Crystallography Open Database

Information card for entry 7705269

Preview

Coordinates	7705269.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Co4Se2(CO)6(Ph2PNHiPr)4
Formula	C66 H72 Co4 N4 O6 P4 Se2
Calculated formula	C66 H72 Co4 N4 O6 P4 Se2
Title of publication	Inorganic clusters as metalloligands: ligand effects on the synthesis and properties of ternary nanopropeller clusters.
Authors of publication	Kephart, Jonathan A.; Boggiano, Andrew C.; Kaminsky, Werner; Velian, Alexandra
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	45
Pages of publication	16464 - 16473
a	22.463 ± 0.003 Å
b	16.532 ± 0.003 Å
c	19.79 ± 0.003 Å
α	90°
β	96.433 ± 0.013°
γ	90°
Cell volume	7303 ± 2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1276
Residual factor for significantly intense reflections	0.0595
Weighted residual factors for significantly intense reflections	0.1402
Weighted residual factors for all reflections included in the refinement	0.1756
Goodness-of-fit parameter for all reflections included in the refinement	0.963
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
260793 (current)	2021-01-07	cif/ Updating files of 7705267, 7705268, 7705269, 7705270, 7705271, 7705272, 7705273 Original log message: Adding full bibliography for 7705267--7705273.cif.	7705269.cif
255647	2020-08-26	cif/ Adding structures of 7705267, 7705268, 7705269, 7705270, 7705271, 7705272, 7705273 via cif-deposit CGI script.	7705269.cif