#------------------------------------------------------------------------------ #$Date: 2020-08-13 04:55:43 +0300 (Thu, 13 Aug 2020) $ #$Revision: 255284 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/51/7705141.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7705141 loop_ _publ_author_name 'Gimeno, Maria Concepcion' 'Johnson, Alice' 'Marzo, Isabel' _publ_section_title ; Heterobimetallic propargyl gold complexes with \p-bound copper or silver with enhanced anticancer activity ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D0DT02113J _journal_year 2020 _chemical_formula_moiety 'C42 H34 Au2 O P2' _chemical_formula_sum 'C42 H34 Au2 O P2' _chemical_formula_weight 1010.618 _space_group_crystal_system orthorhombic _space_group_IT_number 56 _space_group_name_Hall '-P 2ab 2ac' _space_group_name_H-M_alt 'P c c n' _symmetry_Int_Tables_number 56 _audit_creation_date 2020-07-10 _audit_creation_method ; Olex2 1.3-dev (compiled 2020.05.13 svn.r35546bd3 for OlexSys, GUI svn.r5830) ; _audit_update_record ; 2020-07-29 deposited with the CCDC. 2020-08-10 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 21.9189(13) _cell_length_b 9.0536(6) _cell_length_c 17.5745(11) _cell_measurement_reflns_used 9976 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 28.37 _cell_measurement_theta_min 2.43 _cell_volume 3487.6(4) _computing_cell_refinement SMART _computing_data_collection SMART _computing_data_reduction SMART _computing_molecular_graphics 'Olex2 1.3-dev (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3-dev (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)' _computing_structure_solution SHELXS _diffrn_ambient_temperature 100.15 _diffrn_detector_area_resol_mean 8.26 _diffrn_measured_fraction_theta_full 1.0000 _diffrn_measured_fraction_theta_max 0.9608 _diffrn_measurement_device_type 'SMART Apex CCD' _diffrn_measurement_method 'w rotations with narrow frames' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0435 _diffrn_reflns_av_unetI/netI 0.0241 _diffrn_reflns_Laue_measured_fraction_full 1.0000 _diffrn_reflns_Laue_measured_fraction_max 0.9608 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_h_min -29 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 39861 _diffrn_reflns_point_group_measured_fraction_full 1.0000 _diffrn_reflns_point_group_measured_fraction_max 0.9608 _diffrn_reflns_theta_full 25.2417 _diffrn_reflns_theta_max 28.66 _diffrn_reflns_theta_min 1.86 _exptl_absorpt_coefficient_mu 8.528 _exptl_absorpt_correction_T_max 0.3814 _exptl_absorpt_correction_T_min 0.1172 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.925 _exptl_crystal_description prism _exptl_crystal_F_000 1918.279 _exptl_crystal_size_max 0.44 _exptl_crystal_size_mid 0.16 _exptl_crystal_size_min 0.14 _refine_diff_density_max 3.3862 _refine_diff_density_min -1.2712 _refine_diff_density_rms 0.2152 _refine_ls_d_res_high 0.7409 _refine_ls_d_res_low 10.9594 _refine_ls_goodness_of_fit_ref 1.0559 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_constraints 36 _refine_ls_number_parameters 232 _refine_ls_number_reflns 4314 _refine_ls_number_restraints 75 _refine_ls_restrained_S_all 1.0464 _refine_ls_R_factor_all 0.0430 _refine_ls_R_factor_gt 0.0312 _refine_ls_shift/su_max 0.0003 _refine_ls_shift/su_mean 0.0000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0220P)^2^+16.0089P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0618 _refine_ls_wR_factor_ref 0.0675 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 29 _reflns_limit_h_min 0 _reflns_limit_k_max 12 _reflns_limit_k_min 0 _reflns_limit_l_max 23 _reflns_limit_l_min 0 _reflns_number_gt 3558 _reflns_number_total 4314 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL con250s in Pccn CELL 0.71073 21.9189 9.0536 17.5745 90 90 90 ZERR 4 0.0013 0.0006 0.0011 0 0 0 LATT 1 SYMM 0.5-X,0.5-Y,+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,-Y,0.5-Z SFAC C H Au O P UNIT 168 136 8 4 8 SADI 0.001 C2A C1 C1B C1A SADI 0.001 C2 C1A C3 C2A SADI 0.001 O C3 O C2 SIMU 0.001 0.002 2 C1A C2A ISOR 0.001 0.002 C2A C3 O C2 C1A RIGU 0.001 0.001 C1 C3 C2A O C2 C1A C1B Au1 L.S. 20 PLAN 2 SIZE 0.44 0.16 0.14 TEMP -173 CONF LIST 4 BOND MORE -1 BOND $H fmap 2 acta WGHT 0.022039 16.008939 FVAR 0.042785 REM REM REM > REM REM > REM > REM REM Au1 3 0.32309 0.20856 0.18397 11.00000 0.02112 0.02892 0.02602 = -0.00204 -0.00022 0.00069 P1 5 0.38441 0.34271 0.10582 11.00000 0.02475 0.02405 0.02257 = -0.00058 -0.00203 0.00131 PART -1 C1 1 0.28415 0.06458 0.26062 10.50000 10.02932 10.04104 = 10.03844 -10.00703 10.00445 10.00796 C3 1 0.24789 -0.11188 0.37164 10.50000 0.04134 0.04151 0.04056 = -0.00023 0.00013 0.00009 AFIX 23 H3a 2 0.28357 -0.13854 0.40333 10.50000 -1.20000 H3b 2 0.21894 -0.05741 0.40453 10.50000 -1.20000 AFIX 0 PART 0 C4 1 0.36556 0.53418 0.08506 11.00000 0.02546 0.02701 0.03028 = -0.00367 -0.00580 0.00334 C5 1 0.33522 0.61626 0.13992 11.00000 0.02204 0.03329 0.03338 = -0.00156 -0.00091 0.00161 AFIX 43 H5 2 0.32082 0.57006 0.18501 11.00000 -1.20000 AFIX 0 C6 1 0.32604 0.76620 0.12854 11.00000 0.02593 0.03163 0.05202 = -0.01264 -0.01159 0.00547 AFIX 43 H6 2 0.30576 0.82275 0.16641 11.00000 -1.20000 AFIX 0 C7 1 0.34599 0.83406 0.06294 11.00000 0.03673 0.02675 0.05353 = -0.00195 -0.01617 0.00721 AFIX 43 H7 2 0.33963 0.93692 0.05578 11.00000 -1.20000 AFIX 0 C8 1 0.37541 0.75177 0.00737 11.00000 0.04599 0.03122 0.03669 = 0.00865 -0.00793 0.00302 AFIX 43 H8 2 0.38889 0.79780 -0.03820 11.00000 -1.20000 AFIX 0 C9 1 0.38503 0.60186 0.01869 11.00000 0.04664 0.03266 0.02616 = 0.00204 -0.00157 0.00878 AFIX 43 H9 2 0.40510 0.54530 -0.01934 11.00000 -1.20000 AFIX 0 C10 1 0.46049 0.35129 0.14613 11.00000 0.02644 0.02307 0.01594 = -0.00255 -0.00187 0.00415 C11 1 0.48091 0.23414 0.19105 11.00000 0.02698 0.03310 0.02971 = 0.00588 -0.00053 -0.00436 AFIX 43 H11 2 0.45469 0.15255 0.20031 11.00000 -1.20000 AFIX 0 C12 1 0.53880 0.23535 0.22224 11.00000 0.02709 0.03488 0.03984 = 0.01028 -0.00520 0.00208 AFIX 43 H12 2 0.55238 0.15449 0.25224 11.00000 -1.20000 AFIX 0 C13 1 0.57697 0.35491 0.20961 11.00000 0.02460 0.03757 0.02981 = -0.00361 -0.00206 0.00223 AFIX 43 H13 2 0.61675 0.35604 0.23105 11.00000 -1.20000 AFIX 0 C14 1 0.55735 0.47202 0.16606 11.00000 0.03187 0.02971 0.03241 = -0.00204 0.00343 -0.00662 AFIX 43 H14 2 0.58354 0.55404 0.15774 11.00000 -1.20000 AFIX 0 C15 1 0.49982 0.47054 0.13453 11.00000 0.03092 0.02409 0.02914 = 0.00195 -0.00064 -0.00068 AFIX 43 H15 2 0.48671 0.55178 0.10447 11.00000 -1.20000 AFIX 0 C16 1 0.39445 0.25677 0.01282 11.00000 0.03289 0.02011 0.02198 = 0.00252 -0.00303 -0.00318 C17 1 0.34426 0.24904 -0.03566 11.00000 0.04108 0.03220 0.03683 = 0.00238 -0.00801 -0.00519 AFIX 43 H17 2 0.30622 0.28887 -0.01983 11.00000 -1.20000 AFIX 0 C18 1 0.34922 0.18425 -0.10625 11.00000 0.07623 0.03287 0.03105 = 0.00483 -0.02798 -0.01424 AFIX 43 H18 2 0.31493 0.18148 -0.13927 11.00000 -1.20000 AFIX 0 C19 1 0.40388 0.12340 -0.12909 11.00000 0.08958 0.02555 0.02425 = -0.00195 -0.00711 -0.00202 AFIX 43 H19 2 0.40697 0.07712 -0.17745 11.00000 -1.20000 AFIX 0 C20 1 0.45383 0.12952 -0.08213 11.00000 0.06937 0.03101 0.03081 = -0.00413 0.00467 0.00950 AFIX 43 H20 2 0.49152 0.08836 -0.09837 11.00000 -1.20000 AFIX 0 C21 1 0.44957 0.19615 -0.01033 11.00000 0.04171 0.02694 0.02630 = -0.00091 -0.00044 0.00594 AFIX 43 H21 2 0.48414 0.19979 0.02223 11.00000 -1.20000 AFIX 0 PART -1 C2A 1 0.26815 -0.01398 0.31225 10.50000 0.03719 0.03907 0.03798 = -0.00260 0.00051 0.00110 O 4 0.21946 -0.24325 0.34728 10.50000 0.04573 0.04388 0.04693 = -0.00103 -0.00066 -0.00046 C2 1 0.26158 -0.35998 0.34047 10.50000 0.04532 0.04379 0.04486 = -0.00192 -0.00078 -0.00031 AFIX 23 H2a 2 0.29910 -0.32326 0.31544 10.50000 -1.20000 H2b 2 0.27282 -0.39563 0.39184 10.50000 -1.20000 AFIX 0 C1A 1 0.23699 -0.48072 0.29696 10.50000 0.03772 0.03794 0.03694 = 0.00033 0.00049 0.00159 C1B 1 0.21660 -0.57345 0.25488 10.50000 10.02932 10.04104 = 10.03844 -10.00703 10.00445 10.00796 HKLF 4 END Q1 1 0.25 -0.25 0.316667 11 0.05 3.39 Q2 1 0.32 0.1875 0.133333 11 0.05 1.24 REM The information below was added by Olex2. REM REM R1 = 0.0312 for 3558 Fo > 4sig(Fo) and 0.0430 for all 4314 data REM 232 parameters refined using 75 restraints REM Highest difference peak 3.3862, deepest hole -1.2712 REM Mean Shift 0.0000, Max Shift 0.0003. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0430 REM R1_gt = 0.0312 REM wR_ref = 0.0675 REM GOOF = 1.0559 REM Shift_max = 0.0003 REM Shift_mean = 0.0000 REM Reflections_all = 4314 REM Reflections_gt = 3558 REM Parameters = 232 REM Hole = -1.2712 REM Peak = 3.3862 REM Flack = n/a ; _cod_data_source_file d0dt02113j2.cif _cod_data_source_block con250s _cod_database_code 7705141 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups 2. Restrained distances C2A-C1 \\sim C1B-C1A with sigma of 0.001 C2-C1A \\sim C3-C2A with sigma of 0.001 O-C3 \\sim O-C2 with sigma of 0.001 3. Uiso/Uaniso restraints and constraints C1A \\sim C2A: within 2A with sigma of 0.001 and sigma for terminal atoms of 0.002 within 2A Uanis(C2A) \\sim Ueq, Uanis(C3) \\sim Ueq, Uanis(O) \\sim Ueq, Uanis(C2) \\sim Ueq, Uanis(C1A) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002 4. Rigid body (RIGU) restrains C1, C3, C2A, O, C2, C1A, C1B, Au1 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001 5. Others Fixed Sof: C1(0.5) C3(0.5) H3a(0.5) H3b(0.5) C2A(0.5) O(0.5) C2(0.5) H2a(0.5) H2b(0.5) C1A(0.5) C1B(0.5) Fixed U11: C1(0.02932) C1B(0.02932) Fixed U12: C1(0.00796) C1B(0.00796) Fixed U13: C1(0.00445) C1B(0.00445) Fixed U22: C1(0.04104) C1B(0.04104) Fixed U23: C1(-0.00703) C1B(-0.00703) Fixed U33: C1(0.03844) C1B(0.03844) 6.a Secondary CH2 refined with riding coordinates: C3(H3a,H3b), C2(H2a,H2b) 6.b Aromatic/amide H refined with riding coordinates: C5(H5), C6(H6), C7(H7), C8(H8), C9(H9), C11(H11), C12(H12), C13(H13), C14(H14), C15(H15), C17(H17), C18(H18), C19(H19), C20(H20), C21(H21) ; _iucr_refine_fcf_details ; data_con250s_CCDC1 _computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 x+1/2,-y,-z+1/2 3 -x,y+1/2,-z+1/2 4 -x+1/2,-y+1/2,z 5 -x,-y,-z 6 -x-1/2,y,z-1/2 7 x,-y-1/2,z-1/2 8 x-1/2,y-1/2,-z _space_group_crystal_system orthorhombic _space_group_IT_number 56 _space_group_name_H-M_alt 'P c c n' _space_group_name_Hall '-P 2ab 2ac' _symmetry_space_group_name_H-M 'P c c n' _symmetry_space_group_name_Hall '-P 2ab 2ac' _symmetry_Int_Tables_number 56 _cell_length_a 21.9189(13) _cell_length_b 9.0536(6) _cell_length_c 17.5745(11) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 3487.6(4) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status 0 0 2 118131.000 121840.000 1128.960 0.296 o 0 0 4 38790.900 38591.600 466.444 1.913 o 0 0 6 235153.000 237943.000 2276.820 0.083 o 0 0 8 94968.800 92652.500 1144.080 0.420 o 0 0 10 82696.000 86874.800 1067.680 0.506 o 0 0 12 8279.370 7205.340 279.875 12.711 o 0 0 14 67283.200 69223.700 1014.370 0.687 o 0 0 16 52816.700 58206.900 840.002 0.989 o 0 0 18 6687.860 7303.750 331.556 12.307 o 0 0 20 3122.610 3195.700 508.034 9.560 o 0 1 2 194388.000 199075.000 1615.900 0.123 o 0 1 4 526749.000 534882.000 3393.410 0.019 o 0 1 6 92898.900 96711.100 784.593 0.466 o 0 1 8 274.121 308.561 57.030 380.849 o 0 1 10 107995.000 108056.000 889.148 0.366 o 0 1 12 115433.000 117334.000 991.752 0.319 o 0 1 14 15597.900 17045.000 298.943 6.340 o 0 1 16 12647.900 12715.600 289.303 8.217 o 0 1 18 22309.600 24480.400 552.578 3.214 o 0 1 20 17317.700 18684.800 546.928 4.063 o 0 2 0 490467.000 498653.000 7840.460 0.016 o 0 2 2 40554.400 39578.800 389.716 1.893 o 0 2 4 1071.550 1796.920 82.049 104.741 o 0 2 6 148334.000 149982.000 1082.080 0.209 o 0 2 8 93042.800 90860.600 746.520 0.485 o 0 2 10 50880.700 53495.800 482.545 1.268 o 0 2 12 3384.010 3121.830 140.080 38.558 o 0 2 14 49006.500 48503.100 622.322 1.287 o 0 2 16 37056.300 39584.900 645.189 1.741 o 0 2 18 1417.230 1609.010 166.192 57.161 o 0 2 20 2345.280 2575.770 290.160 23.805 o 0 2 22 12523.000 13293.500 503.035 5.578 o 0 3 2 80268.200 80026.500 635.846 0.623 o 0 3 4 128149.000 126290.000 947.064 0.276 o 0 3 6 53810.700 57252.300 491.251 1.157 o 0 3 8 1025.280 982.754 72.266 136.726 o 0 3 10 53705.000 55616.900 530.877 1.158 o 0 3 12 39363.000 39425.300 539.887 1.788 o 0 3 14 3602.550 3878.870 239.259 24.346 o 0 3 16 1508.210 1556.170 167.039 56.055 o 0 3 18 22106.000 23149.600 573.231 3.210 o 0 3 20 12662.600 14005.700 505.694 5.455 o 0 3 22 849.868 1263.430 174.857 63.913 o 0 4 0 54885.100 55035.500 792.420 1.007 o 0 4 2 21116.400 21515.500 272.195 4.727 o 0 4 4 8115.380 9793.250 186.960 14.237 o 0 4 6 63632.300 65024.500 572.695 0.894 o 0 4 8 44473.400 46386.500 482.326 1.541 o 0 4 10 7187.220 7699.060 248.332 14.556 o 0 4 12 3632.220 3711.320 205.594 27.903 o 0 4 14 11141.700 11930.600 360.094 7.978 o 0 4 16 12244.800 12861.900 417.067 6.677 o 0 4 18 1067.780 1192.870 171.186 62.837 o 0 4 20 2308.830 2152.740 224.560 33.641 o 0 5 2 2661.510 2942.180 127.593 46.745 o 0 5 4 19632.800 19042.800 285.088 5.201 o 0 5 6 7951.590 8238.610 212.875 14.568 o 0 5 8 3872.130 3646.990 202.683 27.510 o 0 5 10 9360.350 9828.450 288.116 10.722 o 0 5 12 961.569 1085.290 159.868 71.141 o 0 5 14 1008.860 1015.240 171.115 65.165 o 0 5 16 54.844 -31.078 105.048 257.729 o 0 5 18 6296.510 6812.390 356.553 11.932 o 0 5 20 1441.500 1405.700 205.221 45.384 o 0 6 0 332.316 269.855 107.598 180.305 o 0 6 2 101.869 73.081 70.697 462.249 o 0 6 4 8757.350 8977.220 243.286 12.562 o 0 6 6 3980.990 3729.630 214.521 25.867 o 0 6 8 223.437 547.759 142.962 116.092 o 0 6 10 1531.280 1182.900 152.723 63.790 o 0 6 12 173.777 209.485 116.377 181.158 o 0 6 14 313.702 410.467 127.891 136.433 o 0 6 16 274.918 360.837 119.806 155.524 o 0 6 18 342.672 436.418 151.258 103.518 o 0 6 20 912.298 475.258 223.972 47.752 o 0 7 2 9047.270 9531.630 281.610 11.179 o 0 7 4 5391.850 5659.110 255.900 17.847 o 0 7 6 118.654 94.355 113.834 203.277 o 0 7 8 763.307 757.218 138.300 94.794 o 0 7 10 250.338 461.259 129.429 136.543 o 0 7 12 3583.700 3448.830 272.311 21.880 o 0 7 14 1405.030 700.864 192.452 53.068 o 0 7 16 83.296 44.527 113.161 214.940 o 0 7 18 447.924 164.542 171.935 84.892 o 0 8 0 3570.340 3856.090 361.265 15.303 o 0 8 2 6955.970 7385.490 307.187 12.883 o 0 8 4 4.668 230.893 138.844 145.655 o 0 8 6 2416.960 2159.560 176.035 42.215 o 0 8 8 13021.300 12703.200 352.067 7.274 o 0 8 10 3551.970 3621.880 376.920 14.574 o 0 8 12 973.068 1171.130 163.457 68.260 o 0 8 14 7787.140 7520.230 403.500 9.513 o 0 8 16 4190.680 3440.510 263.028 21.422 o 0 9 2 4792.180 4991.760 392.138 12.324 o 0 9 4 11590.500 11315.700 414.834 7.124 o 0 9 6 7480.960 7591.390 310.931 12.251 o 0 9 8 332.524 238.504 131.812 134.670 o 0 9 10 12276.800 12236.000 422.238 6.691 o 0 9 12 7464.210 6608.280 318.791 12.398 o 0 9 14 3313.540 2948.560 367.773 15.656 o 0 10 0 7821.670 8467.880 661.033 5.017 o 0 10 2 10362.000 10410.800 475.954 6.731 o 0 10 4 79.127 51.109 171.888 97.670 o 0 10 6 14039.000 14228.900 697.506 3.703 o 0 10 8 18426.600 18957.800 602.295 3.614 o 0 10 10 3133.200 3061.720 376.934 15.238 o 0 10 12 606.094 390.732 275.868 35.321 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7 1056.580 1176.180 77.679 123.912 o 10 2 8 3599.080 3466.040 133.909 36.987 o 10 2 9 2899.870 2813.510 137.376 43.508 o 10 2 10 1879.230 1624.220 114.728 68.932 o 10 2 11 18026.800 18019.700 309.564 5.524 o 10 2 12 1002.900 811.745 105.326 112.778 o 10 2 13 12865.500 13406.900 294.053 7.924 o 10 2 14 937.565 922.448 110.172 108.955 o 10 2 15 70.303 182.366 82.004 354.285 o 10 2 16 368.071 365.683 79.379 244.572 o 10 2 17 3814.450 3610.720 198.605 28.192 o 10 2 18 15.322 28.733 70.278 569.832 o 10 2 19 2809.840 2969.470 200.790 33.230 o 10 2 20 2.308 -22.830 101.416 290.508 o 10 2 21 3129.770 2814.450 232.287 28.038 o 10 3 1 102451.000 102664.000 623.429 0.420 o 10 3 2 1984.550 2019.700 73.830 76.124 o 10 3 3 4705.200 5052.810 114.490 29.486 o 10 3 4 1275.300 1051.790 71.223 119.820 o 10 3 5 16900.900 16167.700 233.847 6.567 o 10 3 6 1269.360 1325.150 104.738 92.456 o 10 3 7 41492.300 41068.800 439.438 1.777 o 10 3 8 2748.030 2911.360 146.497 42.701 o 10 3 9 38148.300 38480.400 437.830 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10 4 13 26882.300 26639.900 412.096 3.160 o 10 4 14 735.010 751.850 110.165 123.460 o 10 4 15 11.061 106.632 80.422 418.558 o 10 4 16 609.134 462.757 111.644 138.742 o 10 4 17 7838.220 8299.840 308.159 11.795 o 10 4 18 441.222 415.011 91.175 195.406 o 10 4 19 11052.900 11276.200 323.418 8.735 o 10 4 20 0.765 -128.357 163.435 112.095 o 10 5 1 95098.700 94579.900 614.404 0.477 o 10 5 2 45.829 54.350 71.728 505.479 o 10 5 3 6976.310 6859.750 204.112 17.008 o 10 5 4 350.421 178.436 91.717 227.835 o 10 5 5 23090.900 22183.200 338.163 4.095 o 10 5 6 26.046 -39.587 90.071 356.944 o 10 5 7 56926.700 54484.800 568.257 1.089 o 10 5 8 3482.160 3520.390 178.405 31.961 o 10 5 9 39521.700 37083.100 466.192 1.914 o 10 5 10 150.461 181.442 81.797 322.839 o 10 5 11 653.605 545.369 94.732 157.261 o 10 5 12 44.887 152.336 83.612 361.454 o 10 5 13 14279.700 14301.500 324.524 6.914 o 10 5 14 49.159 76.377 95.579 297.445 o 10 5 15 31836.600 31075.600 530.961 2.355 o 10 5 16 896.881 903.664 137.284 89.049 o 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7 3 7861.830 7486.310 265.405 13.409 o 10 7 4 128.464 125.343 83.801 330.205 o 10 7 5 12288.300 12877.400 280.326 8.457 o 10 7 6 365.632 382.905 93.463 203.084 o 10 7 7 53261.200 53584.000 629.219 1.137 o 10 7 8 758.210 670.463 109.900 124.763 o 10 7 9 22880.700 22837.700 418.997 3.765 o 10 7 10 158.688 11.011 88.633 311.533 o 10 7 11 275.160 235.974 96.045 222.618 o 10 7 12 116.546 102.900 91.598 293.946 o 10 7 13 7565.330 7515.380 274.992 13.362 o 10 7 14 118.580 293.170 97.540 242.335 o 10 7 15 18156.200 18450.400 374.438 5.040 o 10 7 16 48.562 294.045 139.310 139.286 o 10 7 17 9634.180 8574.950 1379.340 1.431 o 10 8 0 177.158 242.938 178.984 84.986 o 10 8 1 2645.420 2824.390 195.753 35.162 o 10 8 2 889.654 735.128 132.512 95.633 o 10 8 3 24392.600 24640.600 472.718 3.305 o 10 8 4 48.061 -132.304 116.573 212.376 o 10 8 5 27246.400 27240.600 503.733 2.851 o 10 8 6 8.711 64.829 93.287 327.625 o 10 8 7 2401.260 2122.900 140.895 50.426 o 10 8 8 681.310 631.926 98.704 145.387 o 10 8 9 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13 21385.400 21698.200 404.002 4.094 o 11 5 14 631.133 523.865 111.780 134.924 o 11 5 15 49.309 58.577 86.241 361.822 o 11 5 16 41.761 86.668 97.882 285.500 o 11 5 17 7643.860 8488.870 301.847 12.053 o 11 5 18 218.779 349.406 102.998 201.805 o 11 5 19 14128.600 15223.200 633.735 4.071 o 11 6 1 53889.700 54652.800 632.307 1.113 o 11 6 2 2221.560 2038.010 141.710 52.606 o 11 6 3 11164.200 11026.500 257.003 9.849 o 11 6 4 226.525 151.332 95.527 242.119 o 11 6 5 15486.100 15960.700 305.694 6.472 o 11 6 6 2825.650 2909.080 165.042 38.961 o 11 6 7 63985.100 61041.800 711.872 0.870 o 11 6 8 1837.540 1870.210 137.337 59.767 o 11 6 9 32240.100 31398.200 461.896 2.453 o 11 6 10 58.996 128.496 90.383 315.682 o 11 6 11 1978.500 1868.690 142.722 56.205 o 11 6 12 111.597 67.925 104.726 239.114 o 11 6 13 13396.800 14014.900 334.907 7.134 o 11 6 14 23.657 9.482 93.938 328.137 o 11 6 15 26597.700 27812.000 516.066 2.845 o 11 6 16 1079.860 1058.430 124.062 90.422 o 11 6 17 7875.110 8136.430 344.689 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11 8 7 22010.100 24008.500 468.309 3.599 o 11 8 8 169.426 207.957 96.885 243.093 o 11 8 9 14393.900 15286.100 322.930 6.741 o 11 8 10 373.054 312.598 83.425 236.395 o 11 8 11 282.822 378.727 80.095 260.376 o 11 8 12 939.676 1076.530 119.542 98.086 o 11 8 13 5636.690 6253.250 225.807 18.592 o 11 8 14 77.344 -62.197 104.010 257.201 o 11 8 15 9254.930 9756.440 863.112 3.190 o 11 9 0 5542.310 5897.020 420.958 10.569 o 11 9 1 2057.960 1982.200 168.255 47.648 o 11 9 2 808.152 1036.440 138.189 89.055 o 11 9 3 12957.200 13610.300 378.097 6.835 o 11 9 4 604.682 449.569 114.420 135.566 o 11 9 5 9380.420 9826.270 352.540 9.332 o 11 9 6 1169.670 753.590 159.312 70.636 o 11 9 7 382.569 98.550 106.089 188.321 o 11 9 8 723.694 603.116 115.581 122.108 o 11 9 9 3474.590 3849.710 238.233 24.819 o 11 9 10 1526.080 1244.860 139.180 69.174 o 11 9 11 7855.000 7907.890 235.112 14.167 o 11 9 12 15.571 130.071 105.196 251.098 o 11 9 13 5268.280 5096.730 770.246 4.341 o 11 10 1 3223.220 3448.260 569.221 7.838 o 11 10 2 2806.560 2336.370 206.843 33.798 o 11 10 3 1129.180 1378.090 183.668 55.616 o 11 10 4 1398.730 939.560 137.245 75.764 o 11 10 5 741.069 907.899 124.724 104.656 o 11 10 6 240.548 105.786 133.460 142.881 o 11 10 7 5598.260 5636.320 311.269 14.827 o 11 10 8 9.236 -82.272 156.023 122.539 o 11 10 10 394.524 841.261 415.168 16.528 o 11 11 2 323.968 355.078 300.450 31.304 o 11 11 3 945.777 453.407 240.360 42.433 o 12 0 0 60569.900 60367.300 859.829 0.859 o 12 0 2 54090.200 55270.000 556.966 1.141 o 12 0 4 4699.370 5106.470 165.196 25.809 o 12 0 6 60776.900 60921.500 733.949 0.905 o 12 0 8 75601.900 76176.300 880.215 0.627 o 12 0 10 5448.000 5802.190 259.514 17.464 o 12 0 12 237.823 301.026 137.928 129.091 o 12 0 14 17034.400 16584.700 531.555 4.332 o 12 0 16 25532.700 25848.800 688.277 2.489 o 12 0 18 5021.280 5407.380 366.271 13.051 o 12 0 20 3621.580 3959.420 305.449 18.736 o 12 1 1 442.194 305.202 44.837 355.086 o 12 1 2 16896.500 17284.400 195.403 6.633 o 12 1 3 405.984 304.305 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21467.100 20527.300 308.645 4.599 o 12 2 6 21940.600 22832.200 329.396 4.250 o 12 2 7 468.252 482.563 78.472 216.421 o 12 2 8 54697.100 55530.500 534.758 1.137 o 12 2 9 9452.790 9220.990 232.900 12.124 o 12 2 10 6173.750 6846.200 218.924 17.594 o 12 2 11 4918.310 4922.990 214.505 21.937 o 12 2 12 2414.750 2629.590 169.654 41.837 o 12 2 13 3048.660 3537.270 188.166 32.616 o 12 2 14 20580.100 21214.900 381.443 4.351 o 12 2 15 748.591 759.583 103.115 130.502 o 12 2 16 12499.800 13607.000 328.799 7.591 o 12 2 17 2135.160 2020.970 144.331 52.973 o 12 2 18 2605.530 2910.890 178.237 38.072 o 12 2 19 5787.170 5739.400 293.794 15.368 o 12 2 20 2237.400 2005.690 214.985 36.056 o 12 2 21 714.526 344.152 311.376 28.100 o 12 3 1 29352.300 29395.100 290.540 3.077 o 12 3 2 13702.700 13898.600 196.052 8.535 o 12 3 3 10996.900 11009.500 189.775 11.056 o 12 3 4 34763.300 34449.300 343.049 2.385 o 12 3 5 10287.500 9981.660 204.797 11.727 o 12 3 6 6696.270 6447.370 201.173 17.872 o 12 3 7 37794.100 36236.800 426.319 2.061 o 12 3 8 2137.030 2200.090 138.624 53.458 o 12 3 9 13163.600 13145.900 266.277 8.191 o 12 3 10 19172.100 20133.400 346.543 4.857 o 12 3 11 22.460 31.938 81.323 426.412 o 12 3 12 17102.300 17533.800 343.421 5.562 o 12 3 13 5402.630 5325.940 229.576 19.598 o 12 3 14 2971.540 3122.500 179.347 35.246 o 12 3 15 9837.440 10024.500 266.345 10.812 o 12 3 16 1365.750 1524.480 121.793 77.749 o 12 3 17 5569.420 5703.760 239.958 18.401 o 12 3 18 5430.540 5716.430 308.903 15.072 o 12 3 19 1.065 138.253 108.542 239.002 o 12 3 20 2968.750 2217.870 447.944 12.088 o 12 4 0 18275.900 18413.700 313.059 5.403 o 12 4 1 3382.880 3517.550 121.549 39.746 o 12 4 2 4137.040 4287.890 127.182 32.652 o 12 4 3 39772.200 38597.600 432.027 1.907 o 12 4 4 2123.130 1940.870 135.526 56.035 o 12 4 5 35400.000 34589.800 420.929 2.237 o 12 4 6 4525.550 4493.840 187.387 25.535 o 12 4 7 3337.190 3104.210 166.486 35.212 o 12 4 8 8585.580 8409.590 231.236 13.294 o 12 4 9 19756.600 18890.400 326.195 4.974 o 12 4 10 3093.570 3016.880 163.732 37.208 o 12 4 11 19995.200 19312.700 333.362 4.851 o 12 4 12 302.230 289.340 90.990 228.771 o 12 4 13 8109.420 7924.130 245.539 13.578 o 12 4 14 10031.600 10309.200 276.349 10.391 o 12 4 15 556.783 560.738 102.062 153.574 o 12 4 16 3108.170 3178.190 190.323 32.870 o 12 4 17 3600.450 3579.350 213.618 27.369 o 12 4 18 581.438 448.079 123.625 124.692 o 12 4 19 9144.230 8968.950 417.273 8.327 o 12 4 20 255.465 216.036 204.288 65.622 o 12 5 1 36162.800 35874.400 393.526 2.196 o 12 5 2 6840.600 6588.850 202.498 17.480 o 12 5 3 3681.350 3727.740 175.935 30.949 o 12 5 4 1171.830 1409.220 129.084 79.977 o 12 5 5 7946.590 7669.950 231.141 14.322 o 12 5 6 266.848 144.215 96.727 230.416 o 12 5 7 29319.900 27819.300 400.641 2.921 o 12 5 8 3.988 -51.706 83.706 424.876 o 12 5 9 16058.900 15359.600 326.142 6.222 o 12 5 10 1296.190 1300.380 122.079 82.070 o 12 5 11 1293.040 1034.010 107.532 94.816 o 12 5 12 2852.650 3372.420 192.152 33.349 o 12 5 13 7829.010 8271.660 269.351 12.957 o 12 5 14 140.781 308.409 102.530 218.948 o 12 5 15 13169.000 12914.800 356.556 7.135 o 12 5 16 334.239 84.414 95.295 228.121 o 12 5 17 6913.780 7411.030 321.065 12.440 o 12 5 18 611.465 753.313 203.354 57.477 o 12 5 19 5.587 366.610 208.159 66.038 o 12 6 0 376.063 377.207 246.888 44.670 o 12 6 1 3450.090 3491.620 221.609 27.131 o 12 6 2 157.651 136.613 110.253 205.447 o 12 6 3 32564.100 33056.100 431.391 2.434 o 12 6 4 3804.770 3807.890 185.832 29.221 o 12 6 5 21500.400 21353.000 353.362 4.330 o 12 6 6 18.610 -131.448 97.349 309.551 o 12 6 7 3053.840 2710.890 161.532 38.722 o 12 6 8 126.309 -11.062 84.002 356.222 o 12 6 9 7036.940 7757.410 247.140 14.732 o 12 6 10 41.434 76.368 85.424 367.564 o 12 6 11 18519.100 18406.400 362.580 5.049 o 12 6 12 24.459 -122.834 89.299 363.676 o 12 6 13 10694.500 10532.300 316.258 9.206 o 12 6 14 808.063 1062.630 128.873 95.719 o 12 6 15 25.101 136.770 102.584 259.917 o 12 6 16 57.347 75.971 119.238 196.566 o 12 6 17 3836.350 3957.290 358.452 15.138 o 12 6 18 51.656 344.152 300.450 32.320 o 12 7 1 29062.700 30034.400 517.258 2.588 o 12 7 2 1035.210 840.853 145.942 80.314 o 12 7 3 782.333 993.448 142.302 87.437 o 12 7 4 3115.280 3266.490 216.524 29.240 o 12 7 5 7055.190 7315.420 235.156 15.406 o 12 7 6 680.765 544.435 101.440 144.990 o 12 7 7 17306.300 17801.300 349.438 5.445 o 12 7 8 222.212 229.879 95.505 235.016 o 12 7 9 14165.700 14565.200 320.320 6.952 o 12 7 10 113.015 13.008 90.189 318.194 o 12 7 11 1376.840 1110.290 121.670 82.671 o 12 7 12 49.910 228.044 91.390 296.323 o 12 7 13 4494.730 4675.340 228.087 22.182 o 12 7 14 543.368 396.396 109.973 148.807 o 12 7 15 10333.500 10812.300 350.189 8.704 o 12 7 16 138.224 42.627 480.721 12.865 o 12 8 0 3816.190 3470.430 344.879 16.203 o 12 8 1 4851.280 4924.050 309.909 16.134 o 12 8 2 1608.350 1352.730 160.169 58.538 o 12 8 3 19693.500 20372.500 435.376 4.271 o 12 8 4 7.622 92.093 95.404 309.556 o 12 8 5 8064.270 8321.650 327.539 11.092 o 12 8 6 1889.380 1768.270 182.470 46.395 o 12 8 7 812.918 722.986 128.898 101.713 o 12 8 8 4993.620 4995.030 234.697 20.354 o 12 8 9 1857.880 1849.430 151.220 55.222 o 12 8 10 1564.050 1316.420 121.620 75.681 o 12 8 11 12233.300 12357.600 328.222 7.936 o 12 8 12 601.480 414.834 118.852 130.788 o 12 8 13 5550.520 5748.720 289.799 15.828 o 12 8 14 1144.080 693.059 159.810 71.434 o 12 9 1 8275.380 8437.410 327.000 10.932 o 12 9 2 4694.740 4946.670 285.917 17.686 o 12 9 3 192.321 370.468 111.774 180.932 o 12 9 4 6929.430 6327.770 299.898 13.636 o 12 9 5 1600.950 1095.770 212.053 43.472 o 12 9 6 1779.860 1288.860 195.318 45.873 o 12 9 7 3958.450 3729.840 251.944 22.528 o 12 9 8 535.851 405.703 120.980 132.303 o 12 9 9 4206.700 4263.640 259.076 20.880 o 12 9 10 1573.860 1061.980 153.613 63.701 o 12 9 11 32.060 16.675 177.975 93.285 o 12 9 12 3615.350 2666.490 233.115 26.636 o 12 10 0 11654.600 13054.100 698.726 3.974 o 12 10 1 322.983 250.684 147.892 112.174 o 12 10 2 3709.770 3510.160 273.262 21.479 o 12 10 3 2406.780 2125.100 197.835 38.026 o 12 10 4 929.275 856.788 208.470 51.332 o 12 10 5 1111.280 1221.570 142.435 76.197 o 12 10 6 2513.450 2028.750 198.495 37.561 o 12 10 7 8.569 -25.743 263.583 43.053 o 12 10 8 3900.930 3162.920 655.528 6.054 o 12 11 1 356.136 -595.438 240.360 48.620 o 12 11 2 6646.520 5757.720 480.721 8.501 o 13 0 2 99268.100 98991.300 862.857 0.421 o 13 0 4 157645.000 154499.000 1313.440 0.186 o 13 0 6 44341.400 43712.400 613.754 1.476 o 13 0 8 5811.220 6086.350 261.499 16.657 o 13 0 10 55431.300 54793.200 751.154 1.022 o 13 0 12 59570.800 58602.600 905.271 0.862 o 13 0 14 8613.190 8371.310 391.195 9.216 o 13 0 16 4188.160 4001.390 319.606 16.972 o 13 0 18 25315.800 26707.800 734.251 2.350 o 13 0 20 13430.900 14402.900 587.865 4.554 o 13 1 0 138213.000 135979.000 1096.890 0.238 o 13 1 1 183.395 134.582 43.786 650.213 o 13 1 2 57990.000 56775.500 411.916 1.108 o 13 1 3 2821.660 3219.130 109.437 47.160 o 13 1 4 57.923 -68.497 53.037 872.722 o 13 1 5 4278.430 4078.730 137.355 31.557 o 13 1 6 79921.400 79691.400 588.928 0.634 o 13 1 7 283.108 218.830 80.012 281.906 o 13 1 8 101902.000 98451.100 813.464 0.416 o 13 1 9 580.931 545.545 102.596 151.308 o 13 1 10 25420.600 24908.000 363.358 3.541 o 13 1 11 34.806 48.064 92.386 326.832 o 13 1 12 5245.460 4886.250 214.226 21.285 o 13 1 13 57.653 235.485 88.838 306.537 o 13 1 14 35991.800 35602.900 534.137 2.018 o 13 1 15 960.989 707.595 104.893 117.880 o 13 1 16 27473.400 27664.100 513.921 2.791 o 13 1 17 5.797 232.402 79.875 389.717 o 13 1 18 3472.720 3949.920 219.781 26.540 o 13 1 19 984.672 774.465 113.161 107.529 o 13 1 20 2724.730 2982.590 221.658 30.573 o 13 2 1 601.111 694.135 56.152 222.406 o 13 2 2 69991.600 68663.500 509.283 0.805 o 13 2 3 4921.890 4587.370 143.252 27.536 o 13 2 4 87943.500 82311.500 602.146 0.561 o 13 2 5 378.564 433.635 73.621 252.731 o 13 2 6 28905.600 28037.600 411.575 2.921 o 13 2 7 10738.800 10353.600 213.214 11.093 o 13 2 8 1449.380 1268.200 122.458 78.468 o 13 2 9 2387.560 2267.590 160.092 45.457 o 13 2 10 37272.800 35955.900 485.691 2.018 o 13 2 11 30.869 41.553 97.535 297.576 o 13 2 12 46200.000 44367.800 562.087 1.457 o 13 2 13 38.087 45.289 114.612 217.274 o 13 2 14 8261.160 7967.250 253.195 13.185 o 13 2 15 609.822 551.015 101.496 150.359 o 13 2 16 1216.020 824.188 107.083 101.820 o 13 2 17 1499.510 1557.100 126.875 72.117 o 13 2 18 17238.400 17392.800 400.339 5.144 o 13 2 19 109.915 147.243 154.854 115.436 o 13 2 20 10799.600 10812.700 1819.090 0.846 o 13 3 0 77272.200 76734.400 908.026 0.606 o 13 3 1 1330.220 1466.690 90.741 96.067 o 13 3 2 29369.100 28950.900 316.815 3.046 o 13 3 3 1252.970 1219.320 93.484 101.986 o 13 3 4 124.253 120.562 76.859 379.886 o 13 3 5 16483.400 15786.000 278.662 6.426 o 13 3 6 36593.300 33783.300 412.958 2.204 o 13 3 7 1124.300 842.810 110.972 102.126 o 13 3 8 37383.900 35317.600 436.008 2.092 o 13 3 9 3582.590 3471.290 169.032 32.756 o 13 3 10 9572.880 9039.020 245.488 11.813 o 13 3 11 1952.640 1940.040 148.607 54.337 o 13 3 12 2865.200 2800.940 176.006 37.237 o 13 3 13 195.198 90.190 92.376 269.576 o 13 3 14 15907.100 15532.700 335.521 6.160 o 13 3 15 777.279 794.181 100.207 130.945 o 13 3 16 14058.700 14224.900 323.459 7.009 o 13 3 17 241.655 179.869 78.923 305.886 o 13 3 18 2035.040 1859.650 153.498 52.451 o 13 3 19 2514.330 2165.570 205.675 35.875 o 13 3 20 907.258 1240.040 349.615 21.542 o 13 4 1 4049.880 4325.180 134.544 32.296 o 13 4 2 20120.500 19137.900 281.387 5.108 o 13 4 3 4097.420 4042.740 174.909 28.805 o 13 4 4 33403.000 31865.100 405.063 2.463 o 13 4 5 130.111 107.602 94.540 274.579 o 13 4 6 5715.630 5255.280 206.199 20.432 o 13 4 7 7851.120 7194.060 227.041 14.825 o 13 4 8 2479.750 2456.210 154.692 45.059 o 13 4 9 4893.930 4685.420 199.244 23.356 o 13 4 10 9024.780 8641.750 233.651 12.719 o 13 4 11 182.023 51.056 83.370 326.439 o 13 4 12 10984.300 10188.000 263.045 10.098 o 13 4 13 203.128 300.706 90.885 248.354 o 13 4 14 2831.580 2822.640 174.198 37.667 o 13 4 15 2576.810 2618.280 178.514 39.100 o 13 4 16 1364.620 1067.970 117.504 85.946 o 13 4 17 1015.490 1095.690 126.099 90.449 o 13 4 18 5657.670 5529.150 275.027 16.562 o 13 4 19 0.011 -418.315 176.555 96.083 o 13 5 0 13300.700 12337.100 352.470 7.237 o 13 5 1 1123.770 1144.570 127.129 85.858 o 13 5 2 1076.450 874.465 122.731 94.445 o 13 5 3 5639.650 5629.660 202.917 20.397 o 13 5 4 132.051 138.719 92.367 280.177 o 13 5 5 11836.200 11353.900 261.863 9.310 o 13 5 6 6905.620 6800.030 230.051 16.116 o 13 5 7 73.407 27.830 91.039 324.787 o 13 5 8 5495.190 4971.020 206.027 21.186 o 13 5 9 1454.210 1387.110 120.424 77.956 o 13 5 10 1999.790 1725.430 131.254 60.449 o 13 5 11 3558.430 3485.380 198.457 29.355 o 13 5 12 1693.180 1364.630 125.623 70.719 o 13 5 13 1674.910 1851.150 146.948 58.950 o 13 5 14 1336.850 1482.650 219.975 41.889 o 13 5 15 195.733 333.288 147.364 116.941 o 13 5 16 772.628 733.838 126.064 105.704 o 13 5 17 626.396 767.279 123.282 114.323 o 13 5 18 66.973 -79.480 279.985 37.861 o 13 6 1 10614.400 11098.800 321.117 9.021 o 13 6 2 393.419 281.214 126.846 137.068 o 13 6 3 41.958 188.838 92.303 300.124 o 13 6 4 194.362 251.737 93.334 246.485 o 13 6 5 3658.700 3727.140 181.560 30.412 o 13 6 6 1.559 13.420 81.617 443.738 o 13 6 7 2087.550 2010.710 142.987 53.946 o 13 6 8 10.171 105.671 84.288 385.082 o 13 6 9 3178.050 3193.460 171.939 35.053 o 13 6 10 8.152 -74.008 83.086 428.460 o 13 6 11 60.438 265.510 88.452 302.728 o 13 6 12 13.542 11.441 81.834 433.913 o 13 6 13 599.296 542.211 112.100 136.020 o 13 6 14 1.293 -32.707 93.924 338.983 o 13 6 15 2506.180 2536.660 199.287 36.053 o 13 6 16 2.625 -124.181 102.962 281.778 o 13 6 17 444.467 923.202 355.078 22.034 o 13 7 0 2610.200 2745.230 313.833 20.738 o 13 7 1 2257.510 2215.190 204.047 37.441 o 13 7 2 2118.570 1763.560 166.121 48.652 o 13 7 3 5133.580 5029.630 258.991 18.565 o 13 7 4 921.693 705.700 132.748 94.854 o 13 7 5 851.024 1022.420 145.683 82.822 o 13 7 6 396.110 201.733 113.531 164.145 o 13 7 7 20.966 121.409 83.665 380.430 o 13 7 8 2930.370 2793.320 173.096 37.352 o 13 7 9 325.715 363.834 92.086 214.652 o 13 7 10 117.074 100.408 90.909 297.844 o 13 7 11 2563.370 2468.570 166.705 41.927 o 13 7 12 75.799 66.299 103.378 252.699 o 13 7 13 1269.870 921.979 152.530 70.664 o 13 7 14 672.990 450.253 119.908 124.085 o 13 7 15 239.291 83.082 136.750 137.929 o 13 8 1 3479.820 3289.640 271.612 22.329 o 13 8 2 3172.530 3394.200 226.870 27.589 o 13 8 3 80.438 14.245 90.605 327.496 o 13 8 4 6900.710 6977.640 280.816 14.059 o 13 8 5 944.453 845.987 137.846 88.092 o 13 8 6 3008.040 2866.240 213.280 30.831 o 13 8 7 303.452 391.051 114.770 161.448 o 13 8 8 58.395 208.221 104.269 237.477 o 13 8 9 1321.440 1693.350 137.390 69.604 o 13 8 10 2486.230 2426.560 158.317 44.370 o 13 8 11 390.627 320.363 98.181 192.195 o 13 8 12 4204.060 3504.870 214.829 25.516 o 13 8 13 2026.650 1986.020 184.527 43.886 o 13 9 0 6800.250 6974.050 656.802 5.310 o 13 9 1 1451.680 1531.200 150.828 63.088 o 13 9 2 6616.450 7208.300 388.193 10.609 o 13 9 3 2535.850 2554.720 211.400 33.833 o 13 9 4 322.500 187.361 169.789 89.922 o 13 9 5 33.155 -79.841 94.445 322.953 o 13 9 6 4810.660 4969.510 288.189 17.372 o 13 9 7 217.575 100.991 178.894 85.869 o 13 9 8 9737.990 9743.110 361.158 9.010 o 13 9 9 24.744 -75.091 145.516 139.701 o 13 9 10 1812.710 1891.360 294.272 25.451 o 13 9 11 904.295 941.198 434.287 14.704 o 13 9 12 20.487 431.556 327.764 27.237 o 13 10 1 740.744 1105.480 155.131 78.340 o 13 10 2 6389.740 6395.080 293.863 14.364 o 13 10 3 127.271 -36.438 120.555 188.425 o 13 10 4 10274.100 11177.600 409.061 7.661 o 13 10 5 204.154 322.623 234.898 50.673 o 13 10 6 4300.500 4394.310 455.424 10.477 o 13 10 7 88.336 366.003 294.988 33.305 o 13 10 8 272.190 852.187 360.540 21.775 o 14 0 0 190986.000 192343.000 2075.650 0.119 o 14 0 2 49843.900 50232.300 552.005 1.292 o 14 0 4 3471.300 3647.990 175.874 32.033 o 14 0 6 83286.300 82735.400 946.785 0.537 o 14 0 8 67779.200 69067.100 858.756 0.732 o 14 0 10 35353.900 35390.800 594.593 1.961 o 14 0 12 3646.600 3331.090 257.295 23.220 o 14 0 14 38133.100 39576.200 877.193 1.418 o 14 0 16 29368.400 30177.800 771.391 2.002 o 14 0 18 2613.510 2890.340 260.482 26.107 o 14 0 20 2931.150 2101.780 636.409 6.642 o 14 1 1 817.476 1021.630 68.421 155.680 o 14 1 2 86106.700 86314.000 615.731 0.558 o 14 1 3 201.753 234.037 54.273 470.213 o 14 1 4 100105.000 100020.000 716.626 0.429 o 14 1 5 1082.030 1037.840 89.393 116.855 o 14 1 6 38507.600 39348.200 419.810 1.960 o 14 1 7 5.823 -48.346 77.433 494.395 o 14 1 8 772.289 756.892 111.327 119.990 o 14 1 9 1368.590 1388.310 128.688 75.836 o 14 1 10 45221.000 45631.300 550.178 1.477 o 14 1 11 624.708 614.070 110.203 134.451 o 14 1 12 63319.100 63557.100 730.525 0.856 o 14 1 13 320.885 330.502 100.586 195.030 o 14 1 14 6700.930 6807.570 263.181 15.039 o 14 1 15 28.806 77.601 84.628 379.875 o 14 1 16 8019.670 7983.480 277.041 12.686 o 14 1 17 75.534 304.395 110.721 203.736 o 14 1 18 17788.700 18198.000 419.887 4.836 o 14 1 19 2.668 71.468 83.438 406.269 o 14 1 20 11215.300 10639.400 558.660 5.470 o 14 2 0 146723.000 147748.000 1201.180 0.209 o 14 2 1 432.484 445.839 61.372 275.939 o 14 2 2 45013.500 45906.800 390.093 1.598 o 14 2 3 5024.670 5560.160 155.998 24.797 o 14 2 4 1472.270 1557.210 103.565 83.563 o 14 2 5 121.634 166.205 69.508 426.313 o 14 2 6 45355.900 44235.500 510.289 1.526 o 14 2 7 37.026 200.916 78.072 395.825 o 14 2 8 46659.100 46540.000 555.189 1.419 o 14 2 9 537.519 451.777 118.089 134.802 o 14 2 10 18674.100 19018.000 358.220 4.987 o 14 2 11 102.037 113.455 91.582 296.922 o 14 2 12 4293.210 4328.820 210.675 24.488 o 14 2 13 1803.760 1624.370 143.983 59.749 o 14 2 14 24463.900 25613.000 432.149 3.387 o 14 2 15 49.371 178.625 80.434 376.556 o 14 2 16 22306.400 23298.700 443.907 3.705 o 14 2 17 32.366 -75.007 80.950 434.160 o 14 2 18 2618.450 2836.280 182.844 37.424 o 14 2 19 31.833 56.781 117.024 208.889 o 14 2 20 2683.710 2299.810 338.690 18.861 o 14 3 1 2550.910 2683.030 133.111 47.897 o 14 3 2 27900.800 28180.800 320.908 3.214 o 14 3 3 453.497 530.399 81.882 206.749 o 14 3 4 52189.200 51405.100 491.422 1.257 o 14 3 5 93.088 149.778 90.647 299.034 o 14 3 6 27331.800 26359.100 370.996 3.240 o 14 3 7 219.939 258.054 93.440 239.956 o 14 3 8 1962.590 1951.750 137.955 57.315 o 14 3 9 838.830 599.247 108.773 123.449 o 14 3 10 19688.200 19561.300 366.365 4.708 o 14 3 11 358.239 338.729 103.789 181.925 o 14 3 12 27198.000 26659.900 440.396 3.053 o 14 3 13 947.996 849.358 107.461 112.577 o 14 3 14 3290.530 3143.760 185.900 32.712 o 14 3 15 553.140 501.017 90.611 176.943 o 14 3 16 1253.160 1267.250 111.636 89.759 o 14 3 17 18.652 254.030 118.136 193.040 o 14 3 18 11095.700 11169.500 326.589 8.688 o 14 3 19 182.768 -10.925 267.674 40.690 o 14 4 0 14889.800 14882.000 333.139 6.554 o 14 4 1 1130.550 927.963 97.880 110.327 o 14 4 2 14565.300 15135.700 257.291 7.338 o 14 4 3 3480.880 3570.050 168.420 33.076 o 14 4 4 2640.940 2837.150 160.634 41.205 o 14 4 5 86.713 190.633 98.062 258.956 o 14 4 6 13838.100 13486.900 281.093 7.677 o 14 4 7 199.503 34.327 88.461 295.141 o 14 4 8 20721.800 19938.700 369.236 4.489 o 14 4 9 14.866 138.925 87.707 348.506 o 14 4 10 4775.020 4710.060 211.351 22.735 o 14 4 11 1680.100 1625.870 143.313 61.770 o 14 4 12 733.479 792.680 114.799 117.397 o 14 4 13 967.268 918.524 129.961 92.003 o 14 4 14 5204.200 4918.770 228.382 20.427 o 14 4 15 539.264 622.397 103.602 150.008 o 14 4 16 7371.120 7553.510 275.014 13.526 o 14 4 17 85.225 119.314 97.816 269.370 o 14 4 18 186.583 115.065 147.345 123.108 o 14 4 19 56.634 0.000 273.137 39.823 o 14 5 1 3290.780 3317.260 193.168 31.387 o 14 5 2 161.245 162.013 97.153 248.826 o 14 5 3 16.977 75.221 97.193 298.619 o 14 5 4 5627.510 5925.330 211.745 19.647 o 14 5 5 749.005 682.314 111.680 122.931 o 14 5 6 10374.100 10713.900 257.803 10.408 o 14 5 7 902.735 790.384 106.987 116.711 o 14 5 8 39.981 51.396 81.098 411.481 o 14 5 9 607.311 608.716 98.259 153.091 o 14 5 10 2732.370 2873.660 160.244 40.514 o 14 5 11 199.326 348.206 92.520 238.166 o 14 5 12 1831.460 1707.440 135.193 61.765 o 14 5 13 28.721 -37.259 108.624 247.405 o 14 5 14 13.026 208.916 91.792 309.324 o 14 5 15 732.010 807.455 127.217 104.782 o 14 5 16 15.397 100.097 110.865 230.560 o 14 5 17 609.617 548.846 164.402 81.762 o 14 5 18 2083.800 3037.280 557.199 8.516 o 14 6 0 2.695 18.856 193.966 79.335 o 14 6 1 17.781 156.095 135.334 154.864 o 14 6 2 27.715 50.773 116.571 211.573 o 14 6 3 547.422 441.793 110.442 145.924 o 14 6 4 531.466 314.892 99.821 171.942 o 14 6 5 1789.330 1662.560 133.727 63.275 o 14 6 6 529.661 604.031 99.434 158.364 o 14 6 7 701.152 653.755 102.258 138.298 o 14 6 8 17.105 103.055 93.472 316.255 o 14 6 9 602.969 669.184 101.412 146.240 o 14 6 10 9.250 108.213 82.830 397.335 o 14 6 11 1179.160 829.460 112.524 99.105 o 14 6 12 13.499 -10.348 86.040 396.856 o 14 6 13 688.602 751.007 128.163 106.864 o 14 6 14 428.135 363.474 114.134 152.686 o 14 6 15 4.641 96.638 131.011 168.929 o 14 6 16 96.173 324.301 218.072 59.512 o 14 7 1 457.231 448.210 139.343 111.805 o 14 7 2 3903.590 3849.610 250.829 22.612 o 14 7 3 702.900 666.495 125.902 110.351 o 14 7 4 1336.510 1387.110 149.624 66.641 o 14 7 5 429.183 320.046 107.806 166.528 o 14 7 6 200.770 205.420 112.223 188.929 o 14 7 7 2255.160 2071.670 137.870 53.039 o 14 7 8 125.452 98.781 86.451 320.452 o 14 7 9 31.516 142.455 85.083 359.212 o 14 7 10 1469.500 866.860 148.042 69.641 o 14 7 11 49.544 209.099 91.516 298.767 o 14 7 12 2336.600 2055.580 161.803 46.413 o 14 7 13 83.548 291.438 108.259 211.245 o 14 7 14 473.591 457.697 137.820 112.606 o 14 7 15 246.046 294.988 338.690 25.180 o 14 8 0 3783.260 4015.800 342.954 16.045 o 14 8 1 3.959 -79.715 150.466 132.044 o 14 8 2 3849.480 3717.440 238.206 24.019 o 14 8 3 617.246 397.480 114.440 136.456 o 14 8 4 17.894 5.649 97.863 305.668 o 14 8 5 1017.980 537.715 170.511 69.386 o 14 8 6 4385.730 4817.190 267.966 19.413 o 14 8 7 134.063 267.883 98.849 236.824 o 14 8 8 9465.760 9797.920 377.328 8.803 o 14 8 9 1621.160 1636.140 146.679 61.334 o 14 8 10 1944.440 1472.460 164.411 52.369 o 14 8 11 281.364 172.477 104.622 201.035 o 14 8 12 83.082 176.041 115.216 198.255 o 14 8 13 10.091 -40.920 149.694 133.020 o 14 9 1 41.321 187.230 99.567 263.704 o 14 9 2 5879.930 6230.820 290.510 15.137 o 14 9 3 710.109 819.126 136.872 96.757 o 14 9 4 14039.600 14560.500 515.567 5.064 o 14 9 5 18.805 168.775 105.156 246.275 o 14 9 6 3302.330 2913.510 224.560 28.227 o 14 9 7 1181.360 1228.140 249.834 36.403 o 14 9 8 244.579 260.832 125.284 151.813 o 14 9 9 394.772 346.262 146.094 109.015 o 14 9 10 5368.110 3596.420 611.826 6.484 o 14 10 0 10453.600 11622.600 684.318 4.285 o 14 10 1 4.077 385.685 197.968 72.518 o 14 10 2 6139.630 5441.950 568.858 6.883 o 14 10 3 89.696 180.270 163.882 104.055 o 14 10 4 48.837 -117.934 379.660 20.704 o 14 10 5 667.213 420.631 355.078 22.086 o 14 10 7 5.176 311.376 322.301 28.362 o 15 0 2 73401.700 72685.400 736.589 0.694 o 15 0 4 68592.200 67135.000 822.624 0.745 o 15 0 6 14130.600 13394.200 357.380 6.751 o 15 0 8 528.534 465.389 137.599 110.183 o 15 0 10 18710.400 18091.900 482.644 4.306 o 15 0 12 53274.300 52976.700 1019.910 0.917 o 15 0 14 4707.920 5106.060 361.436 13.644 o 15 0 16 5511.560 5430.630 375.512 12.304 o 15 0 18 9867.420 10093.900 432.515 7.597 o 15 1 0 95348.000 92451.000 849.464 0.457 o 15 1 1 1408.470 1524.470 89.436 93.064 o 15 1 2 27594.700 26339.500 286.490 3.420 o 15 1 3 2914.520 2995.130 129.350 44.031 o 15 1 4 4412.190 4546.390 153.525 28.642 o 15 1 5 556.310 617.476 84.774 180.638 o 15 1 6 31424.400 30701.400 375.050 2.693 o 15 1 7 376.818 409.895 91.000 205.664 o 15 1 8 49839.500 49122.400 533.624 1.317 o 15 1 9 550.479 337.947 104.533 160.016 o 15 1 10 19494.300 19243.100 352.625 4.846 o 15 1 11 1524.160 1324.350 132.683 71.361 o 15 1 12 3631.610 3425.750 185.851 30.641 o 15 1 13 271.454 254.619 92.334 233.702 o 15 1 14 21993.700 21949.000 421.658 3.919 o 15 1 15 0.757 -68.030 80.841 457.732 o 15 1 16 14801.900 15482.500 383.759 6.019 o 15 1 17 330.059 226.979 83.323 255.572 o 15 1 18 832.246 791.819 105.817 121.600 o 15 1 19 704.489 646.460 125.685 110.957 o 15 2 1 8728.390 8902.810 171.657 14.425 o 15 2 2 48213.600 47123.300 430.375 1.452 o 15 2 3 2568.770 2728.500 127.407 48.663 o 15 2 4 48846.300 47010.800 436.968 1.431 o 15 2 5 2941.940 2859.330 130.978 44.086 o 15 2 6 9246.550 8916.660 207.833 13.022 o 15 2 7 8911.820 8719.530 255.372 12.231 o 15 2 8 1931.660 1865.520 156.005 52.842 o 15 2 9 2790.670 3263.180 186.325 34.772 o 15 2 10 21120.100 20040.500 366.435 4.431 o 15 2 11 258.369 183.201 95.207 233.517 o 15 2 12 29233.300 28463.200 447.173 2.795 o 15 2 13 885.374 892.474 109.390 112.763 o 15 2 14 3479.570 3671.150 189.729 30.308 o 15 2 15 2788.180 3142.610 189.241 34.648 o 15 2 16 3162.940 2641.630 168.973 37.093 o 15 2 17 929.364 938.553 115.507 104.390 o 15 2 18 6897.200 7084.180 262.868 14.679 o 15 2 19 26.373 226.960 314.874 29.760 o 15 3 0 31118.900 30457.800 486.953 2.505 o 15 3 1 1384.210 1243.770 107.229 88.671 o 15 3 2 16540.200 15992.600 263.093 6.496 o 15 3 3 12610.300 12681.400 238.716 8.894 o 15 3 4 8.154 89.361 82.217 408.929 o 15 3 5 16415.400 16326.100 297.026 6.227 o 15 3 6 22864.700 21179.600 338.535 4.199 o 15 3 7 3350.030 3420.490 171.908 33.620 o 15 3 8 18696.700 17444.000 347.877 5.200 o 15 3 9 2589.410 2478.740 167.392 41.571 o 15 3 10 2919.140 2737.130 175.667 37.165 o 15 3 11 9330.950 9941.420 272.703 11.046 o 15 3 12 3198.150 3098.840 184.675 33.412 o 15 3 13 5742.650 6076.600 256.159 17.020 o 15 3 14 9888.510 9576.430 273.504 10.776 o 15 3 15 87.802 46.524 92.144 309.455 o 15 3 16 8855.290 8846.930 271.063 11.826 o 15 3 17 2437.710 2359.670 164.175 43.796 o 15 3 18 920.200 1053.470 110.062 106.935 o 15 3 19 2382.550 2452.770 305.913 22.200 o 15 4 1 16649.800 16667.800 292.736 6.149 o 15 4 2 4422.940 4144.810 196.318 25.605 o 15 4 3 3766.960 3790.550 177.917 30.251 o 15 4 4 9566.200 9127.750 239.529 11.919 o 15 4 5 2210.190 2172.100 148.607 50.245 o 15 4 6 4824.380 4510.830 197.091 23.918 o 15 4 7 16508.300 15955.400 303.668 6.201 o 15 4 8 3072.900 2769.690 159.624 38.723 o 15 4 9 13003.100 12654.500 289.850 8.073 o 15 4 10 7958.020 7673.790 262.101 13.335 o 15 4 11 519.646 338.308 99.850 171.897 o 15 4 12 2699.720 2282.880 164.562 42.030 o 15 4 13 3699.590 3455.990 200.133 28.705 o 15 4 14 1106.340 841.689 129.103 89.485 o 15 4 15 6558.690 6118.620 247.644 16.282 o 15 4 16 157.308 267.419 96.331 241.465 o 15 4 17 2381.620 2097.900 158.846 46.517 o 15 4 18 4191.210 3442.130 438.306 11.399 o 15 5 0 1281.660 1563.840 271.739 30.946 o 15 5 1 5431.670 5508.910 227.136 19.521 o 15 5 2 1257.510 978.613 123.303 86.800 o 15 5 3 21549.900 21225.900 368.038 4.266 o 15 5 4 152.035 185.351 100.672 234.735 o 15 5 5 11745.400 11440.000 262.957 9.319 o 15 5 6 4468.760 4147.490 189.220 26.074 o 15 5 7 570.327 406.011 90.511 180.701 o 15 5 8 3024.890 2472.130 153.038 41.132 o 15 5 9 4351.620 4253.790 192.625 25.975 o 15 5 10 42.221 185.091 91.593 304.640 o 15 5 11 10081.700 9445.000 267.476 10.818 o 15 5 12 508.496 553.213 105.138 153.075 o 15 5 13 4239.590 3724.120 214.857 25.101 o 15 5 14 358.596 466.711 118.514 146.538 o 15 5 15 36.808 117.914 95.208 296.877 o 15 5 16 959.593 958.887 137.863 86.037 o 15 5 17 2103.040 1771.320 271.970 27.785 o 15 6 1 15859.800 15628.700 417.021 5.470 o 15 6 2 548.301 379.481 120.559 132.943 o 15 6 3 2332.750 2556.990 193.091 38.086 o 15 6 4 43.633 63.471 100.064 276.852 o 15 6 5 5129.160 5082.320 223.258 20.741 o 15 6 6 801.583 608.092 107.130 127.230 o 15 6 7 13745.200 13373.500 296.783 7.558 o 15 6 8 2756.250 2676.500 154.464 42.079 o 15 6 9 6513.070 5850.800 228.178 17.410 o 15 6 10 38.267 128.717 80.169 398.033 o 15 6 11 105.570 170.381 94.144 274.603 o 15 6 12 653.485 1027.140 159.694 78.299 o 15 6 13 2739.310 2479.190 178.404 38.541 o 15 6 14 245.231 261.820 116.625 169.728 o 15 6 15 7134.330 6980.840 330.894 12.113 o 15 7 0 7402.930 7944.330 480.289 7.882 o 15 7 1 2797.170 2892.480 220.036 30.690 o 15 7 2 172.684 520.990 123.391 150.590 o 15 7 3 13975.200 14673.000 404.171 6.127 o 15 7 4 1.222 1.135 95.216 329.665 o 15 7 5 8903.760 8782.840 350.817 9.881 o 15 7 6 769.854 860.798 123.764 105.318 o 15 7 7 389.703 320.486 87.064 221.614 o 15 7 8 616.557 666.802 97.150 151.484 o 15 7 9 2524.980 2077.030 142.383 49.062 o 15 7 10 1502.240 1393.810 122.329 75.865 o 15 7 11 6893.010 6706.480 284.461 14.066 o 15 7 12 78.019 138.638 106.910 230.268 o 15 7 13 3766.340 3171.010 215.146 27.330 o 15 7 14 764.000 729.262 205.004 55.110 o 15 8 1 7502.540 7377.380 326.320 11.840 o 15 8 2 3244.950 3107.370 222.645 28.321 o 15 8 3 503.758 227.865 112.121 155.622 o 15 8 4 6221.200 5739.650 297.474 14.728 o 15 8 5 1165.240 1330.160 137.448 76.503 o 15 8 6 1307.950 1380.060 144.229 69.673 o 15 8 7 5941.560 5810.790 291.485 15.259 o 15 8 8 188.229 127.768 112.981 193.615 o 15 8 9 5478.070 4943.800 282.719 16.787 o 15 8 10 3356.610 2836.390 190.417 32.506 o 15 8 11 14.349 26.152 132.142 168.695 o 15 8 12 2661.620 2463.990 273.602 25.024 o 15 8 13 1794.930 1578.730 491.646 11.063 o 15 9 0 6353.310 6220.870 395.070 10.835 o 15 9 1 575.302 500.524 103.793 151.794 o 15 9 2 3524.580 3601.450 240.915 24.753 o 15 9 3 4150.730 3707.060 242.535 22.918 o 15 9 4 101.408 108.448 108.822 221.717 o 15 9 5 2380.290 1836.630 178.387 43.172 o 15 9 6 7219.910 7734.840 356.026 11.027 o 15 9 7 79.763 77.564 113.144 212.873 o 15 9 8 6978.440 7146.020 541.115 6.974 o 15 9 9 630.361 156.331 483.452 12.407 o 15 10 1 1623.150 1536.100 235.374 36.456 o 15 10 2 2114.860 2112.330 249.377 30.499 o 15 10 3 248.409 -72.626 174.827 90.134 o 15 10 4 8698.770 9499.700 786.634 3.737 o 16 0 0 27982.400 28424.700 650.494 2.381 o 16 0 2 7853.330 7751.960 242.391 14.020 o 16 0 4 1866.440 1782.190 176.141 48.232 o 16 0 6 16368.500 16617.900 403.258 5.373 o 16 0 8 13988.000 15148.900 394.657 6.160 o 16 0 10 12318.800 12950.700 415.579 6.663 o 16 0 12 1371.280 1174.090 205.227 46.910 o 16 0 14 9661.800 10355.900 436.696 7.551 o 16 0 16 6351.900 5956.290 398.311 10.812 o 16 0 18 185.307 7.089 118.288 187.014 o 16 1 1 2403.440 2822.150 117.991 51.842 o 16 1 2 21609.500 22381.800 299.378 4.457 o 16 1 3 1843.480 1841.840 108.890 69.637 o 16 1 4 13908.600 14009.500 241.582 7.966 o 16 1 5 953.009 1127.420 112.501 102.080 o 16 1 6 4314.920 4528.800 179.521 26.792 o 16 1 7 6185.830 6211.290 215.516 18.235 o 16 1 8 19.281 17.846 87.814 373.797 o 16 1 9 4743.660 4594.630 210.053 23.044 o 16 1 10 9504.990 9481.200 259.844 11.372 o 16 1 11 36.331 59.390 84.013 385.770 o 16 1 12 13514.900 14038.800 334.575 7.095 o 16 1 13 747.237 658.963 117.090 117.677 o 16 1 14 3520.000 3307.850 205.833 28.976 o 16 1 15 2271.450 2056.870 158.393 47.801 o 16 1 16 2924.630 3069.410 241.511 27.175 o 16 1 17 947.830 1210.610 122.781 93.096 o 16 1 18 3061.320 3042.190 191.165 33.285 o 16 1 19 0.448 -49.165 245.823 49.560 o 16 2 0 10394.400 10295.800 279.432 10.115 o 16 2 1 1482.310 1737.710 115.692 75.498 o 16 2 2 7735.670 8191.860 183.909 15.737 o 16 2 3 8791.060 9366.500 196.314 13.519 o 16 2 4 26.250 120.800 71.632 494.431 o 16 2 5 22498.800 23200.800 322.351 4.167 o 16 2 6 8022.940 8336.130 231.568 13.878 o 16 2 7 345.785 239.147 101.288 196.108 o 16 2 8 8772.410 8852.370 275.141 11.784 o 16 2 9 8382.410 8282.750 255.215 12.873 o 16 2 10 5161.420 4957.080 221.091 20.942 o 16 2 11 8642.740 8329.410 253.168 12.681 o 16 2 12 973.364 983.104 125.655 93.928 o 16 2 13 2569.780 2186.810 152.411 45.921 o 16 2 14 6445.960 6437.990 264.769 15.485 o 16 2 15 618.419 560.932 126.465 116.262 o 16 2 16 6124.650 6598.540 327.732 13.185 o 16 2 17 2196.000 1423.180 136.788 58.081 o 16 2 18 258.906 298.858 98.440 212.652 o 16 2 19 6707.720 5659.390 464.332 8.887 o 16 3 1 11849.400 11788.600 233.978 9.597 o 16 3 2 2270.190 2322.600 143.131 50.210 o 16 3 3 9541.610 9762.840 238.044 11.722 o 16 3 4 4817.980 5085.130 192.382 23.535 o 16 3 5 5947.160 6155.150 207.887 19.063 o 16 3 6 5285.010 5155.240 200.293 21.802 o 16 3 7 29652.500 29359.900 446.200 2.731 o 16 3 8 190.637 181.389 100.377 228.717 o 16 3 9 12708.100 12088.800 294.993 8.249 o 16 3 10 6986.220 7234.760 265.359 14.409 o 16 3 11 16.649 218.748 91.991 305.284 o 16 3 12 6984.740 7270.560 262.620 14.493 o 16 3 13 3449.920 2854.780 178.065 33.692 o 16 3 14 821.898 748.720 112.589 116.303 o 16 3 15 14288.300 13884.800 329.065 6.930 o 16 3 16 534.002 524.942 118.651 131.851 o 16 3 17 5952.140 5843.200 261.088 16.651 o 16 3 18 1018.510 824.873 234.898 42.249 o 16 4 0 4234.320 4724.920 317.514 16.583 o 16 4 1 3847.900 3682.550 174.214 30.544 o 16 4 2 2101.990 2222.200 155.249 49.405 o 16 4 3 26770.700 26351.700 404.911 3.204 o 16 4 4 453.693 182.627 96.244 197.777 o 16 4 5 34850.800 33504.200 441.029 2.269 o 16 4 6 4097.870 4093.100 186.701 27.583 o 16 4 7 2369.140 2068.960 141.290 50.946 o 16 4 8 2789.380 2870.040 180.425 36.754 o 16 4 9 13416.400 12628.800 307.426 7.697 o 16 4 10 50.492 138.805 93.344 299.632 o 16 4 11 24468.800 23324.000 424.747 3.533 o 16 4 12 534.605 582.483 101.333 155.754 o 16 4 13 8393.170 8744.410 271.615 12.215 o 16 4 14 139.043 128.310 87.090 306.801 o 16 4 15 389.955 305.436 98.528 192.447 o 16 4 16 2154.320 1895.260 161.312 48.935 o 16 4 17 4975.450 5124.140 337.407 14.500 o 16 4 18 492.236 245.823 305.913 29.882 o 16 5 1 46388.800 46432.700 711.787 1.305 o 16 5 2 63.253 88.540 94.796 295.476 o 16 5 3 3746.900 3836.840 194.426 28.472 o 16 5 4 2135.290 2256.850 155.177 48.930 o 16 5 5 11405.200 11610.100 369.101 7.803 o 16 5 6 657.369 775.229 106.023 132.353 o 16 5 7 34121.800 33180.600 488.781 2.243 o 16 5 8 1360.440 1207.820 115.026 85.503 o 16 5 9 20615.500 20213.600 534.059 3.667 o 16 5 10 603.335 729.440 110.646 131.498 o 16 5 11 369.959 308.108 94.323 205.866 o 16 5 12 28.087 134.696 89.646 330.696 o 16 5 13 7109.050 6933.960 262.415 14.548 o 16 5 14 86.893 181.425 98.870 256.479 o 16 5 15 15026.400 14692.900 371.148 6.181 o 16 5 16 37.158 -31.828 154.070 124.099 o 16 5 17 7119.790 6659.070 841.261 3.554 o 16 6 0 1053.110 909.163 219.556 46.230 o 16 6 1 5580.550 5997.750 311.226 14.659 o 16 6 2 282.450 217.958 138.800 127.579 o 16 6 3 37307.100 38471.800 605.034 1.805 o 16 6 4 39.298 232.814 97.352 268.752 o 16 6 5 30718.700 31145.900 470.740 2.542 o 16 6 6 74.954 -1.867 101.768 268.428 o 16 6 7 1412.340 1320.750 124.395 77.748 o 16 6 8 129.117 227.430 83.734 311.478 o 16 6 9 7991.150 7344.750 235.243 14.318 o 16 6 10 65.827 123.201 87.420 332.571 o 16 6 11 22783.400 22431.800 450.143 3.675 o 16 6 12 60.888 24.119 90.892 331.272 o 16 6 13 11211.300 11365.700 320.521 8.690 o 16 6 14 357.970 397.210 120.080 146.630 o 16 6 15 2.307 -21.851 208.588 68.799 o 16 7 1 30077.400 30210.600 592.749 2.350 o 16 7 2 1680.800 1463.600 163.079 55.878 o 16 7 3 585.598 706.850 143.240 97.465 o 16 7 4 893.984 636.333 139.634 91.448 o 16 7 5 8052.110 8351.460 300.807 11.826 o 16 7 6 174.687 130.039 104.765 221.097 o 16 7 7 14858.000 14537.500 341.030 6.537 o 16 7 8 32.241 184.367 81.270 377.401 o 16 7 9 13333.400 12986.900 429.420 6.229 o 16 7 10 196.606 506.847 118.219 159.123 o 16 7 11 579.471 606.975 111.256 136.327 o 16 7 12 698.056 336.795 111.639 136.932 o 16 7 13 4823.670 4806.130 388.413 12.518 o 16 7 14 19.883 469.795 333.227 26.325 o 16 8 0 2680.330 2183.640 275.179 25.157 o 16 8 1 5503.490 5405.300 280.912 16.545 o 16 8 2 826.049 468.712 109.668 126.979 o 16 8 3 16462.000 16022.900 424.216 5.250 o 16 8 4 49.522 -83.131 120.528 198.928 o 16 8 5 7177.490 7191.040 318.210 12.413 o 16 8 6 1660.110 1428.230 149.211 61.349 o 16 8 7 547.503 597.496 156.855 88.638 o 16 8 8 1435.630 1632.900 153.607 61.468 o 16 8 9 1937.530 1900.400 201.240 40.963 o 16 8 10 309.266 298.670 130.620 136.130 o 16 8 11 11622.600 10953.900 889.403 2.889 o 16 8 12 9.257 369.588 183.671 83.628 o 16 9 1 8548.730 8351.570 306.990 11.302 o 16 9 2 899.183 916.881 198.987 54.972 o 16 9 3 311.846 390.006 113.357 163.534 o 16 9 4 2719.700 2568.270 203.729 34.152 o 16 9 5 2612.620 2621.640 189.728 36.888 o 16 9 6 1193.200 1052.570 159.351 67.483 o 16 9 7 4582.630 3484.420 977.830 2.901 o 16 9 8 2.871 87.404 322.301 28.695 o 16 9 9 4225.970 4654.250 677.379 5.567 o 16 10 1 619.900 -27.314 229.435 50.474 o 16 10 2 1264.820 783.367 220.053 44.907 o 16 10 3 3338.170 3157.460 344.152 17.004 o 17 0 2 46.198 51.888 94.782 307.039 o 17 0 4 82.894 -117.566 104.077 255.589 o 17 0 6 1481.070 1170.100 164.464 59.877 o 17 0 8 126.936 -58.391 121.597 185.522 o 17 0 10 654.113 534.470 148.238 93.623 o 17 0 12 468.737 331.005 135.342 118.978 o 17 0 14 141.432 292.138 117.217 178.002 o 17 0 16 100.855 135.071 184.860 83.251 o 17 0 18 162.254 181.831 311.376 30.050 o 17 1 0 230.020 301.253 94.513 229.923 o 17 1 1 75.729 175.858 63.395 518.956 o 17 1 2 1843.020 1738.310 111.281 69.787 o 17 1 3 2395.090 2442.760 131.647 50.979 o 17 1 4 228.490 171.185 84.534 284.720 o 17 1 5 6519.070 6830.290 203.893 17.733 o 17 1 6 39.615 43.911 83.826 389.741 o 17 1 7 714.164 615.981 103.567 137.007 o 17 1 8 1292.820 923.197 114.481 92.171 o 17 1 9 2379.640 2374.020 163.066 44.436 o 17 1 10 139.351 141.956 87.749 300.887 o 17 1 11 2767.240 2594.290 178.977 37.924 o 17 1 12 115.173 184.251 88.769 296.494 o 17 1 13 562.210 431.335 94.370 172.744 o 17 1 14 48.313 -7.130 85.843 379.834 o 17 1 15 109.203 40.389 113.301 210.597 o 17 1 16 264.522 466.163 88.569 226.752 o 17 1 17 392.703 437.239 143.003 110.704 o 17 1 18 7.881 -117.449 169.434 104.024 o 17 2 1 15355.600 15453.900 264.981 6.940 o 17 2 2 37.950 113.175 77.148 430.154 o 17 2 3 4706.640 4888.760 163.275 26.268 o 17 2 4 843.418 567.872 90.332 146.343 o 17 2 5 4189.890 4501.110 187.985 26.498 o 17 2 6 562.840 541.962 108.895 143.255 o 17 2 7 29743.500 29407.000 440.104 2.736 o 17 2 8 167.809 112.997 90.802 281.235 o 17 2 9 7582.880 7621.420 245.108 14.283 o 17 2 10 4.870 58.407 82.128 421.316 o 17 2 11 23.603 31.738 80.239 436.610 o 17 2 12 133.360 50.515 78.743 379.179 o 17 2 13 1253.090 1012.350 116.964 90.418 o 17 2 14 82.626 193.127 90.206 297.823 o 17 2 15 4974.390 5138.720 244.010 19.661 o 17 2 16 11.125 219.979 103.633 248.852 o 17 2 17 5306.490 5406.860 255.459 18.197 o 17 2 18 1.687 112.496 175.468 95.360 o 17 3 0 913.843 817.883 159.860 74.782 o 17 3 1 3418.050 3403.100 150.411 36.120 o 17 3 2 2810.470 2731.910 149.015 42.457 o 17 3 3 39970.400 39881.900 468.929 1.833 o 17 3 4 374.652 385.794 103.027 178.903 o 17 3 5 49537.700 48244.500 532.766 1.336 o 17 3 6 598.918 623.640 110.585 135.352 o 17 3 7 665.684 450.327 105.978 143.234 o 17 3 8 453.064 350.925 97.558 183.625 o 17 3 9 15935.000 15980.400 339.018 6.065 o 17 3 10 5.345 88.830 80.379 428.331 o 17 3 11 17914.200 18119.700 366.022 5.174 o 17 3 12 7.014 -53.601 75.802 514.540 o 17 3 13 6657.090 6456.550 251.720 15.767 o 17 3 14 27.634 74.988 74.770 476.421 o 17 3 15 1286.130 1192.290 115.619 87.521 o 17 3 16 22.870 129.223 79.233 415.226 o 17 3 17 3209.070 3135.680 249.518 25.346 o 17 3 18 38.120 -300.450 284.062 36.931 o 17 4 1 46158.500 47084.600 593.971 1.396 o 17 4 2 2258.120 2255.440 157.615 47.202 o 17 4 3 8646.750 9185.710 255.079 12.264 o 17 4 4 580.224 329.614 102.558 161.117 o 17 4 5 11266.800 10837.500 270.763 9.615 o 17 4 6 92.088 76.004 81.501 372.781 o 17 4 7 48195.000 48182.200 607.498 1.320 o 17 4 8 10.373 130.049 96.417 296.477 o 17 4 9 24114.500 23789.600 422.750 3.553 o 17 4 10 53.061 90.935 97.728 282.433 o 17 4 11 38.601 215.216 92.386 296.536 o 17 4 12 12.844 91.191 84.850 382.808 o 17 4 13 6003.100 6108.200 259.994 16.459 o 17 4 14 0.617 25.038 83.313 422.957 o 17 4 15 17477.400 17397.600 381.213 5.231 o 17 4 16 53.433 27.894 96.870 296.428 o 17 4 17 8188.830 6809.070 1327.440 1.564 o 17 5 0 122.144 -122.332 170.311 98.806 o 17 5 1 8025.350 8497.660 339.078 10.755 o 17 5 2 1177.990 919.944 135.865 82.013 o 17 5 3 37802.500 38174.700 510.390 1.912 o 17 5 4 731.571 585.038 109.735 129.110 o 17 5 5 40952.100 40958.300 544.218 1.696 o 17 5 6 6.502 55.548 89.142 360.316 o 17 5 7 1391.750 1047.720 113.652 87.694 o 17 5 8 77.275 -68.771 88.064 349.021 o 17 5 9 11257.300 10921.500 291.059 9.259 o 17 5 10 44.913 321.375 96.646 259.453 o 17 5 11 29573.600 29021.200 492.144 2.645 o 17 5 12 255.564 195.816 122.057 160.186 o 17 5 13 13435.000 13112.200 383.044 6.710 o 17 5 14 15.246 168.357 108.131 234.804 o 17 5 15 276.689 426.523 113.648 164.593 o 17 5 16 93.971 -208.654 187.074 83.193 o 17 6 1 31433.000 31374.900 598.000 2.235 o 17 6 2 254.159 155.928 121.874 162.583 o 17 6 3 4250.840 4205.240 257.359 20.980 o 17 6 4 49.398 -6.459 96.100 306.778 o 17 6 5 7224.100 7201.850 269.929 14.016 o 17 6 6 111.255 54.929 89.837 313.445 o 17 6 7 29535.000 29378.500 467.686 2.691 o 17 6 8 53.054 12.934 78.420 441.381 o 17 6 9 27654.900 26977.400 675.764 2.375 o 17 6 10 42.861 -19.377 108.908 243.132 o 17 6 11 763.084 833.708 133.698 97.342 o 17 6 12 106.921 129.152 100.299 251.762 o 17 6 13 10381.200 10203.900 309.254 9.580 o 17 6 14 2.809 221.328 161.244 110.059 o 17 7 0 42.054 33.851 287.484 35.965 o 17 7 1 9352.880 9941.010 336.549 9.648 o 17 7 2 251.559 172.137 117.941 170.775 o 17 7 3 33251.500 34457.100 643.894 1.992 o 17 7 4 176.658 365.604 105.875 198.695 o 17 7 5 16757.700 16098.100 419.242 5.224 o 17 7 6 112.704 193.295 90.007 289.520 o 17 7 7 1377.850 1329.670 145.409 68.310 o 17 7 8 12.366 198.713 105.932 241.214 o 17 7 9 4909.140 4507.420 213.130 22.528 o 17 7 10 1.713 29.611 104.684 268.977 o 17 7 11 21287.500 20859.000 728.635 2.756 o 17 7 12 2.087 18.154 169.523 103.790 o 17 7 13 12031.200 11872.700 712.604 3.893 o 17 8 1 21695.200 23207.100 530.271 3.419 o 17 8 2 20.295 304.982 98.574 258.923 o 17 8 3 525.853 261.499 97.788 179.742 o 17 8 4 52.418 4.545 103.236 266.418 o 17 8 5 6499.150 6100.330 301.171 14.107 o 17 8 6 18.721 34.079 96.175 310.966 o 17 8 7 12285.400 12019.000 350.956 7.666 o 17 8 8 14.509 103.591 98.849 285.796 o 17 8 9 10447.500 8747.220 704.555 4.266 o 17 8 10 28.720 -53.382 179.967 91.606 o 17 8 11 922.455 660.991 376.929 19.226 o 17 9 0 484.976 350.025 231.931 49.156 o 17 9 1 3059.070 2713.010 204.149 32.201 o 17 9 2 94.635 -52.106 122.851 185.980 o 17 9 3 10224.000 9942.190 327.403 9.383 o 17 9 4 15.223 35.414 186.015 85.688 o 17 9 5 2965.660 2546.050 349.175 17.511 o 17 9 6 13.334 233.755 205.790 68.470 o 18 0 0 43679.500 45275.500 1000.530 1.127 o 18 0 2 2892.590 2977.510 215.088 30.824 o 18 0 4 1814.330 1865.830 186.669 45.521 o 18 0 6 9171.690 8851.790 318.581 10.453 o 18 0 8 2366.740 2365.530 310.847 21.826 o 18 0 10 3419.630 3638.920 273.470 21.922 o 18 0 12 1278.880 1249.460 187.218 53.341 o 18 0 14 7387.430 8032.840 418.505 9.218 o 18 0 16 3513.530 2965.670 349.468 16.562 o 18 1 1 5176.040 5639.950 179.780 22.783 o 18 1 2 9564.330 9639.750 226.067 12.014 o 18 1 3 1397.650 1469.570 117.060 79.990 o 18 1 4 8320.620 8131.970 213.673 14.196 o 18 1 5 2308.700 2566.100 143.701 48.489 o 18 1 6 1436.800 1435.600 129.265 73.577 o 18 1 7 5897.480 6531.300 218.109 18.319 o 18 1 8 24.523 27.742 83.988 401.268 o 18 1 9 2572.460 2545.350 164.434 42.026 o 18 1 10 6621.450 6597.460 242.188 16.122 o 18 1 11 171.516 316.990 88.107 264.851 o 18 1 12 10054.000 10085.800 283.465 10.304 o 18 1 13 216.946 261.743 81.883 286.799 o 18 1 14 576.149 562.288 94.953 163.449 o 18 1 15 1110.390 987.412 109.681 100.826 o 18 1 16 2178.030 2182.050 157.057 48.414 o 18 1 17 951.500 651.734 125.016 101.137 o 18 2 0 13349.900 13448.400 383.591 6.680 o 18 2 1 1978.950 2272.700 132.884 56.509 o 18 2 2 922.478 859.202 98.226 122.382 o 18 2 3 14559.600 14477.900 273.018 7.309 o 18 2 4 318.027 307.822 87.439 235.268 o 18 2 5 20633.700 20697.700 343.697 4.566 o 18 2 6 3912.380 3806.650 192.289 28.164 o 18 2 7 1772.090 1601.220 138.946 62.149 o 18 2 8 4912.830 4774.090 210.439 22.402 o 18 2 9 6320.070 6904.800 241.571 16.342 o 18 2 10 4185.170 4360.690 210.062 24.792 o 18 2 11 6773.620 6440.300 245.841 15.876 o 18 2 12 717.920 685.816 93.308 147.751 o 18 2 13 2903.880 2655.600 177.938 37.118 o 18 2 14 3349.730 3025.960 191.143 32.020 o 18 2 15 363.652 223.842 86.168 238.662 o 18 2 16 1868.790 1306.070 120.275 70.054 o 18 2 17 1240.090 1219.620 306.781 26.136 o 18 3 1 28378.700 28540.000 394.289 2.985 o 18 3 2 2585.560 2510.890 147.423 45.440 o 18 3 3 4465.550 4273.610 191.512 25.698 o 18 3 4 6093.240 6165.730 227.195 17.857 o 18 3 5 6899.880 6895.570 245.515 15.452 o 18 3 6 2389.650 2386.750 158.197 45.354 o 18 3 7 24390.900 23988.200 406.321 3.569 o 18 3 8 840.910 612.432 121.961 109.304 o 18 3 9 12175.000 11775.900 295.054 8.551 o 18 3 10 1830.170 1523.650 149.527 58.188 o 18 3 11 301.661 191.934 79.028 284.614 o 18 3 12 2042.550 1532.150 127.241 62.569 o 18 3 13 4017.680 3441.120 181.796 29.537 o 18 3 14 181.412 126.810 77.160 349.099 o 18 3 15 6728.080 6626.680 249.466 15.667 o 18 3 16 26.240 159.505 97.684 280.548 o 18 3 17 5687.350 4676.910 402.450 11.452 o 18 4 0 2323.470 2450.420 240.133 30.482 o 18 4 1 4409.630 4411.210 236.646 22.015 o 18 4 2 1892.590 1886.770 156.159 53.114 o 18 4 3 35380.500 35076.300 482.844 2.136 o 18 4 4 40.706 154.910 92.579 304.532 o 18 4 5 34278.300 33484.900 481.607 2.238 o 18 4 6 5557.850 5409.540 228.436 19.310 o 18 4 7 2344.610 2130.180 158.309 46.826 o 18 4 8 2062.370 1853.730 149.031 53.443 o 18 4 9 12476.800 12401.100 318.842 7.959 o 18 4 10 17.766 225.192 88.752 323.024 o 18 4 11 17591.400 17819.600 378.412 5.185 o 18 4 12 31.548 222.920 92.149 298.848 o 18 4 13 9499.500 9791.900 280.865 10.803 o 18 4 14 212.367 263.184 93.787 239.751 o 18 4 15 583.503 594.531 110.520 137.500 o 18 4 16 1146.010 796.005 147.912 77.051 o 18 5 1 40278.000 41898.100 685.497 1.550 o 18 5 2 239.512 130.254 115.505 180.288 o 18 5 3 6262.610 6264.810 282.168 15.055 o 18 5 4 1731.650 1592.680 135.084 64.262 o 18 5 5 8274.630 8462.560 255.527 12.881 o 18 5 6 734.214 659.484 117.982 117.365 o 18 5 7 34800.100 33999.300 501.640 2.165 o 18 5 8 1275.040 1312.630 137.350 74.351 o 18 5 9 19224.100 19151.700 387.719 4.704 o 18 5 10 891.758 716.526 105.108 121.130 o 18 5 11 1202.000 1217.030 121.473 86.099 o 18 5 12 54.217 34.179 86.714 361.664 o 18 5 13 8672.600 9084.210 274.593 11.785 o 18 5 14 11.713 -96.583 168.527 104.993 o 18 5 15 14432.500 13541.000 825.862 2.979 o 18 6 0 43.568 198.913 170.449 97.930 o 18 6 1 7101.370 7267.000 335.937 11.871 o 18 6 2 0.263 112.332 107.387 246.814 o 18 6 3 36082.100 37570.100 668.079 1.781 o 18 6 4 642.669 494.407 118.681 126.090 o 18 6 5 23932.200 24302.500 481.043 3.337 o 18 6 6 359.336 308.194 91.771 214.571 o 18 6 7 2671.180 2342.180 147.552 45.404 o 18 6 8 2.525 10.722 93.959 336.054 o 18 6 9 7896.610 7771.980 282.278 12.723 o 18 6 10 372.969 564.616 120.455 138.689 o 18 6 11 22147.100 21739.200 463.406 3.732 o 18 6 12 10.830 296.137 102.445 245.570 o 18 6 13 10149.800 9817.980 460.770 7.098 o 18 6 14 200.181 191.040 202.545 67.763 o 18 7 1 22198.900 22312.800 508.835 3.503 o 18 7 2 2709.320 2083.260 184.091 38.918 o 18 7 3 1513.220 1516.090 141.949 65.820 o 18 7 4 201.562 266.819 103.554 209.113 o 18 7 5 5523.220 5251.800 286.738 16.320 o 18 7 6 146.349 387.041 100.678 217.218 o 18 7 7 19036.000 19042.500 467.088 4.285 o 18 7 8 36.343 -71.889 96.963 305.931 o 18 7 9 13461.200 12996.300 428.822 6.202 o 18 7 10 9.714 -106.409 134.207 165.335 o 18 7 11 788.935 861.800 186.607 62.187 o 18 7 12 300.177 112.437 211.913 61.452 o 18 8 0 617.384 447.475 149.296 95.327 o 18 8 1 2496.130 2331.520 249.057 28.797 o 18 8 2 828.750 728.739 124.955 104.523 o 18 8 3 13751.500 14511.500 403.020 6.215 o 18 8 4 51.487 205.183 96.386 273.776 o 18 8 5 9900.230 9651.050 319.382 9.789 o 18 8 6 133.786 -100.837 123.883 178.504 o 18 8 7 727.268 488.184 215.167 52.668 o 18 8 8 834.339 355.532 170.311 74.823 o 18 8 9 2235.300 1933.550 264.140 28.213 o 18 8 10 273.299 16.388 360.540 22.517 o 18 9 1 9158.480 10118.700 773.497 3.774 o 18 9 2 108.995 112.096 157.754 112.370 o 18 9 3 273.134 -16.388 182.836 82.372 o 18 9 4 1970.810 1600.580 344.152 20.011 o 18 9 5 1374.820 551.736 349.615 21.327 o 18 9 6 848.868 163.882 327.764 25.479 o 19 0 2 46220.700 47471.200 709.085 1.299 o 19 0 4 36426.300 37066.800 625.806 1.837 o 19 0 6 8898.820 9582.800 326.911 10.207 o 19 0 8 37.735 -47.408 152.235 127.026 o 19 0 10 11220.200 10664.500 437.884 7.005 o 19 0 12 35115.400 34600.100 840.668 1.611 o 19 0 14 4640.520 4186.280 330.458 15.693 o 19 0 16 2784.940 2365.080 249.074 27.789 o 19 1 0 47091.500 47723.300 1044.390 1.021 o 19 1 1 409.346 381.010 87.643 211.502 o 19 1 2 23814.900 24242.100 365.361 3.764 o 19 1 3 3491.620 3175.650 167.216 34.135 o 19 1 4 421.238 410.411 85.390 212.990 o 19 1 5 1102.150 1013.920 107.228 102.465 o 19 1 6 13118.600 12925.000 278.157 8.114 o 19 1 7 600.684 422.599 97.781 163.046 o 19 1 8 34630.600 35310.500 503.872 2.136 o 19 1 9 498.944 413.538 94.922 179.890 o 19 1 10 13488.000 13993.900 336.121 7.094 o 19 1 11 373.155 281.040 87.619 226.619 o 19 1 12 1257.030 1253.450 135.193 76.507 o 19 1 13 590.617 610.237 150.574 92.424 o 19 1 14 21165.200 21626.300 467.148 3.838 o 19 1 15 51.187 104.582 89.374 329.333 o 19 1 16 9933.780 10274.400 320.600 9.579 o 19 2 1 7289.560 6718.650 211.737 16.370 o 19 2 2 27621.500 28066.600 380.524 3.107 o 19 2 3 151.358 99.140 82.079 336.901 o 19 2 4 31917.300 32861.100 467.496 2.417 o 19 2 5 1801.200 1484.870 145.855 60.121 o 19 2 6 10096.700 10374.700 266.769 10.520 o 19 2 7 4524.630 4451.340 210.134 23.764 o 19 2 8 48.989 140.780 85.993 345.373 o 19 2 9 5450.730 5739.950 232.480 18.981 o 19 2 10 12013.700 12986.900 306.083 8.202 o 19 2 11 83.915 188.493 71.844 423.635 o 19 2 12 19962.000 20598.700 420.771 4.293 o 19 2 13 2598.630 2587.240 181.895 38.449 o 19 2 14 2526.610 2196.920 170.251 42.477 o 19 2 15 2781.380 2789.780 191.136 35.290 o 19 2 16 2301.790 2232.150 241.357 30.797 o 19 3 0 21104.600 21720.900 488.973 3.740 o 19 3 1 2147.290 2144.640 154.564 49.514 o 19 3 2 12074.300 12089.300 279.790 8.744 o 19 3 3 13522.000 12483.100 280.355 8.011 o 19 3 4 28.104 49.519 86.420 372.834 o 19 3 5 7433.640 7603.620 263.934 13.813 o 19 3 6 13159.900 13303.100 328.368 7.414 o 19 3 7 788.642 819.880 111.345 117.454 o 19 3 8 18592.300 18950.400 366.219 4.961 o 19 3 9 2327.460 2429.070 161.500 44.976 o 19 3 10 3253.150 3290.530 180.817 33.222 o 19 3 11 9472.810 9493.350 279.692 10.945 o 19 3 12 631.227 665.261 90.135 160.923 o 19 3 13 5116.250 4993.570 222.810 20.885 o 19 3 14 5109.610 5066.640 240.287 19.715 o 19 3 15 18.011 -26.352 84.299 410.365 o 19 3 16 4167.050 3624.950 333.883 16.365 o 19 4 1 16760.700 16836.000 380.851 5.439 o 19 4 2 2334.040 2353.130 166.273 44.192 o 19 4 3 1675.040 1895.830 194.491 44.499 o 19 4 4 11802.800 11875.400 306.750 8.524 o 19 4 5 2276.760 2592.030 173.601 42.170 o 19 4 6 6403.430 6469.720 270.853 15.259 o 19 4 7 12412.300 12259.600 324.182 7.940 o 19 4 8 653.058 632.499 114.350 126.782 o 19 4 9 8457.630 8865.370 269.969 12.159 o 19 4 10 3884.060 4026.190 206.324 26.502 o 19 4 11 508.468 597.470 91.380 175.090 o 19 4 12 1897.610 1770.080 132.821 61.110 o 19 4 13 4629.530 4347.890 205.982 23.954 o 19 4 14 998.917 752.595 125.825 96.874 o 19 4 15 7134.650 6904.310 316.837 12.607 o 19 4 16 139.701 381.726 221.881 56.743 o 19 5 0 898.946 826.289 275.967 33.083 o 19 5 1 2170.750 1990.610 211.118 37.194 o 19 5 2 3239.250 3084.540 240.798 26.284 o 19 5 3 18990.900 18975.300 452.771 4.379 o 19 5 4 429.277 282.400 106.068 172.040 o 19 5 5 12212.700 12777.100 297.483 8.280 o 19 5 6 1674.190 1707.360 165.609 53.690 o 19 5 7 741.992 468.372 124.410 114.745 o 19 5 8 2659.900 2660.330 188.566 36.714 o 19 5 9 4609.840 4668.310 257.639 19.848 o 19 5 10 25.409 239.316 91.859 299.782 o 19 5 11 9493.820 9722.120 282.395 10.796 o 19 5 12 179.348 399.578 99.871 213.146 o 19 5 13 5885.840 5604.760 262.575 16.829 o 19 5 14 49.390 49.161 144.839 137.584 o 19 5 15 17.315 -945.053 289.525 35.652 o 19 6 1 16664.100 16984.300 434.097 5.046 o 19 6 2 7.674 -83.865 93.342 340.559 o 19 6 3 1164.290 1249.880 143.254 74.303 o 19 6 4 463.653 626.150 112.744 141.738 o 19 6 5 3845.130 4329.640 246.986 22.529 o 19 6 6 646.201 697.509 102.670 140.130 o 19 6 7 13791.500 14833.900 365.219 6.556 o 19 6 8 782.860 813.733 171.669 70.517 o 19 6 9 6870.660 6543.840 271.679 14.663 o 19 6 10 3.885 217.605 101.015 262.509 o 19 6 11 300.654 29.116 137.700 134.026 o 19 6 12 429.323 322.891 225.571 52.304 o 19 6 13 2795.870 1715.800 256.677 27.794 o 19 7 0 2845.010 2333.370 296.468 22.321 o 19 7 1 1458.360 1763.940 152.793 60.500 o 19 7 2 23.067 80.002 95.566 305.405 o 19 7 3 10359.300 11013.100 370.383 8.300 o 19 7 4 209.766 98.638 99.394 236.601 o 19 7 5 10475.000 10818.000 404.333 7.730 o 19 7 6 260.297 450.547 153.810 103.670 o 19 7 7 1487.280 1627.790 143.112 64.851 o 19 7 8 129.108 -122.850 121.858 184.528 o 19 7 9 2615.550 2018.320 177.346 41.044 o 19 7 10 459.759 243.089 286.487 33.899 o 19 7 11 5960.700 5401.500 507.321 8.183 o 19 8 1 4339.530 4417.440 271.588 19.588 o 19 8 2 1058.160 905.655 131.884 88.058 o 19 8 3 2284.150 2067.310 232.433 32.622 o 19 8 4 2624.510 2392.340 177.275 39.746 o 19 8 5 1068.330 1098.350 123.693 90.410 o 19 8 6 872.778 484.687 261.343 37.220 o 19 8 7 7134.970 6135.880 865.843 3.399 o 19 8 8 29.052 -25.830 183.058 88.558 o 19 8 9 3763.970 3703.730 650.065 6.121 o 19 9 1 813.407 901.351 262.211 36.264 o 19 9 2 2419.910 1917.420 344.152 19.081 o 19 9 3 2631.200 1693.450 305.913 22.466 o 20 0 0 73332.200 77382.500 1356.720 0.521 o 20 0 2 41648.900 44362.800 767.256 1.393 o 20 0 4 729.061 840.522 133.425 98.673 o 20 0 6 33146.500 35288.500 629.799 2.003 o 20 0 8 48963.600 48854.300 864.122 1.112 o 20 0 10 16993.900 18080.400 576.285 3.960 o 20 0 12 1905.230 1956.610 221.354 36.719 o 20 0 14 23362.400 23995.400 711.516 2.596 o 20 0 16 17705.500 19441.900 1245.500 1.493 o 20 1 1 208.769 121.431 92.425 261.941 o 20 1 2 41090.800 43314.300 510.060 1.683 o 20 1 3 40.055 171.724 82.590 366.665 o 20 1 4 55117.300 56417.800 603.892 1.088 o 20 1 5 164.876 217.327 77.678 333.921 o 20 1 6 23636.800 23820.400 381.332 3.755 o 20 1 7 67.936 21.780 82.479 391.745 o 20 1 8 448.282 407.835 92.081 192.840 o 20 1 9 216.534 183.766 87.624 272.524 o 20 1 10 29873.600 29675.400 502.453 2.579 o 20 1 11 1281.370 1388.420 128.101 78.125 o 20 1 12 33639.200 35048.300 607.593 2.023 o 20 1 13 63.435 259.613 122.335 175.806 o 20 1 14 5849.990 5878.240 276.658 16.015 o 20 1 15 258.833 257.205 82.187 274.224 o 20 1 16 3583.240 3720.120 589.975 7.260 o 20 2 0 53241.600 53495.500 1156.110 0.839 o 20 2 1 715.824 821.725 112.751 119.748 o 20 2 2 27103.100 27633.300 407.045 3.107 o 20 2 3 827.080 606.221 100.126 133.929 o 20 2 4 2503.980 2488.300 162.843 43.062 o 20 2 5 111.422 103.304 88.496 312.710 o 20 2 6 29116.900 29120.600 483.388 2.694 o 20 2 7 1422.690 1451.610 128.564 74.034 o 20 2 8 30726.500 29821.800 469.474 2.588 o 20 2 9 266.962 344.119 87.761 240.972 o 20 2 10 8095.160 8442.020 252.152 13.149 o 20 2 11 1979.420 1838.150 147.612 54.918 o 20 2 12 1071.850 796.118 149.303 77.904 o 20 2 13 1323.360 1249.830 117.000 84.843 o 20 2 14 14082.100 13071.000 401.712 6.330 o 20 2 15 188.287 480.173 124.451 149.012 o 20 3 1 2713.420 2638.590 164.149 40.752 o 20 3 2 17298.200 16742.900 348.987 5.567 o 20 3 3 310.419 223.215 136.084 129.874 o 20 3 4 28471.600 28758.800 478.336 2.767 o 20 3 5 337.490 248.262 127.635 140.856 o 20 3 6 9471.050 9146.820 284.475 10.955 o 20 3 7 67.848 181.026 93.744 285.694 o 20 3 8 1464.100 1481.320 144.173 66.021 o 20 3 9 1385.590 1200.580 116.093 84.313 o 20 3 10 14206.100 14150.200 330.313 6.901 o 20 3 11 663.346 628.368 93.939 153.881 o 20 3 12 12769.100 13580.700 333.045 7.446 o 20 3 13 1936.590 1544.400 125.815 64.656 o 20 3 14 2203.540 2370.160 156.501 47.438 o 20 3 15 1015.440 1229.280 153.416 72.157 o 20 4 0 12742.900 12900.100 516.914 5.430 o 20 4 1 1365.340 1191.190 141.905 71.489 o 20 4 2 5902.340 5520.850 262.675 16.859 o 20 4 3 2105.290 2045.630 154.890 50.347 o 20 4 4 402.702 296.837 107.585 170.931 o 20 4 5 383.791 281.147 91.658 213.067 o 20 4 6 6802.850 7022.190 270.588 14.521 o 20 4 7 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606.094 787.860 118.205 120.472 o 20 6 2 1.436 86.668 110.909 234.373 o 20 6 3 1421.630 1482.000 150.911 63.909 o 20 6 4 39.583 51.948 108.909 238.428 o 20 6 5 1474.210 1445.410 141.191 67.421 o 20 6 6 231.784 213.507 99.881 219.999 o 20 6 7 9.299 164.706 112.347 220.196 o 20 6 8 0.926 -21.652 91.532 357.069 o 20 6 9 643.816 247.433 99.398 164.575 o 20 6 10 241.518 151.224 98.711 227.758 o 20 6 11 619.646 1040.060 269.954 35.104 o 20 6 12 157.204 576.030 186.044 76.004 o 20 7 1 308.004 49.886 100.207 219.922 o 20 7 2 920.259 1054.940 128.955 92.063 o 20 7 3 173.494 109.006 93.101 269.526 o 20 7 4 842.700 718.481 153.564 81.562 o 20 7 5 530.438 773.807 134.903 106.318 o 20 7 6 480.061 487.078 109.169 151.621 o 20 7 7 2485.100 2444.130 198.285 36.593 o 20 7 8 4.404 -27.356 199.485 75.175 o 20 7 9 297.559 451.685 253.247 42.922 o 20 7 10 154.980 180.926 193.021 75.084 o 20 8 0 4085.020 3915.760 322.998 16.950 o 20 8 1 79.391 299.557 107.107 215.022 o 20 8 2 1950.560 1801.170 148.198 55.314 o 20 8 3 428.911 288.681 117.862 149.153 o 20 8 4 12.813 334.794 194.418 75.388 o 20 8 5 1734.060 1457.740 209.985 41.779 o 20 8 6 1605.520 1743.480 421.242 14.595 o 20 8 7 143.919 534.404 363.272 21.959 o 21 0 2 32707.000 34738.300 681.172 1.945 o 21 0 4 55157.000 57553.800 923.928 0.916 o 21 0 6 13995.800 15254.100 488.701 5.250 o 21 0 8 4141.690 4280.050 350.981 15.070 o 21 0 10 29110.100 28885.900 755.178 2.073 o 21 0 12 25264.100 25214.800 718.189 2.436 o 21 0 14 4628.290 4969.250 576.119 7.152 o 21 1 0 38667.600 40087.300 741.743 1.559 o 21 1 1 154.410 226.371 100.484 230.951 o 21 1 2 27243.500 29529.500 442.486 2.922 o 21 1 3 169.588 104.355 88.399 293.871 o 21 1 4 868.339 1115.290 114.660 103.978 o 21 1 5 452.359 628.164 109.031 148.311 o 21 1 6 29958.500 32137.200 453.831 2.594 o 21 1 7 8.939 58.087 73.099 520.961 o 21 1 8 46039.400 48201.300 618.386 1.366 o 21 1 9 699.474 600.092 98.118 146.028 o 21 1 10 4813.460 5185.930 245.397 19.821 o 21 1 11 78.219 147.619 82.903 352.343 o 21 1 12 2536.020 2316.340 219.118 33.137 o 21 1 13 7.873 81.222 98.142 295.086 o 21 1 14 15009.000 14471.100 381.950 6.111 o 21 1 15 123.342 112.847 137.804 143.200 o 21 2 1 404.489 451.608 95.614 187.725 o 21 2 2 19507.600 20881.400 472.646 4.066 o 21 2 3 433.218 397.533 113.728 151.532 o 21 2 4 37508.900 38891.200 564.858 1.841 o 21 2 5 133.482 94.004 105.322 229.930 o 21 2 6 11374.200 11682.800 307.831 8.745 o 21 2 7 1960.620 1920.400 157.331 51.847 o 21 2 8 2171.540 2159.110 146.967 51.129 o 21 2 9 151.115 13.845 70.986 444.961 o 21 2 10 15818.000 16652.000 350.928 5.911 o 21 2 11 361.144 314.095 111.698 165.795 o 21 2 12 19749.600 20608.700 424.419 4.304 o 21 2 13 5.226 33.473 78.667 466.301 o 21 2 14 4879.320 4752.480 252.150 19.655 o 21 2 15 24.272 480.721 174.808 89.681 o 21 3 0 14641.700 15195.000 471.396 5.289 o 21 3 1 1013.450 1006.960 119.652 96.606 o 21 3 2 12409.900 12441.900 344.125 7.637 o 21 3 3 91.075 176.897 102.343 241.595 o 21 3 4 640.754 506.025 122.176 121.561 o 21 3 5 2415.190 2668.570 186.591 38.464 o 21 3 6 9060.290 9576.620 280.633 11.178 o 21 3 7 72.928 180.150 88.388 313.363 o 21 3 8 23206.200 23631.600 453.488 3.548 o 21 3 9 2194.310 2093.800 152.342 49.861 o 21 3 10 5260.700 5122.060 219.062 20.702 o 21 3 11 293.019 219.595 78.500 285.345 o 21 3 12 1224.570 1127.260 119.392 88.014 o 21 3 13 25.020 -58.424 73.774 524.557 o 21 3 14 9047.040 8149.540 354.140 9.897 o 21 4 1 146.756 7.859 97.966 267.170 o 21 4 2 8757.150 8933.050 292.859 11.317 o 21 4 3 448.534 279.483 136.271 120.173 o 21 4 4 6811.900 7290.150 290.278 13.647 o 21 4 5 268.906 348.109 139.885 123.063 o 21 4 6 2867.810 2385.390 166.318 40.172 o 21 4 7 3359.980 3295.430 196.746 30.697 o 21 4 8 209.349 304.836 96.136 228.084 o 21 4 9 842.074 791.791 110.008 116.790 o 21 4 10 5510.590 5471.790 308.853 15.120 o 21 4 11 67.812 86.544 85.229 354.357 o 21 4 12 6483.750 6593.500 268.239 15.204 o 21 4 13 146.022 274.293 89.089 272.866 o 21 4 14 751.416 897.340 145.721 87.184 o 21 5 0 699.818 996.469 192.389 59.770 o 21 5 1 745.882 500.426 114.545 124.974 o 21 5 2 2141.580 2164.820 226.454 34.061 o 21 5 3 3029.740 2588.170 190.931 34.570 o 21 5 4 240.415 304.417 117.623 165.851 o 21 5 5 1254.080 984.390 147.445 72.987 o 21 5 6 717.902 857.991 120.146 111.095 o 21 5 7 14.904 231.012 100.703 259.616 o 21 5 8 1892.550 1861.030 164.236 50.916 o 21 5 9 625.742 500.496 107.054 142.791 o 21 5 10 974.588 1067.930 124.675 93.202 o 21 5 11 540.352 621.678 197.088 62.288 o 21 5 12 203.292 166.314 123.114 164.276 o 21 5 13 282.243 805.879 303.182 30.152 o 21 6 1 1951.940 2045.140 165.882 48.961 o 21 6 2 112.296 229.144 112.011 199.953 o 21 6 3 376.234 375.564 118.979 147.946 o 21 6 4 217.298 356.501 137.397 129.471 o 21 6 5 340.908 516.986 109.637 161.940 o 21 6 6 30.870 84.065 135.270 156.997 o 21 6 7 1161.360 843.722 141.635 79.871 o 21 6 8 19.421 74.288 96.002 304.974 o 21 6 9 816.213 771.928 110.089 118.560 o 21 6 10 3.016 -18.744 133.883 166.793 o 21 6 11 144.269 77.048 146.028 128.641 o 21 7 0 2736.480 2258.770 233.047 30.316 o 21 7 1 739.386 475.783 99.529 145.801 o 21 7 2 847.071 383.130 138.266 98.407 o 21 7 3 1948.800 1384.390 131.769 63.650 o 21 7 4 137.951 2.505 97.496 272.395 o 21 7 5 80.578 119.964 122.572 181.208 o 21 7 6 1659.010 1441.900 198.291 45.419 o 21 7 7 140.759 243.837 322.301 28.071 o 21 7 8 1261.490 1092.550 316.839 24.879 o 21 7 9 28.812 49.165 300.450 32.971 o 21 8 1 1186.040 917.739 327.764 23.852 o 21 8 2 2251.350 2697.190 338.963 19.185 o 21 8 3 7.717 483.682 316.839 29.060 o 21 8 4 4701.180 4069.740 639.140 6.110 o 22 0 0 26186.900 25909.100 974.372 1.764 o 22 0 2 20308.200 21534.000 536.104 3.619 o 22 0 4 65.637 412.178 166.366 97.898 o 22 0 6 22108.800 23069.100 572.496 3.217 o 22 0 8 26526.100 26425.600 707.692 2.366 o 22 0 10 2730.020 2773.540 321.259 19.861 o 22 0 12 1889.380 2646.750 320.927 21.468 o 22 0 14 5225.930 5591.380 447.009 10.006 o 22 1 1 801.598 778.758 125.609 104.015 o 22 1 2 11810.200 12936.600 320.451 8.097 o 22 1 3 688.675 787.314 110.262 124.992 o 22 1 4 31408.300 32749.100 483.059 2.423 o 22 1 5 14.311 88.935 78.438 441.716 o 22 1 6 13665.000 13955.200 334.768 7.058 o 22 1 7 463.764 547.071 98.255 169.786 o 22 1 8 2686.750 2668.200 171.097 39.577 o 22 1 9 503.459 493.614 84.190 196.826 o 22 1 10 14821.600 14282.800 342.321 6.572 o 22 1 11 67.927 -211.697 70.368 527.526 o 22 1 12 8333.990 8106.780 293.677 11.905 o 22 1 13 297.114 129.876 81.814 282.929 o 22 1 14 2426.540 2463.620 297.431 22.969 o 22 2 0 15663.500 16236.900 473.120 4.994 o 22 2 1 522.302 574.682 122.917 125.363 o 22 2 2 12590.500 13122.200 346.884 7.415 o 22 2 3 3787.630 4010.280 216.300 25.852 o 22 2 4 6.330 73.157 106.524 253.697 o 22 2 5 4655.470 4529.890 227.666 22.018 o 22 2 6 15595.600 15209.900 351.115 6.149 o 22 2 7 574.308 515.451 105.719 148.227 o 22 2 8 15463.100 15546.700 359.492 6.066 o 22 2 9 1839.710 1595.840 133.814 62.977 o 22 2 10 2426.230 2200.690 177.869 41.621 o 22 2 11 2224.810 2331.400 155.328 47.697 o 22 2 12 885.104 1022.890 110.826 108.484 o 22 2 13 1148.530 1077.780 118.463 91.712 o 22 2 14 5405.270 5014.790 677.379 5.379 o 22 3 1 8410.400 8956.320 301.616 11.328 o 22 3 2 8072.220 7985.130 292.909 12.176 o 22 3 3 1614.810 1722.100 191.371 46.529 o 22 3 4 10732.000 10091.100 317.085 9.282 o 22 3 5 1924.690 1848.630 166.745 49.949 o 22 3 6 4527.040 4318.230 240.238 21.590 o 22 3 7 8732.420 9498.490 280.591 11.438 o 22 3 8 15.533 -89.154 79.344 463.546 o 22 3 9 5448.280 5114.270 243.075 18.913 o 22 3 10 7476.370 7428.400 329.512 11.743 o 22 3 11 318.447 390.382 135.279 125.636 o 22 3 12 6496.780 5888.060 248.283 16.489 o 22 3 13 1947.520 1875.900 168.233 49.184 o 22 3 14 823.585 1131.560 196.389 55.656 o 22 4 0 12741.900 12257.200 516.758 5.492 o 22 4 1 1200.580 1188.530 149.457 70.993 o 22 4 2 2861.270 2427.710 196.207 35.000 o 22 4 3 10298.300 10774.700 354.771 8.647 o 22 4 4 1023.050 905.121 133.251 88.156 o 22 4 5 10460.600 10565.700 360.810 8.516 o 22 4 6 1952.210 1784.450 157.844 52.528 o 22 4 7 1126.380 1322.750 142.247 74.869 o 22 4 8 2257.020 2054.120 147.670 50.606 o 22 4 9 3882.070 3682.690 216.711 26.017 o 22 4 10 1821.850 1881.020 134.449 60.869 o 22 4 11 6273.800 5866.130 288.170 15.005 o 22 4 12 159.464 152.638 134.773 144.745 o 22 4 13 2765.690 2077.280 368.876 16.658 o 22 5 1 8563.170 8067.820 299.258 11.597 o 22 5 2 1893.140 1350.160 140.309 61.729 o 22 5 3 656.836 664.010 120.856 118.052 o 22 5 4 663.365 524.274 144.375 96.907 o 22 5 5 3055.750 2812.540 225.122 29.192 o 22 5 6 38.662 141.090 108.058 233.177 o 22 5 7 9095.930 9353.500 408.556 8.440 o 22 5 8 146.945 179.680 98.262 245.606 o 22 5 9 4507.880 3886.360 194.050 25.934 o 22 5 10 90.680 -151.870 101.790 264.330 o 22 5 11 320.447 250.208 142.139 119.796 o 22 6 0 32.186 -112.025 231.812 55.382 o 22 6 1 1135.200 1017.220 146.962 75.395 o 22 6 2 0.132 141.688 104.559 256.183 o 22 6 3 7135.390 6599.470 292.421 13.590 o 22 6 4 422.248 560.624 118.398 138.515 o 22 6 5 5692.800 4654.190 368.495 12.730 o 22 6 6 699.681 747.721 162.053 78.885 o 22 6 7 447.255 436.033 128.676 126.091 o 22 6 8 50.332 -126.245 185.466 85.732 o 22 6 9 2673.640 2178.580 269.246 25.884 o 22 6 10 109.857 151.740 173.081 93.753 o 22 7 1 8042.140 8028.010 306.807 11.783 o 22 7 2 263.741 272.516 100.380 208.285 o 22 7 3 334.063 174.539 192.415 72.069 o 22 7 4 1626.470 1355.680 153.399 60.788 o 22 7 5 2007.870 1824.550 371.466 17.516 o 22 7 6 390.470 781.171 322.301 26.659 o 23 0 2 1165.160 2006.760 251.413 34.281 o 23 0 4 10236.600 10906.000 391.748 8.007 o 23 0 6 7943.070 8207.200 413.840 9.044 o 23 0 8 53.571 -78.658 136.247 156.518 o 23 0 10 4480.580 3487.350 409.832 12.338 o 23 0 12 2484.790 2249.710 238.390 30.510 o 23 1 0 9305.820 9233.060 432.799 7.929 o 23 1 1 328.043 312.095 128.051 138.571 o 23 1 2 4125.640 4647.830 228.568 23.029 o 23 1 3 1826.120 2060.360 257.316 30.420 o 23 1 4 503.377 449.008 99.900 167.671 o 23 1 5 2322.510 2504.610 175.865 41.691 o 23 1 6 7060.220 7086.360 251.844 14.911 o 23 1 7 215.435 434.111 100.788 202.174 o 23 1 8 5970.370 6347.570 263.791 16.170 o 23 1 9 234.841 337.814 84.749 259.841 o 23 1 10 1498.120 1355.720 161.822 59.388 o 23 1 11 2720.710 2368.800 177.308 39.199 o 23 1 12 231.572 243.604 84.347 274.455 o 23 1 13 1540.750 1458.700 217.565 41.212 o 23 2 1 9701.550 10806.800 318.760 9.597 o 23 2 2 2882.590 3036.880 199.755 32.893 o 23 2 3 517.262 646.272 142.430 101.845 o 23 2 4 8834.140 8799.430 312.547 10.823 o 23 2 5 938.819 961.994 128.136 93.575 o 23 2 6 4033.340 3853.250 203.845 26.545 o 23 2 7 4260.640 4495.450 223.271 23.316 o 23 2 8 513.809 507.480 132.042 116.295 o 23 2 9 6220.640 6090.020 300.504 14.418 o 23 2 10 2814.610 2695.590 184.028 36.512 o 23 2 11 247.413 258.385 77.656 297.118 o 23 2 12 2293.010 2412.190 164.545 44.661 o 23 2 13 2552.340 2037.600 382.391 16.009 o 23 3 0 4600.360 4307.090 438.487 10.923 o 23 3 1 4182.110 4533.440 290.874 18.441 o 23 3 2 1659.380 1447.980 160.712 57.058 o 23 3 3 13823.100 13100.100 356.235 6.902 o 23 3 4 11.610 152.903 102.870 259.905 o 23 3 5 7959.630 8082.200 297.091 12.105 o 23 3 6 1775.910 1814.570 160.707 53.466 o 23 3 7 777.714 800.964 95.776 135.849 o 23 3 8 2566.960 2572.050 169.154 41.063 o 23 3 9 1307.620 996.466 105.832 96.065 o 23 3 10 1318.810 1171.490 111.535 89.272 o 23 3 11 10992.900 10900.200 324.619 8.829 o 23 3 12 526.109 395.734 134.796 115.152 o 23 3 13 5262.250 4790.820 715.618 4.938 o 23 4 1 17707.500 17064.600 449.405 4.749 o 23 4 2 2667.840 2433.830 211.904 33.419 o 23 4 3 1079.440 1104.440 168.274 64.682 o 23 4 4 508.656 450.856 125.674 126.135 o 23 4 5 4602.290 4639.230 286.480 18.011 o 23 4 6 25.695 249.120 97.982 267.203 o 23 4 7 15007.900 14546.800 384.597 6.077 o 23 4 8 3.910 202.129 81.383 386.665 o 23 4 9 11432.400 11093.400 307.485 8.861 o 23 4 10 214.602 114.638 89.481 274.149 o 23 4 11 901.767 1085.900 184.673 59.933 o 23 4 12 1082.710 846.724 398.780 17.057 o 23 5 0 698.884 1122.890 208.158 52.431 o 23 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114.679 132.460 163.434 o 24 0 8 566.911 609.945 183.570 69.383 o 24 0 10 65.258 99.711 145.080 134.431 o 24 0 12 59.801 49.165 169.345 101.254 o 24 1 1 3527.190 3664.330 231.358 25.615 o 24 1 2 28.288 209.700 125.063 175.504 o 24 1 3 141.688 342.148 130.103 147.643 o 24 1 4 46.235 86.199 103.113 258.473 o 24 1 5 1113.240 1057.880 119.699 92.337 o 24 1 6 1.148 -7.114 113.767 231.185 o 24 1 7 1224.390 1326.860 174.524 58.297 o 24 1 8 69.901 243.089 112.269 204.365 o 24 1 9 483.129 711.806 111.467 139.101 o 24 1 10 5.621 -66.070 106.320 263.561 o 24 1 11 119.504 -92.196 87.171 337.386 o 24 1 12 97.216 321.774 199.450 70.390 o 24 1 13 1296.470 1163.560 202.121 48.574 o 24 2 0 58.239 211.191 174.810 92.689 o 24 2 1 4570.280 5135.690 284.622 17.808 o 24 2 2 87.836 -158.732 136.940 152.098 o 24 2 3 10539.300 10753.700 347.154 8.680 o 24 2 4 1.270 95.360 131.143 169.009 o 24 2 5 2787.550 2922.020 214.071 31.505 o 24 2 6 4.697 107.023 96.656 300.578 o 24 2 7 447.566 449.847 89.779 195.308 o 24 2 8 12.170 8.746 93.324 337.053 o 24 2 9 1291.840 951.706 150.983 70.745 o 24 2 10 28.124 -13.894 112.292 232.001 o 24 2 11 8016.190 7611.130 335.024 11.152 o 24 2 12 19.366 60.090 218.509 62.043 o 24 2 13 3542.260 3698.270 366.003 15.144 o 24 3 1 19599.400 22237.800 571.664 3.489 o 24 3 2 0.684 -2.931 119.870 208.337 o 24 3 3 267.758 272.343 181.597 80.246 o 24 3 4 31.202 221.456 92.023 299.889 o 24 3 5 5188.180 4808.370 254.653 18.918 o 24 3 6 9.961 81.829 111.237 231.868 o 24 3 7 8370.870 8083.940 300.180 11.707 o 24 3 8 17.927 40.774 130.161 172.617 o 24 3 9 10439.100 10121.500 288.822 9.960 o 24 3 10 75.426 546.458 95.125 234.061 o 24 3 11 1299.770 1296.220 310.213 25.416 o 24 3 12 115.358 27.314 322.301 28.454 o 24 4 0 194.525 270.450 171.745 90.652 o 24 4 1 6396.440 6510.040 375.512 11.340 o 24 4 2 24.657 200.104 120.628 188.541 o 24 4 3 20384.100 22578.000 574.654 3.385 o 24 4 4 56.675 85.166 99.074 275.356 o 24 4 5 15642.900 16349.600 442.037 5.236 o 24 4 6 71.058 -42.664 97.430 292.146 o 24 4 7 989.900 719.499 115.216 106.692 o 24 4 8 4.038 136.597 106.075 249.070 o 24 4 9 3220.430 2815.420 176.599 35.151 o 24 4 10 1.601 -326.889 111.874 238.977 o 24 4 11 14576.000 14372.500 1092.550 1.960 o 24 5 1 21888.700 22906.500 538.709 3.380 o 24 5 2 118.286 -50.465 121.623 186.520 o 24 5 3 2315.850 1938.390 198.592 38.984 o 24 5 4 1.150 63.555 153.095 125.897 o 24 5 5 6529.760 6181.120 338.733 12.617 o 24 5 6 10.502 -210.514 121.336 201.898 o 24 5 7 17527.700 16928.600 530.565 4.250 o 24 5 8 27.319 -46.289 215.238 64.245 o 24 5 9 13467.800 14557.300 762.825 3.342 o 24 6 0 3.782 153.403 349.615 24.332 o 24 6 1 3837.690 3181.980 482.213 10.090 o 24 6 2 13.604 306.413 143.865 133.212 o 24 6 3 16981.500 18336.800 874.140 2.515 o 24 6 4 36.321 -143.135 237.629 52.679 o 24 6 5 19211.600 17305.900 1190.880 1.590 o 24 7 2 93.034 1114.400 284.062 34.143 o 25 0 2 3937.880 4558.690 353.815 14.984 o 25 0 4 10618.000 10674.700 546.507 5.717 o 25 0 6 3238.510 2846.450 247.191 25.921 o 25 0 8 291.952 275.731 150.365 109.965 o 25 0 10 4229.590 4391.060 583.504 7.166 o 25 0 12 2626.710 1840.940 371.466 16.773 o 25 1 0 4969.460 6234.000 411.703 11.096 o 25 1 1 924.776 972.329 152.648 77.213 o 25 1 2 4679.250 4669.630 274.717 18.609 o 25 1 3 2899.970 3215.570 234.396 27.877 o 25 1 4 260.536 200.861 109.032 189.939 o 25 1 5 1031.420 993.504 135.449 85.184 o 25 1 6 4675.560 4347.510 229.396 22.047 o 25 1 7 8.233 30.855 94.489 326.231 o 25 1 8 8397.480 8218.610 307.822 11.431 o 25 1 9 38.086 54.858 103.875 260.665 o 25 1 10 744.539 575.115 123.580 112.949 o 25 1 11 594.129 106.289 199.390 64.059 o 25 2 1 9452.670 10202.300 376.879 8.730 o 25 2 2 2885.340 3035.330 233.335 28.357 o 25 2 3 236.826 277.419 186.714 76.993 o 25 2 4 6684.970 6700.930 300.237 13.677 o 25 2 5 1138.610 1368.670 193.271 52.064 o 25 2 6 1709.370 1742.890 172.733 50.920 o 25 2 7 2868.820 2557.400 183.672 36.653 o 25 2 8 366.274 104.013 121.044 156.371 o 25 2 9 4894.500 4393.110 223.091 21.973 o 25 2 10 2140.620 2111.370 178.786 43.863 o 25 2 11 352.408 294.988 185.733 75.091 o 25 3 0 2970.990 3197.170 457.429 11.409 o 25 3 1 4213.190 4253.310 379.064 13.612 o 25 3 2 2058.760 1779.780 234.814 33.849 o 25 3 3 14999.700 15219.000 456.674 5.346 o 25 3 4 338.554 284.695 123.425 146.702 o 25 3 5 6759.700 7157.200 373.876 10.963 o 25 3 6 1704.850 1610.520 148.082 59.808 o 25 3 7 406.197 349.517 104.052 175.150 o 25 3 8 3139.010 2924.540 197.095 32.371 o 25 3 9 1426.520 1139.340 187.153 52.370 o 25 3 10 597.058 304.350 135.564 113.042 o 25 4 1 16024.700 15857.100 532.346 4.518 o 25 4 2 2370.360 2013.050 235.167 31.928 o 25 4 3 723.588 556.786 196.700 60.383 o 25 4 4 739.850 663.811 142.509 93.610 o 25 4 5 4348.400 4778.500 363.596 14.002 o 25 4 6 315.813 221.484 107.345 185.860 o 25 4 7 12644.400 13112.900 424.146 6.449 o 25 4 8 16.523 -28.033 206.789 69.753 o 25 4 9 9406.880 8949.320 1212.730 1.804 o 25 5 0 326.723 531.115 205.723 61.477 o 25 5 1 2647.860 2499.230 249.917 27.904 o 25 5 2 598.422 604.784 239.008 44.760 o 25 5 3 16348.200 16036.500 747.477 3.163 o 25 5 4 256.248 454.035 159.186 98.044 o 25 5 5 11642.700 10486.400 515.885 5.897 o 25 5 6 54.605 -142.031 223.972 59.020 o 25 5 8 119.098 -38.239 278.599 37.964 o 25 6 1 13128.900 12885.200 961.488 2.463 o 25 6 2 256.205 158.419 256.749 43.080 o 25 6 3 1343.520 2059.450 398.780 16.140 o 26 0 0 14236.200 15322.500 776.725 3.185 o 26 0 2 11566.000 12784.300 503.967 5.813 o 26 0 4 22.076 266.313 232.731 53.651 o 26 0 6 15149.300 16506.800 1056.180 2.019 o 26 0 8 18366.300 19615.200 727.544 2.991 o 26 1 1 1039.830 1145.280 157.559 70.315 o 26 1 2 6411.690 6924.900 333.084 12.617 o 26 1 3 50.325 89.921 127.068 174.484 o 26 1 4 18153.100 20240.500 535.167 3.937 o 26 1 5 190.973 347.397 136.809 132.307 o 26 1 6 10462.700 11411.300 567.541 5.435 o 26 1 7 424.960 571.674 137.747 112.303 o 26 1 8 1860.560 1551.810 191.428 45.186 o 26 1 9 125.035 111.938 133.131 152.322 o 26 1 10 13573.700 10406.500 715.618 3.798 o 26 2 0 11990.400 13588.300 614.709 4.576 o 26 2 1 249.901 482.559 156.040 101.039 o 26 2 2 7677.630 8779.220 550.037 6.472 o 26 2 3 2395.670 2403.690 222.031 33.100 o 26 2 4 146.591 462.515 117.543 167.512 o 26 2 5 1800.860 1641.920 167.327 52.121 o 26 2 6 12363.600 13472.400 393.798 6.843 o 26 2 7 175.776 386.447 166.742 94.273 o 26 2 8 11123.900 10497.400 461.378 6.723 o 26 2 9 623.681 507.164 126.299 117.545 o 26 2 10 2660.360 2829.700 344.152 18.095 o 26 3 1 4941.330 5684.400 430.443 10.642 o 26 3 2 6691.300 7331.910 476.296 8.307 o 26 3 3 384.921 730.922 262.869 38.781 o 26 3 4 8872.010 9506.170 491.452 7.014 o 26 3 5 1437.610 1142.140 210.506 44.956 o 26 3 6 3093.340 3174.590 256.813 24.827 o 26 3 7 4115.270 3648.210 237.529 23.505 o 26 3 8 152.224 232.392 172.327 91.939 o 26 4 0 8581.660 9531.320 820.661 3.506 o 26 4 1 1076.790 1298.970 309.083 26.135 o 26 4 2 1651.040 1493.730 207.344 42.894 o 26 4 3 6720.060 6403.470 489.645 8.163 o 26 4 4 697.996 847.012 197.796 58.311 o 26 4 5 3965.420 3959.670 803.022 4.183 o 26 4 6 2127.500 1985.130 541.563 9.112 o 26 4 7 423.449 441.571 171.235 82.539 o 26 4 8 3223.360 3998.720 677.379 5.755 o 26 5 1 4652.790 3408.750 508.034 8.949 o 26 5 3 813.259 797.559 273.137 34.090 o 26 5 4 1360.920 387.854 234.898 41.430 o 27 0 2 13472.100 15217.800 753.566 3.370 o 27 0 4 28394.700 33405.200 1003.010 1.555 o 27 0 6 12780.600 15431.000 865.734 2.828 o 27 0 8 887.830 655.528 207.584 53.120 o 27 1 0 22874.200 24925.500 843.000 2.207 o 27 1 1 12.425 64.318 119.774 202.068 o 27 1 2 13131.000 14628.700 414.491 6.237 o 27 1 3 19.444 191.728 128.767 168.126 o 27 1 4 115.805 725.180 173.863 84.646 o 27 1 5 112.854 307.115 195.140 73.161 o 27 1 6 15769.900 16526.500 472.878 4.952 o 27 1 7 47.937 -47.362 166.498 106.082 o 27 1 8 21793.200 19982.700 1119.860 1.653 o 27 1 9 319.548 -169.345 191.196 74.899 o 27 2 1 80.877 400.359 160.350 104.253 o 27 2 2 10221.800 11430.800 451.570 6.984 o 27 2 3 606.439 445.279 169.461 79.416 o 27 2 4 19498.400 21491.900 566.307 3.562 o 27 2 5 37.130 287.072 138.354 142.101 o 27 2 6 7210.140 7561.120 658.178 5.195 o 27 2 7 620.393 478.188 214.335 54.188 o 27 2 8 1103.200 1065.230 469.795 12.545 o 27 3 0 11528.700 12081.200 764.354 3.572 o 27 3 1 97.201 330.401 258.621 42.971 o 27 3 2 4787.390 4342.660 388.290 12.719 o 27 3 3 57.194 376.969 240.787 49.413 o 27 3 4 133.350 99.766 159.646 109.111 o 27 3 5 407.771 222.726 306.737 30.045 o 27 3 6 6733.840 5891.710 401.117 10.530 o 27 3 7 6.897 147.216 227.019 57.160 o 27 4 3 101.289 -382.391 262.211 42.886 o 28 0 0 25873.200 29825.800 1128.420 1.448 o 28 0 2 12298.900 12816.800 612.007 4.610 o 28 0 4 237.284 472.546 268.868 38.700 o 28 1 1 155.500 232.509 156.353 109.459 o 28 1 2 13294.300 14909.200 458.641 5.708 o 28 1 3 13.186 -43.808 141.330 148.897 o 28 1 4 18700.000 20079.000 672.034 3.198 o 28 1 5 123.188 -178.789 401.511 18.428 o 28 1 6 7256.240 9089.990 868.575 3.290 o 28 1 7 38.058 -726.544 202.121 72.591 o 28 2 0 16948.000 20224.700 975.808 2.141 o 28 2 1 608.046 450.348 224.905 50.232 o 28 2 2 8341.520 8853.320 435.089 8.302 o 28 2 3 978.898 832.026 343.385 22.482 o 28 2 4 211.464 453.434 203.838 64.733 o 28 2 5 55.278 486.183 327.764 27.072 o 28 2 6 9348.500 8227.000 1117.130 2.093 o 28 3 4 8259.010 9155.540 901.351 3.041 o 29 0 2 7908.360 9856.980 648.940 5.045 o 29 1 0 13824.500 15425.400 787.998 3.150 o 29 1 1 52.621 270.069 222.187 58.296 o 29 1 3 557.446 770.246 376.929 19.662 o ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 x+1/2,-y,-z+1/2 3 -x,y+1/2,-z+1/2 4 -x+1/2,-y+1/2,z 5 -x,-y,-z 6 -x-1/2,y,z-1/2 7 x,-y-1/2,z-1/2 8 x-1/2,y-1/2,-z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_disorder_group Au1 Au 0.323088(8) 0.20856(2) 0.183965(9) 0.02535(6) Uani 1.000000 . U . P1 P 0.38441(6) 0.34271(13) 0.10582(7) 0.0238(2) Uani 1.000000 . . . C1 C 0.2841(12) 0.065(3) 0.2606(12) 0.036267 Uani 0.500000 D U -1 C3 C 0.2479(5) -0.1119(9) 0.3716(5) 0.0411(12) Uani 0.500000 D U -1 H3a H 0.2836(5) -0.1385(9) 0.4033(5) 0.0494(15) Uiso 0.500000 R . -1 H3b H 0.2189(5) -0.0574(9) 0.4045(5) 0.0494(15) Uiso 0.500000 R . -1 C4 C 0.3656(2) 0.5342(5) 0.0851(3) 0.0276(10) Uani 1.000000 . . . C5 C 0.3352(2) 0.6163(6) 0.1399(3) 0.0296(10) Uani 1.000000 . . . H5 H 0.3208(2) 0.5701(6) 0.1850(3) 0.0355(12) Uiso 1.000000 R . . C6 C 0.3260(2) 0.7662(6) 0.1285(3) 0.0365(12) Uani 1.000000 . . . H6 H 0.3058(2) 0.8228(6) 0.1664(3) 0.0438(14) Uiso 1.000000 R . . C7 C 0.3460(3) 0.8341(6) 0.0629(3) 0.0390(13) Uani 1.000000 . . . H7 H 0.3396(3) 0.9369(6) 0.0558(3) 0.0468(15) Uiso 1.000000 R . . C8 C 0.3754(3) 0.7518(6) 0.0074(3) 0.0380(12) Uani 1.000000 . . . H8 H 0.3889(3) 0.7978(6) -0.0382(3) 0.0456(15) Uiso 1.000000 R . . C9 C 0.3850(3) 0.6019(6) 0.0187(3) 0.0352(12) Uani 1.000000 . . . H9 H 0.4051(3) 0.5453(6) -0.0193(3) 0.0422(14) Uiso 1.000000 R . . C10 C 0.4605(2) 0.3513(5) 0.1461(2) 0.0218(9) Uani 1.000000 . . . C11 C 0.4809(2) 0.2341(6) 0.1911(3) 0.0299(10) Uani 1.000000 . . . H11 H 0.4547(2) 0.1526(6) 0.2003(3) 0.0359(12) Uiso 1.000000 R . . C12 C 0.5388(2) 0.2354(6) 0.2222(3) 0.0339(11) Uani 1.000000 . . . H12 H 0.5524(2) 0.1545(6) 0.2522(3) 0.0407(14) Uiso 1.000000 R . . C13 C 0.5770(2) 0.3549(6) 0.2096(3) 0.0307(10) Uani 1.000000 . . . H13 H 0.6168(2) 0.3560(6) 0.2310(3) 0.0368(13) Uiso 1.000000 R . . C14 C 0.5573(2) 0.4720(6) 0.1661(3) 0.0313(11) Uani 1.000000 . . . H14 H 0.5835(2) 0.5540(6) 0.1577(3) 0.0376(13) Uiso 1.000000 R . . C15 C 0.4998(2) 0.4705(5) 0.1345(3) 0.0280(10) Uani 1.000000 . . . H15 H 0.4867(2) 0.5518(5) 0.1045(3) 0.0337(12) Uiso 1.000000 R . . C16 C 0.3945(2) 0.2568(5) 0.0128(3) 0.0250(10) Uani 1.000000 . . . C17 C 0.3443(3) 0.2490(6) -0.0357(3) 0.0367(12) Uani 1.000000 . . . H17 H 0.3062(3) 0.2889(6) -0.0198(3) 0.0440(14) Uiso 1.000000 R . . C18 C 0.3492(3) 0.1843(6) -0.1062(3) 0.0467(16) Uani 1.000000 . . . H18 H 0.3149(3) 0.1815(6) -0.1393(3) 0.0561(19) Uiso 1.000000 R . . C19 C 0.4039(3) 0.1234(6) -0.1291(3) 0.0465(15) Uani 1.000000 . . . H19 H 0.4070(3) 0.0771(6) -0.1775(3) 0.0558(18) Uiso 1.000000 R . . C20 C 0.4538(3) 0.1295(6) -0.0821(3) 0.0437(14) Uani 1.000000 . . . H20 H 0.4915(3) 0.0884(6) -0.0984(3) 0.0525(17) Uiso 1.000000 R . . C21 C 0.4496(2) 0.1962(5) -0.0103(3) 0.0317(11) Uani 1.000000 . . . H21 H 0.4841(2) 0.1998(5) 0.0222(3) 0.0380(13) Uiso 1.000000 R . . C2A C 0.2681(7) -0.0140(15) 0.3123(6) 0.0381(13) Uani 0.500000 D U -1 O O 0.2195(3) -0.2432(8) 0.3473(5) 0.0455(12) Uani 0.500000 D U -1 C2 C 0.2616(5) -0.3600(10) 0.3405(7) 0.0447(13) Uani 0.500000 D U -1 H2a H 0.2991(5) -0.3233(10) 0.3154(7) 0.0536(16) Uiso 0.500000 R . -1 H2b H 0.2728(5) -0.3956(10) 0.3918(7) 0.0536(16) Uiso 0.500000 R . -1 C1A C 0.2370(7) -0.4807(14) 0.2970(7) 0.0375(14) Uani 0.500000 D U -1 C1B C 0.2166(11) -0.573(3) 0.2549(13) 0.036267 Uani 0.500000 D U -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Au1 0.02112(9) 0.02892(10) 0.02602(9) 0.00069(7) -0.00022(7) -0.00204(7) P1 0.0248(6) 0.0241(6) 0.0226(5) 0.0013(5) -0.0020(4) -0.0006(4) C1 0.029320 0.041040 0.038440 0.007960 0.004450 -0.007030 C3 0.0413(16) 0.0415(13) 0.0406(14) 0.0001(4) 0.0001(4) -0.0002(4) C4 0.025(2) 0.027(2) 0.030(2) 0.0033(19) -0.0058(19) -0.0037(19) C5 0.022(2) 0.033(3) 0.033(2) 0.002(2) -0.0009(18) -0.002(2) C6 0.026(2) 0.032(3) 0.052(3) 0.005(2) -0.012(2) -0.013(2) C7 0.037(3) 0.027(3) 0.054(3) 0.007(2) -0.016(3) -0.002(2) C8 0.046(3) 0.031(3) 0.037(3) 0.003(2) -0.008(2) 0.009(2) C9 0.047(3) 0.033(3) 0.026(2) 0.009(2) -0.002(2) 0.002(2) C10 0.026(2) 0.023(2) 0.0159(19) 0.0041(18) -0.0019(16) -0.0026(16) C11 0.027(2) 0.033(3) 0.030(2) -0.004(2) -0.0005(19) 0.006(2) C12 0.027(3) 0.035(3) 0.040(3) 0.002(2) -0.005(2) 0.010(2) C13 0.025(2) 0.038(3) 0.030(2) 0.002(2) -0.0021(19) -0.004(2) C14 0.032(3) 0.030(3) 0.032(3) -0.007(2) 0.003(2) -0.002(2) C15 0.031(3) 0.024(2) 0.029(2) -0.0007(19) -0.0006(19) 0.0020(18) C16 0.033(3) 0.020(2) 0.022(2) -0.0032(19) -0.0030(18) 0.0025(16) C17 0.041(3) 0.032(3) 0.037(3) -0.005(2) -0.008(2) 0.002(2) C18 0.076(4) 0.033(3) 0.031(3) -0.014(3) -0.028(3) 0.005(2) C19 0.090(5) 0.026(3) 0.024(2) -0.002(3) -0.007(3) -0.002(2) C20 0.069(4) 0.031(3) 0.031(3) 0.009(3) 0.005(3) -0.004(2) C21 0.042(3) 0.027(2) 0.026(2) 0.006(2) -0.000(2) -0.0009(19) C2A 0.0372(17) 0.0391(15) 0.0380(14) 0.0011(4) 0.0005(4) -0.0026(4) O 0.0457(14) 0.0439(12) 0.0469(15) -0.0005(4) -0.0007(4) -0.0010(4) C2 0.0453(15) 0.0438(13) 0.0449(16) -0.0003(4) -0.0008(4) -0.0019(4) C1A 0.0377(17) 0.0379(14) 0.0369(16) 0.0016(4) 0.0005(4) 0.0003(4) C1B 0.029320 0.041040 0.038440 0.007960 0.004450 -0.007030 loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.0030380000826 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' C 0.00347 0.00161 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.215599998832 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' Au -1.84508 8.87037 16.88190 18.59130 25.55820 5.86000 0.46110 8.62160 1.48260 36.39560 12.0657997131 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' O 0.01158 0.00611 3.04850 2.28680 1.54630 0.86700 13.27710 5.70110 0.32390 32.90890 0.250800013542 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' P 0.10434 0.09671 6.43450 4.17910 1.78000 1.49080 1.90670 27.15700 0.52600 68.16450 1.11489999294 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u 0 1 0 1.39 0.14 0 -1 0 1.15 0.18 0 -1 0 1.23 0.12 0 1 0 0.97 0.12 0 1 0 1.05 0.12 0 2 0 906.5 16.25 0 -2 0 889.38 16.25 0 2 0 948.78 15.94 0 -2 0 863.92 17.29 0 2 0 941.72 15.89 0 3 0 0.08 0.18 0 -3 0 0.18 0.15 0 3 0 0.14 0.18 0 3 0 0.39 0.31 0 4 0 102.52 2.49 0 -4 0 96.82 3.1 0 -4 0 99.1 2.56 0 4 0 103.45 2.82 0 -5 0 -0.02 0.19 0 5 0 0.26 0.44 0 -5 0 0.39 0.54 0 5 0 -0.21 0.18 0 6 0 0.17 0.55 0 -6 0 0.77 0.72 0 6 0 0.54 0.29 0 -6 0 0.51 0.34 0 7 0 -0.5 0.55 0 -7 0 0.29 0.72 0 -7 0 0.4 0.34 0 7 0 0.16 0.32 0 -8 0 6.86 0.97 0 8 0 7.31 1.21 0 -8 0 7.11 1.36 0 -9 0 -0.69 0.59 0 9 0 0.09 0.59 0 -10 0 15.83 1.65 0 10 0 15.1 1.78 0 11 0 0.25 0.56 0 -11 0 1.05 0.7 0 12 0 19.13 1.75 0 -12 0 17.52 1.77 0 0 -1 0 0.01 0 1 -1 0.06 0.08 0 1 1 0.02 0.06 0 -1 -1 0.17 0.1 0 -1 -1 0.18 0.07 0 -1 1 0.2 0.08 0 1 -1 0.19 0.07 0 1 -1 0.12 0.06 0 1 1 0.26 0.07 0 1 1 0.33 0.09 0 2 1 -0.19 0.24 0 -2 -1 -0.09 0.19 0 -2 1 0.06 0.32 0 2 -1 -0.08 0.27 0 2 1 0.03 0.18 0 2 -1 0.26 0.2 0 2 1 -0.09 0.17 0 -2 -1 -0.02 0.35 0 -2 1 -0.05 0.16 0 -3 1 -0.13 0.13 0 -3 -1 0.65 0.43 0 3 1 0.05 0.18 0 3 1 -0.21 0.18 0 -3 -1 0.15 0.17 0 3 -1 -0.14 0.16 0 3 -1 -0.06 0.29 0 3 1 0.17 0.28 0 -3 1 -0.12 0.32 0 4 1 0.21 0.21 0 -4 1 0.28 0.45 0 -4 1 0.09 0.21 0 4 -1 0.04 0.18 0 -4 -1 0.2 0.48 0 -4 -1 0.09 0.22 0 4 -1 0.02 0.33 0 4 1 -0.11 0.21 0 4 1 -0.11 0.33 0 -5 1 0.26 0.56 0 -5 -1 -0.18 0.48 0 5 1 0.65 0.31 0 5 -1 0.37 0.45 0 5 1 -0.6 0.34 0 5 -1 0.24 0.22 0 -5 1 -0.05 0.22 0 -5 -1 0.08 0.2 0 6 -1 0.6 0.27 0 -6 -1 0.51 0.3 0 -6 -1 0.34 0.62 0 6 1 0.07 0.48 0 -6 1 -0.13 0.57 0 6 -1 -0.26 0.51 0 -6 1 -0.49 0.27 0 7 -1 -0.61 0.6 0 -7 -1 -0.05 0.29 0 -7 1 -0.11 0.69 0 7 1 -0.36 0.32 0 -7 1 -0.02 0.3 0 -7 -1 -0.12 0.69 0 7 1 0.35 0.63 0 -8 -1 -0.58 0.63 0 8 1 -0.19 0.55 0 -8 1 0.33 0.42 0 -8 1 -0.36 0.65 0 8 -1 -0.34 0.61 0 9 -1 0.02 0.61 0 -9 1 1.19 0.71 0 -9 -1 -0.26 0.68 0 9 1 1.01 0.67 0 -10 1 1.58 0.66 0 10 1 0.19 0.61 0 10 -1 0.14 0.58 0 -10 -1 1.09 0.79 0 -11 -1 0.82 0.71 0 11 -1 -0.43 0.57 0 11 1 -0.14 0.57 0 -11 1 1.15 0.65 0 12 1 0.26 0.63 0 -12 -1 -0.51 0.64 0 0 -2 222.92 4.07 0 0 -2 220.79 4.04 0 0 -2 222.83 4.12 0 0 -2 225.91 4.32 0 1 -2 376.88 6.77 0 -1 -2 367.8 6.52 0 -1 -2 355.72 7.09 0 1 -2 357.6 6.38 0 1 -2 356.98 6.67 0 -1 -2 368.25 6.59 0 1 2 374.63 6.54 0 -1 2 354.65 6.93 0 -2 -2 78.94 2.18 0 2 2 73.85 1.78 0 2 2 71.58 1.74 0 -2 2 69.81 1.78 0 2 -2 71.08 1.58 0 2 2 70.88 1.74 0 2 -2 72.62 1.91 0 -2 2 73.04 1.97 0 3 2 144.44 3.3 0 -3 -2 149.96 3.23 0 3 -2 146.67 3.01 0 3 2 147.24 3.2 0 3 -2 149.84 3.48 0 -3 -2 142.12 3.8 0 3 2 146.82 3.21 0 -3 2 143.59 3.27 0 -4 2 36.64 1.69 0 4 -2 39.14 1.64 0 4 2 38.99 1.41 0 4 2 40.07 1.55 0 4 -2 39.71 1.26 0 -4 -2 40.77 1.43 0 -4 -2 37.76 1.86 0 -4 2 40.31 1.45 0 4 2 39.36 1.41 0 -5 -2 4.88 0.94 0 -5 2 4.77 0.63 0 5 2 5.62 0.68 0 5 2 5.54 0.81 0 -5 2 4.24 0.84 0 -5 -2 5.82 0.71 0 5 2 4.85 0.64 0 5 -2 6.13 0.52 0 5 -2 5.03 0.83 0 -6 -2 0.28 0.65 0 -6 -2 0.43 0.27 0 -6 2 0.63 0.37 0 6 -2 0.33 0.26 0 6 2 -0.41 0.32 0 -6 2 -0.29 0.54 0 6 2 -0.28 0.49 0 6 -2 0.09 0.49 0 -7 -2 18.1 1.73 0 7 2 16.02 1.44 0 7 -2 16.65 1.49 0 7 2 18.41 1.18 0 -7 2 17.99 1.22 0 -7 -2 16.63 1.16 0 -7 2 18.05 1.66 0 8 2 13.89 1.53 0 -8 -2 15.57 1.92 0 -8 2 13.01 1.09 0 8 -2 11.99 1.51 0 -8 2 13.44 1.71 0 8 2 13.79 1.09 0 -9 2 8.6 1.41 0 -9 -2 9.17 1.63 0 9 2 9.16 1.33 0 9 -2 9.58 1.42 0 -10 -2 19.07 1.87 0 10 2 19.15 1.64 0 10 -2 17.96 1.68 0 -10 2 20.08 1.81 0 -11 2 9.21 1.44 0 11 -2 12.01 1.64 0 -11 -2 12.41 1.76 0 11 2 9.53 1.35 0 12 2 15.68 1.88 0 -12 -2 16.09 1.68 0 0 -3 0.69 0.17 0 0 -3 0.68 0.16 0 0 -3 0.36 0.14 0 0 -3 0.25 0.12 0 -1 -3 0.17 0.21 0 1 -3 0.15 0.19 0 -1 3 0.2 0.14 0 1 -3 0.16 0.14 0 -1 -3 0.24 0.14 0 -1 -3 0.53 0.21 0 1 3 0.16 0.12 0 1 -3 0.38 0.22 0 -2 -3 0.42 0.33 0 2 -3 -0.11 0.19 0 2 3 0.37 0.23 0 -2 3 0.23 0.28 0 2 -3 0.59 0.29 0 2 -3 -0.2 0.25 0 -2 -3 0.24 0.19 0 2 3 0.05 0.21 0 2 3 -0.13 0.22 0 3 3 0.3 0.23 0 -3 -3 0.18 0.19 0 3 3 0.19 0.25 0 -3 -3 -0.03 0.35 0 -3 3 0.04 0.19 0 3 3 0.2 0.2 0 -3 3 0.66 0.33 0 3 -3 0.58 0.2 0 3 -3 0.44 0.31 0 -4 -3 -0.32 0.25 0 4 3 0.02 0.27 0 -4 -3 -0.05 0.44 0 -4 3 -0.13 0.27 0 4 3 0.24 0.28 0 4 3 -0.02 0.31 0 4 -3 0.06 0.39 0 4 -3 0.55 0.21 0 -4 3 -0.39 0.35 0 5 3 0.12 0.3 0 -5 -3 0.01 0.5 0 5 -3 -0.09 0.43 0 -5 3 0.11 0.29 0 5 -3 -0.14 0.16 0 -5 3 -0.31 0.43 0 5 3 0.07 0.41 0 -5 -3 0.38 0.28 0 5 3 0.37 0.32 0 -6 -3 0.89 0.7 0 -6 -3 -0.33 0.24 0 6 3 -0.1 0.33 0 6 3 0.37 0.55 0 6 -3 0.07 0.2 0 -6 3 0.1 0.34 0 6 3 -0.33 0.3 0 6 -3 0.05 0.52 0 -6 3 -0.61 0.51 0 7 3 0.41 0.6 0 -7 3 0.1 0.71 0 7 -3 0 0.68 0 7 3 0.18 0.41 0 -7 3 -0.07 0.4 0 -7 -3 -0.27 0.72 0 -8 3 0.62 0.43 0 8 3 0.05 0.35 0 -8 3 0.66 0.74 0 8 3 -0.49 0.52 0 -8 -3 -0.81 0.72 0 8 -3 0.07 0.61 0 9 -3 0.21 0.55 0 9 3 -0.15 0.59 0 -9 -3 -1.11 0.59 0 -9 3 0.04 0.34 0 -9 3 1.06 0.75 0 -10 -3 0.08 0.64 0 10 -3 0.72 0.67 0 10 3 -0.01 0.49 0 -10 3 0.78 0.56 0 11 -3 -0.16 0.5 0 11 3 -0.09 0.53 0 -11 -3 1.72 0.73 0 0 -4 70.83 1.79 0 0 -4 71.69 1.72 0 0 -4 71.67 1.67 0 0 -4 68.4 1.66 0 1 -4 988.27 17.69 0 -1 -4 993.67 17.37 0 -1 -4 973.44 17.3 0 -1 4 951.76 18.19 0 1 4 977.34 17.2 0 1 -4 1000 17.07 0 1 -4 967.88 17.43 0 -1 -4 976.01 18.45 0 2 4 3.3 0.37 0 -2 4 3.03 0.41 0 -2 -4 3.71 0.58 0 -2 -4 3.43 0.34 0 2 -4 3.1 0.3 0 2 -4 3.04 0.48 0 2 -4 3.66 0.5 0 -3 4 223.65 5.1 0 3 4 232.39 4.82 0 -3 -4 224.02 5.47 0 3 -4 239.57 4.47 0 3 4 232.86 4.75 0 3 -4 229.63 5.07 0 3 4 230.73 4.82 0 -3 4 231.91 4.91 0 -4 4 18.42 1.15 0 4 4 17.44 1.03 0 -4 4 16.44 1 0 4 4 19.4 1.04 0 4 -4 17.46 1.18 0 4 4 17.62 1.02 0 -4 -4 18.32 0.91 0 4 -4 17.72 0.81 0 -4 -4 18.69 1.41 0 5 4 35.76 1.61 0 -5 -4 32.93 1.41 0 -5 4 35.59 1.56 0 5 -4 33.06 1.25 0 5 4 34.24 1.52 0 -5 4 36.16 1.8 0 5 4 35.79 1.52 0 -5 -4 38.54 2.08 0 5 -4 34.36 1.75 0 6 4 17.01 1.31 0 6 4 15.8 1.15 0 6 -4 16.75 1.41 0 -6 4 17.61 1.19 0 -6 -4 15.36 1.58 0 -6 -4 13.94 1.03 0 -6 4 18.28 1.5 0 6 4 17.17 1.19 0 7 4 11.32 1.06 0 -7 4 9.44 1.14 0 7 4 11.7 1.32 0 7 4 8.34 1.05 0 -7 -4 11.14 1.59 0 7 -4 10.31 1.38 0 -7 4 10.38 1.42 0 8 4 -0.26 0.56 0 -8 4 1.34 0.69 0 -8 -4 -0.54 0.62 0 -8 4 0.88 0.41 0 8 -4 0.74 0.64 0 8 4 0.35 0.43 0 9 4 20.67 1.67 0 -9 -4 21.75 2.01 0 -9 4 22.62 1.83 0 -9 4 18.9 1.4 0 9 -4 20.62 1.77 0 -10 -4 1.27 0.79 0 10 -4 -0.47 0.58 0 -10 4 0.2 0.6 0 10 4 -0.24 0.48 0 -11 -4 40.98 2.8 0 11 -4 39.04 2.54 0 0 -5 0.08 0.21 0 0 -5 -0.07 0.2 0 0 -5 0.07 0.22 0 0 -5 0.01 0.21 0 -1 -5 0.25 0.22 0 1 -5 0.08 0.2 0 -1 -5 0.29 0.18 0 1 5 0.14 0.14 0 -1 -5 0.47 0.26 0 -1 5 0.09 0.19 0 1 -5 0.07 0.24 0 1 -5 0.04 0.18 0 2 -5 0.11 0.27 0 -2 -5 0.03 0.28 0 2 5 0.21 0.16 0 2 5 -0.11 0.21 0 -2 5 0.14 0.21 0 -2 -5 -0.05 0.14 0 2 -5 0.08 0.22 0 2 5 -0.11 0.24 0 2 -5 0.26 0.14 0 3 5 -0.11 0.25 0 -3 -5 -0.11 0.33 0 3 -5 -0.04 0.27 0 -3 5 -0.27 0.24 0 3 5 -0.45 0.19 0 3 -5 0.34 0.36 0 -3 -5 0.01 0.15 0 3 -5 0.03 0.13 0 3 5 0.5 0.31 0 -4 5 -0.04 0.36 0 -4 -5 -0.43 0.41 0 4 5 0.01 0.33 0 -4 5 -0.02 0.28 0 4 5 -0.56 0.28 0 4 5 0.05 0.31 0 4 -5 0.36 0.16 0 4 -5 0.2 0.4 0 -4 -5 0.11 0.17 0 5 -5 0.72 0.24 0 -5 5 -0.34 0.31 0 5 5 0 0.4 0 5 -5 -0.15 0.46 0 5 5 0.14 0.42 0 5 5 0.05 0.39 0 -5 -5 0.66 0.22 0 -5 -5 0.17 0.54 0 -5 5 0.27 0.49 0 6 5 -0.27 0.41 0 6 -5 -0.1 0.51 0 -6 5 0.07 0.38 0 6 5 0.08 0.51 0 6 5 0.06 0.41 0 -6 5 -0.84 0.52 0 -6 -5 -0.03 0.67 0 -7 -5 0.33 0.77 0 -7 5 -0.11 0.4 0 7 5 0.05 0.49 0 -7 5 -0.59 0.59 0 7 5 0.2 0.49 0 7 -5 0.26 0.65 0 7 5 0.27 0.61 0 8 -5 0.18 0.57 0 -8 -5 -0.73 0.58 0 -8 5 0.3 0.65 0 8 5 0.39 0.63 0 8 5 -0.33 0.39 0 -8 5 0.18 0.44 0 -9 -5 -0.39 0.68 0 9 5 0.57 0.57 0 -9 5 1.37 0.72 0 9 5 0.09 0.36 0 9 -5 0.36 0.57 0 -9 5 0.38 0.39 0 10 5 0.65 0.55 0 -10 -5 0.18 0.7 0 10 -5 -0.4 0.54 0 11 -5 0.03 0.56 0 -11 -5 0.24 0.61 0 0 -6 430.54 8.31 0 0 -6 439.1 8.19 0 0 -6 431.57 8.15 0 0 -6 441.5 8.73 0 -1 -6 176.39 4.12 0 1 -6 170.02 3.8 0 1 6 172.4 3.56 0 -1 -6 180.92 3.69 0 1 -6 173.86 3.92 0 1 -6 181.68 3.97 0 1 -6 180.52 3.62 0 -1 -6 179.95 3.85 0 -2 6 269.19 5.77 0 2 -6 271.92 5.85 0 -2 -6 261.83 5.61 0 -2 -6 278.55 6.17 0 2 -6 279.48 5.22 0 2 6 280.69 5.35 0 -2 -6 278.02 5.31 0 2 -6 274.08 5.73 0 -3 -6 106.02 2.36 0 3 6 100.96 2.76 0 -3 -6 102.88 3.2 0 -3 6 104.52 2.83 0 3 -6 101 2.92 0 3 -6 104.31 2.98 0 3 -6 104.49 2.26 0 3 6 107.44 2.79 0 3 6 109.22 2.59 0 4 6 121.53 3.03 0 -4 -6 112.65 3.72 0 -4 -6 121.72 2.72 0 4 6 120.38 3.21 0 -4 6 117.03 3.29 0 4 6 116.01 3.16 0 4 -6 113.97 3.4 0 -4 6 119.27 3.23 0 4 -6 122.48 2.59 0 -5 -6 15.73 1.49 0 -5 6 14.84 1.21 0 5 6 16.12 1.11 0 5 6 15.34 1.13 0 -5 -6 15 0.79 0 -5 6 14.27 1.09 0 5 -6 14.7 1.26 0 5 6 14.77 1.13 0 -6 -6 6.99 1.3 0 6 6 6.64 0.97 0 6 -6 5.77 1.07 0 -6 6 8.32 1.16 0 6 6 7.29 0.99 0 -6 6 6.42 0.95 0 6 6 6.27 0.96 0 -7 6 -0.14 0.58 0 7 -6 0.93 0.68 0 7 6 -0.02 0.49 0 7 6 0.25 0.61 0 -7 -6 1.25 0.91 0 7 6 0.25 0.49 0 -7 6 -0.52 0.42 0 8 6 3.09 0.73 0 -8 -6 3.45 1.06 0 8 6 5.5 0.96 0 -8 6 4.19 0.93 0 8 6 3.27 0.71 0 -8 6 3.78 0.76 0 8 -6 4.39 1.05 0 -9 -6 14.51 1.93 0 9 -6 13.96 1.78 0 -9 6 12.51 1.1 0 9 6 14.01 1.35 0 9 6 14.02 1.21 0 -9 6 15.31 1.5 0 -10 -6 29.21 2.37 0 -10 6 25.3 1.61 0 10 -6 24.54 2.01 0 -11 -6 16.6 2.22 0 11 -6 14.98 1.93 0 0 -7 0.48 0.24 0 0 -7 0.11 0.18 0 0 -7 -0.38 0.17 0 0 -7 0.2 0.21 0 1 -7 0 0.24 0 1 7 0 0.17 0 1 -7 0.25 0.17 0 1 -7 0.13 0.26 0 -1 -7 0.03 0.24 0 1 -7 0.36 0.24 0 -1 -7 -0.19 0.22 0 -1 -7 0.09 0.17 0 2 -7 0.14 0.13 0 -2 -7 0.24 0.31 0 -2 -7 0.1 0.16 0 2 7 -0.08 0.17 0 2 -7 0.37 0.32 0 2 -7 0.41 0.34 0 -2 -7 0.2 0.35 0 -2 7 0.29 0.25 0 3 7 0.48 0.37 0 3 -7 0.49 0.4 0 3 7 -0.36 0.31 0 3 -7 0.03 0.13 0 -3 7 0.06 0.31 0 -3 -7 0.34 0.41 0 3 7 -0.01 0.21 0 -3 -7 0.02 0.13 0 3 -7 -0.34 0.35 0 -4 7 -0.58 0.3 0 -4 7 -0.02 0.34 0 -4 -7 -0.31 0.42 0 4 7 -0.12 0.36 0 -4 -7 0.13 0.13 0 4 -7 0 0.42 0 4 7 -0.37 0.36 0 4 7 -0.03 0.28 0 4 -7 0.02 0.11 0 5 -7 -0.06 0.52 0 -5 7 0.09 0.4 0 5 7 -0.64 0.36 0 -5 -7 0.08 0.62 0 5 7 0.19 0.42 0 -5 7 0.83 0.49 0 5 7 0.32 0.47 0 6 7 0.84 0.56 0 -6 -7 0.38 0.72 0 -6 7 0.05 0.49 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0.65 0.68 25 0 -7 1.66 0.66 -25 0 7 0.75 0.34 -25 1 7 0.2 0.33 -25 -1 -7 0.22 0.66 25 1 -7 0.11 0.65 25 -1 -7 -0.28 0.54 25 1 7 0.38 0.55 -25 1 -7 -0.74 0.57 -25 -1 7 0.27 0.32 25 2 -7 4.83 0.96 25 -2 7 5.34 0.95 -25 -2 -7 6.08 1.24 -25 2 7 4.29 0.73 25 -2 -7 4.96 1.07 -25 -2 7 2.19 0.85 25 2 7 5.12 1.05 -25 2 -7 4.32 1.02 -25 -3 -7 -0.13 0.85 -25 3 7 0.22 0.4 25 -3 7 0.53 0.37 25 3 -7 0.42 0.54 25 -3 -7 1.36 0.62 -25 -3 7 0.41 0.63 25 3 7 1.65 0.75 -25 3 -7 0.98 0.66 -25 4 7 24.71 1.82 25 -4 7 22.3 1.71 -25 4 -7 24.5 1.82 25 -4 -7 23.79 2.01 -25 -4 7 24.59 2.02 25 4 7 24.34 2.13 -25 0 -8 0.91 0.68 -25 0 8 0.21 0.35 25 0 -8 0.65 0.59 -25 -1 -8 18.5 1.8 25 1 -8 14.67 1.94 -25 1 8 14.63 1.16 -25 -1 8 13.61 1.09 25 1 8 16.31 1.59 25 -1 -8 13.37 1.8 -25 1 -8 15.37 1.87 25 -2 8 -0.61 0.35 -25 2 8 -0.62 0.36 25 2 -8 1 0.6 -25 -2 -8 0.85 0.62 -25 -2 8 0.48 0.34 25 2 8 0 0.56 25 -2 -8 1.32 0.7 -25 2 -8 0.19 0.62 -25 -3 -8 6.86 1.29 25 3 -8 5.88 1.1 -25 3 8 5.25 0.86 25 -3 8 4.71 0.85 -25 3 -8 5.31 1.08 25 -3 -8 4.81 1.07 -25 -3 8 4.98 1.02 25 3 8 5.45 1.1 25 -4 8 -1.16 0.4 25 -4 -8 0.47 0.53 -25 4 -8 0.86 0.55 -25 -4 8 0.03 0.62 25 -5 -8 -0.07 0.51 -25 0 -9 -0.67 0.66 -25 0 9 0.03 0.39 25 0 -9 -0.56 0.51 25 -1 9 0.5 0.36 -25 -1 -9 -0.06 0.67 -25 1 9 -0.26 0.44 25 1 -9 -0.01 0.75 25 -1 -9 -1.06 0.61 -25 1 -9 0.82 0.72 -25 -1 9 0.45 0.35 -25 2 9 7.12 0.95 25 2 -9 9.26 1.44 25 -2 9 7.23 1.11 -25 -2 -9 7.27 1.3 -25 -2 9 7.61 0.71 25 2 9 10.73 1.51 25 -2 -9 9.42 1.51 -25 2 -9 7.62 1.3 25 -3 9 2 0.58 -25 3 9 1.69 0.48 25 -3 -9 2.1 0.74 -25 3 -9 2.64 0.75 -25 -3 9 3.88 0.83 -25 -3 9 0.49 0.33 25 3 9 3.52 0.99 -25 4 -9 18.1 1.6 -25 -4 9 13.66 1.75 25 0 -10 10.02 1.65 -25 0 10 8.15 1 -25 0 -10 5.6 1.29 -25 1 10 1.19 0.43 25 -1 10 1.01 0.44 -25 -1 10 0.78 0.43 25 -1 -10 0.86 0.66 -25 1 -10 1.68 0.89 -25 2 10 3.5 0.63 25 -2 10 3.14 0.67 -25 2 -10 5.25 1.14 -25 -2 10 3.92 0.61 25 2 10 4.3 0.94 25 -3 10 0.59 0.37 -25 -3 10 0.18 0.34 25 3 10 1.2 0.63 -25 0 11 -0.15 0.37 25 0 11 -0.43 0.35 25 -1 11 0.57 0.36 -25 -1 11 -0.16 0.34 25 -2 11 0.54 0.34 25 0 12 3.37 0.68 -26 0 0 27.51 1.94 26 0 0 28.65 2.09 -26 -1 0 0.17 0.63 26 -1 0 0.97 0.61 26 1 0 1.07 0.63 26 2 0 25.81 2.1 26 -2 0 26 1.87 -26 -2 0 22.67 1.9 -26 -3 0 -0.37 0.55 26 3 0 0.53 0.75 -26 -4 0 17.82 2.1 26 4 0 17.04 2.15 -26 0 -1 -0.2 0.61 26 0 -1 0.25 0.61 -26 0 1 0.76 0.65 26 0 1 0.08 0.55 26 1 -1 2.29 0.85 26 -1 1 1.67 0.66 -26 -1 -1 1.59 0.75 -26 -1 1 3.32 0.89 26 -1 -1 1.08 0.68 26 1 1 1.72 0.77 -26 1 -1 3.03 0.83 26 2 -1 1.04 0.73 -26 -2 -1 1.34 0.71 -26 -2 1 0.57 0.56 26 -2 -1 1.46 0.61 26 2 1 0.1 0.63 26 3 -1 8.06 1.45 -26 -3 -1 10.59 1.6 26 3 1 9.91 1.61 -26 -3 1 12.64 1.67 -26 -4 -1 3.89 1.04 26 4 -1 1.46 0.83 26 4 1 2.73 0.84 -26 -4 1 1.24 0.98 -26 5 1 6.24 0.93 26 0 2 21.67 1.79 26 0 -2 21.81 1.88 -26 0 2 24.34 1.8 -26 0 -2 25.5 1.92 26 1 -2 12.73 1.71 26 -1 2 11.61 1.5 -26 -1 -2 11.92 1.61 26 1 2 14.53 1.82 -26 -1 2 11.85 1.49 26 -1 -2 13.83 1.72 -26 1 -2 12.61 1.53 -26 -2 -2 12.29 1.63 26 2 -2 19.4 1.83 26 -2 -2 16.1 1.54 -26 -2 2 17.02 1.63 26 2 2 14.09 1.86 26 3 -2 15.33 1.99 -26 -3 -2 13.39 1.72 26 3 2 13.19 1.77 -26 -3 2 12.15 1.57 -26 4 2 2.14 0.5 -26 -4 -2 3.96 1.01 26 4 -2 3.39 1.04 -26 -4 2 3.13 0.92 26 4 2 1.81 0.87 26 0 -3 -0.78 0.53 -26 0 -3 0.32 0.6 26 0 3 1.04 0.58 -26 -1 -3 1.04 0.7 26 1 -3 -1.02 0.43 -26 1 -3 0.81 0.62 26 1 3 0.34 0.65 26 -1 -3 0.34 0.56 -26 -1 3 0.1 0.54 26 2 -3 5.19 1.15 -26 -2 -3 5.09 1.09 -26 -2 3 4 0.96 -26 2 -3 2.34 0.77 26 2 3 4.73 1.1 26 -2 -3 4.99 1.08 -26 3 3 2.45 0.47 -26 -3 -3 3.13 1.09 26 3 -3 0.05 0.65 -26 -3 3 0.23 0.63 26 -3 -3 0.53 0.53 26 3 3 0.99 0.71 -26 -4 -3 12.12 1.82 -26 4 3 9.82 1.17 26 4 3 15.42 2.09 -26 -4 3 11.51 1.68 -26 5 3 1.46 0.5 26 0 -4 1.5 0.76 -26 0 -4 -0.26 0.6 26 0 4 0.44 0.55 -26 -1 -4 36.44 2.45 26 1 -4 35.87 2.5 26 1 4 38.2 2.4 -26 -1 4 36.55 2.25 -26 1 -4 37.56 2.33 26 -1 -4 37.55 2.5 -26 2 4 0.97 0.38 -26 -2 -4 1.24 0.72 26 2 -4 0.78 0.69 26 2 4 0.92 0.74 -26 -2 4 0.11 0.58 26 -2 -4 0.64 0.59 -26 2 -4 1.28 0.58 -26 3 4 14.7 1.22 26 3 -4 18.13 2.22 -26 -3 -4 14.58 1.93 26 -3 -4 17.39 1.57 26 3 4 20.55 1.9 -26 -3 4 20.06 1.76 -26 4 4 1.84 0.48 26 4 4 0.7 0.78 -26 -4 4 1.8 0.78 26 -5 4 0.71 0.43 26 0 -5 -0.32 0.61 26 0 5 -0.34 0.55 -26 0 -5 0.43 0.62 -26 -1 -5 1.15 0.65 26 1 -5 1.14 0.81 -26 1 5 0.26 0.32 26 1 5 0.1 0.51 -26 1 -5 1.7 0.72 26 -1 -5 0.27 0.55 -26 -2 -5 3.65 1.03 -26 2 5 2.86 0.55 26 2 -5 2.31 0.88 26 2 5 4.56 1.16 -26 2 -5 2.5 0.81 -26 -2 5 2.97 0.78 26 -2 -5 2.51 0.91 -26 3 5 1.31 0.42 26 3 -5 2.73 0.95 -26 -3 -5 0.95 0.8 -26 -3 5 1.55 0.66 26 -3 -5 3.81 0.84 26 3 5 2.44 0.85 -26 4 5 6.32 0.87 -26 -4 5 9.26 1.55 26 0 -6 24.87 2.12 -26 0 -6 30.26 2.21 -26 0 6 33.03 1.78 -26 1 6 19.39 1.39 26 1 -6 15.99 2.05 -26 -1 -6 20 1.85 -26 1 -6 23.39 1.88 26 1 6 24.67 1.95 26 -1 -6 20.52 1.86 -26 -2 -6 23.74 2.03 -26 2 6 25.56 1.61 26 2 -6 24.37 2.09 -26 -2 6 25.14 1.86 26 2 6 26.14 2.08 -26 2 -6 22.91 1.86 26 -2 -6 24.23 1.97 -26 -3 -6 6.5 1.29 -26 3 6 4.99 0.71 -26 3 -6 6.08 1 26 3 6 8.06 1.42 -26 -3 6 4.06 0.96 26 -3 -6 6.34 1.15 26 -4 6 4.43 0.68 -26 -4 6 4.55 1.06 26 -4 -6 1.14 0.66 -26 0 7 0.21 0.35 -26 0 -7 -0.03 0.56 26 0 -7 1.45 0.67 26 1 -7 0.99 0.72 -26 1 7 0.93 0.42 -26 -1 -7 1.16 0.73 -26 1 -7 1.87 0.79 26 1 7 0.72 0.59 26 -1 -7 0.83 0.75 26 2 -7 0 0.59 -26 2 7 0.86 0.42 -26 -2 -7 1.93 0.78 -26 2 -7 1.47 0.63 26 2 7 0.73 0.6 26 -2 -7 -0.52 0.62 -26 3 7 4.84 0.76 26 -3 7 6.77 0.93 26 -3 -7 7.73 1.31 26 3 7 7.52 1.42 -26 3 -7 7.41 1.21 -26 -3 7 7.34 1.25 26 -4 7 0.87 0.37 26 -4 -7 0.71 0.59 -26 0 8 33.84 1.92 26 0 -8 37.08 2.6 -26 0 -8 38.18 2.63 -26 -1 -8 2.56 0.82 -26 1 8 2.25 0.47 26 1 -8 4.71 1.11 -26 1 -8 1.84 0.84 26 -1 -8 3.79 0.99 -26 -1 8 2.83 0.44 -26 2 8 17.61 1.36 -26 2 -8 19.19 1.75 26 2 8 21.16 1.97 26 -2 -8 20.09 1.9 26 -3 8 -0.13 0.35 -26 3 -8 -0.29 0.57 26 -3 -8 0.53 0.61 -26 -3 8 1.64 0.66 26 3 8 0.99 0.68 -26 4 -8 7.32 1.24 -26 0 9 0.02 0.53 -26 1 9 0.33 0.37 -26 1 -9 0.44 0.67 -26 -1 9 -0.05 0.37 26 -2 9 0.4 0.35 26 2 9 1.39 0.72 -26 2 -9 1.39 0.7 -26 -2 9 1.01 0.39 -26 -1 10 19.05 1.31 26 -2 10 5.18 0.63 -27 0 0 1.37 0.64 27 0 0 2.07 0.73 27 1 0 42.57 2.64 27 -1 0 47.99 2.71 -27 -1 0 46.13 2.67 -27 -2 0 -0.81 0.52 27 2 0 0.63 0.69 27 3 0 21.66 2.02 -27 -3 0 22.52 1.94 -27 0 -1 0.27 0.6 27 0 -1 0.26 0.56 -27 0 1 0.57 0.63 27 0 1 1.36 0.65 -27 -1 -1 0.46 0.61 27 -1 1 0.2 0.57 27 1 -1 -0.74 0.5 27 -1 -1 0.97 0.62 27 1 1 -0.35 0.61 -27 1 -1 0.71 0.64 -27 -1 1 -0.17 0.55 27 2 -1 0.87 0.72 -27 -2 -1 0.97 0.74 27 -2 -1 0.52 0.58 27 2 1 -0.09 0.6 -27 -2 1 1.58 0.69 -27 -3 -1 -0.56 0.64 27 3 -1 0.97 0.67 27 3 1 2.01 0.81 -27 -3 1 0.26 0.75 27 0 2 24.98 1.93 27 0 -2 29.9 2.17 -27 0 -2 28.79 2.06 -27 -1 -2 26.04 1.99 27 -1 2 26.74 1.97 27 1 -2 27.1 2.17 27 1 2 25.18 2.04 -27 1 -2 27.92 1.93 27 -1 -2 24.06 1.95 -27 -1 2 29.77 2.03 -27 -2 -2 21.02 1.86 27 2 -2 19.82 1.96 27 -2 -2 20.61 1.71 -27 -2 2 19.62 1.73 27 2 2 23.74 2.05 27 3 -2 7.35 1.41 -27 -3 -2 7.61 1.43 -27 -3 2 7.61 1.3 27 3 2 9.31 1.59 27 0 3 1.98 0.71 27 0 -3 0.05 0.68 -27 0 -3 -0.12 0.57 27 1 -3 0.5 0.64 -27 -1 -3 0.34 0.6 -27 -1 3 -0.1 0.51 27 -1 -3 0.17 0.53 27 1 3 1.17 0.66 -27 1 -3 0.22 0.57 27 2 -3 1.3 0.77 -27 -2 -3 0.79 0.75 27 -2 -3 0.96 0.63 27 2 3 -0.2 0.65 -27 -2 3 1.33 0.7 -27 -3 -3 0.07 0.65 -27 -3 3 0.47 0.66 27 3 3 1.72 0.8 -27 4 3 -0.7 0.48 27 0 -4 60.69 3.3 -27 0 -4 59.1 3.12 27 0 4 63.47 3.13 27 1 -4 0.53 0.73 -27 -1 -4 2.18 0.82 -27 1 -4 0.82 0.63 27 1 4 1.33 0.68 27 -1 -4 1.96 0.74 27 2 -4 38.88 2.73 -27 -2 -4 37.07 2.61 27 -2 -4 41.15 2.58 -27 -2 4 39.27 2.41 27 2 4 41.65 2.66 -27 2 -4 38 2.32 -27 3 4 -0.57 0.36 27 3 4 0.22 0.73 27 -3 -4 0.72 0.53 -27 -3 4 0.88 0.68 27 0 -5 -0.55 0.61 -27 0 -5 -0.5 0.54 -27 -1 -5 1.08 0.67 27 1 -5 -0.05 0.68 27 1 5 1.97 0.68 -27 1 -5 -0.27 0.51 27 -1 -5 0.36 0.65 -27 2 5 0.58 0.34 -27 -2 -5 1.41 0.81 27 -2 -5 0.62 0.6 -27 -2 5 -0.91 0.49 27 2 5 0.64 0.62 -27 2 -5 1.34 0.61 -27 3 5 -0.4 0.36 27 -3 -5 0.49 0.58 -27 -3 5 1.9 0.71 -27 0 -6 27.84 2.17 27 0 -6 28.7 2.32 -27 -1 -6 32.52 2.43 27 1 -6 30.71 2.39 -27 1 6 26.03 1.6 -27 1 -6 31.47 2.22 27 1 6 32.14 2.17 27 -1 -6 31.52 2.33 -27 2 6 11.16 0.94 27 2 6 18.27 1.7 27 -2 -6 14.31 1.84 -27 2 -6 14.61 1.7 -27 3 6 9.88 0.97 -27 -3 6 10.71 1.45 27 -3 -6 12.92 1.67 -27 0 -7 0.35 0.65 -27 0 7 0.38 0.36 -27 1 7 -0.13 0.35 -27 1 -7 -0.01 0.62 -27 2 7 0.31 0.36 -27 2 -7 1.53 0.73 27 2 7 1.32 0.66 -27 3 -7 -0.02 0.56 -27 -3 7 0.59 0.62 -27 0 8 1.2 0.38 -27 1 8 36.58 2.05 27 2 8 1.95 0.86 -27 -1 9 -0.31 0.35 28 0 0 54.21 3.01 -28 0 0 54.94 2.84 -28 -1 0 1.2 0.68 28 -1 0 0.65 0.59 28 1 0 1.5 0.74 28 2 0 36.82 2.61 -28 -2 0 37.2 2.45 28 0 1 0.25 0.61 28 0 -1 0.12 0.64 -28 0 -1 0.18 0.58 -28 -1 -1 1.28 0.67 28 1 -1 0.17 0.67 28 -1 1 -0.24 0.52 -28 -1 1 1.4 0.58 28 -1 -1 0.6 0.75 28 1 1 -0.49 0.6 -28 -2 -1 1.24 0.74 28 2 1 0.22 0.66 -28 -2 1 1.09 0.75 -28 0 -2 24.46 1.97 28 0 2 21.72 1.86 28 0 -2 24.23 2 28 1 -2 27.18 2.25 -28 -1 -2 27.91 2.08 -28 -1 2 28.72 2 28 -1 -2 25.01 2.01 -28 1 -2 28.67 1.94 28 1 2 25.57 2.1 -28 -2 -2 15.44 1.56 28 -2 -2 15.54 1.54 28 2 2 18.73 1.81 -28 -2 2 15.44 1.51 28 0 3 0.55 0.56 28 0 -3 -0.4 0.52 -28 0 -3 1.76 0.72 28 1 -3 0.17 0.67 -28 -1 -3 0.02 0.63 -28 1 -3 -0.31 0.52 28 1 3 0.49 0.56 28 -1 -3 -0.69 0.55 28 -2 -3 2.32 0.69 -28 -2 3 0.2 0.66 28 2 3 2.07 0.77 -28 0 -4 0.57 0.64 28 0 -4 1.22 0.77 -28 -1 -4 33.59 2.37 28 -1 -4 36 2.5 28 1 4 39.9 2.52 -28 1 -4 37.33 2.46 -28 -2 4 1.49 0.65 28 2 4 0.38 0.66 28 -2 -4 0.62 0.63 28 -3 -4 16.76 1.65 -28 0 -5 0.83 0.74 -28 1 -5 -1 0.54 28 1 5 0.47 0.64 -28 2 -5 0.89 0.6 28 1 6 16.64 1.59 -28 2 6 13.98 0.88 -28 2 -6 18.07 1.67 -28 1 7 -1.33 0.37 29 0 0 1.13 0.64 -29 -1 0 29.09 2.04 29 -1 0 27.33 2.04 29 0 1 -0.29 0.55 -29 0 -1 0.37 0.56 -29 -1 -1 1.06 0.61 29 -1 -1 0.78 0.62 -29 -1 1 -0.38 0.63 29 0 2 18.31 1.68 -29 0 -2 17.77 1.68 29 0 3 -0.3 0.61 -29 1 -3 1.41 0.69 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 Au1 P1 168.0(7) . . y C1B Au1 P1 169.9(8) 4_545 . y C1B Au1 C1 2.0(14) 4_545 . y C4 P1 Au1 119.73(17) . . ? C10 P1 Au1 109.30(15) . . ? C10 P1 C4 104.3(2) . . ? C16 P1 Au1 112.64(15) . . ? C16 P1 C4 104.7(2) . . ? C16 P1 C10 104.9(2) . . ? C2A C1 Au1 171(2) . . ? O C3 C2A 115.8(9) . . ? C5 C4 P1 118.7(4) . . ? C9 C4 P1 121.4(4) . . ? C9 C4 C5 119.7(5) . . ? C6 C5 C4 119.6(5) . . ? C7 C6 C5 120.7(5) . . ? C8 C7 C6 119.8(5) . . ? C9 C8 C7 119.7(5) . . ? C8 C9 C4 120.4(5) . . ? C11 C10 P1 118.9(4) . . ? C15 C10 P1 122.9(3) . . ? C15 C10 C11 118.2(4) . . ? C12 C11 C10 120.8(5) . . ? C13 C12 C11 119.8(5) . . ? C14 C13 C12 120.1(5) . . ? C15 C14 C13 120.1(5) . . ? C14 C15 C10 120.9(5) . . ? C17 C16 P1 118.3(4) . . ? C21 C16 P1 122.4(4) . . ? C21 C16 C17 119.2(5) . . ? C18 C17 C16 120.7(6) . . ? C19 C18 C17 120.1(5) . . ? C20 C19 C18 120.1(5) . . ? C21 C20 C19 120.4(6) . . ? C20 C21 C16 119.5(5) . . ? C3 C2A C1 177.6(18) . . ? C2 O C3 111.7(8) . . ? C1A C2 O 111.7(10) . . ? C1B C1A C2 174(2) . . ? C1A C1B Au1 174(2) . 4_545 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Au1 Au1 3.2907(4) 4 y Au1 P1 2.2733(12) . y Au1 C1 2.060(9) . y Au1 C1B 1.951(9) 4_545 y P1 C4 1.819(5) . ? P1 C10 1.814(5) . ? P1 C16 1.824(5) . ? C1 C2A 1.205(2) . ? C3 C2A 1.439(2) . ? C3 O 1.409(2) . ? C4 C5 1.387(6) . ? C4 C9 1.385(7) . ? C5 C6 1.387(7) . ? C6 C7 1.378(8) . ? C7 C8 1.387(8) . ? C8 C9 1.388(7) . ? C10 C11 1.396(6) . ? C10 C15 1.397(6) . ? C11 C12 1.382(7) . ? C12 C13 1.386(7) . ? C13 C14 1.377(7) . ? C14 C15 1.378(7) . ? C16 C17 1.393(7) . ? C16 C21 1.388(7) . ? C17 C18 1.377(8) . ? C18 C19 1.378(9) . ? C19 C20 1.372(8) . ? C20 C21 1.402(7) . ? O C2 1.408(2) . ? C2 C1A 1.439(2) . ? C1A C1B 1.205(2) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag P1 C4 C5 C6 173.3(4) . . . . ? P1 C4 C9 C8 -173.6(4) . . . . ? P1 C10 C11 C12 179.3(4) . . . . ? P1 C10 C15 C14 -179.7(4) . . . . ? P1 C16 C17 C18 -179.5(4) . . . . ? P1 C16 C21 C20 178.9(4) . . . . ? C3 O C2 C1A -164.4(10) . . . . ? C4 C5 C6 C7 0.9(5) . . . . ? C4 C9 C8 C7 -0.1(6) . . . . ? C5 C6 C7 C8 0.3(6) . . . . ? C6 C7 C8 C9 -0.6(6) . . . . ? C10 C11 C12 C13 0.7(6) . . . . ? C10 C15 C14 C13 0.1(5) . . . . ? C11 C12 C13 C14 -0.1(6) . . . . ? C12 C13 C14 C15 -0.3(6) . . . . ? C16 C17 C18 C19 1.4(6) . . . . ? C16 C21 C20 C19 -0.4(6) . . . . ? C17 C18 C19 C20 -1.2(6) . . . . ? C18 C19 C20 C21 0.7(6) . . . . ? loop_ _restr_equal_distance_atom_site_label_1 _restr_equal_distance_atom_site_label_2 _restr_equal_distance_site_symmetry_2 _restr_equal_distance_class_id C3 C2A 1 2 C2A C1 1 1 O C3 1 3 O C2 1 3 C2 C1A 1 2 C1B C1A 1 1 loop_ _restr_equal_distance_class_class_id _restr_equal_distance_class_target_weight_param _restr_equal_distance_class_average _restr_equal_distance_class_esd _restr_equal_distance_class_diff_max 1 0.0010 1.2049 0.0002 0.0002 2 0.0010 1.4392 0.0003 0.0003 3 0.0010 1.4088 0.0005 0.0005 loop_ _restr_U_iso_atom_site_label _restr_U_iso_weight_param C3 0.0010 C2A 0.0010 O 0.0010 C2 0.0010 C1A 0.0010 loop_ _restr_rigu_atom_site_label_1 _restr_rigu_atom_site_label_2 _restr_rigu_target_weight_param _restr_rigu_u13_diff _restr_rigu_u23_diff _restr_rigu_u33_diff Au1 C1 0.001000 -0.003785 0.001839 -0.016983 Au1 C2A 0.001000 0.001358 0.000290 -0.012123 C1 C3 0.001000 0.005612 -0.001886 0.004595 C1 C2A 0.001000 0.004524 -0.001720 0.004843 C3 C2A 0.001000 0.001136 0.000145 0.000340 C3 O 0.001000 0.000416 0.000245 -0.002102 C3 C2 0.001000 -0.001099 -0.000661 -0.001813 C2A O 0.001000 0.001066 -0.000303 -0.004195 O C2 0.001000 -0.000493 -0.000547 0.000497 O C1A 0.001000 0.002163 -0.001531 0.006390 C2 C1A 0.001000 0.000401 -0.000408 0.003282 C2 C1B 0.001000 0.002709 -0.004906 0.003308 C1A C1B 0.001000 0.002655 -0.003803 0.000283