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Information card for entry 7705333
Preview
Coordinates | 7705333.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | IB-282 |
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Formula | C18 H20 N2 O4 P2 S4 |
Calculated formula | C18 H20 N2 O4 P2 S4 |
Title of publication | [4 + 2]-Cycloadditions of a thiazol-based tricyclic 1,4-diphosphinine and a new easy 1,4-diphosphinine protection deprotection strategy. |
Authors of publication | Begum, Imtiaz; Kalisch, Tim; Schnakenburg, Gregor; Kelemen, Zsolt; Nyulászi, László; Streubel, Rainer |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2020 |
Journal volume | 49 |
Journal issue | 36 |
Pages of publication | 12776 - 12779 |
a | 10.1125 ± 0.0006 Å |
b | 10.126 ± 0.0006 Å |
c | 11.907 ± 0.0007 Å |
α | 77.826 ± 0.003° |
β | 75.301 ± 0.003° |
γ | 89.011 ± 0.003° |
Cell volume | 1151.99 ± 0.12 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.071 |
Residual factor for significantly intense reflections | 0.0515 |
Weighted residual factors for significantly intense reflections | 0.1003 |
Weighted residual factors for all reflections included in the refinement | 0.1105 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.061 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
257546 (current) | 2020-10-06 | cif/ Updating files of 7705332, 7705333 Original log message: Adding full bibliography for 7705332--7705333.cif. |
7705333.cif |
255793 | 2020-09-02 | cif/ Adding structures of 7705332, 7705333 via cif-deposit CGI script. |
7705333.cif |
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Users of the data should acknowledge the original authors of the
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