Crystallography Open Database

Information card for entry 7705345

Preview

Coordinates	7705345.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H51 O20 Ru4
Calculated formula	C36 H51 O20 Ru4
Title of publication	Unprecedented metal-metal bonded {Ru<sub>4</sub>(μ<sub>3</sub>-O)<sub>2</sub>} butterfly core in oxido-carboxylato bridged mixed valence cluster-structural elucidation and electronic forms in accessible redox states.
Authors of publication	Bera, Sudip Kumar; Lahiri, Goutam Kumar
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	39
Pages of publication	13573 - 13581
a	11.8572 ± 0.0003 Å
b	13.8306 ± 0.0003 Å
c	14.3293 ± 0.0003 Å
α	74.4373 ± 0.0018°
β	89.4963 ± 0.0017°
γ	80.0332 ± 0.0019°
Cell volume	2227.82 ± 0.09 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0582
Residual factor for significantly intense reflections	0.0438
Weighted residual factors for significantly intense reflections	0.091
Weighted residual factors for all reflections included in the refinement	0.099
Goodness-of-fit parameter for all reflections included in the refinement	1.049
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
258828 (current)	2020-11-06	cif/ Updating files of 7705345 Original log message: Adding full bibliography for 7705345.cif.	7705345.cif
255889	2020-09-04	cif/ Adding structures of 7705345 via cif-deposit CGI script.	7705345.cif