2 2 65.594 67.743 21.080 400.999 o -12 -2 3 1636.950 1760.820 51.665 27.897 o -12 -2 4 2433.540 2439.210 61.760 16.226 o -12 -2 5 1017.020 1007.460 42.966 52.148 o -12 -1 1 1129.060 1208.540 55.661 36.259 o -12 -1 2 1615.550 1657.570 49.756 29.573 o -12 -1 3 628.636 658.002 36.346 86.494 o -12 -1 4 2869.550 2923.480 68.312 12.379 o -12 -1 5 3107.960 3145.190 76.144 10.540 o -12 0 1 545.303 596.329 65.397 39.806 o -12 0 2 2410.480 2410.370 109.733 9.906 o -12 0 3 164.401 170.628 34.231 150.972 o -12 0 4 929.470 893.834 42.200 57.411 o -12 0 5 2904.460 3143.250 72.856 11.442 o -12 0 6 1427.360 1279.110 83.131 19.919 o -12 1 1 27.531 18.463 26.177 289.451 o -12 1 2 781.606 772.567 75.372 28.972 o -12 1 3 2049.040 2142.570 111.950 10.653 o -12 1 4 35.833 23.866 30.069 219.434 o -12 1 5 1042.110 1059.430 78.144 24.711 o -12 2 1 2029.180 2245.390 74.802 16.493 o -12 2 2 173.089 155.020 32.020 169.093 o -12 2 3 1774.440 1821.130 105.300 12.585 o -12 2 4 1582.020 1540.700 98.649 14.742 o -12 2 5 139.076 105.441 35.263 148.487 o -12 3 1 1914.150 2072.660 141.877 7.819 o -12 3 2 380.155 358.157 39.765 98.370 o -12 3 3 1975.990 2165.340 75.909 16.729 o -12 3 4 1721.950 1684.790 106.408 12.703 o -12 4 1 1223.480 1314.120 171.251 6.365 o -12 4 2 1111.430 1154.860 59.319 34.329 o -12 4 3 5.426 -20.506 28.216 256.689 o -12 4 4 1118.020 1058.540 78.698 23.979 o -12 5 1 85.828 134.717 49.325 80.776 o -12 5 2 1185.510 1406.580 89.782 18.664 o -12 5 3 1594.600 1848.840 101.974 13.599 o -12 5 4 194.377 219.467 53.204 66.910 o -11 -9 1 1723.130 1471.980 106.408 12.964 o -11 -8 1 156.112 142.499 33.457 159.375 o -11 -7 1 323.083 334.742 54.312 60.787 o -11 -7 2 909.950 835.747 66.505 33.524 o -11 -6 1 1536.680 1401.040 77.589 20.775 o -11 -6 2 483.544 478.836 52.096 59.925 o -11 -6 3 341.926 283.755 46.553 79.354 o -11 -6 4 601.971 577.204 63.734 40.958 o -11 -6 5 111.330 144.094 42.120 107.682 o -11 -5 1 2355.420 2332.110 98.649 11.389 o -11 -5 2 214.958 212.445 22.343 272.972 o -11 -5 3 99.057 131.452 43.001 104.387 o -11 -5 4 1028.430 1038.730 39.823 54.976 o -11 -5 5 382.395 401.084 37.621 105.324 o -11 -5 6 2399.570 2551.580 118.601 8.926 o -11 -4 1 3755.640 3838.730 72.160 8.360 o -11 -4 2 3465.130 3465.870 73.188 9.389 o -11 -4 3 226.753 206.321 28.514 191.103 o -11 -4 4 957.325 916.137 38.055 61.818 o -11 -4 5 1178.430 1042.360 40.513 49.748 o -11 -4 6 189.347 184.189 24.734 247.961 o -11 -3 1 1060.830 1085.820 43.791 49.024 o -11 -3 2 5218.920 5375.410 92.118 4.656 o -11 -3 3 854.915 862.890 41.406 61.552 o -11 -3 4 177.339 201.710 23.232 272.659 o -11 -3 5 460.424 439.263 31.532 124.479 o -11 -3 6 672.379 637.681 35.917 85.693 o -11 -3 7 344.178 291.318 34.060 129.414 o -11 -2 1 407.270 402.434 28.067 151.798 o -11 -2 2 2985.060 2955.140 63.632 12.356 o -11 -2 3 1434.770 1407.240 44.193 37.059 o -11 -2 4 479.337 464.833 30.387 126.738 o -11 -2 5 367.422 341.753 50.337 68.082 o -11 -2 6 1328.780 1345.840 55.334 32.661 o -11 -2 7 35.793 7.888 20.084 478.261 o -11 -1 1 3487.150 3630.690 71.205 9.255 o -11 -1 2 156.584 146.815 22.945 294.414 o -11 -1 3 2357.050 2404.710 58.090 17.365 o -11 -1 4 1645.990 1711.240 75.019 19.990 o -11 -1 5 170.950 144.711 24.119 268.697 o -11 -1 6 1072.390 1074.160 41.887 50.852 o -11 -1 7 769.523 757.530 39.886 69.354 o -11 0 1 4952.000 5243.770 114.372 4.468 o -11 0 2 4054.660 4069.100 98.755 6.466 o -11 0 3 242.405 194.917 25.187 226.824 o -11 0 4 2068.830 2045.640 55.448 21.156 o -11 0 5 31.765 57.180 20.431 448.896 o -11 0 6 540.742 523.470 34.394 102.446 o -11 0 7 1861.570 1824.820 54.993 24.037 o -11 1 1 1606.750 1736.150 61.074 24.766 o -11 1 2 6864.750 7152.800 190.648 2.131 o -11 1 3 662.293 602.763 43.782 68.913 o -11 1 4 722.929 676.089 36.639 80.126 o -11 1 5 1287.410 1227.420 55.813 33.748 o -11 1 6 68.787 29.207 21.259 404.160 o -11 1 7 1245.360 1327.350 59.702 31.332 o -11 1 8 3461.840 3548.050 140.769 5.617 o -11 2 1 24.632 21.703 24.259 335.658 o -11 2 2 3220.360 3510.570 91.998 8.653 o -11 2 3 5836.000 5741.900 127.294 3.490 o -11 2 4 21.405 -38.795 35.469 161.379 o -11 2 5 1986.860 1970.520 98.095 12.974 o -11 2 6 590.418 552.637 35.300 95.041 o -11 2 7 256.892 274.492 29.593 171.046 o -11 2 8 2019.100 2115.970 107.517 11.318 o -11 3 1 2140.490 2230.560 72.903 16.347 o -11 3 2 787.785 871.243 60.409 39.835 o -11 3 3 4768.940 4838.730 115.270 4.760 o -11 3 4 1367.190 1240.700 57.125 31.826 o -11 3 5 215.635 152.962 48.770 78.810 o -11 3 6 1511.850 1362.250 94.216 16.273 o -11 3 7 32.142 95.513 24.655 310.361 o -11 3 8 248.705 212.816 48.770 77.047 o -11 4 1 2698.450 2765.210 83.925 11.551 o -11 4 2 170.886 196.054 33.925 151.401 o -11 4 3 651.280 635.503 50.987 55.932 o -11 4 4 4242.950 4229.000 233.876 2.615 o -11 4 5 60.410 39.962 29.009 229.239 o -11 4 6 521.630 494.762 73.156 33.506 o -11 5 1 595.338 622.561 47.297 63.935 o -11 5 2 4098.350 4323.890 112.223 5.745 o -11 5 3 45.250 56.122 39.903 125.066 o -11 5 4 2508.070 2634.140 130.793 7.693 o -11 5 5 2115.740 2077.500 76.174 16.210 o -11 5 6 98.041 54.902 30.951 196.458 o -11 5 7 609.656 606.305 67.614 36.952 o -11 6 1 264.628 184.746 35.243 134.212 o -11 6 2 2843.550 2849.870 268.791 2.447 o -11 6 3 1246.930 1324.920 65.413 28.246 o -11 6 4 1226.160 1346.760 111.950 13.245 o -11 6 5 2777.960 2815.380 124.143 7.708 o -11 6 6 136.391 202.840 54.312 65.629 o -11 6 7 276.858 187.323 53.204 65.548 o -11 7 1 3.712 38.472 57.638 61.507 o -11 7 2 1463.070 1591.860 137.444 8.997 o -11 7 3 2872.340 2922.900 130.793 7.069 o -11 7 4 563.032 542.016 69.830 35.744 o -10 -10 1 266.419 180.672 55.421 61.113 o -10 -9 1 442.696 376.497 41.451 88.838 o -10 -9 2 1259.150 1243.170 63.586 29.492 o -10 -9 3 2898.220 2966.130 146.311 6.115 o -10 -8 1 2426.790 2429.030 82.117 13.217 o -10 -8 2 19.383 -21.947 42.674 111.940 o -10 -8 3 1281.440 1296.850 97.541 16.350 o -10 -7 1 3268.470 3302.150 101.420 8.133 o -10 -7 2 3139.810 3254.730 229.997 3.062 o -10 -7 3 143.168 158.504 38.795 122.953 o -10 -7 4 1985.830 2001.990 142.432 7.734 o -10 -7 5 3263.020 3251.750 89.739 8.988 o -10 -7 6 57.885 23.277 33.252 178.180 o -10 -6 1 2545.660 2666.860 94.770 10.922 o -10 -6 2 6113.550 6159.670 234.914 2.005 o -10 -6 3 1091.520 1113.770 75.927 25.235 o -10 -6 4 180.269 160.116 31.036 176.891 o -10 -6 5 1987.660 1991.720 138.552 8.070 o -10 -6 6 1241.030 1180.350 88.673 19.257 o -10 -6 7 7.139 48.770 35.469 160.542 o -10 -5 1 29.011 24.189 14.497 866.446 o -10 -5 2 2576.830 2661.930 61.802 14.919 o -10 -5 3 4507.560 4370.280 78.998 6.337 o -10 -5 4 893.042 861.578 35.627 69.321 o -10 -5 5 411.736 376.555 57.638 52.950 o -10 -5 6 2908.320 2858.380 154.624 5.725 o -10 -5 7 544.625 524.589 41.794 79.751 o -10 -4 1 3009.130 3037.760 60.492 12.402 o -10 -4 2 534.935 530.754 28.232 127.129 o -10 -4 3 5444.100 5372.060 90.867 4.487 o -10 -4 4 4957.820 4863.530 111.769 4.677 o -10 -4 5 138.272 140.564 21.375 336.765 o -10 -4 6 566.767 550.808 31.513 109.729 o -10 -4 7 1480.350 1292.770 58.355 29.493 o -10 -4 8 9.382 48.770 38.795 134.420 o -10 -3 1 3460.680 3466.520 65.896 9.857 o -10 -3 2 966.463 937.863 35.497 64.694 o -10 -3 3 5081.480 4947.310 85.779 5.123 o -10 -3 4 3985.630 3976.430 75.516 7.619 o -10 -3 5 2861.190 2809.760 62.593 13.228 o -10 -3 6 89.757 87.411 24.261 301.247 o -10 -3 7 1234.500 1173.330 72.776 25.443 o -10 -3 8 1517.790 1471.200 48.462 32.820 o -10 -2 1 1417.680 1508.020 57.089 29.592 o -10 -2 2 3062.810 3082.430 62.620 11.933 o -10 -2 3 16.976 11.993 26.434 287.660 o -10 -2 4 1722.620 1641.780 46.563 29.586 o -10 -2 5 4856.840 5059.670 105.488 4.829 o -10 -2 6 984.806 1011.880 39.581 57.118 o -10 -2 7 556.912 562.344 33.626 102.510 o -10 -2 8 2487.910 2391.120 86.937 12.423 o -10 -2 9 140.769 138.813 24.370 274.450 o -10 -1 1 435.607 417.743 32.350 123.971 o -10 -1 2 3050.850 2985.780 61.421 12.258 o -10 -1 3 5373.850 5407.880 91.689 4.516 o -10 -1 4 68.349 56.130 19.688 453.196 o -10 -1 5 4222.150 4414.560 82.203 6.611 o -10 -1 6 3710.210 3624.290 73.471 8.621 o -10 -1 7 17.723 7.927 24.780 326.852 o -10 -1 8 250.826 217.672 31.712 158.444 o -10 -1 9 917.697 848.612 40.637 60.759 o -10 0 1 3327.170 3531.430 67.963 9.999 o -10 0 2 679.813 736.774 32.733 90.444 o -10 0 3 3881.270 3967.590 154.624 4.618 o -10 0 4 548.100 610.946 32.331 105.831 o -10 0 5 2420.920 2545.510 59.691 16.329 o -10 0 6 1850.160 1940.560 52.772 24.273 o -10 0 7 2698.970 2585.890 62.343 14.450 o -10 0 8 77.673 54.480 21.145 395.796 o -10 0 9 1058.700 1054.250 52.808 40.898 o -10 1 1 2859.340 2874.870 60.248 13.349 o -10 1 2 16.782 26.909 16.366 714.338 o -10 1 3 1805.990 1958.090 49.945 25.509 o -10 1 4 2139.170 2137.960 111.396 10.542 o -10 1 5 456.489 424.037 34.862 110.644 o -10 1 6 1605.320 1520.540 48.047 31.392 o -10 1 7 2935.290 3078.960 69.247 11.784 o -10 1 8 1208.570 1199.590 45.198 42.915 o -10 1 9 400.187 419.666 32.969 124.152 o -10 1 10 1900.680 1928.650 103.083 12.477 o -10 2 1 655.325 661.735 110.842 15.336 o -10 2 2 465.977 532.089 37.231 97.304 o -10 2 3 4.382 -11.986 16.614 736.188 o -10 2 4 3907.100 4157.210 80.551 7.382 o -10 2 5 5559.290 5450.140 123.129 3.802 o -10 2 6 404.416 328.147 28.694 153.231 o -10 2 7 1255.110 1327.720 47.088 39.255 o -10 2 8 2248.440 2104.660 57.971 19.050 o -10 2 9 7.759 5.271 22.055 416.284 o -10 2 10 304.903 213.925 54.312 62.342 o -10 3 1 173.885 205.976 30.297 181.677 o -10 3 2 1610.240 1535.190 69.276 22.642 o -10 3 3 1477.630 1433.580 56.934 29.400 o -10 3 4 1362.240 1367.340 57.638 30.819 o -10 3 5 6712.260 6898.150 127.122 2.807 o -10 3 6 1104.230 1130.730 43.426 47.711 o -10 3 7 546.596 525.887 35.049 99.686 o -10 3 8 1040.100 1071.540 44.129 49.392 o -10 3 9 1367.250 1397.440 57.281 30.763 o -10 3 10 119.509 103.083 44.337 98.306 o -10 4 1 695.006 731.918 46.393 60.879 o -10 4 2 106.129 130.204 53.758 68.138 o -10 4 3 2033.250 2123.460 69.751 17.841 o -10 4 4 6.201 19.951 25.864 302.140 o -10 4 5 1943.280 2059.730 70.331 18.413 o -10 4 6 5054.780 5138.530 122.865 4.244 o -10 4 7 854.158 855.751 42.353 60.265 o -10 4 8 373.495 346.871 34.471 122.242 o -10 4 9 1424.890 1345.220 51.039 33.759 o -10 4 10 11.133 60.963 46.553 93.533 o -10 5 1 3468.840 3549.000 95.722 7.916 o -10 5 2 57.415 89.423 27.816 243.435 o -10 5 3 249.004 261.548 35.500 130.731 o -10 5 4 1582.950 1585.130 64.572 24.352 o -10 5 5 3.702 -15.102 25.044 326.014 o -10 5 6 4012.320 4139.360 107.510 6.126 o -10 5 7 3220.460 3096.060 149.082 5.644 o -10 5 8 3.823 -12.343 23.401 373.153 o -10 5 9 528.432 454.451 62.071 44.539 o -10 5 10 311.772 238.310 50.987 69.294 o -10 6 1 1189.520 1227.530 58.984 33.068 o -10 6 2 997.074 1090.630 56.496 38.524 o -10 6 3 14.821 29.808 28.968 239.129 o -10 6 4 1241.470 1299.750 60.647 31.002 o -10 6 5 597.003 620.394 50.433 58.348 o -10 6 6 1047.290 943.518 57.935 37.710 o -10 6 7 3599.690 3776.300 164.046 4.549 o -10 6 8 386.287 362.123 43.086 86.558 o -10 6 9 14.728 35.469 46.553 93.793 o -10 7 1 572.702 718.079 49.654 59.026 o -10 7 2 1619.880 1641.360 68.066 22.588 o -10 7 3 34.617 9.904 29.985 221.936 o -10 7 4 309.637 261.202 69.830 39.106 o -10 7 5 2295.560 2329.120 108.625 10.345 o -10 7 6 33.283 18.843 32.106 193.883 o -10 7 7 753.253 723.118 79.252 27.037 o -10 7 8 1920.490 2032.840 111.950 11.031 o -10 8 1 6.985 -11.084 32.144 197.787 o -10 8 2 278.819 286.738 85.348 26.873 o -10 8 3 1238.740 1347.080 66.734 27.557 o -10 8 4 398.816 393.771 53.204 60.732 o -10 8 5 962.101 1045.770 78.698 25.005 o -9 -11 1 1332.810 1215.930 98.649 16.037 o -9 -10 1 1537.660 1450.240 78.144 20.446 o -9 -10 2 855.669 935.308 89.782 21.047 o -9 -10 3 73.173 159.612 55.421 64.556 o -9 -9 1 29.585 20.657 25.299 308.186 o -9 -9 2 1138.270 1162.520 59.012 34.135 o -9 -9 3 468.733 447.303 42.452 83.002 o -9 -9 4 307.465 302.253 38.648 108.861 o -9 -9 5 2025.290 1953.030 120.818 9.821 o -9 -9 6 2046.520 2161.410 105.300 11.501 o -9 -8 1 3230.000 3278.150 93.808 8.743 o -9 -8 2 296.811 247.893 34.555 132.790 o -9 -8 3 312.003 298.153 36.216 120.311 o -9 -8 4 306.053 281.692 27.793 178.230 o -9 -8 5 864.491 818.547 40.840 62.877 o -9 -8 6 2932.090 3010.460 123.034 7.444 o -9 -7 1 7226.400 6865.640 144.932 2.462 o -9 -7 2 458.360 447.329 29.215 135.868 o -9 -7 3 1415.380 1286.690 44.284 38.489 o -9 -7 4 1304.390 1233.980 44.425 41.124 o -9 -7 5 109.518 94.864 25.463 270.322 o -9 -7 6 2307.450 2289.240 73.279 15.341 o -9 -7 7 2061.530 2174.720 103.083 11.752 o -9 -6 1 4333.290 4165.200 80.103 6.704 o -9 -6 2 4358.820 4293.340 82.672 6.484 o -9 -6 3 459.982 478.199 30.173 129.105 o -9 -6 4 1557.390 1445.330 54.434 29.557 o -9 -6 5 441.525 438.425 60.963 47.223 o -9 -6 6 732.189 664.378 63.180 39.345 o -9 -6 7 2025.430 2001.300 68.972 18.414 o -9 -6 8 2626.350 2759.960 120.818 8.217 o -9 -5 1 516.449 515.175 23.209 155.574 o -9 -5 2 4185.390 4112.880 80.981 6.942 o -9 -5 3 1273.240 1214.160 38.846 46.394 o -9 -5 4 831.613 850.334 64.288 36.023 o -9 -5 5 1715.040 1734.580 60.213 24.099 o -9 -5 6 143.839 150.832 28.213 214.340 o -9 -5 7 1775.390 1638.000 106.408 12.629 o -9 -5 8 4987.900 4887.910 117.909 4.498 o -9 -5 9 1017.660 944.372 74.264 27.221 o -9 -4 1 1602.330 1641.880 36.625 35.742 o -9 -4 2 1937.350 2051.340 72.854 17.890 o -9 -4 3 5943.830 5585.220 90.323 4.022 o -9 -4 4 5.654 -1.341 15.452 846.868 o -9 -4 5 2302.930 2212.920 52.500 19.372 o -9 -4 6 1042.890 1037.470 37.917 56.777 o -9 -4 7 104.263 124.782 26.038 257.691 o -9 -4 8 2251.950 2145.310 71.635 16.241 o -9 -4 9 3498.200 3404.400 94.797 8.048 o -9 -3 1 12182.000 12228.900 178.793 0.989 o -9 -3 2 72.448 74.638 25.953 274.192 o -9 -3 3 4010.070 3988.800 71.260 7.741 o -9 -3 4 1064.320 1079.790 36.401 57.091 o -9 -3 5 2009.830 1963.150 48.909 23.708 o -9 -3 6 2082.500 2035.530 51.487 22.047 o -9 -3 7 526.620 519.955 32.682 109.977 o -9 -3 8 66.354 64.625 18.895 484.169 o -9 -3 9 2935.820 2710.770 84.240 10.908 o -9 -3 10 3072.900 2980.740 97.541 9.088 o -9 -2 1 6223.800 6389.410 98.124 3.479 o -9 -2 2 4225.200 4048.630 71.388 7.289 o -9 -2 3 41.371 48.564 17.375 594.342 o -9 -2 4 2685.660 2582.290 55.687 15.375 o -9 -2 5 36.079 40.218 17.209 616.205 o -9 -2 6 2907.880 2771.920 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9.604 o -9 3 2 3400.120 3443.530 124.697 6.491 o -9 3 3 112.775 60.364 17.458 507.045 o -9 3 4 3574.960 3479.560 75.820 8.952 o -9 3 5 3975.030 3815.850 75.770 7.776 o -9 3 6 982.876 885.344 38.606 60.670 o -9 3 7 1706.690 1726.590 56.355 25.566 o -9 3 8 205.664 175.511 24.093 254.229 o -9 3 9 929.844 905.468 39.804 60.532 o -9 3 10 3723.030 3660.600 78.533 8.287 o -9 3 11 2512.320 2310.680 62.937 15.963 o -9 4 1 2339.750 2269.140 114.721 9.654 o -9 4 2 4577.400 4586.740 116.384 5.007 o -9 4 3 986.226 958.399 47.816 48.175 o -9 4 4 549.062 650.270 57.564 48.427 o -9 4 5 3660.200 3535.680 137.200 5.597 o -9 4 6 1840.100 1638.570 49.748 26.963 o -9 4 7 2082.130 1919.910 55.126 21.637 o -9 4 8 1912.890 1883.640 55.819 23.052 o -9 4 9 71.495 31.161 20.480 429.431 o -9 4 10 1977.770 1919.700 66.079 19.656 o -9 4 11 4188.090 4126.870 94.520 6.412 o -9 5 1 671.326 671.640 43.703 67.501 o -9 5 2 4684.290 4525.710 205.611 2.920 o -9 5 3 2443.660 2425.710 74.149 14.305 o -9 5 4 1550.690 1444.180 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131.727 o -8 -2 2 155.226 157.418 14.862 519.701 o -8 -2 3 4800.420 4709.390 78.047 5.755 o -8 -2 4 960.585 946.767 32.556 69.119 o -8 -2 5 3368.850 3289.570 63.269 10.542 o -8 -2 6 7657.360 7255.900 111.829 2.504 o -8 -2 7 1316.790 1272.280 40.011 43.689 o -8 -2 8 34.448 38.723 17.386 608.016 o -8 -2 9 1767.950 1626.430 46.635 29.062 o -8 -2 10 46.993 48.547 18.395 532.107 o -8 -2 11 1373.060 1343.690 60.998 29.089 o -8 -2 12 3483.330 3404.960 97.887 7.889 o -8 -1 1 1848.270 1920.370 36.872 29.363 o -8 -1 2 7.091 17.000 13.056 1137.670 o -8 -1 3 2153.990 2170.940 40.005 23.380 o -8 -1 4 8446.440 8042.690 165.640 1.842 o -8 -1 5 91.775 147.424 19.351 417.123 o -8 -1 6 4399.110 4163.070 75.494 6.763 o -8 -1 7 5056.350 4861.430 84.864 5.214 o -8 -1 8 35.552 16.668 25.332 306.195 o -8 -1 9 843.080 865.401 38.863 65.986 o -8 -1 10 855.128 811.611 37.001 69.779 o -8 -1 11 39.740 32.423 19.399 496.871 o -8 -1 12 1518.180 1380.070 62.306 26.794 o -8 0 1 1879.130 1866.920 42.441 27.566 o -8 0 2 2543.590 2562.180 51.541 16.785 o -8 0 3 833.635 865.301 39.623 65.110 o -8 0 4 5428.310 5300.420 74.020 4.827 o -8 0 5 5095.600 5048.580 85.391 5.065 o -8 0 6 1007.570 921.966 35.764 62.967 o -8 0 7 4885.830 4769.700 84.075 5.468 o -8 0 8 1877.670 1936.310 49.945 24.872 o -8 0 9 5.552 30.742 17.712 627.422 o -8 0 10 1180.860 1092.730 40.560 48.946 o -8 0 11 906.586 882.915 38.216 64.162 o -8 0 12 220.307 194.193 24.275 244.806 o -8 1 1 1341.860 1392.750 36.826 43.916 o -8 1 2 3332.380 3430.800 63.612 10.418 o -8 1 3 400.240 405.237 26.021 166.252 o -8 1 4 307.432 336.119 22.683 221.996 o -8 1 5 11188.900 11126.200 164.878 1.172 o -8 1 6 255.651 275.182 19.720 288.218 o -8 1 7 936.828 1041.310 50.041 46.000 o -8 1 8 5052.860 4953.600 88.428 5.090 o -8 1 9 840.343 777.162 36.956 71.293 o -8 1 10 330.990 311.193 26.860 179.456 o -8 1 11 1750.530 1780.870 52.136 26.326 o -8 1 12 99.066 130.182 22.670 325.544 o -8 1 13 1522.180 1572.860 51.351 30.633 o -8 2 1 27.709 47.915 14.726 818.771 o -8 2 2 138.015 161.732 17.996 423.117 o -8 2 3 6999.910 6812.930 134.948 2.638 o -8 2 4 8.877 1.740 15.588 823.693 o -8 2 5 5892.960 5782.020 118.229 3.582 o -8 2 6 12113.400 11791.200 173.696 1.024 o -8 2 7 7.430 4.197 14.903 899.573 o -8 2 8 1847.190 1944.420 51.406 24.699 o -8 2 9 2743.370 2652.150 67.213 13.513 o -8 2 10 211.243 247.422 24.838 232.518 o -8 2 11 601.031 515.088 33.286 102.145 o -8 2 12 388.203 323.453 28.334 158.240 o -8 2 13 9.433 15.727 20.686 467.553 o -8 3 1 10414.300 10442.400 229.122 1.127 o -8 3 2 824.241 752.165 41.385 64.668 o -8 3 3 1008.160 1055.860 36.237 59.742 o -8 3 4 1017.570 1025.620 43.550 51.223 o -8 3 5 1406.100 1409.150 42.205 38.788 o -8 3 6 7216.110 6818.120 112.691 2.749 o -8 3 7 3827.060 3729.350 75.134 8.179 o -8 3 8 11.228 -2.526 16.072 773.162 o -8 3 9 2695.540 2732.880 100.173 9.929 o -8 3 10 250.694 258.261 27.954 188.092 o -8 3 11 29.930 50.198 20.300 457.906 o -8 3 12 1515.900 1453.690 50.211 32.089 o -8 3 13 791.682 895.733 87.813 22.203 o -8 4 1 11211.000 10612.900 194.567 1.129 o -8 4 2 2263.220 2322.670 67.063 16.557 o -8 4 3 1457.550 1480.000 75.304 21.790 o -8 4 4 813.606 881.832 35.055 73.585 o -8 4 5 126.928 132.107 28.787 211.942 o -8 4 6 584.532 578.314 46.047 67.423 o -8 4 7 7069.790 6852.400 129.359 2.655 o -8 4 8 804.849 746.505 60.484 40.405 o -8 4 9 71.381 65.532 19.038 473.641 o -8 4 10 2415.570 2341.660 59.356 16.991 o -8 4 11 70.894 92.599 22.056 361.999 o -8 4 12 1359.980 1384.830 63.387 27.839 o -8 4 13 2267.650 2237.160 61.980 17.711 o -8 5 1 2694.840 2786.180 155.178 5.891 o -8 5 2 3266.810 3169.270 82.016 9.633 o -8 5 3 54.079 68.722 26.602 267.529 o -8 5 4 415.666 406.985 27.409 154.467 o -8 5 5 2173.150 2091.220 53.792 20.538 o -8 5 6 92.420 85.286 20.778 390.429 o -8 5 7 3704.660 3647.440 76.708 8.435 o -8 5 8 6880.960 6745.610 118.344 2.853 o -8 5 9 150.899 112.793 24.907 265.898 o -8 5 10 601.218 581.442 39.837 80.869 o -8 5 11 595.054 591.827 32.938 100.885 o -8 5 12 497.366 499.825 35.217 103.446 o -8 5 13 1492.950 1535.310 62.842 26.064 o -8 6 1 117.604 123.720 66.505 45.091 o -8 6 2 1487.690 1580.900 57.856 28.028 o -8 6 3 2735.810 2684.840 86.457 11.285 o -8 6 4 297.723 253.997 32.463 145.613 o -8 6 5 2413.250 2416.700 73.914 14.488 o -8 6 6 1174.060 1090.440 42.622 47.222 o -8 6 7 1833.100 1802.830 53.929 24.754 o -8 6 8 4480.300 4425.420 90.228 5.985 o -8 6 9 2144.540 2075.910 67.367 17.845 o -8 6 10 33.372 -31.320 23.162 367.792 o -8 6 11 1056.680 1127.200 42.556 49.858 o -8 6 12 221.312 209.089 32.681 154.881 o -8 7 1 3192.570 3195.530 114.167 7.522 o -8 7 2 102.531 134.591 29.009 213.224 o -8 7 3 3532.890 3664.130 95.379 7.725 o -8 7 4 21.745 8.699 25.722 302.536 o -8 7 5 2179.460 2227.980 73.562 16.039 o -8 7 6 2779.870 2709.800 82.251 11.569 o -8 7 7 485.141 428.320 41.518 85.398 o -8 7 8 780.443 756.404 41.380 66.229 o -8 7 9 4297.180 4260.330 91.481 6.287 o -8 7 10 575.082 602.704 40.679 79.471 o -8 7 11 355.633 313.501 37.840 109.002 o -8 7 12 1438.500 1396.270 45.837 36.124 o -8 7 13 63.897 123.034 52.096 73.284 o -8 8 1 7262.820 7012.950 164.046 2.268 o -8 8 2 196.329 213.728 32.667 157.514 o -8 8 3 1957.320 1957.140 78.698 16.738 o -8 8 4 382.857 396.814 39.165 99.380 o -8 8 5 0.457 -28.247 25.044 327.078 o -8 8 6 1176.510 1135.200 65.951 29.587 o -8 8 7 3701.290 3923.280 105.397 6.756 o -8 8 8 69.101 44.968 30.773 203.458 o -8 8 9 2590.830 2569.890 70.982 13.836 o -8 8 10 2794.590 2737.390 74.568 12.313 o -8 8 11 80.694 -10.776 26.133 278.511 o -8 9 1 6314.910 6079.320 137.777 3.031 o -8 9 2 1618.060 1653.320 67.063 22.898 o -8 9 3 62.662 60.394 41.566 114.634 o -8 9 4 1138.670 1120.780 59.140 34.318 o -8 9 5 609.375 544.933 46.511 66.225 o -8 9 6 171.099 167.318 34.379 149.367 o -8 9 7 3120.310 3257.980 97.150 8.744 o -8 9 8 1669.690 1714.080 87.011 16.703 o -8 9 9 480.949 516.408 60.409 46.837 o -8 9 10 1426.530 1395.200 68.963 24.721 o -8 9 11 593.520 458.885 68.722 36.832 o -8 10 1 571.619 538.552 45.924 68.766 o -8 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2653.770 93.661 10.341 o -7 -5 9 4860.770 4796.470 242.189 2.305 o -7 -5 10 2519.290 2633.890 79.114 12.924 o -7 -5 11 126.439 114.721 28.216 221.078 o -7 -4 1 8965.680 8843.330 107.865 1.903 o -7 -4 2 1334.490 1362.630 33.117 47.123 o -7 -4 3 319.578 335.789 18.727 265.208 o -7 -4 4 6279.040 6009.640 92.343 3.627 o -7 -4 5 369.356 363.775 20.456 224.505 o -7 -4 6 6349.450 5939.440 124.224 3.216 o -7 -4 7 5344.240 4837.590 112.504 4.362 o -7 -4 8 161.009 147.005 25.722 245.453 o -7 -4 9 2677.870 2519.580 74.038 13.196 o -7 -4 10 2364.150 2326.050 72.840 15.071 o -7 -4 11 554.624 508.291 41.451 80.563 o -7 -4 12 396.451 408.199 39.949 95.436 o -7 -3 1 9674.040 9738.770 103.271 1.663 o -7 -3 2 15331.600 15517.700 176.150 0.669 o -7 -3 3 968.524 976.941 27.425 75.770 o -7 -3 4 1222.100 1209.570 30.561 55.199 o -7 -3 5 3487.120 3402.330 55.045 10.537 o -7 -3 6 2807.020 2731.980 55.539 14.414 o -7 -3 7 6768.220 6265.700 99.606 3.199 o -7 -3 8 4658.890 4308.370 100.657 5.524 o -7 -3 9 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64.111 9.854 o -7 1 5 4322.000 4218.680 74.311 6.881 o -7 1 6 1279.730 1280.740 33.917 49.285 o -7 1 7 2297.840 2243.150 44.306 20.855 o -7 1 8 278.208 273.161 23.919 223.715 o -7 1 9 2859.980 2824.120 61.333 13.338 o -7 1 10 7731.380 7481.050 119.559 2.388 o -7 1 11 2098.290 2062.880 53.721 21.263 o -7 1 12 66.589 86.661 20.689 407.936 o -7 1 13 1881.000 1813.500 52.136 24.792 o -7 1 14 284.528 322.565 30.119 159.708 o -7 2 1 7525.360 7942.490 99.745 2.506 o -7 2 2 10656.700 10815.800 154.102 1.281 o -7 2 3 59.246 60.824 14.538 755.333 o -7 2 4 109.354 149.655 17.404 471.325 o -7 2 5 5328.730 5158.290 87.014 4.754 o -7 2 6 2861.290 2728.970 57.510 13.950 o -7 2 7 4028.210 3791.300 61.212 8.323 o -7 2 8 6978.450 6442.030 90.208 3.133 o -7 2 9 296.864 265.876 38.700 110.423 o -7 2 10 7141.900 6900.570 112.449 2.764 o -7 2 11 3450.930 3475.010 72.177 9.476 o -7 2 12 120.883 121.358 21.663 342.247 o -7 2 13 50.265 34.802 19.437 485.623 o -7 2 14 1656.150 1695.860 78.110 19.096 o -7 3 1 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46.562 24.559 o -7 4 12 3922.470 3905.540 95.236 6.917 o -7 4 13 419.645 482.044 67.899 39.169 o -7 4 14 90.269 129.648 24.491 289.396 o -7 5 1 5696.730 5611.280 118.601 3.744 o -7 5 2 317.850 291.206 28.715 168.035 o -7 5 3 3794.810 3788.460 136.349 5.398 o -7 5 4 10266.500 9812.490 247.332 1.119 o -7 5 5 100.800 133.743 20.024 394.506 o -7 5 6 168.783 121.565 24.734 262.426 o -7 5 7 2692.390 2590.140 60.538 14.701 o -7 5 8 1003.360 912.347 39.666 58.055 o -7 5 9 2925.940 2881.120 87.601 10.387 o -7 5 10 5160.900 5111.240 81.166 5.055 o -7 5 11 43.853 29.563 17.451 598.135 o -7 5 12 2420.400 2428.000 53.650 17.641 o -7 5 13 1074.790 1093.660 43.981 48.375 o -7 5 14 318.992 367.620 40.929 97.019 o -7 6 1 1970.920 1826.100 59.495 21.770 o -7 6 2 7225.520 7049.150 147.420 2.412 o -7 6 3 414.914 333.690 31.233 136.153 o -7 6 4 4287.180 4359.170 91.906 6.220 o -7 6 5 4113.880 3972.080 77.171 7.326 o -7 6 6 173.264 117.749 22.006 312.503 o -7 6 7 536.404 524.033 45.779 70.520 o -7 6 8 982.224 923.172 41.370 56.368 o -7 6 9 271.879 255.017 28.783 177.241 o -7 6 10 5210.250 5026.120 98.911 4.680 o -7 6 11 1210.570 1234.790 40.267 46.557 o -7 6 12 5.694 12.128 18.714 573.785 o -7 6 13 2426.460 2442.000 57.072 17.007 o -7 6 14 1099.040 1146.890 54.319 38.198 o -7 7 1 398.385 378.427 74.818 33.444 o -7 7 2 4230.000 4324.790 101.664 5.971 o -7 7 3 1867.380 1984.100 65.272 20.393 o -7 7 4 3074.350 3103.630 83.764 10.056 o -7 7 5 5198.670 4907.500 113.204 4.432 o -7 7 6 1108.590 1005.790 41.587 51.113 o -7 7 7 68.993 35.075 21.041 409.792 o -7 7 8 1097.440 1129.860 44.731 46.641 o -7 7 9 87.302 106.399 24.810 287.595 o -7 7 10 1050.880 1019.990 46.854 46.957 o -7 7 11 5440.170 5487.180 107.860 4.139 o -7 7 12 1143.660 1136.940 40.885 49.045 o -7 7 13 888.767 869.980 38.451 64.748 o -7 7 14 1153.860 1339.600 49.893 38.976 o -7 8 1 195.227 232.120 30.773 172.416 o -7 8 2 2227.990 2340.710 85.348 13.611 o -7 8 3 3654.070 3706.080 94.749 7.519 o -7 8 4 42.886 30.490 25.463 298.905 o -7 8 5 1547.220 1581.300 61.858 25.737 o -7 8 6 3705.170 3698.830 97.178 7.317 o -7 8 7 292.701 290.173 29.382 166.497 o -7 8 8 124.166 133.483 25.987 252.342 o -7 8 9 2365.340 2247.270 84.767 13.377 o -7 8 10 1.138 -18.412 23.273 378.413 o -7 8 11 3657.250 3587.240 84.320 8.180 o -7 8 12 2376.280 2377.370 110.817 9.892 o -7 8 13 3.170 18.713 20.989 457.622 o -7 9 1 566.734 611.867 54.312 53.005 o -7 9 2 190.984 174.322 31.233 172.691 o -7 9 3 3009.470 2903.180 84.549 10.417 o -7 9 4 4275.780 4352.790 108.499 5.666 o -7 9 5 174.852 156.550 45.999 88.977 o -7 9 6 1898.160 2041.210 94.770 13.691 o -7 9 7 1345.570 1372.580 96.987 16.152 o -7 9 8 1.516 14.273 28.215 256.042 o -7 9 9 1249.900 1145.410 50.353 38.656 o -7 9 10 949.495 891.641 46.704 51.145 o -7 9 11 623.747 660.680 42.686 71.552 o -7 9 12 3086.740 3100.090 98.159 8.892 o -7 9 13 759.685 785.944 50.433 52.362 o -7 10 1 629.123 691.476 48.121 60.460 o -7 10 2 771.858 716.898 60.963 40.613 o -7 10 3 1225.780 1246.990 78.698 22.724 o -7 10 4 5460.070 5523.470 129.698 3.725 o -7 10 5 943.617 944.523 55.218 41.699 o -7 10 6 906.195 864.829 73.710 28.692 o -7 10 7 756.091 688.408 60.409 41.592 o -7 10 8 721.226 696.388 88.119 22.809 o -7 10 9 47.523 35.984 32.224 189.729 o -7 10 10 2162.290 2131.210 80.641 15.050 o -7 10 11 133.099 73.903 33.024 169.370 o -7 10 12 1254.800 1200.420 88.673 19.153 o -7 11 1 299.676 246.615 36.439 122.049 o -7 11 2 1904.390 1868.540 73.129 18.523 o -7 11 3 1.763 13.597 29.196 239.252 o -7 11 4 3342.700 3499.820 101.097 7.856 o -7 11 5 2029.190 2040.620 77.982 16.348 o -7 11 6 401.637 381.721 43.494 84.233 o -7 11 7 354.568 242.501 62.071 48.142 o -7 11 8 627.422 614.043 50.974 56.788 o -7 11 9 187.675 145.203 45.445 90.723 o -7 11 10 1051.100 1070.730 83.131 22.450 o -7 11 11 1553.780 1285.760 91.999 16.810 o -7 12 1 108.840 68.579 32.973 172.859 o -7 12 2 1013.780 1021.400 61.343 35.020 o -7 12 3 410.765 395.598 43.452 83.688 o -7 12 4 15.524 36.160 35.469 160.369 o -7 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10 10 714.522 734.697 47.791 58.009 o 1 10 11 1144.970 1169.620 57.507 35.017 o 1 10 12 872.708 934.561 54.366 43.870 o 1 10 13 213.111 181.218 34.459 144.152 o 1 10 14 8146.780 8234.150 175.517 1.830 o 1 10 15 3132.540 3150.080 96.165 8.899 o 1 10 16 40.188 68.643 32.224 188.634 o 1 10 17 661.490 739.644 54.753 49.243 o 1 10 18 306.467 276.018 44.452 87.245 o 1 11 0 11276.100 11630.800 172.778 1.117 o 1 11 1 4621.250 4833.730 86.808 5.666 o 1 11 2 138.873 153.853 19.925 369.384 o 1 11 3 325.822 325.006 23.661 208.588 o 1 11 4 2194.530 2223.030 73.044 16.073 o 1 11 5 268.991 268.667 24.303 222.082 o 1 11 6 7663.390 7691.310 170.863 2.026 o 1 11 7 6472.060 6433.080 109.194 3.207 o 1 11 8 538.326 486.695 40.313 84.939 o 1 11 9 3667.860 3751.230 98.746 7.255 o 1 11 10 621.240 638.502 46.629 64.149 o 1 11 11 15.589 19.686 27.749 260.999 o 1 11 12 1901.910 1999.980 172.359 5.756 o 1 11 13 1054.140 1037.340 56.958 37.690 o 1 11 14 824.897 805.908 54.012 46.346 o 1 11 15 5992.120 6302.510 149.183 2.977 o 1 11 16 1937.710 2142.850 82.462 15.633 o 1 11 17 31.602 11.497 33.024 184.107 o 1 12 0 1878.430 2016.310 65.781 20.074 o 1 12 1 3746.480 4051.510 79.768 7.800 o 1 12 2 1986.130 2143.290 66.607 18.761 o 1 12 3 179.723 183.445 27.432 213.915 o 1 12 4 1757.730 1875.720 155.733 6.955 o 1 12 5 2016.420 2143.430 56.368 20.962 o 1 12 6 5033.340 5230.030 96.514 4.798 o 1 12 7 6275.160 6359.460 178.455 2.516 o 1 12 8 1408.330 1502.790 62.687 27.101 o 1 12 9 130.239 170.343 31.735 176.104 o 1 12 10 2002.710 2043.250 73.254 17.469 o 1 12 11 21.787 52.234 28.183 248.604 o 1 12 12 649.941 675.106 67.614 36.193 o 1 12 13 4473.100 4379.460 116.340 5.200 o 1 12 14 107.364 153.453 34.713 153.455 o 1 12 15 1489.580 1497.920 69.882 23.466 o 1 12 16 1937.110 2046.200 82.195 15.897 o 1 13 0 446.257 535.366 59.855 47.936 o 1 13 1 1654.410 1963.010 96.432 14.292 o 1 13 2 2702.820 2842.620 82.296 11.597 o 1 13 3 628.601 729.420 109.179 15.753 o 1 13 4 1829.390 1994.800 105.854 12.146 o 1 13 5 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540.147 535.805 47.791 65.945 o 2 -9 0 1340.620 1374.160 38.779 42.817 o 2 -9 1 8503.250 8528.140 128.531 1.966 o 2 -9 2 272.097 268.152 20.452 271.944 o 2 -9 3 1711.740 1672.790 55.152 26.228 o 2 -9 4 4057.380 3847.380 165.708 4.211 o 2 -9 5 3894.630 3565.330 88.893 7.529 o 2 -9 6 590.811 544.371 39.188 83.990 o 2 -9 7 6348.150 6198.310 135.779 3.014 o 2 -9 8 1632.510 1644.360 85.902 17.283 o 2 -9 9 551.302 574.332 45.021 70.799 o 2 -9 10 1670.650 1682.260 67.793 22.149 o 2 -9 11 22.824 7.316 25.391 310.155 o 2 -9 12 813.938 890.505 57.151 42.447 o 2 -8 0 929.673 895.684 31.701 73.269 o 2 -8 1 835.198 880.369 31.440 79.313 o 2 -8 2 2417.230 2435.300 49.620 18.292 o 2 -8 3 149.847 186.482 17.447 422.025 o 2 -8 4 2896.630 2956.620 58.192 13.230 o 2 -8 5 7950.890 7279.260 223.346 1.669 o 2 -8 6 629.106 622.655 38.743 81.249 o 2 -8 7 2103.590 2073.100 66.496 18.281 o 2 -8 8 6121.170 5871.840 130.042 3.269 o 2 -8 9 22.530 11.352 34.915 165.887 o 2 -8 10 895.977 888.400 62.626 36.358 o 2 -8 11 617.004 615.800 46.629 64.635 o 2 -8 12 20.850 10.454 22.568 390.153 o 2 -8 13 1352.060 1362.230 90.336 17.902 o 2 -7 0 13091.700 12590.200 172.305 0.908 o 2 -7 1 2627.040 2588.600 42.280 17.414 o 2 -7 2 7559.440 7320.870 93.516 2.650 o 2 -7 3 1303.860 1264.470 33.090 49.465 o 2 -7 4 1613.700 1551.460 40.941 34.344 o 2 -7 5 8872.510 8649.210 127.857 1.867 o 2 -7 6 5740.230 5405.900 114.724 3.844 o 2 -7 7 206.133 178.773 34.361 145.617 o 2 -7 8 4812.360 4657.420 107.664 4.999 o 2 -7 9 2433.090 2271.960 71.271 15.131 o 2 -7 10 281.950 282.451 33.248 140.626 o 2 -7 11 2278.800 2219.030 74.446 15.435 o 2 -7 12 855.352 909.203 52.900 45.984 o 2 -7 13 224.655 232.213 55.421 61.397 o 2 -7 14 3157.820 3467.180 102.885 8.086 o 2 -6 0 35810.000 36022.200 399.979 0.127 o 2 -6 1 5196.390 5200.360 68.760 5.209 o 2 -6 2 21.178 33.353 8.033 2304.600 o 2 -6 3 5489.030 5641.270 73.920 4.611 o 2 -6 4 141.354 166.632 17.330 440.003 o 2 -6 5 847.836 822.297 27.521 88.238 o 2 -6 6 13270.300 12929.800 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257.711 34.087 138.436 o 5 6 19 1257.010 1315.690 85.348 19.955 o 5 6 20 1341.500 1483.060 90.890 17.546 o 5 7 0 11015.900 11033.400 159.350 1.210 o 5 7 1 11135.900 11345.300 162.091 1.171 o 5 7 2 52.566 54.788 12.443 985.343 o 5 7 3 13443.400 13486.000 245.259 0.753 o 5 7 4 466.160 493.092 22.788 168.700 o 5 7 5 8174.150 7936.460 159.935 1.947 o 5 7 6 7226.820 7300.600 112.169 2.653 o 5 7 7 3003.700 2945.160 58.432 12.792 o 5 7 8 1766.970 1805.640 45.427 28.370 o 5 7 9 4327.710 4128.280 75.720 6.896 o 5 7 10 2725.250 2530.960 56.512 15.198 o 5 7 11 2380.020 2249.130 54.372 18.363 o 5 7 12 689.889 735.814 43.086 66.850 o 5 7 13 205.193 205.248 23.724 255.596 o 5 7 14 5248.000 5134.320 94.889 4.682 o 5 7 15 2739.610 2711.570 92.312 10.627 o 5 7 16 1271.930 1230.660 46.605 40.211 o 5 7 17 137.353 126.588 26.441 242.854 o 5 7 18 873.579 1016.070 56.366 41.200 o 5 7 19 4.275 -29.927 36.578 153.089 o 5 8 0 2372.680 2353.540 52.180 18.446 o 5 8 1 18739.000 19485.600 274.663 0.418 o 5 8 2 850.301 926.047 78.698 26.096 o 5 8 3 2435.660 2479.820 68.134 15.123 o 5 8 4 472.298 527.887 39.254 90.424 o 5 8 5 179.370 197.357 18.200 377.202 o 5 8 6 7155.630 7145.250 112.169 2.711 o 5 8 7 8970.660 8733.230 132.879 1.814 o 5 8 8 2172.060 2035.400 49.251 21.797 o 5 8 9 4321.280 3998.890 75.298 7.026 o 5 8 10 3064.550 2754.630 60.561 12.728 o 5 8 11 298.494 229.505 23.172 233.046 o 5 8 12 4004.650 3891.970 77.364 7.581 o 5 8 13 677.306 694.350 35.937 83.762 o 5 8 14 534.620 570.004 33.652 103.797 o 5 8 15 2965.580 3048.850 70.511 11.615 o 5 8 16 3861.330 3945.100 106.275 6.488 o 5 8 17 295.049 305.956 41.566 97.362 o 5 8 18 1006.680 1041.330 89.228 20.391 o 5 8 19 1420.300 1450.210 67.350 25.213 o 5 9 0 170.876 163.300 19.680 355.422 o 5 9 1 8527.800 9041.560 143.476 1.830 o 5 9 2 5345.530 5499.250 118.279 4.010 o 5 9 3 37.968 8.356 20.198 471.435 o 5 9 4 1789.900 1732.950 64.288 22.163 o 5 9 5 410.909 381.111 32.106 129.366 o 5 9 6 3168.770 3167.300 64.067 11.304 o 5 9 7 14157.400 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14 2087.340 2176.410 78.626 15.645 o 6 -5 15 2170.300 2152.370 81.410 14.838 o 6 -5 16 433.307 436.717 69.830 37.354 o 6 -4 0 7063.630 7111.040 90.541 2.928 o 6 -4 1 15531.000 15594.300 211.877 0.629 o 6 -4 2 1834.150 1903.470 42.902 27.755 o 6 -4 3 171.747 188.401 17.021 417.374 o 6 -4 4 367.777 374.223 30.990 140.535 o 6 -4 5 4046.730 3965.110 71.004 7.705 o 6 -4 6 12439.800 11986.600 171.961 0.989 o 6 -4 7 10561.100 10324.300 152.726 1.330 o 6 -4 8 315.964 265.532 22.318 233.458 o 6 -4 9 3888.900 3688.320 71.477 8.271 o 6 -4 10 1044.520 998.389 36.860 58.686 o 6 -4 11 99.898 84.510 20.217 403.945 o 6 -4 12 1507.180 1453.700 45.165 34.845 o 6 -4 13 1066.070 1059.950 41.425 51.723 o 6 -4 14 18.093 -4.139 16.466 726.015 o 6 -4 15 4335.240 4261.390 114.141 5.463 o 6 -4 16 1768.160 1743.120 73.989 19.457 o 6 -3 0 467.172 515.259 18.043 197.539 o 6 -3 1 11503.700 11651.000 159.074 1.120 o 6 -3 2 4625.830 4482.630 72.963 6.269 o 6 -3 3 4453.050 4335.880 71.875 6.663 o 6 -3 4 3087.510 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42.658 52.981 o 7 7 9 101.502 112.517 18.252 461.597 o 7 7 10 828.224 854.273 34.510 74.558 o 7 7 11 507.679 449.834 28.244 134.878 o 7 7 12 1539.810 1514.340 46.690 33.053 o 7 7 13 4735.480 4735.850 90.214 5.500 o 7 7 14 97.607 88.910 23.392 317.482 o 7 7 15 2660.350 2632.170 65.686 14.095 o 7 7 16 2849.450 2788.970 84.240 11.042 o 7 7 17 425.039 463.003 41.540 87.341 o 7 7 18 113.326 125.106 58.192 58.436 o 7 7 19 284.099 230.228 35.655 128.227 o 7 7 20 8.789 22.168 43.228 109.088 o 7 8 0 1163.040 1238.180 39.940 48.041 o 7 8 1 4391.010 4357.300 103.670 5.698 o 7 8 2 8023.430 8131.150 161.405 1.950 o 7 8 3 2096.690 2243.350 68.852 17.337 o 7 8 4 1183.780 1243.410 68.722 27.529 o 7 8 5 420.957 445.692 34.555 113.880 o 7 8 6 1023.890 986.281 66.048 31.849 o 7 8 7 8305.660 8185.970 192.357 1.709 o 7 8 8 4114.810 4037.900 76.708 7.286 o 7 8 9 2854.170 2777.900 60.940 13.502 o 7 8 10 71.226 90.178 18.765 475.153 o 7 8 11 4106.950 3775.020 76.365 7.545 o 7 8 12 365.933 337.242 27.418 167.120 o 7 8 13 4599.740 4488.650 108.152 5.270 o 7 8 14 2045.540 1922.860 60.031 20.681 o 7 8 15 30.556 37.441 21.335 421.088 o 7 8 16 1985.810 2038.520 61.689 20.282 o 7 8 17 1315.530 1260.230 48.765 37.614 o 7 8 18 447.099 418.403 41.926 86.169 o 7 8 19 542.584 574.160 68.722 36.768 o 7 9 0 828.219 796.270 65.397 35.477 o 7 9 1 71.322 112.767 26.828 253.979 o 7 9 2 2098.370 2153.940 69.882 17.364 o 7 9 3 3052.260 3137.790 85.258 9.946 o 7 9 4 355.593 371.088 53.758 60.830 o 7 9 5 3971.040 3900.660 233.876 2.715 o 7 9 6 1791.980 1829.120 63.002 22.164 o 7 9 7 1838.720 1673.890 63.734 22.183 o 7 9 8 4773.100 4643.150 85.870 5.625 o 7 9 9 5939.090 5811.610 101.939 3.782 o 7 9 10 34.777 45.821 18.470 541.409 o 7 9 11 2516.200 2347.500 58.659 16.510 o 7 9 12 268.936 257.777 25.551 209.265 o 7 9 13 1129.040 1045.020 43.682 47.916 o 7 9 14 3873.660 3695.630 81.290 7.822 o 7 9 15 874.108 762.924 41.723 62.137 o 7 9 16 79.991 54.899 23.951 317.246 o 7 9 17 2161.260 2065.060 123.294 9.242 o 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5.167 o 8 -9 8 902.453 1000.440 51.332 45.799 o 8 -9 9 158.787 94.216 43.228 101.651 o 8 -8 0 3800.000 3877.940 161.829 4.469 o 8 -8 1 10.835 22.907 24.235 341.153 o 8 -8 2 1746.910 1715.760 110.288 11.984 o 8 -8 3 193.159 245.762 57.638 57.490 o 8 -8 4 25.674 38.776 38.795 133.759 o 8 -8 5 3643.570 3567.240 95.451 7.615 o 8 -8 6 435.453 414.179 38.604 97.879 o 8 -8 7 112.213 109.677 22.919 318.641 o 8 -8 8 4148.760 4146.110 86.282 6.770 o 8 -8 9 1966.260 2005.810 58.427 21.380 o 8 -8 10 45.570 94.216 30.567 205.880 o 8 -7 0 5973.120 5732.650 126.710 3.427 o 8 -7 1 1133.330 1047.750 50.796 41.311 o 8 -7 2 158.986 178.117 29.009 199.690 o 8 -7 3 1572.650 1572.900 100.312 14.380 o 8 -7 4 13.172 12.078 33.252 183.575 o 8 -7 5 475.841 466.912 30.222 127.782 o 8 -7 6 2971.260 3050.670 68.046 11.821 o 8 -7 7 1346.090 1208.700 43.853 40.936 o 8 -7 8 1922.500 1876.880 54.716 23.315 o 8 -7 9 2631.240 2542.520 107.593 9.550 o 8 -7 10 330.858 334.440 29.905 154.401 o 8 -7 11 524.354 541.797 36.606 95.449 o 8 -7 12 126.897 82.023 44.337 98.424 o 8 -6 0 3757.120 3925.950 96.508 7.093 o 8 -6 1 8601.210 8706.310 170.166 1.720 o 8 -6 2 1165.400 1210.380 110.288 13.855 o 8 -6 3 840.392 823.507 45.805 56.168 o 8 -6 4 247.490 264.237 23.887 233.205 o 8 -6 5 68.937 82.679 19.880 436.132 o 8 -6 6 6296.480 6135.010 106.537 3.410 o 8 -6 7 2382.270 2303.050 57.842 17.564 o 8 -6 8 280.428 262.819 26.327 198.223 o 8 -6 9 2361.600 2352.670 77.450 14.297 o 8 -6 10 401.065 405.964 37.293 105.271 o 8 -6 11 49.716 59.901 22.542 365.599 o 8 -6 12 1681.630 1666.530 54.187 26.947 o 8 -6 13 681.321 669.941 40.120 74.496 o 8 -5 0 555.668 565.442 45.445 69.877 o 8 -5 1 8710.900 8501.260 166.817 1.736 o 8 -5 2 2986.620 2799.280 100.866 9.180 o 8 -5 3 210.343 212.438 21.670 285.888 o 8 -5 4 784.853 763.987 34.106 80.035 o 8 -5 5 146.407 183.555 21.022 331.244 o 8 -5 6 726.251 753.599 86.457 23.416 o 8 -5 7 5450.530 5463.570 96.987 4.335 o 8 -5 8 650.674 665.763 36.931 83.545 o 8 -5 9 11.863 4.584 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4667.850 4968.630 101.464 5.151 o 8 -3 3 4487.240 4590.700 80.080 6.180 o 8 -3 4 54.124 96.186 17.527 544.887 o 8 -3 5 2649.390 2692.040 57.674 15.027 o 8 -3 6 349.468 326.970 23.951 200.164 o 8 -3 7 1067.240 1071.150 43.793 49.045 o 8 -3 8 5380.500 5159.160 107.776 4.307 o 8 -3 9 4430.120 4103.050 79.706 6.619 o 8 -3 10 522.645 481.373 29.801 124.096 o 8 -3 11 2845.570 2744.600 68.935 12.733 o 8 -3 12 571.441 546.938 33.413 102.731 o 8 -3 13 3.138 6.948 25.011 325.923 o 8 -3 14 1691.060 1798.480 65.809 22.195 o 8 -3 15 455.472 517.809 42.452 82.040 o 8 -3 16 236.601 205.057 43.228 95.975 o 8 -3 17 2466.800 2459.580 110.842 9.634 o 8 -2 0 4933.570 5056.700 83.434 5.273 o 8 -2 1 4021.010 4084.160 70.999 7.641 o 8 -2 2 1716.810 1732.950 42.292 30.713 o 8 -2 3 13513.600 13519.600 190.148 0.820 o 8 -2 4 3430.010 3602.430 67.213 9.676 o 8 -2 5 248.169 247.360 23.209 244.218 o 8 -2 6 1166.070 1212.930 38.012 50.069 o 8 -2 7 346.282 327.205 23.661 203.599 o 8 -2 8 1228.710 1187.090 39.453 47.404 o 8 -2 9 8487.600 7954.120 127.138 2.050 o 8 -2 10 4748.780 4490.310 93.556 5.531 o 8 -2 11 121.105 143.159 21.433 342.745 o 8 -2 12 5006.940 4617.900 89.144 5.295 o 8 -2 13 20.641 -4.212 22.134 407.926 o 8 -2 14 1669.220 1560.590 60.593 25.178 o 8 -2 15 1566.350 1568.390 62.479 25.374 o 8 -2 16 307.859 402.261 38.814 105.050 o 8 -2 17 471.144 493.246 55.421 54.360 o 8 -1 0 5737.410 6054.200 80.862 4.132 o 8 -1 1 8539.100 8872.900 111.244 1.993 o 8 -1 2 817.546 804.177 25.032 96.690 o 8 -1 3 4772.680 4843.110 111.194 4.859 o 8 -1 4 1625.310 1630.620 41.071 33.427 o 8 -1 5 3422.640 3427.560 64.518 10.103 o 8 -1 6 2496.870 2364.260 52.190 17.591 o 8 -1 7 1973.190 1846.450 45.996 25.505 o 8 -1 8 420.100 398.945 25.129 169.703 o 8 -1 9 3837.020 3704.630 114.239 6.318 o 8 -1 10 10125.000 9655.560 161.488 1.416 o 8 -1 11 949.867 878.058 44.954 53.452 o 8 -1 12 1112.470 1112.710 49.396 42.282 o 8 -1 13 556.221 537.214 38.349 88.353 o 8 -1 14 198.704 215.541 31.159 169.650 o 8 -1 15 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175.844 167.932 28.407 204.517 o 8 3 15 960.592 881.189 49.210 48.122 o 8 3 16 574.632 657.951 65.397 39.128 o 8 3 17 297.248 289.184 36.137 122.199 o 8 3 18 3061.640 3092.770 93.111 9.342 o 8 4 0 2653.800 2682.620 45.821 16.511 o 8 4 1 5961.040 6216.590 81.127 3.904 o 8 4 2 2725.390 2871.500 42.550 15.899 o 8 4 3 197.325 205.379 13.082 507.955 o 8 4 4 18624.400 19274.700 191.637 0.461 o 8 4 5 4040.130 4239.700 73.956 7.349 o 8 4 6 1688.840 1746.580 42.200 31.058 o 8 4 7 3848.600 3911.770 69.706 8.206 o 8 4 8 216.511 262.644 20.082 301.184 o 8 4 9 505.790 529.320 27.401 134.460 o 8 4 10 6605.420 6423.700 104.488 3.192 o 8 4 11 5283.250 5190.410 114.302 4.239 o 8 4 12 368.346 341.285 33.138 129.931 o 8 4 13 4152.250 4011.690 98.671 6.377 o 8 4 14 1257.080 1097.190 53.758 36.499 o 8 4 15 4804.460 4779.250 121.926 4.587 o 8 4 16 2184.560 2113.540 72.777 16.443 o 8 4 17 29.169 22.036 25.553 302.246 o 8 4 18 564.806 510.184 64.288 41.227 o 8 4 19 1941.690 2129.270 118.601 10.068 o 8 5 0 39.930 52.078 12.469 1030.680 o 8 5 1 4708.430 4783.040 66.736 6.107 o 8 5 2 8696.980 9091.180 124.215 1.872 o 8 5 3 1019.600 1092.180 23.412 75.069 o 8 5 4 2285.700 2435.570 51.329 18.915 o 8 5 5 7945.580 8192.060 123.669 2.186 o 8 5 6 1393.040 1428.470 39.297 40.681 o 8 5 7 2335.410 2404.020 83.635 13.371 o 8 5 8 821.307 778.840 31.701 82.598 o 8 5 9 40.584 48.017 16.417 657.390 o 8 5 10 7795.690 7400.170 117.791 2.391 o 8 5 11 4920.640 4835.700 87.256 5.316 o 8 5 12 4412.150 4336.790 103.670 5.686 o 8 5 13 2019.930 1902.810 65.711 19.525 o 8 5 14 3237.550 3174.690 88.109 9.245 o 8 5 15 96.615 131.679 28.407 222.572 o 8 5 16 2466.180 2490.960 79.411 13.337 o 8 5 17 778.771 785.962 52.096 49.769 o 8 5 18 40.657 7.626 34.915 164.449 o 8 5 19 1192.720 1290.200 97.541 16.652 o 8 6 0 2332.090 2311.670 53.069 18.710 o 8 6 1 1830.800 1859.770 46.849 26.777 o 8 6 2 7730.400 7686.240 151.954 2.139 o 8 6 3 4107.550 4191.860 200.069 3.269 o 8 6 4 596.346 621.900 50.433 58.345 o 8 6 5 1769.980 1871.440 44.980 28.072 o 8 6 6 6049.690 5949.850 97.610 3.725 o 8 6 7 689.172 693.611 30.096 98.511 o 8 6 8 8678.790 8357.260 129.154 1.941 o 8 6 9 529.020 508.815 27.551 132.181 o 8 6 10 660.304 696.938 31.911 95.392 o 8 6 11 10502.600 10264.600 156.890 1.331 o 8 6 12 3901.490 3905.190 78.312 7.716 o 8 6 13 775.140 758.305 40.460 68.050 o 8 6 14 2077.890 1940.950 68.496 18.389 o 8 6 15 1319.380 1334.190 101.420 15.238 o 8 6 16 834.023 805.223 49.543 51.545 o 8 6 17 1844.110 1836.120 73.156 18.957 o 8 6 18 1453.370 1633.470 94.770 15.868 o 8 6 19 395.731 353.585 60.963 48.435 o 8 7 0 2277.380 2335.050 55.362 18.583 o 8 7 1 1185.890 1267.730 53.478 36.474 o 8 7 2 1682.590 1630.170 59.427 25.156 o 8 7 3 6856.030 7027.210 144.156 2.567 o 8 7 4 4328.030 4315.700 101.314 5.873 o 8 7 5 368.944 403.663 33.457 125.288 o 8 7 6 9234.990 9193.090 140.067 1.682 o 8 7 7 2200.350 2158.100 67.141 17.337 o 8 7 8 435.646 428.783 26.202 157.560 o 8 7 9 2034.340 1978.650 52.804 22.385 o 8 7 10 43.382 48.618 17.123 607.143 o 8 7 11 1279.420 1277.590 42.531 42.598 o 8 7 12 5511.070 5204.340 115.556 4.049 o 8 7 13 5852.080 5563.080 101.700 3.926 o 8 7 14 114.929 118.449 27.657 230.762 o 8 7 15 1222.780 1135.450 55.499 35.527 o 8 7 16 238.371 229.219 49.325 75.564 o 8 7 17 2506.440 2432.850 81.501 13.012 o 8 7 18 961.072 923.356 55.152 41.644 o 8 7 19 301.891 253.828 58.746 53.853 o 8 8 0 1147.520 1231.070 55.235 36.116 o 8 8 1 2946.980 2884.550 82.462 10.804 o 8 8 2 510.075 465.741 95.324 20.890 o 8 8 3 2633.070 2710.740 78.626 12.452 o 8 8 4 8950.120 8905.140 175.066 1.615 o 8 8 5 1143.280 1153.490 98.649 16.736 o 8 8 6 2774.870 2768.510 94.770 10.226 o 8 8 7 4406.960 4210.180 133.010 4.823 o 8 8 8 25.184 8.796 16.263 723.851 o 8 8 9 1707.900 1606.660 46.556 30.022 o 8 8 10 1838.880 1714.770 48.306 27.039 o 8 8 11 122.903 113.677 22.353 326.506 o 8 8 12 2516.150 2489.410 61.138 15.750 o 8 8 13 4080.100 3990.190 82.745 7.140 o 8 8 14 1019.250 923.611 41.767 54.719 o 8 8 15 1331.110 1309.410 49.251 36.606 o 8 8 16 526.773 477.661 43.086 78.177 o 8 8 17 105.567 116.000 30.447 196.768 o 8 8 18 1347.400 1335.060 64.572 27.638 o 8 8 19 1808.820 1899.830 109.733 11.725 o 8 9 0 124.816 91.968 28.819 215.515 o 8 9 1 1380.390 1371.380 77.035 22.009 o 8 9 2 399.049 404.118 36.737 107.742 o 8 9 3 315.877 313.233 34.379 129.192 o 8 9 4 5766.180 6061.160 134.333 3.338 o 8 9 5 6313.280 6603.300 180.118 2.450 o 8 9 6 1847.690 1659.880 62.217 22.635 o 8 9 7 1006.300 1026.310 51.117 43.669 o 8 9 8 1526.210 1474.650 77.589 20.619 o 8 9 9 1186.390 1171.770 42.225 46.261 o 8 9 10 4777.950 4636.660 88.911 5.542 o 8 9 11 1121.240 1080.290 41.717 49.603 o 8 9 12 147.823 115.926 28.108 218.268 o 8 9 13 2705.130 2573.520 65.473 14.055 o 8 9 14 2504.880 2413.880 64.628 15.478 o 8 9 15 124.292 111.264 26.097 253.331 o 8 9 16 716.257 661.646 39.419 74.638 o 8 9 17 137.781 164.186 66.505 44.763 o 8 9 18 1143.130 1056.320 85.348 21.150 o 8 10 0 784.751 746.926 105.854 16.300 o 8 10 1 383.394 342.652 38.795 102.371 o 8 10 2 1325.040 1385.170 59.495 30.169 o 8 10 3 48.174 -1.345 23.895 340.674 o 8 10 4 2212.070 2174.190 74.347 15.868 o 8 10 5 6108.530 6176.740 138.667 3.089 o 8 10 6 7787.830 7757.200 162.973 2.041 o 8 10 7 118.988 73.377 31.036 191.263 o 8 10 8 1949.580 1962.130 69.703 18.814 o 8 10 9 200.281 213.111 32.519 158.273 o 8 10 10 1215.470 1218.420 56.787 34.186 o 8 10 11 2292.750 2053.890 57.101 19.098 o 8 10 12 978.003 834.514 40.885 58.589 o 8 10 13 136.897 177.854 25.658 248.638 o 8 10 14 5619.050 5474.630 106.435 4.041 o 8 10 15 1081.490 1059.320 68.111 29.640 o 8 10 16 583.663 521.892 42.544 76.271 o 8 10 17 1310.750 1334.740 66.197 27.208 o 8 11 0 3181.060 3335.180 132.456 6.392 o 8 11 1 120.119 109.506 30.088 199.201 o 8 11 2 2071.220 2161.910 76.841 16.092 o 8 11 3 1677.090 1655.890 66.058 22.770 o 8 11 4 265.746 207.613 36.578 125.343 o 8 11 5 1455.090 1501.970 64.212 25.996 o 8 11 6 3783.090 3919.950 105.310 6.651 o 8 11 7 1396.910 1507.700 64.925 26.198 o 8 11 8 754.247 747.893 72.601 31.076 o 8 11 9 489.715 468.802 42.667 81.026 o 8 11 10 92.630 113.613 31.351 188.662 o 8 11 11 2554.490 2396.410 80.334 13.063 o 8 11 12 4944.380 4758.570 96.802 5.100 o 8 11 13 615.272 534.756 51.350 57.427 o 8 11 14 677.164 609.263 39.450 77.558 o 8 11 15 1351.830 1296.570 65.119 27.518 o 8 11 16 36.201 -25.780 24.526 328.412 o 8 12 0 1366.260 1440.050 67.851 25.501 o 8 12 1 1158.150 1336.510 64.544 29.535 o 8 12 2 697.525 711.601 83.131 25.285 o 8 12 3 2559.820 2538.190 85.258 12.174 o 8 12 4 1034.310 1046.460 111.396 14.079 o 8 12 5 1.601 30.112 25.722 305.298 o 8 12 6 2157.220 2142.310 78.271 15.475 o 8 12 7 3395.060 3517.230 147.974 5.380 o 8 12 8 313.197 348.135 40.358 100.031 o 8 12 9 1253.580 1295.860 63.874 29.123 o 8 12 10 780.458 725.192 51.729 50.863 o 8 12 11 1712.010 1881.800 176.793 5.643 o 8 12 12 3188.640 3144.600 95.581 8.834 o 8 12 13 1619.470 1750.000 72.419 20.812 o 8 12 14 174.103 126.045 26.106 239.118 o 8 12 15 985.803 904.744 56.787 39.908 o 8 13 4 2069.460 2037.510 79.056 15.954 o 8 13 5 1148.260 1231.480 93.107 18.158 o 8 13 6 273.925 273.835 40.358 104.180 o 8 13 7 2964.830 3071.240 145.203 6.066 o 8 13 8 1778.220 1888.400 109.733 11.806 o 8 13 9 474.072 463.593 46.222 72.656 o 8 13 10 1192.360 1267.600 65.837 28.838 o 8 13 11 14.241 26.602 42.120 114.543 o 8 13 12 548.871 488.812 63.180 42.766 o 9 -10 0 1966.910 2037.130 78.743 16.493 o 9 -10 1 11.825 -25.384 47.108 92.173 o 9 -10 2 1151.570 1048.560 77.589 24.288 o 9 -10 3 1172.460 1256.950 85.348 20.511 o 9 -9 0 2153.590 2358.760 90.336 13.074 o 9 -9 1 1006.440 982.732 56.638 39.099 o 9 -9 2 35.264 -2.035 49.325 83.575 o 9 -9 3 1727.150 1796.420 69.882 20.708 o 9 -9 4 2094.880 2058.490 75.049 16.581 o 9 -9 5 302.123 220.065 35.035 130.721 o 9 -9 6 727.693 755.941 67.614 34.987 o 9 -9 7 413.684 373.537 53.204 60.629 o 9 -8 0 3.784 -30.109 45.445 99.261 o 9 -8 1 3541.040 3579.450 98.419 7.613 o 9 -8 2 533.957 469.186 41.008 83.613 o 9 -8 3 687.039 741.041 70.385 33.278 o 9 -8 4 3709.770 3791.260 101.949 7.003 o 9 -8 5 952.371 900.110 53.469 43.623 o 9 -8 6 73.553 85.865 32.698 178.601 o 9 -8 7 727.100 658.848 48.194 58.071 o 9 -8 8 402.504 348.115 43.228 85.718 o 9 -8 9 824.453 832.461 50.873 49.782 o 9 -7 0 717.085 722.604 47.502 58.561 o 9 -7 1 980.441 977.351 51.588 44.205 o 9 -7 2 4565.540 4542.620 126.914 4.740 o 9 -7 3 37.235 61.803 25.829 288.140 o 9 -7 4 350.270 364.608 68.168 40.078 o 9 -7 5 2984.250 2812.310 84.259 10.633 o 9 -7 6 2712.580 2719.620 83.162 11.661 o 9 -7 7 623.115 558.455 44.954 68.698 o 9 -7 8 2351.470 2304.740 84.567 13.354 o 9 -7 9 6.213 -14.398 22.465 403.515 o 9 -7 10 2563.890 2582.450 68.331 14.279 o 9 -7 11 1525.300 1513.010 64.572 25.166 o 9 -6 0 3156.130 3253.400 88.192 9.333 o 9 -6 1 150.253 156.486 30.297 188.765 o 9 -6 2 3868.070 4144.130 103.022 6.488 o 9 -6 3 1440.460 1596.630 96.432 15.592 o 9 -6 4 331.085 291.608 38.240 109.528 o 9 -6 5 1939.020 2073.150 161.829 6.335 o 9 -6 6 4458.880 4344.150 85.261 6.224 o 9 -6 7 530.661 493.206 32.207 112.622 o 9 -6 8 2174.370 2150.300 58.318 19.331 o 9 -6 9 495.500 492.946 33.557 110.187 o 9 -6 10 164.184 161.257 26.189 236.092 o 9 -6 11 3236.630 3059.040 74.546 10.428 o 9 -6 12 1288.250 1294.440 51.087 36.245 o 9 -6 13 281.530 279.321 48.770 75.164 o 9 -5 0 2680.860 2664.450 76.510 12.617 o 9 -5 1 1385.710 1436.040 59.855 29.014 o 9 -5 2 174.875 140.397 37.686 127.961 o 9 -5 3 8629.320 8444.400 212.262 1.531 o 9 -5 4 674.819 762.214 108.625 15.775 o 9 -5 5 16.039 13.536 17.916 611.568 o 9 -5 6 2843.030 2810.790 64.346 13.112 o 9 -5 7 1358.500 1318.100 45.196 38.682 o 9 -5 8 583.518 513.363 32.454 106.464 o 9 -5 9 4172.680 4129.530 84.748 6.805 o 9 -5 10 1587.260 1633.500 52.411 28.947 o 9 -5 11 1673.030 1647.740 73.039 20.608 o 9 -5 12 2880.950 2873.560 92.351 10.073 o 9 -5 13 654.189 532.913 64.214 40.102 o 9 -5 14 36.840 8.867 34.361 169.970 o 9 -4 0 23.911 10.967 22.081 405.219 o 9 -4 1 3239.340 3306.180 85.221 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2795.220 66.040 12.635 o 9 -3 11 869.820 840.976 39.718 64.038 o 9 -3 12 85.489 78.254 26.899 253.515 o 9 -3 13 3484.130 3533.670 94.681 7.964 o 9 -3 14 1298.890 1383.780 61.074 29.642 o 9 -3 15 193.162 217.250 45.445 89.241 o 9 -2 0 2445.550 2488.400 68.804 14.956 o 9 -2 1 10.699 30.541 21.570 425.849 o 9 -2 2 4729.120 4742.410 103.924 5.136 o 9 -2 3 2239.790 2286.570 52.599 19.545 o 9 -2 4 1474.880 1452.170 44.119 35.982 o 9 -2 5 8019.480 7874.130 123.542 2.212 o 9 -2 6 1836.950 1862.490 48.381 26.193 o 9 -2 7 111.085 116.366 19.575 407.416 o 9 -2 8 1681.770 1704.570 49.858 28.405 o 9 -2 9 137.584 123.075 20.975 351.013 o 9 -2 10 20.049 27.485 18.745 549.923 o 9 -2 11 3738.370 3575.440 91.186 7.673 o 9 -2 12 2068.690 1968.110 67.063 18.688 o 9 -2 13 1091.690 1098.730 53.962 38.992 o 9 -2 14 1352.330 1364.540 59.969 29.727 o 9 -2 15 684.546 710.456 64.288 38.602 o 9 -2 16 147.545 116.384 38.795 123.993 o 9 -1 0 6489.960 6722.190 106.218 3.157 o 9 -1 1 2114.920 2257.850 63.755 18.229 o 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19.667 o 10 -7 3 913.984 978.060 60.409 37.342 o 10 -7 4 183.277 256.460 105.854 17.927 o 10 -7 5 75.323 54.094 27.617 246.595 o 10 -7 6 1455.810 1442.170 63.863 26.417 o 10 -7 7 2035.790 1977.840 73.369 17.442 o 10 -7 8 718.868 751.647 64.288 37.945 o 10 -7 10 1096.920 1227.020 89.782 19.417 o 10 -6 0 160.239 170.256 32.973 161.463 o 10 -6 1 2974.300 2861.120 149.636 5.921 o 10 -6 2 3329.490 3451.760 95.607 8.263 o 10 -6 3 1410.560 1578.320 64.362 25.991 o 10 -6 4 1059.980 1083.510 54.555 39.163 o 10 -6 5 614.816 567.378 43.703 71.493 o 10 -6 6 76.805 61.086 42.120 111.102 o 10 -6 7 2533.520 2637.170 166.817 5.470 o 10 -6 8 989.552 1040.630 88.119 20.875 o 10 -6 9 230.985 212.343 38.255 118.545 o 10 -6 10 1085.340 1054.930 48.380 44.333 o 10 -6 11 1264.470 1246.530 66.399 27.954 o 10 -5 0 1306.390 1268.940 74.818 23.689 o 10 -5 1 278.680 274.113 37.686 116.180 o 10 -5 2 4293.650 4275.150 106.282 5.765 o 10 -5 3 3651.370 3556.620 95.793 7.593 o 10 -5 4 375.842 320.200 35.346 118.819 o 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2274.720 75.968 15.814 o 10 0 5 1519.040 1590.370 47.337 32.474 o 10 0 6 1381.330 1473.670 77.978 21.355 o 10 0 7 3.918 -33.142 19.407 541.380 o 10 0 8 6884.730 6732.810 136.726 2.679 o 10 0 9 1323.690 1340.200 53.342 33.941 o 10 0 10 40.892 55.984 27.156 262.070 o 10 0 11 1942.670 1925.500 65.160 20.105 o 10 0 12 1454.380 1450.280 59.770 28.229 o 10 0 13 581.997 484.102 41.794 79.000 o 10 0 14 2321.640 2228.690 107.517 10.523 o 10 0 15 885.419 899.298 66.505 33.448 o 10 1 0 2315.080 2511.790 54.193 17.958 o 10 1 1 871.076 910.695 34.092 71.796 o 10 1 2 501.610 528.181 23.123 157.426 o 10 1 3 3925.280 4175.620 75.873 7.532 o 10 1 4 3982.590 4211.720 76.756 7.362 o 10 1 5 13.434 28.970 16.797 683.949 o 10 1 6 5775.950 5792.840 119.477 3.628 o 10 1 7 755.111 737.713 39.765 70.594 o 10 1 8 2051.700 2054.880 70.939 17.673 o 10 1 9 3245.070 3264.380 84.187 9.412 o 10 1 10 649.721 733.037 42.575 69.384 o 10 1 11 82.948 130.400 26.899 248.015 o 10 1 12 2311.010 2174.470 71.001 15.990 o 10 1 13 3134.610 3011.610 86.476 9.799 o 10 1 14 604.444 593.300 44.654 69.366 o 10 1 15 1422.960 1408.000 63.755 26.939 o 10 1 16 100.146 124.621 33.284 167.816 o 10 2 0 3316.600 3467.050 65.200 10.304 o 10 2 1 5192.870 5506.290 79.302 4.862 o 10 2 2 427.914 462.497 21.752 186.448 o 10 2 3 1192.640 1370.120 33.792 50.672 o 10 2 4 4507.810 4863.970 72.376 6.184 o 10 2 5 3413.980 3600.220 88.673 8.391 o 10 2 6 873.822 842.791 43.863 57.640 o 10 2 7 4451.000 4427.490 198.961 3.132 o 10 2 8 69.766 35.119 24.939 301.523 o 10 2 9 2360.760 2391.000 104.745 10.578 o 10 2 10 3571.490 3533.550 89.878 8.082 o 10 2 11 1702.480 1726.430 61.864 23.684 o 10 2 12 1407.360 1467.310 94.216 16.460 o 10 2 13 2707.680 2546.270 78.975 12.437 o 10 2 14 796.514 761.883 48.291 54.701 o 10 2 15 2220.110 2166.690 76.510 15.458 o 10 2 16 747.023 607.414 47.502 59.344 o 10 3 0 376.980 340.346 38.681 103.282 o 10 3 1 7467.580 7707.450 100.259 2.567 o 10 3 2 2941.540 3013.040 51.407 13.564 o 10 3 3 32.486 13.293 15.410 780.859 o 10 3 4 3396.300 3577.120 68.130 9.741 o 10 3 5 5052.460 5118.140 87.277 5.033 o 10 3 6 2221.480 2299.520 65.809 17.077 o 10 3 7 1884.460 1911.740 60.963 21.707 o 10 3 8 1526.550 1558.150 56.334 28.395 o 10 3 9 467.876 442.035 35.346 107.156 o 10 3 10 7859.720 7534.350 152.739 2.119 o 10 3 11 1633.610 1606.680 60.285 25.413 o 10 3 12 301.489 287.388 32.754 141.539 o 10 3 13 493.401 522.173 41.451 83.031 o 10 3 14 1932.280 1941.290 70.070 18.892 o 10 3 15 168.210 181.355 31.678 171.136 o 10 3 16 3312.730 3360.980 131.902 6.267 o 10 4 0 830.000 901.136 29.874 82.047 o 10 4 1 190.046 199.454 17.786 380.181 o 10 4 2 5865.070 6196.530 127.574 3.350 o 10 4 3 4736.180 5023.160 110.802 4.822 o 10 4 4 433.098 425.619 25.418 163.291 o 10 4 5 3601.840 3814.040 88.311 7.855 o 10 4 6 6294.560 6325.760 103.899 3.390 o 10 4 7 39.985 24.671 15.973 709.181 o 10 4 8 4545.330 4523.570 103.924 5.433 o 10 4 9 316.758 298.382 31.678 146.276 o 10 4 10 2382.100 2287.670 70.692 15.426 o 10 4 11 3600.670 3549.460 92.577 7.862 o 10 4 12 2133.220 2162.420 71.327 16.863 o 10 4 13 286.562 320.540 35.142 127.162 o 10 4 14 1741.870 1747.880 67.186 21.579 o 10 4 15 1284.750 1326.550 141.323 8.901 o 10 4 16 789.296 785.570 52.442 49.118 o 10 5 0 1919.530 1932.220 41.053 27.079 o 10 5 1 738.326 712.598 41.186 69.057 o 10 5 2 4393.720 4518.610 106.095 5.529 o 10 5 3 6963.090 7126.320 145.680 2.500 o 10 5 4 2603.810 2728.620 77.127 12.703 o 10 5 5 879.107 897.335 45.605 54.313 o 10 5 6 2593.610 2814.640 60.067 14.696 o 10 5 7 1453.290 1569.360 44.284 35.250 o 10 5 8 2430.160 2386.180 54.765 17.529 o 10 5 9 834.490 744.435 43.124 61.591 o 10 5 10 551.206 470.930 37.548 92.950 o 10 5 11 1404.620 1399.740 68.722 24.980 o 10 5 12 4912.260 4686.430 113.090 4.758 o 10 5 13 1068.810 1047.260 56.529 37.730 o 10 5 14 560.462 512.406 59.855 46.401 o 10 5 15 971.354 985.153 80.360 24.350 o 10 5 16 68.438 60.560 28.906 227.420 o 10 6 0 2003.160 1983.180 65.643 19.388 o 10 6 1 1516.950 1484.050 58.720 27.852 o 10 6 2 64.291 58.639 24.259 314.924 o 10 6 3 4967.820 5037.670 116.293 4.493 o 10 6 4 5261.950 5283.740 119.009 4.127 o 10 6 5 1637.730 1636.180 59.648 25.473 o 10 6 6 1082.480 1152.630 50.974 41.131 o 10 6 7 2678.490 2817.920 61.487 14.120 o 10 6 8 7.263 16.232 16.808 702.118 o 10 6 9 2872.380 2958.030 64.270 12.715 o 10 6 10 3347.980 3394.060 89.309 8.691 o 10 6 11 134.672 117.394 41.011 112.647 o 10 6 12 2845.600 2742.950 82.016 11.346 o 10 6 13 1725.320 1633.590 64.700 22.930 o 10 6 14 206.044 221.290 75.372 34.613 o 10 6 15 174.338 165.154 31.159 176.184 o 10 6 16 1042.990 905.126 54.265 41.202 o 10 7 0 0.906 5.369 25.044 326.050 o 10 7 1 1394.790 1494.340 61.784 27.689 o 10 7 2 317.225 319.604 32.890 137.426 o 10 7 3 677.066 668.366 44.817 65.242 o 10 7 4 5544.730 5851.240 153.516 3.205 o 10 7 5 3627.500 3570.610 93.896 7.724 o 10 7 6 16.586 20.346 24.939 321.101 o 10 7 7 1341.780 1312.110 56.285 32.169 o 10 7 8 2161.860 2110.850 68.308 17.452 o 10 7 9 1376.690 1321.720 43.168 39.629 o 10 7 10 2752.280 2670.400 62.242 14.030 o 10 7 11 573.273 557.384 32.568 105.125 o 10 7 12 273.704 214.766 32.224 152.099 o 10 7 13 1167.040 1101.810 55.383 36.690 o 10 7 14 1763.820 1654.920 75.927 19.210 o 10 7 15 122.150 97.358 30.596 194.001 o 10 7 16 1412.980 1393.790 65.711 26.226 o 10 8 0 826.540 843.998 64.842 35.670 o 10 8 1 408.064 337.271 37.401 106.636 o 10 8 2 3093.140 3058.420 90.320 9.533 o 10 8 3 554.110 543.946 41.142 80.587 o 10 8 4 4974.200 4955.720 119.009 4.457 o 10 8 5 3872.440 4142.740 285.972 1.996 o 10 8 6 2080.240 2114.890 71.558 17.223 o 10 8 7 68.601 70.385 27.432 249.343 o 10 8 8 1085.760 1036.640 51.904 41.348 o 10 8 9 202.061 167.251 29.506 188.228 o 10 8 10 1381.640 1377.670 53.014 33.034 o 10 8 11 1935.350 1852.520 53.321 23.715 o 10 8 12 357.131 329.017 28.434 161.600 o 10 8 13 1397.600 1310.750 99.758 15.422 o 10 8 14 3754.110 3665.380 214.479 3.167 o 10 8 15 296.302 327.724 39.435 105.334 o 10 8 16 210.252 206.166 47.662 81.542 o 10 9 0 1921.270 2062.720 122.480 9.714 o 10 9 1 59.983 60.653 29.384 222.064 o 10 9 2 3732.940 3952.250 108.733 6.541 o 10 9 3 1777.480 1873.940 71.992 19.547 o 10 9 4 200.917 219.944 69.830 40.091 o 10 9 5 1945.190 2089.640 113.613 10.707 o 10 9 6 1530.280 1591.690 66.142 24.178 o 10 9 7 1165.660 1213.640 57.935 34.146 o 10 9 8 929.850 1035.450 142.986 9.170 o 10 9 9 1192.460 1293.610 149.082 8.196 o 10 9 10 1.730 -6.667 26.247 297.435 o 10 9 11 3103.960 3012.440 88.831 9.681 o 10 9 12 1949.980 1895.260 56.702 22.429 o 10 9 13 125.054 114.096 24.595 278.945 o 10 9 14 1054.430 1039.430 128.576 10.954 o 10 9 15 817.440 664.549 51.225 51.375 o 10 10 0 1387.700 1374.230 131.348 9.931 o 10 10 1 1321.250 1434.380 97.541 15.994 o 10 10 2 432.300 449.997 45.276 76.718 o 10 10 3 2786.190 2890.700 91.970 10.318 o 10 10 4 1274.990 1154.320 89.782 18.818 o 10 10 5 148.607 155.017 45.445 91.927 o 10 10 6 2294.590 2308.890 167.925 5.670 o 10 10 7 2596.110 2715.300 181.226 4.774 o 10 10 8 46.501 16.842 28.085 248.824 o 10 10 9 1675.590 1757.970 69.334 21.355 o 10 10 10 975.965 824.706 69.830 30.660 o 10 10 11 1638.820 1549.980 67.350 23.039 o 10 10 12 3256.160 3118.080 93.964 8.841 o 10 10 13 373.349 386.560 55.191 57.653 o 10 10 14 50.528 2.979 24.934 312.972 o 10 10 15 465.148 352.477 55.421 55.823 o 10 11 3 973.705 959.096 145.757 8.849 o 10 11 4 3851.070 4152.770 140.215 5.056 o 10 11 5 370.478 453.036 45.062 79.524 o 10 11 6 1761.720 1726.490 72.777 19.882 o 10 11 7 1439.040 1498.410 68.918 24.226 o 10 11 8 608.260 570.648 47.374 64.182 o 10 11 9 103.284 48.687 31.321 191.930 o 10 11 10 1107.860 1013.610 106.408 15.074 o 10 11 11 74.455 62.071 32.135 185.824 o 10 11 12 2509.810 2680.150 125.251 8.090 o 10 11 13 1634.980 1604.990 99.758 14.257 o 10 11 14 553.836 514.306 66.505 39.053 o 11 -7 0 835.376 888.818 57.727 41.547 o 11 -7 1 573.483 578.968 58.192 47.795 o 11 -7 2 416.508 433.569 67.059 40.306 o 11 -7 3 2942.970 3014.000 95.005 9.535 o 11 -7 4 406.683 462.071 45.445 76.990 o 11 -7 5 106.737 94.216 48.770 82.525 o 11 -6 0 1132.780 1208.660 60.647 32.843 o 11 -6 1 182.066 215.540 45.445 89.670 o 11 -6 2 390.393 394.071 42.766 86.684 o 11 -6 3 1602.300 1576.350 67.521 23.159 o 11 -6 4 4520.990 4645.700 118.990 4.957 o 11 -6 5 400.085 471.223 50.987 64.183 o 11 -6 6 1447.410 1268.210 62.335 28.048 o 11 -6 7 514.070 579.679 52.650 57.099 o 11 -6 8 120.169 155.178 52.096 71.822 o 11 -5 0 233.638 253.731 67.614 42.211 o 11 -5 1 199.678 173.336 33.248 154.802 o 11 -5 2 1261.010 1322.250 60.285 30.848 o 11 -5 3 20.998 12.639 29.562 230.228 o 11 -5 4 5553.080 5638.900 132.682 3.588 o 11 -5 5 1901.580 1934.420 73.064 18.367 o 11 -5 6 1.480 -9.422 45.999 96.953 o 11 -5 7 939.839 1030.000 56.989 39.470 o 11 -5 8 291.411 291.961 52.650 65.342 o 11 -5 9 2.882 15.739 27.131 276.261 o 11 -5 10 622.856 598.152 49.868 58.921 o 11 -5 11 717.166 717.429 54.130 49.170 o 11 -4 0 1332.820 1354.370 156.841 7.371 o 11 -4 1 71.967 83.059 29.985 210.106 o 11 -4 2 1678.690 1767.180 84.794 17.078 o 11 -4 3 730.806 744.689 48.121 56.917 o 11 -4 4 1850.870 2006.940 71.327 18.875 o 11 -4 5 2300.950 2605.630 82.218 13.338 o 11 -4 6 1683.820 1752.230 125.251 10.008 o 11 -4 7 314.588 280.720 34.886 127.893 o 11 -4 8 1195.270 1212.890 58.192 33.591 o 11 -4 9 116.439 94.435 23.852 299.602 o 11 -4 10 411.786 392.383 37.883 102.682 o 11 -4 11 1372.600 1341.190 90.890 17.706 o 11 -3 0 1507.520 1607.350 61.864 25.988 o 11 -3 1 204.477 189.842 43.782 95.493 o 11 -3 2 1288.950 1317.890 85.902 19.615 o 11 -3 3 464.974 407.424 38.814 95.623 o 11 -3 4 717.966 827.900 59.855 41.695 o 11 -3 5 2513.880 2529.990 78.084 13.268 o 11 -3 6 4011.780 4057.590 103.022 6.357 o 11 -3 7 414.499 419.034 31.886 128.264 o 11 -3 8 828.716 1002.730 54.772 43.636 o 11 -3 9 571.504 556.154 48.791 62.788 o 11 -3 10 22.739 -3.524 26.177 293.270 o 11 -3 11 1267.470 1198.690 58.532 32.538 o 11 -3 12 1829.210 1792.740 69.544 20.142 o 11 -2 0 3427.200 3606.850 166.817 4.610 o 11 -2 1 169.073 232.314 43.228 98.292 o 11 -2 2 350.763 305.899 34.555 125.501 o 11 -2 3 2198.560 2349.870 73.028 15.752 o 11 -2 4 1637.700 1697.770 135.227 8.970 o 11 -2 5 201.566 183.385 65.397 45.574 o 11 -2 6 4817.700 4938.450 92.534 5.242 o 11 -2 7 1991.980 2112.030 67.259 18.672 o 11 -2 8 0.934 -18.116 18.063 627.918 o 11 -2 9 570.826 566.188 41.097 79.441 o 11 -2 10 941.332 900.253 49.868 47.611 o 11 -2 11 268.495 214.514 33.925 140.905 o 11 -2 12 2410.280 2503.770 118.601 8.947 o 11 -2 13 1474.850 1583.580 89.228 17.241 o 11 -1 0 25.412 49.679 23.895 339.880 o 11 -1 1 1452.390 1551.990 57.411 28.784 o 11 -1 2 473.820 512.629 38.189 94.189 o 11 -1 3 1133.740 1287.610 53.927 36.819 o 11 -1 4 3410.010 3655.970 92.577 8.111 o 11 -1 5 1091.000 1169.370 69.276 28.391 o 11 -1 6 1168.140 1211.570 42.686 45.816 o 11 -1 7 3019.520 3251.600 152.407 5.589 o 11 -1 8 2734.870 2825.090 78.743 11.909 o 11 -1 9 48.409 79.871 26.099 277.123 o 11 -1 10 1012.790 967.142 49.868 45.355 o 11 -1 11 181.120 201.555 32.473 161.500 o 11 -1 12 1797.570 1847.370 70.331 19.954 o 11 -1 13 3135.050 3191.610 93.599 9.042 o 11 -1 14 644.547 638.449 75.372 30.440 o 11 0 0 1538.190 1664.670 58.072 26.948 o 11 0 1 910.548 969.084 46.511 51.381 o 11 0 2 993.054 1156.300 58.746 36.332 o 11 0 3 21.904 -2.561 22.689 388.116 o 11 0 4 3142.650 3242.910 83.688 9.719 o 11 0 5 2903.550 2988.130 113.686 8.156 o 11 0 6 1903.820 1900.600 61.784 21.373 o 11 0 7 4113.700 4118.080 97.934 6.387 o 11 0 8 2458.870 2470.770 73.129 14.296 o 11 0 9 212.003 199.041 29.985 179.612 o 11 0 10 830.786 879.524 48.606 51.923 o 11 0 11 313.705 321.667 34.346 129.196 o 11 0 12 129.343 141.551 29.017 207.819 o 11 0 13 1828.570 1885.910 71.117 19.429 o 11 0 14 2168.300 2204.690 126.914 8.769 o 11 1 0 4813.510 5110.570 111.438 4.702 o 11 1 1 255.422 252.548 28.968 178.358 o 11 1 2 1612.020 1622.110 78.698 19.374 o 11 1 3 187.817 206.002 26.828 217.372 o 11 1 4 197.524 174.266 22.141 289.452 o 11 1 5 4403.040 4610.740 103.741 5.544 o 11 1 6 4447.070 4651.770 104.946 5.438 o 11 1 7 256.001 253.333 30.892 162.004 o 11 1 8 3529.950 3708.250 116.938 6.566 o 11 1 9 673.592 613.737 41.186 73.717 o 11 1 10 104.601 91.003 28.819 219.263 o 11 1 11 794.673 823.844 53.758 47.048 o 11 1 12 494.549 447.666 39.399 90.928 o 11 1 13 76.263 103.345 29.017 220.555 o 11 1 14 2022.660 1971.880 73.691 17.457 o 11 2 0 6129.050 6420.350 102.946 3.468 o 11 2 1 1243.260 1243.960 68.897 26.918 o 11 2 2 591.853 621.490 37.958 85.237 o 11 2 3 1500.450 1615.400 67.059 23.980 o 11 2 4 160.141 142.969 26.357 236.795 o 11 2 5 934.324 895.591 65.951 33.346 o 11 2 6 5004.210 5218.840 114.302 4.438 o 11 2 7 904.691 1035.220 61.517 36.196 o 11 2 8 484.587 466.506 36.613 100.380 o 11 2 9 1592.610 1582.220 78.698 19.591 o 11 2 10 1072.430 1024.350 51.091 42.429 o 11 2 11 1212.990 1299.070 56.638 33.763 o 11 2 12 559.511 588.586 44.029 72.449 o 11 2 13 227.356 218.791 35.469 134.533 o 11 2 14 1507.920 1522.530 65.487 24.912 o 11 2 15 2726.910 2678.360 200.624 4.032 o 11 3 0 2558.250 2668.580 57.664 15.554 o 11 3 1 2943.820 3153.330 62.830 12.217 o 11 3 2 17.846 -24.385 24.385 338.661 o 11 3 3 876.168 849.149 43.807 57.550 o 11 3 4 1008.990 1063.940 51.541 42.854 o 11 3 5 4.877 4.570 64.288 49.604 o 11 3 6 1197.970 1311.730 55.975 34.304 o 11 3 7 3873.780 4001.950 155.178 4.594 o 11 3 8 1457.290 1518.500 58.019 28.636 o 11 3 9 2688.490 2596.460 76.841 12.671 o 11 3 10 2416.570 2515.300 76.379 13.908 o 11 3 11 4.698 -26.021 22.761 393.922 o 11 3 12 1634.530 1726.430 65.020 23.178 o 11 3 13 368.330 482.245 42.280 87.220 o 11 3 14 48.262 38.159 28.455 240.247 o 11 3 15 2752.200 2805.890 89.766 10.730 o 11 4 0 83.860 37.343 18.145 514.459 o 11 4 1 2409.100 2404.160 95.324 11.566 o 11 4 2 1468.290 1511.040 56.625 29.204 o 11 4 3 107.764 114.223 25.391 269.413 o 11 4 4 895.702 970.934 46.714 51.495 o 11 4 5 158.660 166.011 20.346 345.146 o 11 4 6 9.457 12.448 20.198 491.069 o 11 4 7 8866.340 8873.430 172.168 1.646 o 11 4 8 3673.020 3534.950 91.210 7.822 o 11 4 9 65.582 100.568 43.228 105.348 o 11 4 10 1932.630 1908.720 65.643 20.107 o 11 4 11 155.512 128.594 29.262 201.553 o 11 4 12 124.526 69.678 53.758 68.351 o 11 4 13 1411.450 1380.440 89.782 17.775 o 11 4 14 1066.180 1155.070 59.803 34.587 o 11 4 15 843.758 744.933 51.588 49.441 o 11 5 0 2615.920 2592.590 103.083 9.971 o 11 5 1 1612.940 1590.030 60.175 25.732 o 11 5 2 4790.150 5102.320 117.909 4.569 o 11 5 3 664.022 669.046 42.452 70.313 o 11 5 4 209.673 196.576 28.873 191.115 o 11 5 5 1461.740 1508.560 57.745 28.769 o 11 5 6 182.412 211.936 28.407 199.420 o 11 5 7 1714.130 1687.290 73.156 20.190 o 11 5 8 7750.880 7776.050 156.816 2.089 o 11 5 9 1233.050 1190.140 68.722 27.329 o 11 5 10 54.208 105.211 26.836 258.820 o 11 5 11 821.882 766.577 49.879 51.858 o 11 5 12 56.104 76.481 55.421 65.462 o 11 5 13 2392.390 2518.550 165.154 5.685 o 11 5 14 2608.640 2494.350 82.681 12.406 o 11 5 15 1147.880 1169.280 60.436 33.035 o 11 6 0 5618.300 5845.800 192.865 2.621 o 11 6 1 295.119 320.749 60.963 50.000 o 11 6 2 3074.500 3105.300 103.083 8.543 o 11 6 3 2701.290 2885.110 84.473 11.306 o 11 6 4 12.288 -6.760 23.895 354.593 o 11 6 5 1292.720 1358.460 57.411 31.862 o 11 6 6 1018.850 1046.740 51.904 42.497 o 11 6 7 80.657 130.507 26.614 253.210 o 11 6 8 2666.790 2640.940 61.264 14.609 o 11 6 9 5147.240 5127.670 117.519 4.295 o 11 6 10 463.213 534.694 68.722 37.701 o 11 6 11 2191.570 2251.640 74.461 15.761 o 11 6 12 144.530 106.387 27.668 225.761 o 11 6 13 301.838 256.576 35.687 125.539 o 11 6 14 2014.290 2011.190 143.540 7.610 o 11 6 15 1951.540 1868.720 95.324 13.699 o 11 7 0 4154.370 4257.430 155.178 4.333 o 11 7 1 3648.250 3793.150 103.315 7.024 o 11 7 2 228.255 235.752 69.830 39.830 o 11 7 3 996.502 1002.840 53.927 41.465 o 11 7 4 1088.830 1090.510 55.152 38.164 o 11 7 5 354.735 364.132 55.975 56.818 o 11 7 6 2140.780 2192.970 104.191 11.386 o 11 7 7 2410.880 2500.100 77.840 13.750 o 11 7 8 82.496 50.838 27.156 253.041 o 11 7 9 5916.950 5894.890 132.117 3.336 o 11 7 10 2023.600 2038.360 68.804 18.353 o 11 7 11 185.509 193.796 32.184 163.852 o 11 7 12 975.379 981.513 53.797 42.147 o 11 7 13 313.564 293.794 64.842 44.635 o 11 7 14 292.954 231.782 36.137 124.762 o 11 7 15 1901.680 1923.100 103.083 12.482 o 11 8 0 885.590 911.538 58.072 40.261 o 11 8 1 3459.230 3671.080 142.986 5.472 o 11 8 2 2442.930 2475.400 83.764 12.854 o 11 8 3 91.868 126.706 34.361 159.078 o 11 8 4 1696.670 1723.890 82.577 17.639 o 11 8 5 116.632 100.379 36.024 144.909 o 11 8 6 1490.490 1538.720 64.572 25.361 o 11 8 7 3592.500 3755.030 100.879 7.259 o 11 8 8 586.438 546.737 43.556 73.291 o 11 8 9 662.236 632.546 45.725 64.631 o 11 8 10 2954.190 2907.420 101.974 9.046 o 11 8 11 757.791 630.690 67.614 35.319 o 11 8 12 156.290 144.339 30.962 181.944 o 11 8 13 841.267 924.308 53.342 45.632 o 11 8 14 22.587 57.638 37.686 141.163 o 11 8 15 1811.290 1867.680 104.191 12.611 o 11 9 0 455.122 481.053 68.722 38.024 o 11 9 1 2392.190 2418.880 86.391 12.761 o 11 9 2 3813.990 4088.950 155.178 4.604 o 11 9 3 311.489 289.419 39.880 103.684 o 11 9 4 1008.650 1122.740 146.311 8.696 o 11 9 5 653.294 582.183 47.374 62.659 o 11 9 6 96.967 75.499 30.951 195.154 o 11 9 7 964.397 899.155 94.216 19.100 o 11 9 8 2172.700 2164.140 116.938 9.815 o 11 9 9 312.300 263.635 36.737 118.928 o 11 9 10 1548.200 1471.280 113.059 12.236 o 11 9 11 4702.800 4775.390 310.357 1.637 o 11 9 12 46.292 36.578 44.337 102.188 o 11 9 13 693.260 595.220 65.397 38.140 o 11 9 14 195.780 161.829 45.445 90.139 o 11 10 3 1135.530 740.423 75.372 26.520 o 11 10 4 4.022 44.870 30.951 210.502 o 11 10 5 1440.350 1391.190 68.066 24.994 o 11 10 6 220.494 278.595 40.085 108.210 o 11 10 7 376.656 395.456 43.367 85.382 o 11 10 8 1724.800 1727.970 72.689 20.131 o 11 10 9 1824.930 1852.440 111.950 11.421 o 11 10 10 3.646 -14.724 26.247 296.914 o 11 10 11 1572.820 1739.110 98.649 14.463 o 11 10 12 842.637 744.857 70.939 31.478 o 11 10 13 54.211 18.843 39.903 125.582 o 12 -5 0 1138.940 1263.800 63.586 30.663 o 12 -5 1 1793.630 2120.750 78.416 17.198 o 12 -5 2 66.818 25.658 36.578 147.528 o 12 -5 3 1439.040 1508.810 68.492 24.353 o 12 -5 4 1767.550 1833.640 140.215 8.250 o 12 -5 5 8.891 3.739 31.036 211.575 o 12 -5 6 1421.160 1435.400 103.083 14.441 o 12 -5 7 540.515 464.427 73.156 33.478 o 12 -5 8 215.715 135.227 52.096 70.009 o 12 -4 0 652.582 597.955 49.879 58.138 o 12 -4 1 2430.520 2531.590 130.793 7.856 o 12 -4 2 934.833 965.645 56.192 40.771 o 12 -4 3 78.514 65.807 31.389 193.356 o 12 -4 4 2019.890 2243.390 79.530 15.625 o 12 -4 5 1103.470 1250.850 60.556 33.002 o 12 -4 6 211.516 213.429 36.028 132.592 o 12 -4 7 2011.070 2149.850 78.084 16.157 o 12 -4 8 45.410 78.698 46.553 92.279 o 12 -3 0 10.106 -12.747 26.648 286.429 o 12 -3 1 2979.010 3258.060 93.700 9.296 o 12 -3 2 1445.110 1490.200 108.071 13.321 o 12 -3 3 1117.340 1203.680 58.392 34.558 o 12 -3 4 210.292 222.535 34.555 141.828 o 12 -3 5 3246.540 3309.870 94.487 8.632 o 12 -3 6 112.134 94.412 30.773 193.672 o 12 -3 7 1853.450 1981.880 149.636 7.293 o 12 -3 8 1524.390 1406.580 80.915 19.773 o 12 -3 9 167.781 157.395 42.120 104.768 o 12 -3 10 1356.550 1335.640 89.782 18.096 o 12 -3 11 471.440 492.137 63.180 43.711 o 12 -2 0 745.287 747.602 72.047 31.534 o 12 -2 1 101.308 111.043 29.752 206.072 o 12 -2 2 1730.610 1847.460 68.308 20.971 o 12 -2 3 4136.920 4183.390 106.621 5.986 o 12 -2 4 237.506 205.398 45.999 85.991 o 12 -2 5 878.882 916.669 52.691 45.673 o 12 -2 6 984.844 949.735 51.444 44.533 o 12 -2 7 339.935 262.695 46.553 79.778 o 12 -2 8 2900.720 2765.500 113.059 8.390 o 12 -2 9 1324.210 1323.130 58.532 31.064 o 12 -2 10 173.828 206.432 33.138 156.663 o 12 -2 11 849.961 836.855 75.372 28.242 o 12 -2 12 523.695 589.678 69.830 35.883 o 12 -1 0 2607.250 2748.510 80.641 12.237 o 12 -1 1 1089.330 1307.660 56.814 35.307 o 12 -1 2 1207.480 1262.040 63.734 29.855 o 12 -1 3 2984.210 3188.330 87.520 9.864 o 12 -1 4 1557.210 1688.070 90.336 16.425 o 12 -1 5 280.474 282.001 34.246 134.578 o 12 -1 6 811.281 833.530 63.180 37.295 o 12 -1 7 1000.910 1002.010 68.722 30.304 o 12 -1 8 1580.460 1552.530 60.998 25.901 o 12 -1 9 2821.250 2837.630 133.564 7.002 o 12 -1 10 494.696 511.616 42.236 81.054 o 12 -1 11 192.620 129.325 31.389 173.991 o 12 -1 12 1176.970 1244.750 90.890 18.694 o 12 0 0 2410.820 2726.710 118.601 8.764 o 12 0 1 2272.800 2381.350 84.240 13.547 o 12 0 2 54.209 52.331 25.829 284.705 o 12 0 3 2556.980 2896.810 80.981 12.119 o 12 0 4 1119.620 1275.460 55.421 36.071 o 12 0 5 1287.190 1387.740 74.264 23.634 o 12 0 6 335.590 333.634 44.337 85.318 o 12 0 7 2485.900 2558.760 84.794 12.437 o 12 0 8 49.999 81.891 25.829 281.753 o 12 0 9 2464.720 2567.350 78.698 13.299 o 12 0 10 3277.900 3269.510 91.540 8.812 o 12 0 11 130.122 160.286 30.773 186.413 o 12 0 12 934.401 973.631 54.753 42.044 o 12 0 13 677.528 762.591 76.481 29.051 o 12 1 0 22.255 -37.686 35.469 161.308 o 12 1 1 3298.990 3546.940 133.010 6.129 o 12 1 2 1385.130 1448.500 56.625 30.573 o 12 1 3 26.283 73.156 35.469 157.926 o 12 1 4 3294.020 3309.740 116.384 7.163 o 12 1 5 3303.510 3634.500 125.251 6.464 o 12 1 6 94.174 69.152 25.829 271.373 o 12 1 7 1089.150 1202.020 52.232 39.538 o 12 1 8 1540.060 1620.740 86.457 17.603 o 12 1 9 752.986 705.975 45.276 61.356 o 12 1 10 3409.950 3293.550 91.540 8.522 o 12 1 11 2383.300 2462.790 80.915 13.484 o 12 1 12 173.516 133.856 38.795 121.827 o 12 1 13 539.745 573.052 70.939 34.865 o 12 2 0 541.574 517.033 39.399 86.623 o 12 2 1 27.845 25.374 34.915 164.798 o 12 2 4 2275.500 2418.570 96.432 11.769 o 12 2 5 2964.740 3101.320 82.462 10.457 o 12 2 6 2016.710 2220.150 123.034 9.374 o 12 2 7 507.346 510.017 75.927 31.433 o 12 2 8 698.559 742.926 45.445 62.205 o 12 2 9 954.640 995.740 119.155 12.712 o 12 2 10 1383.590 1378.040 106.962 13.822 o 12 2 11 3194.560 3363.690 232.214 2.990 o 12 2 12 780.144 778.378 131.902 10.915 o 12 2 13 158.651 163.096 34.007 153.630 o 12 3 0 1779.390 2012.560 66.022 20.706 o 12 3 1 867.042 980.950 63.180 35.703 o 12 3 4 212.867 237.201 47.662 80.991 o 12 3 5 1421.010 1513.410 73.710 22.489 o 12 3 6 1028.760 1005.630 49.788 44.700 o 12 3 7 1433.660 1568.180 59.803 27.807 o 12 3 8 1639.040 1563.080 61.384 25.149 o 12 3 9 1619.430 1598.240 62.479 24.756 o 12 3 10 3.280 -0.182 25.553 313.326 o 12 3 11 2394.700 2474.000 109.733 9.874 o 12 3 12 2543.680 2688.150 132.456 7.492 o 12 3 13 45.782 93.431 31.115 199.154 o 12 4 0 1145.950 1156.080 69.830 27.672 o 12 4 1 1959.820 1995.150 89.782 14.448 o 12 4 2 130.553 48.770 38.795 127.137 o 12 4 3 3373.250 3974.790 138.552 5.601 o 12 4 4 1782.740 1917.560 97.541 13.756 o 12 4 5 361.442 305.923 48.770 72.474 o 12 4 6 546.856 478.836 58.746 48.306 o 12 4 7 2407.340 2462.000 146.311 6.801 o 12 4 8 359.734 339.686 35.419 118.969 o 12 4 9 1790.340 1865.060 67.035 20.861 o 12 4 10 1805.210 1901.390 69.111 20.062 o 12 4 11 329.335 383.564 68.722 39.593 o 12 4 12 1972.770 1801.130 70.692 18.918 o 12 4 13 1450.460 1398.010 64.362 26.456 o 12 5 0 8.149 -1.108 29.927 227.838 o 12 5 1 1247.300 1202.630 78.698 22.728 o 12 5 2 400.414 483.270 56.529 53.988 o 12 5 3 889.269 917.829 107.517 15.433 o 12 5 4 5051.500 5277.440 186.214 2.997 o 12 5 5 1697.920 1873.230 100.866 13.475 o 12 5 6 340.219 304.815 53.204 62.965 o 12 5 7 889.362 1143.890 80.915 24.110 o 12 5 8 462.735 491.633 40.210 88.899 o 12 5 9 296.065 312.739 35.945 122.381 o 12 5 10 1730.290 1661.820 65.229 22.605 o 12 5 11 1545.930 1446.060 74.818 21.498 o 12 5 12 1583.450 1583.790 66.025 23.817 o 12 5 13 1649.740 1778.660 71.483 20.805 o 12 6 0 1263.580 1415.450 86.457 19.328 o 12 6 1 177.062 199.515 48.770 79.233 o 12 6 2 1695.000 1871.050 70.422 20.517 o 12 6 3 18.680 -6.944 26.338 290.853 o 12 6 4 3866.690 4050.950 105.240 6.457 o 12 6 5 3485.380 3609.760 97.036 7.759 o 12 6 6 128.510 131.769 29.752 200.026 o 12 6 7 57.795 66.505 39.903 124.114 o 12 6 8 699.399 745.965 70.939 32.731 o 12 6 9 503.171 422.307 65.397 41.244 o 12 6 10 2282.230 2261.840 117.492 9.477 o 12 6 11 2552.230 2584.230 82.677 12.444 o 12 6 12 25.922 14.469 35.469 160.406 o 12 6 13 1095.720 1084.030 77.589 24.537 o 12 7 0 1891.730 1818.910 100.866 13.007 o 12 7 1 68.091 97.541 44.337 100.312 o 12 7 2 1336.790 1335.700 63.253 28.385 o 12 7 3 1400.160 1448.530 64.487 26.634 o 12 7 4 588.443 540.040 44.236 71.811 o 12 7 5 2557.240 2831.680 87.261 11.501 o 12 7 6 2163.370 2205.870 99.203 11.987 o 12 7 7 400.987 466.368 95.878 20.967 o 12 7 8 1506.300 1599.450 99.758 14.652 o 12 7 9 474.401 344.718 56.529 53.904 o 12 7 11 2845.620 2811.060 123.589 7.658 o 12 7 12 954.718 953.686 54.262 42.326 o 12 7 13 2.883 58.746 36.578 151.049 o 12 8 1 978.824 900.035 87.565 21.453 o 12 8 2 368.283 325.689 40.874 95.765 o 12 8 3 2160.950 2184.450 113.613 10.191 o 12 8 4 960.787 887.227 55.937 41.223 o 12 8 5 657.223 689.505 49.996 56.666 o 12 8 6 3334.000 3416.880 186.768 4.064 o 12 8 7 1192.840 1249.300 62.217 30.944 o 12 8 8 214.546 175.083 31.877 164.062 o 12 8 9 611.350 589.678 70.939 34.179 o 12 8 10 184.314 221.684 50.987 72.570 o 12 8 13 679.385 749.290 68.722 34.609 o 12 9 4 3540.480 3430.550 155.178 5.016 o 12 9 5 80.519 55.289 52.096 73.621 o 12 9 6 1527.250 1532.560 78.698 20.096 o 12 9 7 1392.560 1524.940 68.415 24.694 o 12 9 8 48.582 58.746 41.011 118.362 o 12 9 9 232.351 365.778 54.312 62.276 o 12 9 10 1111.400 1110.630 80.915 22.915 o 13 -4 4 137.296 182.889 56.529 60.989 o 13 -4 5 158.225 89.782 50.987 74.693 o 13 -3 0 763.720 699.099 101.974 17.532 o 13 -3 1 1714.710 1745.140 71.648 20.442 o 13 -3 2 22.669 -15.119 29.321 234.762 o 13 -3 3 476.051 464.485 44.654 76.426 o 13 -3 4 716.438 802.979 65.397 36.700 o 13 -3 5 21.079 43.228 48.770 85.291 o 13 -3 6 1238.260 1149.430 95.324 17.338 o 13 -2 0 226.367 240.760 36.613 126.878 o 13 -2 1 837.729 1008.530 56.958 41.289 o 13 -2 2 1085.720 1248.490 60.285 33.414 o 13 -2 3 21.175 6.830 28.873 241.626 o 13 -2 4 1253.750 1349.060 62.217 29.721 o 13 -2 5 1119.790 1136.410 59.803 34.013 o 13 -2 6 200.470 202.840 48.770 78.539 o 13 -2 7 2318.390 2399.720 109.733 10.102 o 13 -1 0 3724.850 3973.680 157.395 4.628 o 13 -1 1 1.776 -10.040 33.807 179.400 o 13 -1 2 891.235 997.717 53.808 43.515 o 13 -1 3 156.185 140.985 41.566 108.274 o 13 -1 4 762.980 751.507 66.505 35.541 o 13 -1 5 2439.550 2800.970 116.384 8.853 o 13 -1 6 1781.980 2058.330 99.758 13.164 o 13 -1 7 51.713 84.240 37.686 138.335 o 13 -1 8 1659.980 1733.570 91.999 15.571 o 13 -1 10 179.103 100.866 48.770 80.522 o 13 0 0 4106.520 4322.830 160.721 4.187 o 13 0 1 1567.580 1734.670 98.649 14.486 o 13 0 2 1121.170 1179.440 56.171 36.227 o 13 0 3 351.401 336.959 48.770 72.315 o 13 0 4 40.561 24.385 38.795 133.306 o 13 0 5 1032.090 1190.440 76.481 25.120 o 13 0 6 2281.380 2232.350 98.649 11.713 o 13 0 7 543.940 540.908 57.638 49.342 o 13 0 8 294.364 266.020 49.879 72.106 o 13 0 9 1441.060 1440.710 61.432 27.652 o 13 0 10 444.596 434.500 60.963 47.208 o 13 0 11 1489.720 1537.380 99.758 14.796 o 13 1 0 2732.510 2781.110 88.673 10.927 o 13 1 4 387.059 483.270 54.312 57.992 o 13 1 5 177.003 85.348 38.795 123.124 o 13 1 6 1194.960 1137.240 73.156 25.704 o 13 1 7 1728.750 1895.390 91.999 15.029 o 13 1 8 97.696 134.304 30.447 196.577 o 13 1 9 1579.640 1656.240 89.228 16.664 o 13 1 10 932.498 847.225 51.904 46.140 o 13 1 11 107.279 90.890 49.879 79.076 o 13 2 5 46.103 67.614 34.361 166.306 o 13 2 6 1173.520 1028.610 70.939 27.403 o 13 2 7 2301.090 2507.630 159.058 6.086 o 13 2 8 1817.890 1865.940 68.492 20.264 o 13 2 9 63.413 12.668 35.469 157.347 o 13 2 10 1522.950 1486.430 64.373 25.385 o 13 2 11 433.726 449.436 43.556 81.319 o 13 3 6 8.096 5.542 42.120 115.238 o 13 3 7 1412.870 1428.520 60.285 28.550 o 13 3 8 2885.770 2935.910 86.734 10.501 o 13 3 9 903.604 926.009 52.650 45.140 o 13 3 10 434.700 383.049 39.678 94.994 o 13 3 11 1761.360 1801.020 70.859 20.188 o 13 4 0 2050.620 2138.140 97.541 12.635 o 13 4 1 189.406 151.853 42.120 103.888 o 13 4 5 2888.310 2953.930 128.576 7.173 o 13 4 6 657.515 765.917 74.264 30.632 o 13 4 7 122.083 129.685 49.879 78.255 o 13 4 8 2167.060 2211.030 74.644 15.940 o 13 4 9 2442.680 2575.130 82.063 12.911 o 13 4 10 31.585 14.971 28.090 252.024 o 13 4 11 807.190 776.615 52.380 48.913 o 13 5 0 3038.870 3096.920 129.685 6.839 o 13 5 1 1522.550 1444.270 89.782 17.188 o 13 5 2 232.495 217.250 44.337 91.729 o 13 5 5 1861.850 2004.020 105.300 12.139 o 13 5 7 382.086 395.705 62.071 46.830 o 13 5 8 901.354 1070.730 88.673 20.990 o 13 5 9 1350.490 1333.430 97.541 16.064 o 13 5 10 1841.390 1944.630 72.085 18.926 o 13 5 11 10.131 39.903 36.578 151.208 o 13 5 12 880.197 855.699 75.372 27.953 o 13 6 1 3332.110 3514.790 141.877 5.698 o 13 6 2 2029.980 2098.230 105.300 11.616 o 13 6 3 331.670 261.587 48.770 73.977 o 13 6 4 1391.760 1341.190 62.129 28.344 o 13 6 5 15.171 -98.649 35.469 161.892 o 13 6 6 1825.290 1797.850 105.300 12.486 o 13 6 7 808.806 799.169 76.481 28.019 o 13 6 8 571.011 571.944 73.156 32.834 o 13 6 9 883.036 677.243 76.481 27.927 o 13 6 11 610.756 610.738 62.071 42.401 o 13 7 3 186.009 157.395 48.770 79.566 o 13 7 4 674.457 661.193 49.210 57.833 o 13 7 5 265.992 271.874 38.309 114.044 o 13 7 6 28.127 50.987 44.337 102.572 o 13 7 7 1699.260 1614.960 104.191 13.232 o 13 7 8 1262.780 1304.610 95.324 16.979 o 13 8 6 158.366 164.046 49.879 76.940 o 14 -1 2 993.645 883.409 76.481 26.443 o 14 -1 3 118.306 76.481 45.445 94.328 o 14 0 4 419.798 561.968 63.180 43.918 o 14 0 5 1470.760 1499.690 89.782 17.286 o 14 1 5 458.541 491.029 58.746 49.611 o 14 2 7 584.651 575.269 58.746 46.936 o 14 2 9 1011.070 1043.020 89.782 20.170 o 14 3 8 6.786 43.228 36.578 151.332 o 14 4 8 942.235 924.420 84.240 22.941 o 14 5 7 241.919 227.226 59.855 53.057 o ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_disorder_group Au1 Au 0.654544(8) 0.889505(8) 0.669648(6) 0.01923(4) Uani 1.000000 . . . Cu1 Cu 0.81546(3) 1.07253(3) 0.462561(19) 0.01945(7) Uani 1.000000 . . . P1 P 0.48974(6) 0.83216(6) 0.79044(4) 0.01963(12) Uani 1.000000 . . . N1 N 0.6570(2) 1.17925(18) 0.49022(14) 0.0225(4) Uani 1.000000 . . . N2 N 0.9040(2) 1.20423(18) 0.50553(14) 0.0207(4) Uani 1.000000 . . . N3 N 0.9272(2) 1.15310(18) 0.34302(14) 0.0203(4) Uani 1.000000 . . . C1 C 0.7959(2) 0.9172(2) 0.55898(17) 0.0216(5) Uani 1.000000 . . . C2 C 0.8859(2) 0.9056(2) 0.49670(16) 0.0199(5) Uani 1.000000 . . . C3 C 0.9942(2) 0.8499(2) 0.44319(17) 0.0225(5) Uani 1.000000 . . . H3a H 1.0324(2) 0.9098(2) 0.38769(17) 0.0270(6) Uiso 1.000000 R . . H3b H 0.9606(2) 0.7887(2) 0.42504(17) 0.0270(6) Uiso 1.000000 R . . C4 C 0.5419(3) 1.1783(2) 0.46954(19) 0.0282(6) Uani 1.000000 . . . H4 H 0.5318(3) 1.1225(2) 0.44002(19) 0.0338(7) Uiso 1.000000 R . . C5 C 0.4376(3) 1.2537(3) 0.4887(2) 0.0340(6) Uani 1.000000 . . . H5 H 0.3573(3) 1.2488(3) 0.4742(2) 0.0408(8) Uiso 1.000000 R . . C6 C 0.4534(3) 1.3365(3) 0.5298(2) 0.0334(6) Uani 1.000000 . . . H6 H 0.3839(3) 1.3904(3) 0.5435(2) 0.0401(8) Uiso 1.000000 R . . C7 C 0.5714(3) 1.3402(2) 0.55072(18) 0.0277(6) Uani 1.000000 . . . H7 H 0.5844(3) 1.3978(2) 0.57771(18) 0.0333(7) Uiso 1.000000 R . . C8 C 0.6707(3) 1.2589(2) 0.53190(16) 0.0229(5) Uani 1.000000 . . . C9 C 0.7942(2) 1.2496(2) 0.56423(18) 0.0248(5) Uani 1.000000 . . . H9a H 0.7833(2) 1.1966(2) 0.62633(18) 0.0297(6) Uiso 1.000000 R . . H9b H 0.8130(2) 1.3281(2) 0.56581(18) 0.0297(6) Uiso 1.000000 R . . C10 C 0.9516(3) 1.2942(2) 0.42116(17) 0.0231(5) Uani 1.000000 . . . H10a H 0.8834(3) 1.3576(2) 0.41071(17) 0.0278(6) Uiso 1.000000 R . . H10b H 1.0276(3) 1.3292(2) 0.42737(17) 0.0278(6) Uiso 1.000000 R . . C11 C 0.9896(2) 1.2460(2) 0.34070(16) 0.0208(5) Uani 1.000000 . . . C12 C 1.0828(2) 1.2989(2) 0.26577(17) 0.0239(5) Uani 1.000000 . . . H12 H 1.1245(2) 1.3653(2) 0.26520(17) 0.0287(6) Uiso 1.000000 R . . C13 C 1.1137(2) 1.2540(2) 0.19260(17) 0.0259(5) Uani 1.000000 . . . H13 H 1.1774(2) 1.2886(2) 0.14115(17) 0.0311(7) Uiso 1.000000 R . . C14 C 1.0499(3) 1.1570(2) 0.19540(17) 0.0257(5) Uani 1.000000 . . . H14 H 1.0700(3) 1.1239(2) 0.14606(17) 0.0309(6) Uiso 1.000000 R . . C15 C 0.9574(3) 1.1098(2) 0.27085(17) 0.0238(5) Uani 1.000000 . . . C16 C 0.5404(2) 0.7896(2) 0.89733(17) 0.0223(5) Uani 1.000000 . . . C17 C 0.5495(3) 0.6736(2) 0.94910(18) 0.0254(5) Uani 1.000000 . . . H17 H 0.5207(3) 0.6129(2) 0.93202(18) 0.0304(6) Uiso 1.000000 R . . C18 C 0.6009(3) 0.6462(2) 1.02615(19) 0.0293(6) Uani 1.000000 . . . H18 H 0.6065(3) 0.5668(2) 1.06151(19) 0.0351(7) Uiso 1.000000 R . . C19 C 0.6438(3) 0.7333(3) 1.05151(18) 0.0276(6) Uani 1.000000 . . . H19 H 0.6798(3) 0.7141(3) 1.10363(18) 0.0331(7) Uiso 1.000000 R . . C20 C 0.6340(3) 0.8491(3) 1.0003(2) 0.0322(6) Uani 1.000000 . . . H20 H 0.6624(3) 0.9095(3) 1.0179(2) 0.0387(7) Uiso 1.000000 R . . C21 C 0.5830(3) 0.8775(2) 0.92375(19) 0.0298(6) Uani 1.000000 . . . H21 H 0.5771(3) 0.9572(2) 0.88899(19) 0.0357(7) Uiso 1.000000 R . . C22 C 0.3570(2) 0.9411(2) 0.80093(18) 0.0237(5) Uani 1.000000 . . . C23 C 0.3508(3) 1.0395(2) 0.7285(2) 0.0268(5) Uani 1.000000 . . . H23 H 0.4132(3) 1.0475(2) 0.6737(2) 0.0322(7) Uiso 1.000000 R . . C24 C 0.2527(3) 1.1270(3) 0.7361(2) 0.0349(7) Uani 1.000000 . . . H24 H 0.2479(3) 1.1942(3) 0.6864(2) 0.0419(8) Uiso 1.000000 R . . C25 C 0.1627(3) 1.1156(3) 0.8159(2) 0.0379(7) Uani 1.000000 . . . H25 H 0.0968(3) 1.1756(3) 0.8214(2) 0.0455(9) Uiso 1.000000 R . . C26 C 0.1680(3) 1.0175(3) 0.8879(2) 0.0394(7) Uani 1.000000 . . . H26 H 0.1050(3) 1.0098(3) 0.9423(2) 0.0473(9) Uiso 1.000000 R . . C27 C 0.2650(3) 0.9296(3) 0.8813(2) 0.0309(6) Uani 1.000000 . . . H27 H 0.2686(3) 0.8623(3) 0.9311(2) 0.0371(7) Uiso 1.000000 R . . C28 C 0.4267(3) 0.7028(2) 0.78044(16) 0.0247(5) Uani 1.000000 . . . C29 C 0.2959(3) 0.6836(3) 0.8007(2) 0.0367(7) Uani 1.000000 . . . H29 H 0.2342(3) 0.7352(3) 0.8262(2) 0.0440(8) Uiso 1.000000 R . . C30 C 0.2563(4) 0.5872(3) 0.7830(3) 0.0539(11) Uani 1.000000 . . . H30 H 0.1666(4) 0.5745(3) 0.7956(3) 0.0647(13) Uiso 1.000000 R . . C31 C 0.3431(5) 0.5112(3) 0.7480(2) 0.0531(11) Uani 1.000000 . . . H31 H 0.3140(5) 0.4467(3) 0.7356(2) 0.0637(13) Uiso 1.000000 R . . C32 C 0.4737(5) 0.5281(3) 0.7306(2) 0.0587(12) Uani 1.000000 . . . H32 H 0.5349(5) 0.4737(3) 0.7081(2) 0.0704(14) Uiso 1.000000 R . . C33 C 0.5156(4) 0.6244(3) 0.7460(2) 0.0445(9) Uani 1.000000 . . . H33 H 0.6055(4) 0.6367(3) 0.7328(2) 0.0534(10) Uiso 1.000000 R . . C34 C 0.6819(3) 1.2376(3) 0.8233(3) 0.0428(8) Uani 1.000000 . . . H34a H 0.7209(3) 1.3103(3) 0.7814(3) 0.0513(9) Uiso 1.000000 R . . H34b H 0.6335(3) 1.2563(3) 0.8792(3) 0.0513(9) Uiso 1.000000 R . . C35 C 0.914(3) 0.4311(18) 0.919(2) 0.036(4) Uani 0.42(7) D U 1 H35a H 0.947(3) 0.4315(18) 0.855(2) 0.044(5) Uiso 0.42(7) DR . 1 H35b H 0.921(3) 0.5110(18) 0.923(2) 0.044(5) Uiso 0.42(7) DR . 1 Cl1 Cl 0.57338(7) 1.19097(7) 0.77369(5) 0.03302(15) Uani 1.000000 . . . Cl2 Cl 0.80557(9) 1.13083(8) 0.84927(8) 0.0586(3) Uani 1.000000 . . . Cl3 Cl 0.7488(16) 0.395(2) 0.952(2) 0.042(2) Uani 0.42(7) D U 1 Cl4 Cl 1.0087(10) 0.3312(17) 0.9859(7) 0.061(3) Uani 0.42(7) D U 1 O1B O 0.7649(5) 0.5411(5) 0.5853(3) 0.0513(12) Uani 0.800000 . U 1 H1Ba H 0.811(5) 0.500(5) 0.623(3) 0.0769(19) Uiso 0.800000 G . 1 H1Bb H 0.821(4) 0.567(7) 0.535(2) 0.0769(19) Uiso 0.800000 G . 1 C35A C 0.9397(17) 0.4235(18) 0.9030(13) 0.040(3) Uani 0.58(7) D U 2 H35c H 0.976(5) 0.407(5) 0.845(3) 0.057(19) Uiso 0.58(7) D . 2 H35d H 0.965(6) 0.499(4) 0.907(4) 0.07(2) Uiso 0.58(7) D . 2 Cl3A Cl 0.7699(13) 0.4259(18) 0.9292(12) 0.0405(19) Uani 0.58(7) D U 2 Cl4A Cl 1.0047(7) 0.3108(17) 0.9836(5) 0.0542(19) Uani 0.58(7) D U 2 O6 O 0.793(2) 0.550(2) 0.5380(18) 0.068(6) Uani 0.200000 . U 2 H6a H 0.83(2) 0.57(3) 0.480(3) 0.102(10) Uiso 0.200000 G . 2 H6b H 0.848(19) 0.499(19) 0.562(15) 0.102(10) Uiso 0.200000 G . 2 N1_1 N 1.0316(4) 1.4063(3) 0.6675(3) 0.0382(8) Uani 0.800000 D U 1 O1_1 O 1.1212(5) 1.4002(4) 0.7051(3) 0.0658(11) Uani 0.800000 D U 1 O2_1 O 1.0523(5) 1.4042(4) 0.5872(3) 0.0552(12) Uani 0.800000 D U 1 O3_1 O 0.9171(5) 1.4189(4) 0.7083(2) 0.0509(11) Uani 0.800000 D U 1 N1_2 N 0.9686(17) 1.4103(16) 0.6888(13) 0.064(7) Uani 0.200000 D U 2 O1_2 O 1.0527(15) 1.4094(18) 0.7320(12) 0.067(5) Uani 0.200000 D U 2 O2_2 O 0.8568(15) 1.4454(13) 0.7161(12) 0.051(4) Uani 0.200000 D U 2 O3_2 O 1.003(2) 1.4016(18) 0.6092(13) 0.079(7) Uani 0.200000 D U 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Au1 0.01852(5) 0.01832(5) 0.01914(5) -0.00323(3) -0.00149(3) -0.00378(4) Cu1 0.02447(15) 0.01667(14) 0.01789(14) -0.00581(11) -0.00233(11) -0.00570(11) P1 0.0189(3) 0.0192(3) 0.0200(3) -0.0031(2) -0.0012(2) -0.0058(2) N1 0.0269(11) 0.0203(10) 0.0208(10) -0.0036(8) -0.0050(8) -0.0059(8) N2 0.0226(10) 0.0207(10) 0.0191(10) -0.0027(8) -0.0020(8) -0.0075(8) N3 0.0258(11) 0.0169(10) 0.0184(10) -0.0030(8) -0.0049(8) -0.0043(8) C1 0.0245(12) 0.0187(12) 0.0219(12) -0.0051(9) -0.0055(9) -0.0044(9) C2 0.0234(12) 0.0158(11) 0.0216(12) -0.0057(9) -0.0046(9) -0.0052(9) C3 0.0269(13) 0.0229(12) 0.0199(12) -0.0037(10) -0.0038(9) -0.0093(10) C4 0.0352(15) 0.0242(13) 0.0307(14) -0.0042(11) -0.0135(11) -0.0099(11) C5 0.0355(16) 0.0294(15) 0.0459(17) 0.0035(12) -0.0225(13) -0.0151(13) C6 0.0370(16) 0.0273(14) 0.0417(17) 0.0112(12) -0.0189(13) -0.0150(12) C7 0.0341(14) 0.0253(13) 0.0287(14) 0.0022(11) -0.0125(11) -0.0118(11) C8 0.0296(13) 0.0206(12) 0.0190(12) -0.0047(10) -0.0057(10) -0.0045(9) C9 0.0252(13) 0.0289(14) 0.0237(13) -0.0017(10) -0.0036(10) -0.0139(11) C10 0.0300(13) 0.0174(12) 0.0230(12) -0.0055(10) -0.0038(10) -0.0068(10) C11 0.0250(12) 0.0168(11) 0.0203(12) -0.0020(9) -0.0073(9) -0.0024(9) C12 0.0237(12) 0.0218(13) 0.0231(12) -0.0050(10) -0.0066(10) 0.0013(10) C13 0.0224(12) 0.0307(14) 0.0183(12) 0.0010(10) -0.0017(9) -0.0004(10) C14 0.0288(13) 0.0282(13) 0.0195(12) 0.0052(10) -0.0050(10) -0.0081(10) C15 0.0291(13) 0.0225(12) 0.0204(12) 0.0016(10) -0.0082(10) -0.0054(10) C16 0.0176(11) 0.0271(13) 0.0209(12) -0.0021(10) -0.0005(9) -0.0072(10) C17 0.0249(13) 0.0243(13) 0.0270(13) -0.0039(10) -0.0039(10) -0.0076(10) C18 0.0317(14) 0.0261(14) 0.0269(14) 0.0011(11) -0.0045(11) -0.0051(11) C19 0.0234(13) 0.0386(16) 0.0222(13) -0.0008(11) -0.0053(10) -0.0108(11) C20 0.0370(16) 0.0345(16) 0.0321(15) -0.0088(12) -0.0103(12) -0.0148(12) C21 0.0362(15) 0.0236(13) 0.0308(14) -0.0058(11) -0.0085(11) -0.0068(11) C22 0.0171(11) 0.0277(13) 0.0301(13) -0.0024(10) -0.0048(9) -0.0136(11) C23 0.0210(12) 0.0244(13) 0.0366(15) -0.0029(10) -0.0062(10) -0.0099(11) C24 0.0264(14) 0.0256(14) 0.056(2) 0.0000(11) -0.0133(13) -0.0138(13) C25 0.0233(14) 0.0396(17) 0.062(2) 0.0066(12) -0.0125(13) -0.0316(16) C26 0.0238(14) 0.058(2) 0.0431(18) 0.0028(13) -0.0015(12) -0.0303(16) C27 0.0230(13) 0.0417(17) 0.0316(15) -0.0005(12) -0.0051(11) -0.0163(13) C28 0.0343(14) 0.0229(13) 0.0168(12) -0.0081(10) -0.0045(10) -0.0038(10) C29 0.0342(16) 0.0252(14) 0.0534(19) -0.0043(12) -0.0235(14) -0.0030(13) C30 0.062(2) 0.0286(17) 0.079(3) -0.0153(16) -0.051(2) 0.0052(17) C31 0.110(3) 0.0257(16) 0.0332(17) -0.0244(19) -0.0341(19) -0.0000(13) C32 0.103(3) 0.0332(18) 0.0337(18) -0.028(2) 0.0212(18) -0.0186(14) C33 0.056(2) 0.0303(16) 0.0402(18) -0.0176(14) 0.0206(15) -0.0179(14) C34 0.0272(15) 0.0413(18) 0.069(2) 0.0008(13) -0.0111(14) -0.0291(17) C35 0.054(10) 0.023(6) 0.029(8) -0.006(6) -0.017(7) 0.006(5) Cl1 0.0343(4) 0.0356(4) 0.0295(3) -0.0071(3) -0.0018(3) -0.0112(3) Cl2 0.0421(5) 0.0418(5) 0.0945(8) 0.0006(4) -0.0272(5) -0.0138(5) Cl3 0.033(2) 0.043(4) 0.057(5) -0.003(3) -0.009(3) -0.023(4) Cl4 0.065(5) 0.061(4) 0.061(4) 0.001(2) -0.042(4) -0.003(2) O1B 0.036(2) 0.048(2) 0.080(3) 0.0000(16) -0.017(2) -0.030(3) C35A 0.028(5) 0.057(7) 0.031(6) -0.003(3) -0.006(4) -0.008(4) Cl3A 0.030(2) 0.044(4) 0.052(3) 0.004(2) -0.009(2) -0.022(3) Cl4A 0.040(2) 0.072(4) 0.0365(19) 0.0144(17) -0.0117(18) 0.0023(15) O6 0.063(14) 0.050(11) 0.113(17) 0.013(9) -0.059(13) -0.028(14) N1_1 0.061(2) 0.0165(15) 0.043(2) -0.0104(14) -0.0243(15) -0.0028(12) O1_1 0.075(3) 0.061(2) 0.083(3) 0.014(2) -0.050(2) -0.031(2) O2_1 0.084(3) 0.044(2) 0.0456(19) -0.0182(19) -0.0134(17) -0.0186(14) O3_1 0.066(3) 0.049(3) 0.0398(19) -0.0176(19) -0.0178(18) -0.0053(15) N1_2 0.057(9) 0.070(15) 0.076(10) 0.002(6) -0.026(6) -0.029(7) O1_2 0.045(7) 0.096(13) 0.067(9) -0.004(7) -0.012(6) -0.032(7) O2_2 0.057(8) 0.025(7) 0.072(9) -0.009(5) -0.021(6) -0.007(5) O3_2 0.091(13) 0.079(14) 0.079(10) -0.007(8) -0.023(6) -0.035(6) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source C 0.00347 0.00161 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.215599998832 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' Cl 0.14873 0.16029 11.46040 7.19640 6.25560 1.64550 0.01040 1.16620 18.51940 47.77840 -9.55739974976 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.0030380000826 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' O 0.01158 0.00611 3.04850 2.28680 1.54630 0.86700 13.27710 5.70110 0.32390 32.90890 0.250800013542 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' N 0.00653 0.00323 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750 0.58260 -11.5290002823 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' P 0.10434 0.09671 6.43450 4.17910 1.78000 1.49080 1.90670 27.15700 0.52600 68.16450 1.11489999294 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' Au -1.84508 8.87037 16.88190 18.59130 25.55820 5.86000 0.46110 8.62160 1.48260 36.39560 12.0657997131 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' Cu 0.34125 1.28947 13.33800 7.16760 5.61580 1.67350 3.58280 0.24700 11.39660 64.81260 1.19099998474 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u 1 0 0 24.16 0.55 2 0 0 1.34 0.1 2 0 0 1.18 0.09 2 0 0 1.34 0.11 2 0 0 1.27 0.09 3 0 0 79.89 1.86 3 0 0 80.1 1.83 3 0 0 80.64 1.83 3 0 0 81.2 1.82 4 0 0 23.67 0.66 4 0 0 24.97 0.65 4 0 0 24.57 0.71 4 0 0 23.92 0.65 5 0 0 22.69 0.65 5 0 0 23.03 0.67 5 0 0 22.74 0.73 5 0 0 22.07 0.65 6 0 0 119.79 2.77 6 0 0 121.64 2.86 6 0 0 119.22 2.77 6 0 0 119.58 2.78 -7 0 0 109.38 2.57 7 0 0 110.49 2.57 7 0 0 108.09 2.66 7 0 0 108.12 2.58 -8 0 0 3.89 0.33 8 0 0 4.47 0.42 8 0 0 4.57 0.35 8 0 0 4.29 0.33 -9 0 0 44.96 1.26 9 0 0 43.19 1.24 9 0 0 44.24 1.37 -10 0 0 27.56 0.93 10 0 0 26.97 1.04 10 0 0 28.46 0.93 -11 0 0 15.23 0.7 11 0 0 14.74 0.79 12 0 0 24.6 1.07 13 0 0 39 1.45 13 -1 0 35.85 1.42 12 -1 0 24.92 1.1 -12 1 0 24.7 0.97 11 -1 0 0.25 0.31 -11 1 0 0.64 0.3 10 -1 0 3.46 0.46 -10 1 0 4.75 0.43 9 -1 0 58.96 1.75 9 -1 0 61.55 1.6 -9 1 0 61.12 1.64 8 -1 0 54.57 1.42 8 -1 0 52.96 1.56 -8 1 0 55.71 1.41 -8 1 0 54.89 1.46 7 -1 0 48.59 1.25 7 -1 0 48.38 1.39 -7 1 0 48.22 1.29 -7 1 0 48.42 1.25 6 -1 0 176.96 4.14 6 -1 0 179.32 4.04 -6 1 0 179.17 4.02 -6 1 0 180.03 4.05 5 -1 0 32.57 0.97 5 -1 0 34.47 0.89 -5 1 0 34.36 0.91 -5 1 0 34.31 0.88 4 -1 0 11.41 0.45 4 -1 0 11.32 0.4 4 -1 0 11.95 0.38 -4 1 0 11.68 0.38 3 -1 0 92.7 2.25 3 -1 0 99.91 2.21 3 -1 0 99.99 2.2 -3 1 0 99 2.19 2 -1 0 329.66 6.99 2 -1 0 306.73 7.02 2 -1 0 328.99 7.03 -2 1 0 323.52 6.98 1 -1 0 49.86 1.14 1 -1 0 52.99 1.12 -1 1 0 48.98 1.12 -1 1 0 47 1.11 0 -1 0 208.94 4.55 -1 -1 0 47.17 0.89 -1 -1 0 47.18 1.07 1 1 0 49.19 1.08 1 1 0 45.95 1.08 1 1 0 47.74 1.04 2 1 0 2.06 0.15 2 1 0 2.11 0.12 2 1 0 2.26 0.15 2 1 0 1.84 0.14 3 1 0 5.8 0.24 3 1 0 5.62 0.25 3 1 0 5.77 0.21 3 1 0 5.51 0.26 4 1 0 348.78 7.54 4 1 0 343.39 7.63 4 1 0 347.81 7.61 4 1 0 347.02 7.6 5 1 0 127.48 2.83 5 1 0 123.1 2.89 5 1 0 124.62 2.88 5 1 0 125.05 2.88 6 1 0 110.2 2.59 6 1 0 112.96 2.55 6 1 0 107.89 2.6 6 1 0 112.35 2.64 7 1 0 64.56 1.68 7 1 0 62.79 1.62 7 1 0 66.24 1.64 7 1 0 63.38 1.58 -8 -1 0 4.8 0.35 8 1 0 4.83 0.37 8 1 0 4.82 0.39 8 1 0 3.83 0.4 -9 -1 0 13.04 0.56 9 1 0 10.92 0.63 9 1 0 11.2 0.55 -10 -1 0 22.64 0.81 10 1 0 22.58 0.91 10 1 0 22.75 0.83 11 1 0 45.7 1.48 11 1 0 46.45 1.37 12 1 0 -0.34 0.32 -13 -1 0 24.11 1.17 -13 -1 0 25.71 0.96 13 -2 0 2.2 0.5 -13 2 0 2.15 0.44 12 -2 0 6 0.63 -12 2 0 7.3 0.6 11 -2 0 30.84 1.24 -11 2 0 33.85 1.14 10 -2 0 3.22 0.48 -10 2 0 3.19 0.39 9 -2 0 22.45 0.95 -9 2 0 22.45 0.82 8 -2 0 45.63 1.41 8 -2 0 46.67 1.23 -8 2 0 44.4 1.29 7 -2 0 19.03 0.8 7 -2 0 21.9 0.66 -7 2 0 20.64 0.71 -7 2 0 20.77 0.65 6 -2 0 22.5 0.8 6 -2 0 23.08 0.67 -6 2 0 23.01 0.66 -6 2 0 22 0.72 5 -2 0 60.89 1.64 5 -2 0 64.14 1.52 -5 2 0 65.8 1.52 -5 2 0 64.64 1.58 4 -2 0 98.87 2.23 4 -2 0 93.01 2.32 -4 2 0 97.61 2.26 -4 2 0 100.38 2.21 3 -2 0 16.07 0.43 3 -2 0 15.2 0.51 -3 2 0 15.53 0.43 -3 2 0 14.03 0.45 2 -2 0 719.02 15.39 2 -2 0 728.08 15.45 -2 2 0 702.04 15.35 -2 2 0 693.12 15.33 1 -2 0 134.92 3.1 1 -2 0 146.31 3.11 -1 2 0 139.05 3.07 -1 2 0 139.48 3.07 0 -2 0 18.8 0.48 0 -2 0 17.93 0.46 0 2 0 19.05 0.46 0 2 0 18.15 0.48 1 2 0 21.69 0.54 1 2 0 21.06 0.57 -2 -2 0 9.45 0.25 -2 -2 0 9.33 0.3 2 2 0 9.2 0.25 2 2 0 9.03 0.31 2 2 0 9.26 0.35 -3 -2 0 2.66 0.16 -3 -2 0 2.66 0.19 3 2 0 2.76 0.2 3 2 0 2.5 0.14 -4 -2 0 218.14 4.95 -4 -2 0 218.62 4.14 4 2 0 227.14 4.99 4 2 0 219.13 4.99 4 2 0 234.32 4.89 -5 -2 0 138.38 3.24 -5 -2 0 139.09 2.71 5 2 0 142.51 3.24 5 2 0 143.58 3.16 5 2 0 142.89 3.27 6 2 0 0.06 0.14 6 2 0 0.1 0.17 6 2 0 0.2 0.12 6 2 0 0.21 0.15 7 2 0 9.1 0.48 7 2 0 9.6 0.46 7 2 0 8.72 0.48 7 2 0 9.44 0.4 8 2 0 52.67 1.46 8 2 0 54.83 1.51 8 2 0 56.14 1.5 -9 -2 0 61.65 1.77 -9 -2 0 64.61 1.48 -9 -2 0 66.41 1.65 9 2 0 65.65 1.75 9 2 0 62.26 1.7 -10 -2 0 32 0.94 -10 -2 0 30.89 1.12 10 2 0 30.72 1.02 -11 -2 0 57.79 1.46 -11 -2 0 57.95 1.76 11 2 0 58.07 1.65 -12 -2 0 4.58 0.56 -12 -2 0 4.72 0.46 13 -3 0 5.25 0.65 -13 3 0 7.09 0.65 12 -3 0 -0.13 0.34 -12 3 0 -0.1 0.34 11 -3 0 14.45 0.85 -11 3 0 14.54 0.74 10 -3 0 38.23 1.38 -10 3 0 39.95 1.26 9 -3 0 4.85 0.51 -9 3 0 4.89 0.43 8 -3 0 32.52 1.17 -8 3 0 35.53 1.08 7 -3 0 75.73 1.82 7 -3 0 71.85 2 -7 3 0 74.61 1.9 -7 3 0 75.96 1.8 6 -3 0 4.47 0.39 6 -3 0 4.68 0.29 -6 3 0 4.77 0.3 -6 3 0 4.57 0.35 5 -3 0 42.35 1.23 5 -3 0 46.02 1.1 -5 3 0 42.07 1.15 -5 3 0 44.35 1.1 4 -3 0 164.13 3.92 4 -3 0 172.14 3.82 -4 3 0 171.64 3.8 -4 3 0 174.5 3.85 3 -3 0 16.84 0.49 3 -3 0 15.21 0.55 -3 3 0 16.49 0.47 -3 3 0 14.94 0.49 2 -3 0 165.15 3.68 2 -3 0 169.16 3.66 -2 3 0 160.58 3.61 -2 3 0 159.1 3.62 1 -3 0 154.63 3.44 1 -3 0 157.04 3.43 -1 3 0 153.16 3.4 -1 3 0 150.17 3.39 0 -3 0 130.4 2.93 0 -3 0 131.67 2.94 0 3 0 130.84 2.93 0 3 0 132.16 2.9 -1 -3 0 1.55 0.13 -1 -3 0 1.02 0.11 1 3 0 1.18 0.13 1 3 0 1.27 0.14 -2 -3 0 313.4 6.75 2 3 0 317.7 6.68 2 3 0 309.56 6.8 2 3 0 295.15 6.79 -3 -3 0 79.31 1.56 -3 -3 0 80.44 1.86 3 3 0 81.55 1.89 3 3 0 76.81 1.92 3 3 0 83.7 1.79 -4 -3 0 52.42 1.11 -4 -3 0 52.79 1.32 4 3 0 53.59 1.34 4 3 0 56.19 1.25 -5 -3 0 139.76 3.22 -5 -3 0 139.29 2.69 5 3 0 145.4 3.13 5 3 0 135.36 3.28 5 3 0 142.48 3.24 -6 -3 0 29.53 0.87 -6 -3 0 28.79 0.72 6 3 0 28.51 0.85 6 3 0 29.05 0.77 6 3 0 28.28 0.91 -7 -3 0 17.17 0.56 -7 -3 0 18.08 0.68 7 3 0 18.32 0.56 7 3 0 17.43 0.65 7 3 0 18.37 0.72 -8 -3 0 33.23 0.87 -8 -3 0 32.53 1.04 8 3 0 33.35 1.07 8 3 0 31.32 1 -9 -3 0 49.42 1.47 -9 -3 0 50.13 1.23 9 3 0 49.29 1.42 9 3 0 52.94 1.5 -10 -3 0 2.8 0.41 -10 -3 0 3.7 0.37 10 3 0 2.49 0.34 -11 -3 0 23.96 0.82 -11 -3 0 24.37 1 11 3 0 23.97 0.91 -12 -3 0 16.68 0.87 -12 -3 0 19.14 0.74 12 3 0 18.09 0.82 12 -4 0 4.87 0.63 -12 4 0 5.77 0.58 11 -4 0 10.51 0.8 -11 4 0 13.34 0.73 10 -4 0 41.56 1.49 -10 4 0 44.03 1.38 9 -4 0 0.05 0.31 -9 4 0 0.14 0.26 8 -4 0 29.42 1.13 -8 4 0 31.26 1.02 7 -4 0 34.79 1.22 -7 4 0 40.65 1.15 6 -4 0 63.5 1.77 6 -4 0 64.86 1.57 -6 4 0 64.24 1.56 -6 4 0 63.83 1.66 5 -4 0 2.41 0.2 5 -4 0 2.21 0.29 -5 4 0 1.79 0.23 -5 4 0 1.95 0.19 4 -4 0 49.57 1.39 4 -4 0 53.22 1.28 -4 4 0 51.75 1.26 -4 4 0 50.64 1.31 3 -4 0 2.77 0.27 3 -4 0 3.18 0.24 -3 4 0 3.08 0.21 -3 4 0 2.61 0.22 2 -4 0 16.41 0.53 2 -4 0 16.27 0.56 -2 4 0 17.14 0.51 -2 4 0 16.52 0.52 1 -4 0 51.48 1.26 1 -4 0 51.09 1.23 -1 4 0 50.66 1.21 -1 4 0 48.78 1.22 0 -4 0 420.1 9.2 0 -4 0 425.77 9.15 0 4 0 417.18 9.1 0 4 0 414.18 9.16 -1 -4 0 2.47 0.18 -1 -4 0 2.22 0.19 1 4 0 2.85 0.21 1 4 0 2.31 0.18 -2 -4 0 94.66 2.16 -2 -4 0 92.5 2.19 2 4 0 95.51 2.1 2 4 0 92.58 2.21 -3 -4 0 165.18 3.78 3 4 0 174.42 3.68 3 4 0 169.46 3.82 3 4 0 165.32 3.86 -4 -4 0 1.39 0.17 4 4 0 0.89 0.11 4 4 0 0.87 0.2 4 4 0 0.72 0.17 -5 -4 0 0.47 0.15 -5 -4 0 0.43 0.12 5 4 0 0.21 0.18 5 4 0 0.29 0.11 5 4 0 0.63 0.17 -6 -4 0 29.21 0.86 -6 -4 0 28.77 0.72 6 4 0 28.34 0.95 6 4 0 28.45 0.87 6 4 0 29.37 0.75 -7 -4 0 80.75 1.69 -7 -4 0 82.51 2.03 7 4 0 79.81 2.03 7 4 0 79.29 2.11 -8 -4 0 23.34 0.71 -8 -4 0 24.88 0.86 8 4 0 24.39 0.85 8 4 0 24.59 0.94 -9 -4 0 29.99 1 -9 -4 0 28.72 0.83 9 4 0 30.67 1.07 9 4 0 27.75 0.98 -10 -4 0 8.31 0.57 -10 -4 0 8.11 0.47 10 4 0 7.56 0.53 10 4 0 8.64 0.62 -11 -4 0 0.14 0.26 -11 -4 0 0.61 0.32 11 4 0 0.31 0.28 12 4 0 10.43 0.63 13 4 0 19.29 0.88 12 -5 0 11.29 0.86 -12 5 0 11.49 0.77 11 -5 0 1.49 0.47 -11 5 0 2.71 0.46 10 -5 0 10.66 0.77 -10 5 0 12.01 0.69 9 -5 0 23.46 1.03 -9 5 0 24.49 0.93 8 -5 0 4.6 0.52 -8 5 0 5.42 0.45 7 -5 0 11.37 0.67 -7 5 0 11.7 0.59 6 -5 0 155.03 3.86 -6 5 0 162.43 3.76 -6 5 0 163.68 3.64 5 -5 0 0.7 0.16 5 -5 0 0.61 0.25 -5 5 0 0.8 0.2 -5 5 0 1 0.17 4 -5 0 25.33 0.75 4 -5 0 25 0.86 -4 5 0 26.04 0.73 -4 5 0 25.01 0.78 3 -5 0 76.05 1.89 3 -5 0 72.65 1.81 -3 5 0 72.4 1.8 -3 5 0 76.82 1.77 2 -5 0 86.38 2.07 2 -5 0 85.27 2.1 -2 5 0 87.33 2.03 -2 5 0 87.21 2.04 1 -5 0 8.24 0.39 1 -5 0 7.64 0.35 -1 5 0 7.58 0.36 -1 5 0 7.58 0.35 0 -5 0 143.38 3.27 0 -5 0 143.6 3.27 0 5 0 145.83 3.23 0 5 0 141.75 3.27 -1 -5 0 85.91 2.02 -1 -5 0 83.91 2.03 1 5 0 87.52 2.06 1 5 0 86.13 2.02 -2 -5 0 32.92 0.86 -2 -5 0 31.06 0.88 2 5 0 31.19 0.92 -3 -5 0 94.25 2.3 -3 -5 0 96.03 2.25 3 5 0 99.97 2.15 3 5 0 94.44 2.34 -4 -5 0 91.04 2.16 4 5 0 89.63 2.27 4 5 0 90.05 2.19 4 5 0 93.49 2.03 -5 -5 0 39.87 1.08 5 5 0 40.65 1.21 5 5 0 40.5 1.12 -6 -5 0 55.76 1.42 6 5 0 53.71 1.44 6 5 0 52.35 1.53 -7 -5 0 75.66 1.88 -7 -5 0 73.75 1.57 7 5 0 73.34 2.01 7 5 0 72.57 1.9 -8 -5 0 0.19 0.18 -8 -5 0 0.69 0.23 8 5 0 0.58 0.24 8 5 0 0.51 0.29 -9 -5 0 11.64 0.6 -9 -5 0 12 0.51 9 5 0 11.04 0.6 9 5 0 12.91 0.73 -10 -5 0 17.66 0.77 -10 -5 0 17.55 0.64 10 5 0 17.65 0.85 10 5 0 16.86 0.75 11 5 0 23.39 0.93 12 5 0 -0.01 0.27 -13 -5 0 27.94 1.17 11 -6 0 10.56 0.8 -11 6 0 11.19 0.75 10 -6 0 1.72 0.46 -10 6 0 1.37 0.39 9 -6 0 29.44 1.19 -9 6 0 29.28 1.07 8 -6 0 34.84 1.29 -8 6 0 35.89 1.18 7 -6 0 7.41 0.6 -7 6 0 7.69 0.52 6 -6 0 31.12 1.13 -6 6 0 34.79 1.06 5 -6 0 30 1.05 -5 6 0 29.39 0.95 -5 6 0 32.21 0.88 4 -6 0 0.31 0.17 4 -6 0 0.03 0.21 -4 6 0 0.07 0.13 -4 6 0 0.34 0.18 3 -6 0 19.41 0.69 3 -6 0 21.48 0.77 -3 6 0 21.52 0.68 -3 6 0 20.6 0.65 2 -6 0 331.34 7.26 2 -6 0 325.58 7.26 -2 6 0 322.68 7.18 -2 6 0 320.31 7.17 1 -6 0 156.89 3.61 1 -6 0 157.02 3.59 -1 6 0 154.88 3.57 -1 6 0 157.2 3.55 0 -6 0 67.52 1.71 0 -6 0 68.83 1.7 0 6 0 68.94 1.71 0 6 0 71.28 1.68 -1 -6 0 33.96 0.94 -1 -6 0 33.71 0.94 1 6 0 32.85 0.97 1 6 0 33.78 0.94 -2 -6 0 2.13 0.22 -2 -6 0 2.23 0.24 2 6 0 1.66 0.19 2 6 0 2.51 0.27 -3 -6 0 2.52 0.26 -3 -6 0 2.64 0.23 3 6 0 2.53 0.29 3 6 0 3.16 0.2 -4 -6 0 83.29 2.08 -4 -6 0 83.93 2.01 4 6 0 81.68 2.12 -5 -6 0 93.69 2.27 -5 -6 0 94.51 2.36 5 6 0 96.02 2.43 -6 -6 0 1.87 0.24 6 6 0 1.77 0.32 6 6 0 2.14 0.29 -7 -6 0 40.96 1.17 7 6 0 40.16 1.34 7 6 0 40.99 1.21 -8 -6 0 21.14 0.78 8 6 0 20.8 0.93 8 6 0 20.59 0.8 -9 -6 0 0.28 0.23 9 6 0 0.4 0.32 9 6 0 0.37 0.26 10 6 0 17.58 0.78 10 6 0 18.3 0.91 11 6 0 52.74 1.74 -12 -6 0 12.77 0.78 11 -7 0 8.42 0.81 -11 7 0 7.71 0.68 10 -7 0 5.94 0.65 -10 7 0 6.62 0.62 9 -7 0 6.68 0.65 -9 7 0 6.39 0.57 8 -7 0 51.73 1.68 -8 7 0 51.71 1.56 7 -7 0 20.94 0.95 -7 7 0 21.56 0.86 6 -7 0 0.47 0.3 -6 7 0 1.76 0.32 5 -7 0 35.01 1.2 -5 7 0 35.66 1.1 -5 7 0 37.84 1.03 4 -7 0 13.48 0.66 -4 7 0 13.08 0.59 -4 7 0 14.43 0.54 3 -7 0 4.35 0.41 3 -7 0 4.22 0.36 -3 7 0 4.19 0.35 -3 7 0 4.36 0.36 2 -7 0 116.21 2.73 2 -7 0 111.47 2.76 -2 7 0 116.22 2.68 -2 7 0 110.19 2.67 1 -7 0 33.75 1.01 1 -7 0 33.75 0.96 -1 7 0 34.95 0.96 -1 7 0 32.34 0.96 0 -7 0 4.31 0.33 0 -7 0 4.39 0.31 0 7 0 4.24 0.33 0 7 0 3.97 0.32 -1 -7 0 102.33 2.49 -1 -7 0 102.84 2.48 1 7 0 105.19 2.52 1 7 0 105.56 2.48 -2 -7 0 85.08 2.04 -2 -7 0 82.87 2.06 2 7 0 81.8 2.1 -3 -7 0 119.53 2.78 -3 -7 0 116.47 2.83 3 7 0 116.09 2.87 -4 -7 0 35.77 1.09 -4 -7 0 36.27 1.02 4 7 0 36 1.16 -5 -7 0 98.81 2.4 -5 -7 0 98.74 2.5 5 7 0 101.2 2.58 -6 -7 0 0.18 0.17 -6 -7 0 0.43 0.24 6 7 0 0.87 0.31 -7 -7 0 0.92 0.29 -7 -7 0 1.28 0.25 7 7 0 0.85 0.34 -8 -7 0 21.68 0.79 -8 -7 0 21.11 0.87 8 7 0 20.03 0.96 -9 -7 0 18.47 0.85 9 7 0 17.95 0.92 -10 -7 0 0 0.31 10 7 0 0.1 0.33 -11 -7 0 38.41 1.4 -12 -7 0 16.41 0.91 10 -8 0 17.67 1.01 -10 8 0 16.69 0.89 9 -8 0 -0.7 0.35 -9 8 0 0.12 0.32 8 -8 0 33.34 1.33 -8 8 0 36.26 1.22 7 -8 0 20.63 0.94 -7 8 0 20.02 0.84 6 -8 0 9.95 0.66 -6 8 0 10.59 0.6 5 -8 0 1.05 0.32 -5 8 0 0.93 0.27 4 -8 0 54.82 1.65 -4 8 0 60.2 1.51 -4 8 0 55.84 1.55 3 -8 0 48.36 1.45 -3 8 0 50.59 1.34 -3 8 0 48.61 1.36 2 -8 0 9.09 0.51 2 -8 0 7.76 0.46 -2 8 0 7.99 0.45 -2 8 0 7.52 0.46 1 -8 0 59.08 1.62 1 -8 0 59.48 1.56 -1 8 0 59.83 1.57 -1 8 0 59.63 1.54 0 -8 0 5.68 0.39 0 -8 0 5.1 0.36 0 8 0 6.12 0.42 0 8 0 5.43 0.39 -1 -8 0 2.53 0.28 -1 -8 0 2.21 0.26 1 8 0 1.9 0.28 1 8 0 2.58 0.31 -2 -8 0 82.58 2.02 -2 -8 0 80.1 2.04 2 8 0 78.61 2.08 -3 -8 0 74.97 1.88 -3 -8 0 72.53 1.93 3 8 0 75.07 1.99 -4 -8 0 3.66 0.37 -4 -8 0 4.35 0.36 4 8 0 3.8 0.41 -5 -8 0 21.55 0.83 -5 -8 0 21.16 0.74 5 8 0 20.96 0.9 -6 -8 0 33.99 1.13 -6 -8 0 33.19 1.01 6 8 0 31.88 1.19 -7 -8 0 10.83 0.63 -7 -8 0 11.39 0.55 7 8 0 11.22 0.73 -8 -8 0 10.94 0.66 8 8 0 11.32 0.76 -9 -8 0 45.26 1.51 9 8 0 47.79 1.64 -10 -8 0 8.12 0.66 10 8 0 6.95 0.7 -11 -8 0 7.93 0.7 11 8 0 8.57 0.79 9 -9 0 20.34 1.09 -9 9 0 21.97 0.97 8 -9 0 0.43 0.4 -8 9 0 0.81 0.34 7 -9 0 9.58 0.71 -7 9 0 9.87 0.62 6 -9 0 14.24 0.8 -6 9 0 13.23 0.69 5 -9 0 0.79 0.34 -5 9 0 0.84 0.28 4 -9 0 47.92 1.55 -4 9 0 51.32 1.46 -4 9 0 53.07 1.41 3 -9 0 61.19 1.76 -3 9 0 60.87 1.67 -3 9 0 63.37 1.64 2 -9 0 11.86 0.63 -2 9 0 12.3 0.6 -2 9 0 12.92 0.59 1 -9 0 0.43 0.2 1 -9 0 0.46 0.25 -1 9 0 0.56 0.22 -1 9 0 0.77 0.23 0 -9 0 29.13 0.97 0 -9 0 27.8 0.92 0 9 0 30.4 0.95 0 9 0 27.2 0.94 -1 -9 0 45.27 1.29 -1 -9 0 44.41 1.28 1 9 0 43.57 1.31 -2 -9 0 7.71 0.46 -2 -9 0 7.48 0.49 2 9 0 6.66 0.51 -3 -9 0 55.11 1.49 -3 -9 0 55.98 1.56 3 9 0 53.48 1.6 -4 -9 0 10.08 0.52 -4 -9 0 9.99 0.58 4 9 0 9.15 0.61 -5 -9 0 1.74 0.28 -5 -9 0 1.11 0.3 5 9 0 1.35 0.34 -6 -9 0 13.94 0.71 6 9 0 13.34 0.77 -7 -9 0 6.66 0.56 7 9 0 7.84 0.68 -8 -9 0 0.61 0.3 8 9 0 1.13 0.41 -9 -9 0 40.89 1.41 9 9 0 37.97 1.5 -10 -9 0 19.56 0.95 10 9 0 17.35 1.03 11 9 0 4.34 0.62 9 -10 0 18.17 1.07 -9 10 0 18.54 0.95 8 -10 0 3.81 0.57 -8 10 0 5.1 0.54 7 -10 0 1.36 0.43 -7 10 0 1.56 0.38 6 -10 0 10.52 0.74 -6 10 0 10.73 0.65 5 -10 0 23.13 1.04 -5 10 0 25.06 0.94 4 -10 0 11.57 0.71 -4 10 0 11.49 0.64 3 -10 0 47.36 1.51 -3 10 0 48.7 1.38 -3 10 0 47.6 1.41 2 -10 0 34.75 1.17 -2 10 0 33.79 1.08 -2 10 0 33.31 1.09 1 -10 0 9.28 0.57 -1 10 0 9.66 0.55 -1 10 0 9.63 0.57 0 -10 0 28.36 0.96 0 -10 0 26.64 0.97 0 10 0 28.65 0.98 -1 -10 0 58.17 1.62 -1 -10 0 59.22 1.63 1 10 0 56.53 1.64 -2 -10 0 11.57 0.61 -2 -10 0 11.69 0.58 2 10 0 10.98 0.64 -3 -10 0 14.67 0.65 -3 -10 0 14.67 0.69 3 10 0 13.45 0.73 -4 -10 0 17.97 0.78 -4 -10 0 18.15 0.73 4 10 0 16.75 0.83 -5 -10 0 9.51 0.6 5 10 0 9.09 0.65 -6 -10 0 0.82 0.32 6 10 0 0.44 0.31 -7 -10 0 50.61 1.6 -8 -10 0 7.51 0.61 8 10 0 5.6 0.64 -9 -10 0 1.6 0.39 9 10 0 1.33 0.44 -10 -10 0 13.4 0.83 10 10 0 11.03 0.88 8 -11 0 20.89 1.11 -8 11 0 21.45 1.01 7 -11 0 4.69 0.61 -7 11 0 4.4 0.52 6 -11 0 13.68 0.87 -6 11 0 13.22 0.75 5 -11 0 45.49 1.57 -5 11 0 44.29 1.42 4 -11 0 0.29 0.34 -4 11 0 0.67 0.3 3 -11 0 0.68 0.35 -3 11 0 0.89 0.31 -3 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0.43 7 0 18 0.99 0.33 8 0 18 -0.02 0.3 3 -1 -18 21.63 1.06 -3 1 18 21.39 1.01 2 -1 -18 3.43 0.5 -2 1 18 3.99 0.51 1 -1 -18 13.27 0.79 -1 1 18 11.71 0.73 -3 -1 -18 28.12 1.15 -4 -1 -18 27.98 1.17 4 1 18 29.04 1.05 -5 -1 -18 -0.25 0.34 5 1 18 0.37 0.28 -6 -1 -18 11.71 0.81 6 1 18 11.43 0.68 -7 -1 -18 14.5 0.92 7 1 18 14.72 0.78 -8 -1 -18 10.74 0.85 8 1 18 11.82 0.73 -4 2 18 1.09 0.38 3 -2 -18 11.62 0.83 -3 2 18 11.93 0.75 2 -2 -18 14 0.86 1 -2 -18 1.18 0.39 0 -2 -18 0.16 0.35 2 2 18 13.45 0.69 -3 -2 -18 4.32 0.53 3 2 18 4.24 0.45 -4 -2 -18 10.59 0.75 4 2 18 12.5 0.68 -5 -2 -18 2.05 0.46 5 2 18 2.45 0.38 -6 -2 -18 -0.03 0.38 6 2 18 0.87 0.32 -7 -2 -18 10.68 0.81 7 2 18 10.75 0.7 -8 -2 -18 34.15 1.39 8 2 18 34.17 1.27 -4 3 18 9.47 0.7 3 -3 -18 0.23 0.41 2 -3 -18 6.47 0.66 1 -3 -18 21.69 1.03 0 -3 -18 10.7 0.75 -1 -3 -18 14.36 0.81 1 3 18 14.79 0.74 2 3 18 14.62 0.74 3 3 18 1.91 0.35 -4 -3 -18 4.29 0.53 4 3 18 3.83 0.45 -5 -3 -18 21.97 1.03 5 3 18 21.12 0.92 -6 -3 -18 15.63 0.9 6 3 18 15.8 0.81 -7 -3 -18 3.4 0.56 7 3 18 3.64 0.49 -8 -3 -18 27.47 1.23 8 3 18 28.27 1.15 3 -4 -18 0.87 0.46 2 -4 -18 -0.16 0.4 1 -4 -18 42.67 1.54 0 -4 -18 26.8 1.14 0 4 18 27.98 1.05 -1 -4 -18 3.39 0.5 1 4 18 2.88 0.41 -2 -4 -18 20.82 0.99 2 4 18 20.99 0.91 3 4 18 7.87 0.6 -4 -4 -18 -0.31 0.34 4 4 18 0.97 0.33 -5 -4 -18 25.29 1.09 5 4 18 24.97 1.04 -6 -4 -18 41.63 1.48 6 4 18 41.98 1.43 -7 -4 -18 2.95 0.52 7 4 18 2.58 0.44 -8 -4 -18 5.21 0.63 8 4 18 4.05 0.53 -9 -4 -18 5.05 0.65 3 -5 -18 8.29 0.8 2 -5 -18 1.31 0.47 1 -5 -18 18.7 1.02 -1 5 18 20.16 0.9 0 -5 -18 29.99 1.27 0 5 18 31.56 1.17 -1 -5 -18 0.58 0.41 1 5 18 0.66 0.3 -2 -5 -18 1.4 0.45 2 5 18 1.79 0.37 -3 -5 -18 14.86 0.87 3 5 18 14.05 0.77 4 5 18 22.09 0.98 -5 -5 -18 1.94 0.42 5 5 18 0.76 0.35 -6 -5 -18 45.67 1.57 6 5 18 47.21 1.57 -7 -5 -18 6.45 0.63 7 5 18 5.67 0.58 -8 -5 -18 0.43 0.43 8 5 18 -0.2 0.32 -9 -5 -18 0.79 0.47 3 -6 -18 23.32 1.2 2 -6 -18 22.54 1.17 -2 6 18 24.66 1.03 1 -6 -18 0.65 0.46 -1 6 18 0.69 0.34 0 -6 -18 11.33 0.86 0 6 18 12.1 0.73 -1 -6 -18 4.12 0.6 1 6 18 4.58 0.52 -2 -6 -18 3.94 0.57 2 6 18 3.91 0.48 -3 -6 -18 7.26 0.68 3 6 18 7.01 0.61 -4 -6 -18 39.55 1.43 4 6 18 38.9 1.38 -5 -6 -18 2.38 0.44 5 6 18 2.27 0.43 -6 -6 -18 5.98 0.62 6 6 18 7.38 0.64 -7 -6 -18 5.3 0.6 7 6 18 4.73 0.56 -8 -6 -18 15.6 0.92 8 6 18 13.89 0.86 -9 -6 -18 -0.65 0.38 -3 7 18 11.4 0.78 2 -7 -18 32.05 1.42 -2 7 18 33.57 1.27 1 -7 -18 7.77 0.77 -1 7 18 7.67 0.67 0 -7 -18 1.14 0.5 0 7 18 0.83 0.36 -1 -7 -18 3.38 0.6 1 7 18 4.28 0.53 -2 -7 -18 26.17 1.21 2 7 18 26.68 1.11 -3 -7 -18 0.8 0.46 3 7 18 1.09 0.37 -4 -7 -18 30.45 1.27 4 7 18 31.42 1.22 -5 -7 -18 8.71 0.74 5 7 18 9.54 0.7 -6 -7 -18 5.05 0.57 6 7 18 5.36 0.58 -7 -7 -18 0.58 0.39 7 7 18 1.63 0.44 -8 -7 -18 8.55 0.73 8 7 18 8.13 0.68 -3 8 18 0.15 0.37 -2 8 18 4.69 0.56 1 -8 -18 5.66 0.73 -1 8 18 4.84 0.56 0 -8 -18 6.57 0.73 0 8 18 8.27 0.68 -1 -8 -18 7.39 0.77 1 8 18 8.2 0.71 -2 -8 -18 31.22 1.33 2 8 18 28.73 1.2 -3 -8 -18 2.49 0.55 3 8 18 1.67 0.42 -4 -8 -18 3.61 0.56 4 8 18 3.63 0.52 -5 -8 -18 10.25 0.8 5 8 18 8.64 0.69 -6 -8 -18 23.77 1.11 6 8 18 19.72 1 -7 -8 -18 3.76 0.53 7 8 18 3.79 0.54 -8 -8 -18 12.32 0.85 8 8 18 11.79 0.8 1 -9 -18 5.41 0.74 -1 9 18 6.39 0.67 0 -9 -18 18.62 1.11 0 9 18 19.53 1 -1 -9 -18 0.87 0.5 1 9 18 0.51 0.39 -2 -9 -18 10.72 0.88 2 9 18 10.45 0.75 -3 -9 -18 8.04 0.78 3 9 18 7.91 0.71 -4 -9 -18 5.42 0.66 4 9 18 4.93 0.6 -5 -9 -18 4.11 0.61 5 9 18 3.28 0.51 -6 -9 -18 29.77 1.27 6 9 18 28.94 1.24 -7 -9 -18 3.08 0.53 -7 -9 -18 2.84 0.5 7 9 18 3.23 0.52 -8 -9 -18 9.53 0.77 0 10 18 25.79 1.17 -1 -10 -18 2.38 0.63 1 10 18 2.56 0.52 -2 -10 -18 1.76 0.56 2 10 18 2.38 0.49 -3 -10 -18 3.11 0.61 3 10 18 2.23 0.49 -4 -10 -18 16.65 1.02 4 10 18 15.06 0.89 -5 -10 -18 1.13 0.5 5 10 18 0.55 0.36 -6 -10 -18 4.35 0.61 6 10 18 3.21 0.52 -7 -10 -18 6.29 0.7 -4 -11 -18 34.7 1.47 -5 -11 -18 13.67 0.97 1 -2 19 11.28 0.79 -3 2 -19 23.57 1.13 -1 -1 19 2.73 0.43 0 -1 19 0.86 0.34 -3 1 -19 3.34 0.56 -4 1 -19 5.65 0.63 -5 1 -19 6.69 0.69 -2 0 19 6.22 0.61 -1 0 19 11.63 0.78 -3 0 -19 3.86 0.55 -4 0 -19 0.02 0.39 -5 0 -19 14.14 0.9 -6 0 -19 2.27 0.5 6 0 19 1.63 0.36 7 0 19 9.67 0.68 2 -1 -19 0.83 0.42 -4 -1 -19 5.2 0.59 -5 -1 -19 16.28 0.94 5 1 19 17.47 0.82 -6 -1 -19 11.2 0.82 6 1 19 10.61 0.68 -7 -1 -19 0.63 0.45 7 1 19 0.26 0.31 2 -2 -19 1.14 0.46 1 -2 -19 12.57 0.8 3 2 19 22.49 0.93 -4 -2 -19 3.39 0.52 4 2 19 3.01 0.42 -5 -2 -19 10.21 0.79 5 2 19 11.13 0.68 -6 -2 -19 23.64 1.12 6 2 19 23.59 1.01 -7 -2 -19 14.44 0.94 7 2 19 14.07 0.8 2 -3 -19 7.51 0.7 1 -3 -19 -0.09 0.39 0 -3 -19 4.65 0.58 2 3 19 9.83 0.64 3 3 19 5.63 0.53 4 3 19 4.79 0.49 -5 -3 -19 -0.78 0.35 5 3 19 0.2 0.3 -6 -3 -19 1.23 0.43 6 3 19 1.71 0.4 -7 -3 -19 13.36 0.9 7 3 19 12.93 0.78 2 -4 -19 5.66 0.68 1 -4 -19 7.35 0.69 0 -4 -19 -0.09 0.41 -1 -4 -19 38.84 1.42 1 4 19 40.16 1.35 2 4 19 19.87 0.91 3 4 19 -0.43 0.25 4 4 19 4.49 0.5 -5 -4 -19 14.49 0.89 5 4 19 15.07 0.8 -6 -4 -19 13.26 0.88 6 4 19 13.14 0.79 -7 -4 -19 2.91 0.54 7 4 19 3.74 0.52 -8 -4 -19 19.21 1.07 2 -5 -19 -0.14 0.46 1 -5 -19 26.49 1.22 0 -5 -19 6.5 0.67 0 5 19 6.91 0.6 -1 -5 -19 6.09 0.65 1 5 19 7.73 0.63 -2 -5 -19 28.17 1.2 2 5 19 26.71 1.08 3 5 19 0.61 0.33 4 5 19 0.33 0.33 5 5 19 22.82 1.02 -6 -5 -19 30.48 1.28 6 5 19 33.47 1.27 -7 -5 -19 -0.03 0.42 7 5 19 0.11 0.35 -8 -5 -19 11.64 0.88 1 -6 -19 32.06 1.39 -1 6 19 34.53 1.28 0 -6 -19 34.95 1.42 0 6 19 35.23 1.3 -1 -6 -19 1.15 0.48 1 6 19 1.34 0.38 -2 -6 -19 0.6 0.45 2 6 19 0.93 0.35 -3 -6 -19 0.56 0.44 3 6 19 0.71 0.37 4 6 19 10.5 0.72 5 6 19 11.87 0.77 -6 -6 -19 42.44 1.52 6 6 19 43.13 1.52 -7 -6 -19 3.42 0.53 7 6 19 3.52 0.53 -8 -6 -19 3.19 0.55 -2 7 19 5.87 0.62 1 -7 -19 5.13 0.7 -1 7 19 7.23 0.65 0 -7 -19 28.98 1.32 0 7 19 27.26 1.15 -1 -7 -19 9.26 0.83 1 7 19 9.39 0.7 -2 -7 -19 1.5 0.51 2 7 19 1.32 0.36 -3 -7 -19 17.56 0.99 3 7 19 17.9 0.92 -4 -7 -19 27.98 1.22 4 7 19 27.54 1.16 5 7 19 -0.27 0.33 6 7 19 15.3 0.88 -7 -7 -19 1.81 0.46 7 7 19 2.28 0.45 -8 -7 -19 2.29 0.53 -1 8 19 0.73 0.38 0 -8 -19 1.58 0.55 0 8 19 1.25 0.41 -1 -8 -19 8.69 0.83 1 8 19 10.83 0.75 -2 -8 -19 6.27 0.72 2 8 19 8.12 0.71 -3 -8 -19 7.69 0.75 3 8 19 8.28 0.69 -4 -8 -19 34.58 1.42 4 8 19 35.02 1.35 -5 -8 -19 13.01 0.88 5 8 19 13.15 0.84 6 8 19 0.84 0.39 -7 -8 -19 5.18 0.62 -8 -8 -19 17.14 0.99 -1 -9 -19 3.02 0.64 1 9 19 2.87 0.51 -2 -9 -19 17.18 1.06 2 9 19 16.65 0.94 -3 -9 -19 0.86 0.52 3 9 19 0.4 0.35 -4 -9 -19 9.65 0.82 4 9 19 8.3 0.75 -5 -9 -19 7.04 0.73 5 9 19 7.7 0.73 -6 -9 -19 8.44 0.76 -3 -10 -19 2.87 0.63 -4 -10 -19 2.59 0.58 -5 -10 -19 2.31 0.55 -6 -10 -19 14.93 0.97 -7 -10 -19 0.92 0.49 -4 0 -20 2.11 0.49 -4 -1 -20 3.9 0.58 -5 -1 -20 18.11 1.01 6 1 20 3.46 0.46 -5 -2 -20 26.72 1.22 5 2 20 29.71 1.12 -6 -2 -20 2.62 0.54 6 2 20 3.8 0.48 1 -3 -20 28.33 1.23 3 3 20 21.41 0.94 4 3 20 4.41 0.52 -5 -3 -20 7.08 0.7 5 3 20 8.57 0.66 -6 -3 -20 4.46 0.63 6 3 20 5.9 0.58 1 -4 -20 4.2 0.62 0 -4 -20 8.04 0.74 -1 -4 -20 16.26 0.93 2 4 20 0.33 0.3 3 4 20 24.49 1.03 4 4 20 15.85 0.84 5 4 20 -0.05 0.29 -6 -4 -20 4.46 0.6 6 4 20 5.08 0.57 -7 -4 -20 12.88 0.93 0 -5 -20 3.07 0.58 -1 -5 -20 31.69 1.31 1 5 20 32.7 1.22 -2 -5 -20 16.03 0.93 2 5 20 15.58 0.84 3 5 20 7.99 0.67 4 5 20 3.5 0.47 5 5 20 2.63 0.45 -6 -5 -20 0.68 0.45 6 5 20 0.1 0.31 -7 -5 -20 14.46 0.95 0 -6 -20 0.53 0.48 0 6 20 0.43 0.36 -1 -6 -20 16.21 0.99 1 6 20 15.48 0.86 -2 -6 -20 10.17 0.83 2 6 20 10.35 0.73 3 6 20 0.32 0.35 4 6 20 0.21 0.31 5 6 20 13.38 0.82 -7 -6 -20 6.31 0.66 0 7 20 11.4 0.78 -1 -7 -20 -0.33 0.47 1 7 20 0.33 0.36 -2 -7 -20 4.44 0.65 2 7 20 4.09 0.54 -3 -7 -20 4.75 0.63 3 7 20 4.35 0.54 4 7 20 3.4 0.53 -7 -7 -20 0.2 0.39 -2 -8 -20 -0.33 0.48 -3 -8 -20 16.14 1.03 -4 -8 -20 8.25 0.78 -4 -9 -20 9.3 0.84 -5 -9 -20 0.59 0.49 4 3 21 0.39 0.33 3 4 21 20.03 0.95 4 4 21 1.19 0.37 -1 -5 -21 7.75 0.76 2 5 21 1.63 0.41 3 5 21 24.77 1.08 -2 -6 -21 3.84 0.64 -3 -7 -21 0.57 0.52 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 Au1 P1 171.15(7) . . y N2 Cu1 N1 79.63(8) . . y N3 Cu1 N1 109.17(8) . . y N3 Cu1 N2 80.69(8) . . y C1 Cu1 N1 108.27(9) . . y C1 Cu1 N2 111.27(9) . . y C1 Cu1 N3 142.18(9) . . y C2 Cu1 N1 142.73(9) . . y C2 Cu1 N2 116.78(9) . . y C2 Cu1 N3 106.54(9) . . y C2 Cu1 C1 35.70(10) . . y C16 P1 Au1 113.34(8) . . ? C22 P1 Au1 115.23(9) . . ? C22 P1 C16 105.56(12) . . ? C28 P1 Au1 107.15(9) . . ? C28 P1 C16 106.82(12) . . ? C28 P1 C22 108.37(12) . . ? C4 N1 Cu1 125.92(18) . . ? C8 N1 Cu1 116.31(17) . . ? C8 N1 C4 117.8(2) . . ? C3 N2 Cu1 112.87(15) 2_776 . ? C9 N2 Cu1 103.77(15) . . ? C9 N2 C3 109.58(19) . 2_776 ? C10 N2 Cu1 104.58(15) . . ? C10 N2 C3 113.4(2) . 2_776 ? C10 N2 C9 112.2(2) . . ? C11 N3 Cu1 116.52(16) . . ? C15 N3 Cu1 124.08(17) . . ? C15 N3 C11 118.6(2) . . ? Cu1 C1 Au1 123.23(13) . . ? C2 C1 Au1 164.7(2) . . ? C2 C1 Cu1 71.51(16) . . ? C1 C2 Cu1 72.79(16) . . ? C3 C2 Cu1 127.12(17) . . ? C3 C2 C1 160.1(3) . . ? C2 C3 N2 111.9(2) . 2_776 ? C5 C4 N1 123.8(3) . . ? C6 C5 C4 118.0(3) . . ? C7 C6 C5 119.3(3) . . ? C8 C7 C6 119.4(3) . . ? C7 C8 N1 121.8(2) . . ? C9 C8 N1 117.0(2) . . ? C9 C8 C7 121.0(2) . . ? C8 C9 N2 111.7(2) . . ? C11 C10 N2 112.8(2) . . ? C10 C11 N3 117.5(2) . . ? C12 C11 N3 121.7(2) . . ? C12 C11 C10 120.7(2) . . ? C13 C12 C11 119.4(2) . . ? C14 C13 C12 118.8(2) . . ? C15 C14 C13 119.0(2) . . ? C14 C15 N3 122.4(2) . . ? C17 C16 P1 123.2(2) . . ? C21 C16 P1 117.5(2) . . ? C21 C16 C17 119.1(2) . . ? C18 C17 C16 120.1(3) . . ? C19 C18 C17 120.6(3) . . ? C20 C19 C18 119.4(3) . . ? C21 C20 C19 120.5(3) . . ? C20 C21 C16 120.3(3) . . ? C23 C22 P1 118.9(2) . . ? C27 C22 P1 121.3(2) . . ? C27 C22 C23 119.8(3) . . ? C24 C23 C22 120.0(3) . . ? C25 C24 C23 119.9(3) . . ? C26 C25 C24 120.3(3) . . ? C27 C26 C25 120.5(3) . . ? C26 C27 C22 119.5(3) . . ? C29 C28 P1 123.1(2) . . ? C33 C28 P1 117.0(2) . . ? C33 C28 C29 119.7(3) . . ? C30 C29 C28 118.9(3) . . ? C31 C30 C29 121.5(3) . . ? C32 C31 C30 119.6(3) . . ? C33 C32 C31 120.0(4) . . ? C32 C33 C28 120.2(3) . . ? Cl2 C34 Cl1 112.41(18) . . ? Cl4 C35 Cl3 111.6(10) . . ? Cl4A C35A Cl3A 110.8(9) . . ? O2_1 N1_1 O1_1 121.0(5) . . ? O3_1 N1_1 O1_1 120.2(4) . . ? O3_1 N1_1 O2_1 118.8(4) . . ? O2_2 N1_2 O1_2 118.8(18) . . ? O3_2 N1_2 O1_2 120(2) . . ? O3_2 N1_2 O2_2 119.5(19) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Au1 P1 2.2694(6) . y Au1 C1 1.999(3) . y Cu1 N1 2.033(2) . y Cu1 N2 2.264(2) . y Cu1 N3 2.017(2) . y Cu1 C1 2.019(2) . y Cu1 C2 2.004(2) . y P1 C16 1.815(3) . ? P1 C22 1.815(3) . ? P1 C28 1.817(3) . ? N1 C4 1.345(3) . ? N1 C8 1.348(3) . ? N2 C3 1.482(3) 2_776 ? N2 C9 1.472(3) . ? N2 C10 1.470(3) . ? N3 C11 1.346(3) . ? N3 C15 1.352(3) . ? C1 C2 1.233(4) . ? C2 C3 1.479(3) . ? C4 C5 1.380(4) . ? C5 C6 1.381(4) . ? C6 C7 1.383(4) . ? C7 C8 1.389(4) . ? C8 C9 1.503(4) . ? C10 C11 1.507(3) . ? C11 C12 1.395(3) . ? C12 C13 1.378(4) . ? C13 C14 1.396(4) . ? C14 C15 1.378(4) . ? C16 C17 1.388(4) . ? C16 C21 1.397(4) . ? C17 C18 1.395(4) . ? C18 C19 1.379(4) . ? C19 C20 1.385(4) . ? C20 C21 1.384(4) . ? C22 C23 1.386(4) . ? C22 C27 1.396(4) . ? C23 C24 1.398(4) . ? C24 C25 1.379(5) . ? C25 C26 1.378(5) . ? C26 C27 1.391(4) . ? C28 C29 1.386(4) . ? C28 C33 1.386(4) . ? C29 C30 1.395(4) . ? C30 C31 1.359(6) . ? C31 C32 1.380(6) . ? C32 C33 1.386(5) . ? C34 Cl1 1.765(3) . ? C34 Cl2 1.752(3) . ? C35 Cl3 1.777(19) . ? C35 Cl4 1.744(19) . ? C35A Cl3A 1.755(16) . ? C35A Cl4A 1.762(17) . ? N1_1 O1_1 1.225(5) . ? N1_1 O2_1 1.251(5) . ? N1_1 O3_1 1.254(6) . ? N1_2 O1_2 1.249(13) . ? N1_2 O2_2 1.236(13) . ? N1_2 O3_2 1.264(13) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Au1 C1 C2 Cu1 165.9(9) . . . . ? Au1 C1 C2 C3 -13.6(11) . . . . ? Cu1 N1 C4 C5 -179.1(2) . . . . ? Cu1 N1 C8 C7 177.04(18) . . . . ? Cu1 N1 C8 C9 -7.92(19) . . . . ? Cu1 N2 C3 C2 60.25(15) . . 2_776 2_776 ? Cu1 N2 C9 C8 -35.56(15) . . . . ? Cu1 N2 C10 C11 -29.16(15) . . . . ? Cu1 N3 C11 C10 -11.0(2) . . . . ? Cu1 N3 C11 C12 171.18(17) . . . . ? Cu1 N3 C15 C14 -169.4(2) . . . . ? Cu1 C1 C2 C3 -179.5(4) . . . . ? Cu1 C2 C3 N2 124.8(2) . . . 2_776 ? P1 C16 C17 C18 173.8(2) . . . . ? P1 C16 C21 C20 -174.1(2) . . . . ? P1 C22 C23 C24 -177.3(2) . . . . ? P1 C22 C27 C26 177.2(2) . . . . ? P1 C28 C29 C30 174.1(3) . . . . ? P1 C28 C33 C32 -175.5(3) . . . . ? N1 C4 C5 C6 1.5(3) . . . . ? N1 C8 C7 C6 2.8(3) . . . . ? N1 C8 C9 N2 31.9(2) . . . . ? N2 C3 C2 C1 -55.9(5) 2_776 . . . ? N2 C9 C8 C7 -153.0(2) . . . . ? N2 C10 C11 N3 29.1(3) . . . . ? N2 C10 C11 C12 -153.0(2) . . . . ? N3 C11 C12 C13 -1.1(3) . . . . ? N3 C15 C14 C13 -1.0(3) . . . . ? C4 C5 C6 C7 -0.6(3) . . . . ? C5 C6 C7 C8 -1.5(4) . . . . ? C6 C7 C8 C9 -172.0(3) . . . . ? C10 C11 C12 C13 -178.9(2) . . . . ? C11 C12 C13 C14 0.4(3) . . . . ? C12 C13 C14 C15 0.5(3) . . . . ? C16 C17 C18 C19 -0.4(3) . . . . ? C16 C21 C20 C19 0.3(3) . . . . ? C17 C18 C19 C20 0.8(3) . . . . ? C18 C19 C20 C21 -0.8(3) . . . . ? C22 C23 C24 C25 0.4(3) . . . . ? C22 C27 C26 C25 -0.3(3) . . . . ? C23 C24 C25 C26 -0.9(3) . . . . ? C24 C25 C26 C27 0.8(3) . . . . ? C28 C29 C30 C31 1.2(4) . . . . ? C28 C33 C32 C31 1.2(4) . . . . ? C29 C30 C31 C32 0.9(4) . . . . ? C30 C31 C32 C33 -2.1(4) . . . . ? loop_ _restr_distance_atom_site_label_1 _restr_distance_atom_site_label_2 _restr_distance_site_symmetry_2 _restr_distance_target _restr_distance_target_weight_param _restr_distance_diff N1_1 O1_1 1 1.2500 0.0200 0.0248 N1_1 O2_1 1 1.2400 0.0200 -0.0112 N1_1 O3_1 1 1.2500 0.0200 -0.0036 N1_2 O1_2 1 1.2500 0.0200 0.0014 N1_2 O2_2 1 1.2400 0.0200 0.0042 N1_2 O3_2 1 1.2500 0.0200 -0.0137 loop_ _restr_equal_distance_atom_site_label_1 _restr_equal_distance_atom_site_label_2 _restr_equal_distance_site_symmetry_2 _restr_equal_distance_class_id C35 H35a 1 11 C35 H35b 1 6 C35 Cl3 1 8 C35 Cl4 1 4 H35a H35b 1 12 H35a Cl3 1 9 H35a Cl4 1 10 H35b Cl3 1 7 H35b Cl4 1 3 Cl3 Cl4 1 5 C35A H35c 1 11 C35A H35d 1 6 C35A Cl3A 1 8 C35A Cl4A 1 4 H35c H35d 1 12 H35c Cl3A 1 9 H35c Cl4A 1 10 H35d Cl3A 1 7 H35d Cl4A 1 3 Cl3A Cl4A 1 5 N1_1 O1_1 1 2 N1_1 O2_1 1 2 N1_1 O3_1 1 2 O1_1 O2_1 1 1 O2_1 O3_1 1 1 O3_1 O1_1 1 1 N1_2 O1_2 1 2 N1_2 O2_2 1 2 N1_2 O3_2 1 2 O1_2 O2_2 1 1 O2_2 O3_2 1 1 O3_2 O1_2 1 1 loop_ _restr_equal_distance_class_class_id _restr_equal_distance_class_target_weight_param _restr_equal_distance_class_average _restr_equal_distance_class_esd _restr_equal_distance_class_diff_max 1 0.0400 2.1550 0.0101 0.0170 2 0.0200 1.2463 0.0125 0.0211 3 0.0400 2.2667 0.0057 0.0057 4 0.0200 1.7528 0.0088 0.0088 5 0.0400 2.9038 0.0085 0.0085 6 0.0200 0.9934 0.0034 0.0034 7 0.0400 2.2816 0.0212 0.0212 8 0.0200 1.7665 0.0110 0.0110 9 0.0400 2.3079 0.0050 0.0050 10 0.0400 2.2542 0.0181 0.0181 11 0.0200 0.9848 0.0052 0.0052 12 0.0400 1.6285 0.0271 0.0271 loop_ _restr_U_similar_atom_site_label_1 _restr_U_similar_atom_site_label_2 _restr_U_similar_weight_param Au1 P1 0.0400 Au1 C1 0.0400 Cu1 N1 0.0400 Cu1 N2 0.0400 Cu1 N3 0.0400 Cu1 C1 0.0400 Cu1 C2 0.0400 P1 C16 0.0400 P1 C22 0.0400 P1 C28 0.0400 N1 C4 0.0400 N1 C8 0.0400 N2 C9 0.0400 N2 C10 0.0400 N3 C11 0.0400 N3 C15 0.0400 C1 C2 0.0400 C2 C3 0.0400 C3 H3a 0.0800 C3 H3b 0.0800 C4 H4 0.0800 C4 C5 0.0400 C5 H5 0.0800 C5 C6 0.0400 C6 H6 0.0800 C6 C7 0.0400 C7 H7 0.0800 C7 C8 0.0400 C8 C9 0.0400 C9 H9a 0.0800 C9 H9b 0.0800 C10 H10a 0.0800 C10 H10b 0.0800 C10 C11 0.0400 C11 C12 0.0400 C12 H12 0.0800 C12 C13 0.0400 C13 H13 0.0800 C13 C14 0.0400 C14 H14 0.0800 C14 C15 0.0400 C16 C17 0.0400 C16 C21 0.0400 C17 H17 0.0800 C17 C18 0.0400 C18 H18 0.0800 C18 C19 0.0400 C19 H19 0.0800 C19 C20 0.0400 C20 H20 0.0800 C20 C21 0.0400 C21 H21 0.0800 C22 C23 0.0400 C22 C27 0.0400 C23 H23 0.0800 C23 C24 0.0400 C24 H24 0.0800 C24 C25 0.0400 C25 H25 0.0800 C25 C26 0.0400 C26 H26 0.0800 C26 C27 0.0400 C27 H27 0.0800 C28 C29 0.0400 C28 C33 0.0400 C29 H29 0.0800 C29 C30 0.0400 C30 H30 0.0800 C30 C31 0.0400 C31 H31 0.0800 C31 C32 0.0400 C32 H32 0.0800 C32 C33 0.0400 C33 H33 0.0800 C34 H34a 0.0800 C34 H34b 0.0800 C34 Cl1 0.0800 C34 Cl2 0.0800 C35 H35a 0.0800 C35 H35b 0.0800 C35 Cl3 0.0800 C35 Cl4 0.0800 O1B H1Ba 0.0800 O1B H1Bb 0.0800 C35A H35c 0.0800 C35A H35d 0.0800 C35A Cl3A 0.0800 C35A Cl4A 0.0800 O6 H6a 0.0800 O6 H6b 0.0800 N1_1 O1_1 0.0800 N1_1 O2_1 0.0800 N1_1 O3_1 0.0800 N1_2 O1_2 0.0800 N1_2 O2_2 0.0800 N1_2 O3_2 0.0800 loop_ _restr_chirality_atom_site_label_1 _restr_chirality_atom_site_label_2 _restr_chirality_atom_site_label_3 _restr_chirality_atom_site_label_4 _restr_chirality_site_symmetry_1 _restr_chirality_site_symmetry_2 _restr_chirality_site_symmetry_3 _restr_chirality_site_symmetry_4 _restr_chirality_volume_target _restr_chirality_weight_param _restr_chirality_diff O2_1 O1_2 O3_1 N1_2 1 1 1 1 0.0000 0.1000 -0.1468 O3_1 N1_2 N1_1 O2_2 1 1 1 1 0.0000 0.1000 0.0136 N1_2 N1_1 O2_2 O1_1 1 1 1 1 0.0000 0.1000 -0.2238 O1_2 O3_1 N1_2 N1_1 1 1 1 1 0.0000 0.1000 0.0442 O3_2 O2_1 O1_2 O3_1 1 1 1 1 0.0000 0.1000 0.2628 loop_ _restr_rigu_atom_site_label_1 _restr_rigu_atom_site_label_2 _restr_rigu_target_weight_param _restr_rigu_u13_diff _restr_rigu_u23_diff _restr_rigu_u33_diff N1_1 O1_1 0.004000 0.009936 -0.005060 -0.000325 N1_1 O2_1 0.004000 0.012990 -0.000498 0.003172 N1_1 O3_1 0.004000 0.011837 0.001414 -0.002005 O1_1 O2_1 0.004000 0.031718 -0.015987 -0.001997 O1_1 O3_1 0.004000 0.021865 0.024443 -0.001688 O2_1 O3_1 0.004000 0.003806 -0.014135 -0.002022 N1_2 O1_2 0.004000 0.001048 0.003721 -0.001658 N1_2 O2_2 0.004000 -0.001679 -0.000677 -0.002984 N1_2 O3_2 0.004000 -0.000008 0.003103 -0.000077 O1_2 O2_2 0.004000 -0.003713 -0.010460 -0.006391 O1_2 O3_2 0.004000 0.012325 0.002583 -0.007691 O2_2 O3_2 0.004000 -0.013195 0.015044 -0.005883