Crystallography Open Database

Information card for entry 7705289

Preview

Coordinates	7705289.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C5 H51 Mo9 N6 O44 V
Calculated formula	C5 H51 Mo9 N6 O44 V
Title of publication	{VMo<sub>9</sub>O<sub>31</sub>[RC(CH<sub>2</sub>O)<sub>3</sub>]}<sup>6-</sup>: the first class of triol ligand covalently-decorated Keggin-type polyoxomolybdates.
Authors of publication	Qu, Di; Liu, Xiaoting; Duan, Fengxue; Xue, Rong; Li, Bao; Wu, Lixin
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	37
Pages of publication	12950 - 12954
a	13.8761 ± 0.0009 Å
b	16.0198 ± 0.001 Å
c	20.6578 ± 0.0013 Å
α	90°
β	90°
γ	90°
Cell volume	4592.1 ± 0.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	36
Hermann-Mauguin space group symbol	C m c 21
Hall space group symbol	C 2c -2
Residual factor for all reflections	0.0278
Residual factor for significantly intense reflections	0.026
Weighted residual factors for significantly intense reflections	0.0677
Weighted residual factors for all reflections included in the refinement	0.0693
Goodness-of-fit parameter for all reflections included in the refinement	1.075
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
257516 (current)	2020-10-06	cif/ Updating files of 7705288, 7705289, 7705290 Original log message: Adding full bibliography for 7705288--7705290.cif.	7705289.cif
255703	2020-08-28	cif/ Adding structures of 7705288, 7705289, 7705290 via cif-deposit CGI script.	7705289.cif