Crystallography Open Database

Information card for entry 7705209

Preview

Coordinates	7705209.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33.5 H43 Au Cl F6 N3 P2
Calculated formula	C33.5 H43 Au Cl F6 N3 P2
Title of publication	Terphenyl(bisamino)phosphines: electron-rich ligands for gold-catalysis.
Authors of publication	Siewert, Jan-Erik; Schumann, André; Fischer, Malte; Schmidt, Christoph; Taeufer, Tobias; Hering-Junghans, Christian
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	35
Pages of publication	12354 - 12364
a	21.8546 ± 0.0013 Å
b	11.6516 ± 0.0007 Å
c	28.9714 ± 0.0018 Å
α	90°
β	104.839 ± 0.003°
γ	90°
Cell volume	7131.3 ± 0.8 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0459
Residual factor for significantly intense reflections	0.042
Weighted residual factors for significantly intense reflections	0.1023
Weighted residual factors for all reflections included in the refinement	0.1051
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
257564 (current)	2020-10-06	cif/ Updating files of 7705201, 7705202, 7705203, 7705204, 7705205, 7705206, 7705207, 7705208, 7705209 Original log message: Adding full bibliography for 7705201--7705209.cif.	7705209.cif
255464	2020-08-20	cif/ Adding structures of 7705201, 7705202, 7705203, 7705204, 7705205, 7705206, 7705207, 7705208, 7705209 via cif-deposit CGI script.	7705209.cif