Crystallography Open Database

Information card for entry 7705163

Preview

Coordinates	7705163.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H46 Br0.84 Cl3.16 Mn N4 Si2
Calculated formula	C30 H46 Br0.84 Cl3.16 Mn N4 Si2
Title of publication	Aminolysis of bis[bis(trimethylsilyl)amido]-manganese, -iron, and -cobalt for the synthesis of mono- and bis-silylene complexes.
Authors of publication	He, Zhiyuan; Xue, Xiaolian; Liu, Yilan; Yu, Na; Krogman, Jeremy P.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	36
Pages of publication	12586 - 12591
a	10.5954 ± 0.0009 Å
b	10.9184 ± 0.0008 Å
c	17.2222 ± 0.0014 Å
α	77.08 ± 0.004°
β	79.212 ± 0.004°
γ	73.855 ± 0.004°
Cell volume	1848.6 ± 0.3 Å³
Cell temperature	150.03 K
Ambient diffraction temperature	150.03 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0916
Residual factor for significantly intense reflections	0.0461
Weighted residual factors for significantly intense reflections	0.0936
Weighted residual factors for all reflections included in the refinement	0.1096
Goodness-of-fit parameter for all reflections included in the refinement	1.022
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
257536 (current)	2020-10-06	cif/ Updating files of 7705159, 7705160, 7705161, 7705162, 7705163, 7705164, 7705165, 7705166, 7705167, 7705168 Original log message: Adding full bibliography for 7705159--7705168.cif.	7705163.cif
255334	2020-08-15	cif/ Adding structures of 7705159, 7705160, 7705161, 7705162, 7705163, 7705164, 7705165, 7705166, 7705167, 7705168 via cif-deposit CGI script.	7705163.cif