#------------------------------------------------------------------------------ #$Date: 2021-06-05 21:59:26 +0300 (Sat, 05 Jun 2021) $ #$Revision: 266097 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/71/7707170.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7707170 loop_ _publ_author_name 'Jing, Huiru' 'Dan, Wenyan' 'Zhu, Jiaxing' 'Ling, Yun' 'Jia, Yu' 'Yang, Yongtai' 'Liu, Xiaofeng' 'Chen, Zhenxia' 'Zhou, Yaming' _publ_section_title ; Multimetal lanthanide phosphonocarboxylate frameworks: structures, colour tuning and near-infrared emission. ; _journal_issue 21 _journal_name_full 'Dalton transactions (Cambridge, England : 2003)' _journal_page_first 7380 _journal_page_last 7387 _journal_paper_doi 10.1039/d1dt01052b _journal_volume 50 _journal_year 2021 _chemical_formula_moiety 'Gd7 (C14 O7 P H7)6 (C3 N H7 O)4 (H2 O)3' _chemical_formula_sum 'C96 H76 Gd7 N4 O49 P6' _chemical_formula_weight 3356.17 _chemical_name_systematic GdPCF _space_group_crystal_system orthorhombic _space_group_IT_number 58 _space_group_name_Hall '-P 2 2n' _space_group_name_H-M_alt 'P n n m' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2016/6 _audit_update_record ; 2021-02-16 deposited with the CCDC. 2021-04-21 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 14.4962(6) _cell_length_b 20.3758(8) _cell_length_c 22.8688(11) _cell_measurement_reflns_used 9989 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 61.83 _cell_measurement_theta_min 3.66 _cell_volume 6754.8(5) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2016)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 296(2) _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type GaK\a _diffrn_radiation_wavelength 1.34139 _diffrn_reflns_av_R_equivalents 0.0789 _diffrn_reflns_av_unetI/netI 0.0574 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 26 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_number 48154 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_theta_full 53.594 _diffrn_reflns_theta_max 61.957 _diffrn_reflns_theta_min 3.140 _exptl_absorpt_coefficient_mu 18.561 _exptl_absorpt_correction_T_max 0.328 _exptl_absorpt_correction_T_min 0.134 _exptl_absorpt_correction_type multi-scan _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.650 _exptl_crystal_description rod-like _exptl_crystal_F_000 3220 _exptl_crystal_size_max 0.130 _exptl_crystal_size_mid 0.110 _exptl_crystal_size_min 0.060 _refine_diff_density_max 2.689 _refine_diff_density_min -1.251 _refine_diff_density_rms 0.219 _refine_ls_extinction_coef 0.00042(4) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2016/6 (Sheldrick 2016)' _refine_ls_goodness_of_fit_ref 1.048 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 476 _refine_ls_number_reflns 8210 _refine_ls_number_restraints 783 _refine_ls_restrained_S_all 1.021 _refine_ls_R_factor_all 0.0789 _refine_ls_R_factor_gt 0.0567 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1039P)^2^+16.5510P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1571 _refine_ls_wR_factor_ref 0.1742 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6088 _reflns_number_total 8210 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt01052b2.cif _cod_data_source_block GdPCF _cod_depositor_comments 'Adding full bibliography for 7707169--7707171.cif.' _cod_database_code 7707170 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.196 _shelx_estimated_absorpt_t_max 0.402 _shelx_res_file ; TITL 1_a.res in Pnnm 1_a_sq.res created by SHELXL-2016/6 at 10:51:16 on 16-Feb-2021 REM Old TITL 1 in Pnnm REM SHELXT solution in Pnnm REM R1 0.189, Rweak 0.006, Alpha 0.049, Orientation as input REM Formula found by SHELXT: C82 Gd6 N25 O42 P8 CELL 1.34139 14.4962 20.3758 22.8688 90.000 90.000 90.000 ZERR 2.000 0.0006 0.0008 0.0011 0.000 0.000 0.000 LATT 1 SYMM -X, -Y, Z SYMM 1/2-X, 1/2+Y, 1/2-Z SYMM 1/2+X, 1/2-Y, 1/2-Z SFAC C H GD N O P UNIT 192 152 14 8 98 12 OMIT 1 1 0 OMIT 0 1 7 OMIT 1 0 7 LIST 4 ! automatically inserted. Change 6 to 4 for CHECKCIF!! TEMP 23.000 L.S. 10 0 102 BOND $H SIMU 0.02 0.04 2.2 SIMU 0.04 0.08 1.0 ISOR 0.006 o4w o3w DELU eadp o3w o4w ACTA ISOR 0.01 o6w o5w EADP o1w o6w eadp Gd4 Gd3 size 0.06 0.11 0.13 conf FMAP 2 PLAN 60 ABIN WGHT 0.103900 16.550999 EXTI 0.000416 FVAR 0.10623 0.56478 0.58547 0.33058 0.60246 GD1 3 0.406918 0.619566 0.646673 11.00000 0.02469 0.02056 = 0.03808 -0.00112 -0.00135 0.00166 GD2 3 0.000000 1.000000 0.273634 10.50000 0.03187 0.02388 = 0.03000 0.00000 0.00000 0.00441 PART -1 40.25 AFIX 1 GD3 3 0.633376 0.460896 0.500000 40.25000 0.02657 0.02657 = 0.02657 0.00000 0.00000 0.00000 AFIX 0 O1W 5 10.684846 10.573606 10.500000 40.25000 0.08197 0.03396 = 0.03050 0.00851 -0.00098 -0.01482 O2W 5 10.469826 10.440187 10.500000 40.25000 0.01880 0.04174 = 0.03890 0.00003 -0.00146 0.02057 O3W 5 10.797565 10.441502 10.503986 40.25000 0.02137 0.03110 = 0.01279 0.00206 -0.00103 -0.01840 PART -2 -40.25 GD4 3 10.681773 10.455367 10.500000 -40.25000 0.02657 0.02657 = 0.02657 0.00000 0.00000 0.00000 O4W 5 0.824768 0.428893 0.556196 -40.25000 0.02137 0.03110 = 0.01279 0.00206 -0.00103 -0.01840 O5W 5 10.517835 10.481284 10.500000 -40.25000 0.03458 0.07679 = 0.03003 0.00103 -0.00050 0.00582 O6W 5 10.735783 10.566936 10.500000 -40.25000 0.08197 0.03396 = 0.03050 0.00851 -0.00098 -0.01482 PART 0 RESI 1 P1 6 0.624717 0.531536 0.640658 11.00000 0.01874 0.01608 = 0.03467 0.00089 0.00140 0.00106 O1 5 0.549564 0.580423 0.624715 11.00000 0.02101 0.02158 = 0.04155 0.00168 0.00062 0.00107 O2 5 0.602979 0.491603 0.695897 11.00000 0.02369 0.02171 = 0.02877 0.00105 0.00310 -0.00260 O3 5 0.639893 0.479131 0.593527 11.00000 0.03032 0.01991 = 0.02852 -0.00061 0.00470 0.00122 O4 5 1.241574 0.610417 0.663653 11.00000 0.02721 0.02370 = 0.08015 -0.00697 0.00260 0.00105 O5 5 1.306430 0.703391 0.687855 11.00000 0.02258 0.02649 = 0.06058 -0.01164 -0.00398 0.00043 O6 5 1.095613 0.903198 0.705594 11.00000 0.02775 0.02343 = 0.05330 -0.00311 0.00323 -0.00083 O7 5 0.971379 0.882917 0.757413 11.00000 0.03181 0.02214 = 0.03274 -0.00757 0.00585 0.00267 SAME_1 C1 C2a C3a C4 C5a C6a AFIX 66 C1 1 0.730196 0.577470 0.653150 11.00000 0.02288 0.01713 = 0.03583 -0.00020 0.00476 -0.00330 PART 1 31.00 C2 1 0.812480 0.545191 0.665264 31.00000 0.02792 0.02023 = 0.04831 0.00496 -0.01246 0.00101 AFIX 43 H2 2 0.814373 0.499571 0.665616 31.00000 -1.20000 AFIX 65 C3 1 0.891933 0.581098 0.676852 31.00000 0.02884 0.02042 = 0.05563 0.00231 -0.00797 0.00024 AFIX 43 H3 2 0.946986 0.559501 0.684957 31.00000 -1.20000 AFIX 65 PART 0 C4 1 0.889104 0.649283 0.676325 11.00000 0.02147 0.02473 = 0.05151 -0.00689 0.00294 -0.00314 PART 1 31.00 C5 1 0.806822 0.681563 0.664211 31.00000 0.02550 0.01762 = 0.05777 0.00594 0.00340 -0.00675 AFIX 43 H5 2 0.804929 0.727184 0.663860 31.00000 -1.20000 AFIX 65 C6 1 0.727368 0.645658 0.652623 31.00000 0.02145 0.01726 = 0.06013 0.00422 0.00602 -0.00134 AFIX 43 H6 2 0.672315 0.667255 0.644518 31.00000 -1.20000 AFIX 0 PART 0 PART 2 -31.00 C2A 1 0.814605 0.551763 0.641421 -31.00000 0.02574 0.02433 = 0.05820 -0.00802 -0.00853 0.00095 AFIX 43 H2A 2 0.818269 0.509716 0.625773 -31.00000 -1.20000 AFIX 0 C3A 1 0.895737 0.586141 0.652001 -31.00000 0.02672 0.02646 = 0.06597 -0.01016 -0.00637 0.00352 AFIX 43 H3A 2 0.952853 0.567842 0.643217 -31.00000 -1.20000 AFIX 0 PART 0 PART 2 -31.00 C5A 1 0.803891 0.675119 0.686057 -31.00000 0.02620 0.02034 = 0.05809 -0.00654 0.00655 -0.00349 AFIX 43 H5A 2 0.799116 0.717716 0.700345 -31.00000 -1.20000 AFIX 0 C6A 1 0.724218 0.639809 0.675295 -31.00000 0.01917 0.02899 = 0.05699 -0.00954 0.01476 -0.00520 AFIX 43 H6A 2 0.666846 0.658286 0.683053 -31.00000 -1.20000 AFIX 0 PART 0 C7 1 0.974902 0.688873 0.687716 11.00000 0.02627 0.01845 = 0.05347 -0.00464 0.00332 -0.00352 C8 1 1.062498 0.662232 0.679004 11.00000 0.02908 0.02100 = 0.05079 -0.01067 0.00623 0.00025 AFIX 43 H8 2 1.068109 0.618726 0.667233 11.00000 -1.20000 AFIX 0 C9 1 1.142084 0.699917 0.687690 11.00000 0.01975 0.02158 = 0.04627 -0.00302 0.00194 0.00180 C10 1 1.134712 0.765154 0.703101 11.00000 0.02420 0.02372 = 0.03794 -0.00422 0.00142 0.00348 AFIX 43 H10 2 1.187279 0.790820 0.707631 11.00000 -1.20000 AFIX 0 C11 1 1.047926 0.791915 0.711738 11.00000 0.02807 0.01976 = 0.03401 -0.00230 0.00886 -0.00473 C12 1 0.970025 0.754779 0.706346 11.00000 0.02564 0.02126 = 0.04324 -0.00679 0.00803 -0.00020 AFIX 43 H12 2 0.912952 0.773178 0.715074 11.00000 -1.20000 AFIX 0 C13 1 1.235507 0.669578 0.679974 11.00000 0.02810 0.01904 = 0.04711 -0.00529 0.00376 0.00068 C14 1 1.039518 0.862580 0.726250 11.00000 0.02413 0.02043 = 0.03530 -0.00700 -0.00408 0.00297 RESI 0 SADI_2 C11 O4 C11 O4a RESI 2 P1 6 0.370555 0.695639 0.500000 10.50000 0.04787 0.02681 = 0.03530 0.00000 0.00000 0.00375 O1 5 0.367095 0.651651 0.553746 11.00000 0.05233 0.04658 = 0.03274 0.00582 -0.00255 0.01321 O2 5 0.453280 0.740081 0.500000 10.50000 0.05951 0.04500 = 0.07828 0.00000 0.00000 -0.01130 O3 5 -0.087581 0.955091 0.345092 11.00000 0.07196 0.04717 = 0.04481 0.01371 0.02484 0.01633 PART 1 21.00 O4 5 -0.225615 0.954115 0.390645 21.00000 0.05065 0.13609 = 0.04533 0.01510 0.00373 0.01323 PART 2 -21.00 O4A 5 -0.191749 1.005816 0.400429 -21.00000 0.07333 0.11871 = 0.05195 0.02466 0.01370 0.05643 PART 0 AFIX 66 C1 1 0.265770 0.747031 0.500000 10.50000 0.06310 0.03935 = 0.03661 0.00000 0.00000 0.01736 PART -1 10.5 C2 1 0.201794 0.746589 0.544964 10.50000 0.07512 0.09022 = 0.05483 0.03377 0.01873 0.03444 AFIX 43 H2 2 0.209537 0.718299 0.576497 10.50000 -1.20000 AFIX 65 C3 1 0.126026 0.788344 0.543064 10.50000 0.07018 0.09637 = 0.04235 0.01736 0.00911 0.03493 AFIX 43 H3 2 0.082748 0.786906 0.573056 10.50000 -1.20000 AFIX 65 PART 0 C4 1 0.114203 0.830558 0.498896 10.50000 0.06495 0.07371 = 0.04186 0.00000 0.00000 0.03154 PART -1 10.5 C5 1 0.178216 0.830979 0.450621 10.50000 0.06016 0.05125 = 0.03472 0.00874 0.00289 0.02061 AFIX 43 H5 2 0.168975 0.858662 0.418823 10.50000 -1.20000 AFIX 65 C6 1 0.253984 0.789225 0.452521 10.50000 0.06123 0.04293 = 0.02973 0.00437 0.00414 0.01536 AFIX 43 H6 2 0.296745 0.789409 0.422205 10.50000 -1.20000 AFIX 0 PART 0 C7 1 0.030776 0.874493 0.500000 10.50000 0.04479 0.06862 = 0.04078 0.00000 0.00000 0.01437 C8 1 -0.008333 0.896376 0.447746 11.00000 0.05578 0.06644 = 0.04199 0.00939 0.01269 0.02070 AFIX 43 H8 2 0.018980 0.884953 0.412384 11.00000 -1.20000 AFIX 0 C10 1 -0.127305 0.952038 0.500000 10.50000 0.04612 0.05629 = 0.04666 0.00000 0.00000 0.00801 AFIX 43 H10 2 -0.182273 0.975573 0.499999 10.50000 -1.20000 AFIX 0 C11 1 -0.132093 0.955711 0.392570 11.00000 0.06050 0.11378 = 0.05122 0.03354 0.01833 0.03967 C9 1 -0.087499 0.934995 0.447671 11.00000 0.04345 0.06553 = 0.04562 0.01363 0.01020 0.01333 RESI 0 SADI_DMF 0.02 N1 C2 N1 C3 SADI_DMF 0.02 N1 C1 SADI_DMF 0.02 C1 O1 SADI_DMF 0.04 C2 C3 SADI_DMF 0.04 C1 C3 SADI_DMF 0.04 C1 C2 FLAT_DMF C1 > C3 SIMU_DMF C1 > C3 RIGU_DMF C1 > C3 SAME_DMF C1 > C3 RESI DMF 3 PART 1 51.00 AFIX 1 C1 1 0.483500 0.774000 0.652500 51.00000 0.05000 0.05000 = 0.05000 0.00000 0.00000 0.00000 AFIX 43 H1 2 0.422029 0.784203 0.659768 51.00000 -1.20000 AFIX 0 O1 5 0.498265 0.716942 0.645921 51.00000 0.03426 0.03357 = 0.05917 0.00377 0.00974 -0.00743 N1 4 0.536889 0.823149 0.651322 51.00000 0.08072 0.05184 = 0.13289 -0.00024 0.01437 -0.01745 C2 1 0.639064 0.807735 0.641811 51.00000 0.06456 0.10651 = 0.15147 0.01985 -0.02385 -0.01386 AFIX 137 H2A 2 0.650117 0.762148 0.649769 51.00000 -1.50000 H2AB 2 0.675723 0.834150 0.667663 51.00000 -1.50000 H2AC 2 0.655477 0.817234 0.602032 51.00000 -1.50000 AFIX 0 C3 1 0.515220 0.896290 0.649408 51.00000 0.17050 0.05695 = 0.23780 -0.02795 0.01226 0.00381 AFIX 137 H3A 2 0.515066 0.911009 0.609530 51.00000 -1.50000 H3AB 2 0.561243 0.919960 0.671002 51.00000 -1.50000 H3AC 2 0.455697 0.903983 0.666484 51.00000 -1.50000 AFIX 0 RESI 0 PART 2 -51.00 RESI 4 DMF C1 1 0.550585 0.735142 0.603385 -51.00000 0.07714 0.07316 = 0.11008 0.00530 0.01526 -0.02065 AFIX 43 H1 2 0.564882 0.705844 0.573549 -51.00000 -1.20000 AFIX 0 O1 5 0.489674 0.718315 0.635156 -51.00000 0.05884 0.01485 = 0.07842 -0.01158 0.00400 -0.00496 N1 4 0.598970 0.787494 0.604387 -51.00000 0.09155 0.08404 = 0.13144 0.00459 0.01558 -0.03354 C2 1 0.668665 0.801792 0.555599 -51.00000 0.11885 0.14962 = 0.16417 0.03526 0.03955 -0.03828 AFIX 33 H2A 2 0.698776 0.842876 0.563213 -51.00000 -1.50000 H2AB 2 0.713803 0.767349 0.554267 -51.00000 -1.50000 H2AC 2 0.637060 0.804105 0.518767 -51.00000 -1.50000 AFIX 0 C3 1 0.587477 0.841637 0.650824 -51.00000 0.09620 0.09032 = 0.16217 -0.01477 -0.01001 -0.01443 AFIX 33 H3A 2 0.630661 0.876342 0.643291 -51.00000 -1.50000 H3AB 2 0.525807 0.858709 0.649185 -51.00000 -1.50000 H3AC 2 0.598799 0.823605 0.688936 -51.00000 -1.50000 RESI 0 AFIX 0 HKLF 4 REM 1_a.res in Pnnm REM R1 = 0.0567 for 6088 Fo > 4sig(Fo) and 0.0789 for all 8210 data REM 476 parameters refined using 783 restraints END WGHT 0.1023 16.4559 REM Highest difference peak 2.689, deepest hole -1.251, 1-sigma level 0.219 Q1 1 0.7544 0.4695 0.5000 10.50000 0.05 2.69 Q2 1 0.5942 0.4574 0.5000 10.50000 0.05 2.05 Q3 1 0.7872 0.5377 0.5000 10.50000 0.05 2.04 Q4 1 0.5000 0.5000 0.4836 10.50000 0.05 1.71 Q5 1 0.8415 0.4221 0.5000 10.50000 0.05 1.69 Q6 1 0.6042 0.5997 0.5000 10.50000 0.05 1.49 Q7 1 0.6363 0.6726 0.5000 10.50000 0.05 1.24 Q8 1 0.6718 0.6237 0.5000 10.50000 0.05 1.22 Q9 1 0.6237 0.6799 0.5301 11.00000 0.05 1.18 Q10 1 0.5876 0.6174 0.6474 11.00000 0.05 1.12 Q11 1 1.0027 0.7630 0.7254 11.00000 0.05 1.10 Q12 1 0.6774 0.5008 0.7740 11.00000 0.05 1.06 Q13 1 0.5093 0.9451 0.6168 11.00000 0.05 1.00 Q14 1 0.6762 0.7847 0.5000 10.50000 0.05 0.98 Q15 1 0.0000 1.0000 0.4334 10.50000 0.05 0.95 Q16 1 0.5185 0.4500 0.5000 10.50000 0.05 0.95 Q17 1 -0.0937 0.8791 0.4479 11.00000 0.05 0.95 Q18 1 0.4976 0.8082 0.5954 11.00000 0.05 0.90 Q19 1 0.7783 0.6209 0.6475 11.00000 0.05 0.84 Q20 1 0.4433 0.8459 0.6562 11.00000 0.05 0.84 Q21 1 0.5351 0.9538 0.7085 11.00000 0.05 0.81 Q22 1 -0.2130 0.8858 0.5000 10.50000 0.05 0.79 Q23 1 0.0953 0.8813 0.3994 11.00000 0.05 0.78 Q24 1 1.3196 0.6172 0.6485 11.00000 0.05 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8.80 4 -6 -5 60.49 11.40 -4 -6 5 47.20 6.80 -4 6 -5 51.39 4.70 -4 6 -5 57.39 5.20 4 6 5 44.60 8.50 4 6 5 42.50 7.40 -5 6 5 405.76 32.40 5 -6 5 315.87 31.10 5 6 -5 373.56 25.90 5 6 -5 387.36 25.50 5 6 -5 368.96 22.10 5 -6 -5 351.56 28.80 5 6 5 360.96 25.10 -5 -6 5 399.76 22.70 -5 6 -5 376.16 22.00 -5 -6 5 345.67 22.60 5 6 5 378.66 26.30 -5 6 -5 365.06 22.50 -6 6 5 19.20 7.50 6 6 -5 17.00 6.50 6 6 -5 15.40 2.60 6 6 -5 4.30 5.50 6 -6 -5 9.20 3.80 6 -6 -5 20.10 7.70 -6 6 -5 13.40 3.20 6 6 5 9.20 5.20 6 6 5 6.80 3.80 -6 6 -5 17.70 2.90 -7 6 5 103.29 16.00 7 6 -5 101.99 7.30 7 6 -5 117.99 12.60 7 -6 5 106.09 8.10 -7 6 -5 99.79 8.20 7 6 5 104.89 11.70 -7 6 -5 110.59 7.40 7 6 5 105.69 10.20 7 -6 -5 113.19 9.50 8 6 -5 11.90 7.10 8 6 -5 13.20 6.60 8 -6 5 13.30 3.20 8 6 5 10.10 6.00 -8 6 -5 11.00 3.20 8 -6 -5 5.00 4.10 8 6 5 5.50 2.40 9 6 -5 30.30 8.80 9 -6 5 42.00 5.20 9 6 -5 33.90 9.30 9 -6 -5 28.80 6.30 -9 6 -5 40.80 5.80 9 6 5 29.30 7.70 10 6 -5 -5.30 6.40 10 -6 5 3.60 3.50 10 6 -5 3.10 7.60 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13.50 -1 -7 -5 75.49 10.50 1 7 5 70.69 11.90 -1 7 -5 71.89 6.10 1 -7 -5 67.99 10.80 -1 7 -5 69.09 6.10 2 7 -5 21.50 4.00 2 -7 5 12.50 7.60 -2 7 5 26.90 8.80 2 7 -5 28.40 3.70 2 7 -5 24.20 6.40 -2 -7 -5 42.10 8.10 2 7 -5 34.70 6.60 -2 7 -5 28.80 4.10 2 7 5 31.80 8.80 -2 7 -5 29.00 4.00 -2 -7 5 19.10 6.00 2 -7 -5 33.50 8.80 -3 -7 -5 6.70 3.90 3 7 -5 1.90 2.10 -3 7 5 -6.10 5.60 3 -7 5 3.30 4.70 3 7 -5 4.00 2.50 3 7 -5 1.50 5.00 3 7 -5 -0.20 4.80 -3 -7 5 8.50 3.70 3 -7 -5 7.40 5.30 3 7 5 -3.00 3.90 -3 7 -5 3.30 2.30 -3 7 -5 6.20 2.70 4 -7 5 75.29 13.90 4 7 -5 62.79 9.90 4 7 -5 79.89 9.90 4 7 -5 74.79 6.30 -4 -7 -5 71.79 8.40 -4 7 5 101.09 15.40 -4 7 -5 73.29 6.10 4 7 5 64.89 9.00 4 7 5 83.39 10.40 -4 7 -5 72.69 6.50 4 -7 -5 75.39 11.20 -4 -7 5 68.19 8.20 5 7 -5 44.80 4.80 -5 7 5 33.30 10.50 5 7 -5 49.10 8.90 5 7 -5 47.50 9.00 -5 -7 5 51.79 5.20 5 7 5 42.20 9.70 -5 7 -5 42.30 5.20 -5 -7 5 46.80 4.90 -5 7 -5 43.50 4.40 5 7 5 41.40 8.70 6 -7 5 342.77 21.40 6 7 -5 381.86 26.10 6 7 -5 370.06 21.40 -6 7 5 387.36 33.60 6 7 -5 310.77 28.50 6 7 5 352.66 25.30 -6 7 -5 349.57 21.30 6 7 5 346.97 25.20 -6 7 -5 349.27 22.00 7 -7 5 6.60 4.10 7 7 -5 4.30 5.70 7 7 -5 0.40 2.00 -7 7 5 3.30 6.80 7 7 -5 6.40 6.60 -7 7 -5 7.70 3.20 7 7 5 3.70 5.00 -7 7 -5 5.80 2.10 7 7 5 6.30 3.30 7 -7 -5 2.70 3.90 8 7 -5 89.99 12.90 8 7 -5 101.19 7.60 8 7 -5 104.49 13.80 8 -7 5 93.19 8.10 -8 7 -5 104.09 8.50 8 -7 -5 115.99 10.30 8 7 5 104.59 13.00 9 -7 5 2.90 3.20 9 7 -5 3.60 7.10 9 7 -5 9.50 7.60 9 7 5 4.70 6.40 9 -7 -5 7.00 5.40 -9 7 -5 3.30 3.20 10 7 -5 47.90 11.30 10 7 -5 55.59 11.90 -10 7 -5 50.09 5.80 10 7 5 35.30 9.80 10 -7 -5 43.40 9.40 11 7 -5 5.30 8.40 11 7 -5 3.60 8.40 11 -7 -5 -0.90 7.40 11 7 5 9.00 7.40 -11 7 -5 -1.30 2.70 11 -7 -5 -4.90 5.60 12 7 -5 26.10 11.30 12 7 -5 25.20 9.90 12 7 5 27.30 9.50 12 -7 -5 33.20 9.30 12 -7 -5 35.30 11.00 13 7 -5 5.40 7.80 13 -7 5 2.40 6.80 13 7 -5 -7.70 8.40 13 -7 -5 -1.50 7.00 13 -7 -5 -9.50 8.60 13 7 5 20.20 7.80 14 7 -5 31.70 11.50 14 7 -5 28.00 9.90 14 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1.00 2.60 -3 8 5 5.50 7.20 -3 8 -5 3.40 2.60 -3 -8 5 5.60 3.80 -3 8 -5 3.80 2.90 3 -8 -5 0.90 4.30 3 8 5 2.80 4.40 3 8 5 11.90 5.70 4 8 -5 51.39 5.50 -4 -8 -5 67.99 8.40 4 8 -5 57.99 9.70 4 8 -5 49.99 9.00 4 8 -5 60.49 5.30 -4 8 5 71.59 14.40 -4 -8 5 65.59 11.30 4 8 5 65.79 10.30 4 8 5 66.69 9.70 -4 8 -5 63.09 5.80 -4 8 -5 69.49 6.30 5 8 -5 95.59 7.60 5 8 -5 80.29 11.40 -5 8 5 113.69 17.20 5 8 -5 99.59 7.00 5 8 -5 92.39 12.00 5 8 5 107.19 12.10 -5 -8 5 95.99 7.70 -5 8 -5 87.19 7.90 -5 -8 5 87.19 8.20 5 8 5 92.39 11.00 -5 8 -5 101.39 7.50 6 8 -5 18.00 6.80 6 8 -5 19.60 3.60 -6 8 -5 21.50 4.20 6 8 5 25.60 6.80 -6 8 -5 24.90 3.90 6 8 5 16.60 5.70 7 8 -5 142.29 15.20 7 8 -5 128.49 9.20 7 8 -5 106.09 13.80 7 -8 5 128.09 9.70 -7 8 5 136.49 18.90 7 8 5 119.29 11.90 7 8 5 139.09 15.70 -7 8 -5 144.59 9.30 -7 8 -5 129.69 10.40 7 -8 -5 146.99 11.80 8 8 -5 3.20 2.30 8 -8 5 -3.10 2.70 8 8 -5 1.50 6.30 8 8 -5 0.90 6.80 -8 8 -5 -1.00 2.90 8 8 5 0.50 5.80 -8 8 -5 1.10 1.90 8 -8 -5 1.40 4.50 9 -8 5 57.09 6.70 9 8 -5 64.79 13.40 9 8 -5 62.59 12.50 9 8 5 55.59 11.50 -9 8 -5 65.39 7.20 9 -8 -5 66.79 9.40 10 -8 5 3.50 3.70 10 8 -5 5.30 7.40 -10 8 -5 6.30 3.30 10 -8 -5 5.30 6.10 10 8 5 11.20 7.80 11 8 -5 81.59 16.60 11 8 -5 55.29 12.30 11 8 5 55.69 18.30 -11 8 -5 64.09 7.30 11 -8 -5 64.69 11.70 11 -8 -5 72.29 14.00 12 8 -5 27.10 12.10 12 8 -5 33.40 10.10 -12 8 -5 16.50 4.20 12 8 5 32.40 9.40 12 -8 -5 21.80 8.70 12 -8 -5 23.50 11.00 13 8 -5 16.80 11.40 13 8 -5 18.50 9.30 13 -8 -5 15.20 9.00 13 -8 -5 22.40 10.90 13 8 5 23.90 9.10 14 8 -5 11.60 11.40 14 8 -5 5.60 17.30 14 -8 5 1.60 12.20 14 -8 -5 3.60 13.70 14 -8 -5 9.90 12.80 15 -8 5 32.20 9.00 15 8 -5 24.80 11.50 15 8 -5 13.70 7.70 15 -8 -5 28.30 9.60 15 -8 -5 15.80 11.00 16 8 -5 -8.10 4.60 16 -8 5 1.60 5.30 16 8 -5 43.40 11.50 16 -8 -5 -0.40 9.20 16 -8 -5 9.20 7.30 17 8 -5 -3.10 6.20 17 -8 -5 -21.70 6.40 17 -8 -5 3.90 8.10 0 -9 -5 737.83 50.39 0 -9 5 679.33 56.29 0 9 -5 753.22 46.30 0 9 5 780.22 53.19 0 9 -5 755.12 43.70 0 9 -5 751.52 43.60 -1 9 5 17.40 8.00 1 9 -5 16.60 5.10 1 9 -5 21.20 3.90 1 9 -5 16.80 5.80 1 9 -5 16.20 3.40 1 -9 5 15.80 8.20 -1 -9 -5 14.70 6.30 -1 -9 5 8.80 6.10 1 9 5 10.10 7.10 1 -9 -5 18.90 6.80 -1 9 -5 13.90 3.50 -1 9 -5 12.70 3.30 2 9 -5 124.09 9.80 2 9 -5 155.08 12.80 -2 9 5 162.48 19.80 -2 -9 -5 122.49 14.70 2 9 -5 140.79 9.70 2 9 -5 123.69 13.10 -2 -9 5 126.29 15.20 -2 9 -5 138.59 10.00 2 9 5 134.09 16.40 -2 9 -5 136.59 9.90 -3 -9 -5 26.90 7.70 3 9 -5 23.10 6.60 3 9 -5 24.00 3.80 3 9 -5 22.20 3.90 3 9 -5 17.40 6.40 -3 9 5 20.20 9.10 -3 9 -5 23.10 4.50 -3 -9 5 26.50 7.40 3 9 5 15.80 6.70 -3 9 -5 20.60 3.80 -4 -9 -5 66.09 9.60 4 9 -5 64.99 6.50 -4 9 5 89.99 16.20 4 9 -5 59.99 10.00 4 9 -5 89.49 11.40 4 9 -5 77.89 6.20 -4 -9 5 58.59 9.30 4 9 5 84.09 11.60 -4 9 -5 75.89 7.00 -4 9 -5 69.39 6.40 4 9 5 81.29 10.70 -5 9 5 19.60 9.20 5 9 -5 7.30 6.70 5 9 -5 8.00 2.30 5 9 -5 5.20 2.70 5 9 -5 3.30 6.30 5 9 5 7.20 4.60 -5 9 -5 2.40 3.60 -5 9 -5 4.40 2.80 5 9 5 0.90 5.10 -5 -9 5 0.60 2.80 -6 9 5 145.69 20.90 6 9 -5 120.49 14.20 6 9 -5 124.99 14.80 6 9 -5 138.19 10.70 6 9 -5 132.39 9.70 -6 9 -5 130.99 9.50 6 9 5 121.89 14.00 -6 9 -5 138.59 10.40 6 9 5 130.19 14.00 7 9 -5 5.00 6.40 7 9 -5 2.80 6.00 7 -9 5 3.30 3.10 7 9 -5 3.90 2.40 7 9 5 5.80 3.80 7 -9 -5 3.80 5.10 -7 9 -5 4.60 3.60 7 9 5 10.00 6.70 -7 9 -5 6.30 2.70 8 9 -5 39.70 9.90 8 9 -5 38.80 10.40 8 -9 5 39.60 5.30 8 9 -5 30.80 4.40 8 9 5 38.70 9.50 -8 9 -5 46.60 6.00 -8 9 -5 32.40 4.50 8 -9 -5 42.90 8.30 9 -9 5 3.20 3.40 9 9 -5 12.00 7.90 9 9 -5 6.70 8.90 -9 9 -5 -1.40 3.50 9 -9 -5 6.60 5.70 9 9 5 8.40 7.70 10 -9 5 39.30 6.60 10 9 -5 41.40 10.80 10 9 -5 42.20 12.10 -10 9 -5 39.50 6.30 10 9 5 27.00 10.10 10 -9 -5 38.30 8.80 11 9 -5 -10.70 7.40 11 9 -5 -6.70 7.30 11 -9 -5 1.00 7.30 11 -9 -5 -6.70 8.60 11 9 5 4.00 8.00 -11 9 -5 0.20 5.10 12 9 -5 28.10 11.90 12 9 -5 47.90 11.90 -12 9 -5 56.99 6.60 12 -9 -5 64.39 13.20 12 -9 -5 51.09 10.90 12 9 5 42.70 11.10 13 9 -5 0.00 9.90 13 9 -5 -3.10 7.40 13 9 5 -9.10 7.50 13 -9 -5 -0.80 7.80 13 -9 -5 5.40 10.50 14 -9 5 13.50 9.00 14 9 -5 15.20 8.20 14 9 -5 4.80 10.30 14 9 5 34.90 9.20 14 -9 -5 25.80 9.70 14 -9 -5 7.20 11.90 15 9 -5 16.80 10.50 15 9 -5 5.70 5.70 15 -9 5 14.00 7.40 15 -9 -5 7.50 11.10 15 -9 -5 1.80 7.90 16 -9 5 7.40 5.90 16 9 -5 20.10 9.20 16 -9 -5 12.00 11.00 16 -9 -5 6.80 7.90 17 9 -5 -3.90 6.10 17 -9 -5 -7.50 7.70 17 -9 -5 16.40 9.70 0 -10 5 1.00 6.00 0 10 -5 1.00 3.20 0 10 5 -2.40 5.30 0 10 -5 2.80 4.80 0 10 -5 1.60 2.80 1 10 -5 204.18 14.70 1 10 -5 145.49 11.40 -1 -10 -5 155.48 16.90 -1 10 5 184.18 21.00 1 10 -5 131.39 14.10 1 10 -5 158.78 11.20 -1 -10 5 164.38 18.60 -1 10 -5 157.98 11.50 -1 10 -5 162.68 11.70 1 10 5 175.58 19.90 -2 -10 -5 8.10 5.50 2 10 -5 3.70 2.60 -2 10 5 -5.60 5.60 2 10 -5 1.70 5.30 2 10 -5 -2.70 2.60 2 10 -5 -1.60 4.90 -2 10 -5 1.10 2.90 -2 10 -5 0.30 2.90 -2 -10 5 8.70 5.90 2 10 5 -1.40 5.40 -3 -10 -5 72.29 11.10 3 10 -5 77.69 7.30 3 10 -5 90.19 12.10 3 10 -5 94.39 11.00 3 10 -5 75.59 6.60 -3 10 5 93.09 16.80 -3 10 -5 84.99 7.10 -3 -10 5 68.69 11.70 -3 10 -5 74.79 7.30 3 10 5 87.09 13.50 4 10 -5 16.80 8.60 4 10 -5 20.50 3.90 4 10 -5 28.90 8.10 -4 10 5 4.70 8.80 4 10 -5 17.70 4.10 4 10 5 28.40 7.20 -4 10 -5 16.70 3.90 -4 -10 5 25.50 7.00 4 10 5 24.50 7.50 -4 10 -5 21.20 4.40 -5 -10 -5 172.18 15.50 -5 10 5 192.18 24.20 5 10 -5 175.08 17.20 5 10 -5 169.58 11.80 5 10 -5 150.98 15.40 5 10 -5 159.18 11.00 5 10 5 174.98 16.40 -5 10 -5 160.68 12.20 5 10 5 158.28 17.10 -5 10 -5 161.48 11.70 -5 -10 5 155.68 13.50 6 10 -5 11.70 7.90 6 10 -5 0.20 5.90 6 10 -5 1.30 3.00 6 10 -5 5.90 2.70 -6 10 5 -2.80 7.40 6 10 5 8.40 6.50 -6 10 -5 4.90 2.80 6 10 5 3.50 4.40 -6 10 -5 -3.10 3.10 7 10 -5 41.90 6.20 7 10 -5 34.20 9.50 7 -10 5 43.50 5.90 7 10 -5 62.99 12.70 -7 10 -5 49.90 6.80 -7 10 -5 59.39 7.00 7 10 5 44.70 9.80 -8 10 5 -5.30 2.70 8 10 -5 3.80 7.00 8 10 -5 -3.80 6.80 8 10 -5 -3.70 2.50 8 10 5 4.50 7.00 -8 10 -5 5.80 4.00 8 -10 -5 -0.10 5.60 -8 10 -5 3.40 4.90 9 -10 5 10.90 3.80 9 10 -5 10.20 8.00 9 -10 -5 7.60 6.80 9 10 5 18.80 9.00 -9 10 -5 9.50 4.70 10 10 -5 -5.10 9.10 10 10 -5 2.20 7.20 10 -10 5 1.90 4.30 10 -10 -5 10.10 7.50 11 10 -5 50.49 13.70 11 10 -5 58.99 12.50 -11 10 -5 62.29 7.60 11 -10 -5 41.90 10.50 11 10 5 46.60 11.60 12 10 -5 -1.40 9.30 12 10 -5 1.10 7.70 12 -10 -5 -1.90 9.50 -12 10 -5 -1.30 3.70 12 10 5 7.10 8.00 12 -10 -5 4.80 8.40 13 10 -5 46.50 11.00 13 10 -5 58.59 15.00 13 -10 -5 75.19 17.00 13 10 5 72.09 14.80 13 -10 -5 71.99 14.20 14 -10 5 -1.70 8.70 14 10 -5 11.70 11.00 14 10 -5 17.10 7.30 14 -10 -5 21.50 9.70 14 -10 -5 11.40 12.00 14 10 5 23.40 8.20 15 10 -5 13.60 9.20 15 -10 5 10.10 7.20 15 10 -5 8.50 6.30 15 -10 -5 13.30 9.20 15 -10 -5 14.10 11.50 16 10 -5 7.10 9.50 16 -10 5 -4.10 5.00 16 -10 -5 -5.00 13.20 16 -10 -5 8.10 7.30 17 10 -5 8.60 7.00 17 -10 -5 7.30 8.70 0 11 5 61.69 14.70 0 11 -5 81.59 10.30 0 11 -5 56.99 6.40 1 11 -5 35.10 8.10 -1 11 5 54.79 14.10 1 11 -5 46.10 5.50 -1 11 -5 43.40 5.70 1 11 5 37.40 10.80 2 11 -5 20.00 4.00 -2 11 5 25.40 10.40 2 11 -5 23.40 4.70 2 11 -5 31.40 7.60 2 11 -5 12.80 6.90 -2 11 -5 26.30 5.30 -2 -11 5 24.80 7.40 -2 11 -5 22.00 4.40 2 11 5 12.60 7.10 3 11 -5 -0.40 3.40 3 11 -5 2.80 2.70 -3 11 5 8.60 8.60 3 11 -5 10.70 5.80 3 11 -5 0.00 5.90 -3 11 -5 4.40 3.30 -3 -11 5 -1.10 4.80 -3 11 -5 6.30 3.70 3 11 5 7.90 6.00 -4 -11 -5 78.59 11.90 -4 11 5 77.89 17.20 4 11 -5 89.19 7.40 4 11 -5 97.79 13.20 4 11 -5 109.29 12.40 4 11 -5 99.79 8.30 -4 -11 5 88.39 12.80 -4 11 -5 95.19 8.20 4 11 5 73.19 12.90 -4 11 -5 91.09 8.60 5 11 -5 19.30 7.20 5 11 -5 17.50 7.70 -5 11 5 6.00 8.30 5 11 -5 19.50 4.30 5 11 -5 24.90 4.20 -5 -11 -5 0.10 6.30 -5 -11 5 24.40 5.70 5 11 5 17.90 7.70 -5 11 -5 11.90 4.60 5 11 5 34.40 9.30 -5 11 -5 18.00 3.90 6 11 -5 149.69 17.30 6 11 -5 123.19 9.70 6 11 -5 151.18 15.80 -6 11 5 154.78 23.90 6 11 -5 134.29 10.40 -6 11 -5 139.39 11.30 6 11 5 133.49 14.90 -6 11 -5 130.89 10.30 6 11 5 148.09 16.40 7 11 -5 -0.80 6.60 7 11 -5 2.50 3.30 7 11 -5 5.40 7.70 7 11 5 3.90 7.00 -7 11 -5 5.20 3.10 -7 11 -5 6.90 4.30 -8 11 5 8.00 3.30 8 11 -5 6.70 3.40 8 11 -5 -1.90 6.70 8 -11 5 -3.50 3.60 8 11 -5 5.10 9.30 8 -11 -5 6.40 6.90 -8 11 -5 7.30 4.70 -8 11 -5 5.30 2.90 8 11 5 10.10 8.00 9 11 -5 -1.10 3.20 9 11 -5 -4.10 8.90 9 -11 5 1.90 4.00 9 11 -5 11.90 8.30 -9 11 -5 9.30 5.20 9 -11 -5 3.40 7.20 9 11 5 4.80 8.20 10 11 -5 28.60 11.80 10 11 -5 31.10 10.10 10 -11 5 32.30 8.20 10 -11 -5 35.70 9.80 -10 11 -5 56.39 7.80 10 11 5 48.40 11.80 11 11 -5 28.80 12.70 11 11 -5 37.10 10.60 -11 11 -5 31.40 6.00 11 11 5 10.60 10.30 11 -11 -5 24.70 9.50 12 11 -5 54.79 15.00 12 11 -5 73.19 13.40 12 -11 -5 64.29 12.70 12 -11 -5 67.49 15.20 -12 11 -5 63.09 8.00 12 11 5 61.69 13.10 13 11 -5 0.40 11.30 13 11 -5 11.20 8.00 -13 11 -5 3.40 3.80 13 11 5 -0.70 8.80 13 -11 -5 12.70 17.90 13 -11 -5 9.30 12.60 14 11 -5 9.20 5.90 14 -11 5 16.70 9.90 14 11 -5 20.60 11.70 14 11 5 10.00 7.20 14 -11 -5 -7.70 8.00 14 -11 -5 22.00 12.50 15 -11 5 -3.60 7.00 15 11 -5 15.10 6.50 15 11 -5 13.30 9.40 15 -11 -5 8.70 7.40 15 -11 -5 9.20 11.00 16 11 -5 24.70 9.00 16 -11 5 9.10 6.60 16 -11 -5 11.70 8.00 16 -11 -5 16.00 10.50 17 11 -5 -9.10 5.40 17 -11 -5 11.00 8.20 0 12 -5 3.20 3.50 0 12 -5 10.30 4.20 0 12 5 19.30 8.40 1 12 -5 176.98 16.30 -1 12 5 158.08 22.10 1 12 -5 152.18 11.90 1 12 -5 169.48 12.40 -1 12 -5 161.88 12.10 -1 12 -5 162.68 12.40 -2 12 5 13.30 9.30 2 12 -5 5.70 6.40 2 12 -5 5.40 6.60 2 12 -5 2.80 3.50 2 12 -5 2.70 3.10 -2 12 -5 5.60 3.80 -2 12 -5 4.10 3.80 2 12 5 8.40 6.80 3 12 -5 4.80 6.60 3 12 -5 18.40 7.10 -3 12 5 7.00 8.60 3 12 -5 8.10 4.10 3 12 -5 6.90 3.30 -3 -12 5 4.90 7.70 -3 12 -5 5.60 4.00 3 12 5 8.40 6.70 -3 12 -5 7.90 4.00 -4 12 5 9.00 8.40 4 12 -5 15.30 3.40 4 12 -5 10.10 4.20 4 12 -5 -3.90 6.50 4 12 -5 10.10 6.90 -4 12 -5 12.50 4.10 -4 -12 5 13.90 6.90 4 12 5 3.60 5.70 -4 12 -5 6.10 4.30 -5 12 5 191.08 28.00 5 12 -5 222.98 15.70 5 12 -5 247.78 15.20 5 12 -5 203.48 21.60 5 12 -5 257.37 20.60 -5 12 -5 215.98 15.60 5 12 5 260.77 21.90 -5 12 -5 232.88 16.60 5 12 5 214.18 22.10 6 12 -5 -1.10 6.60 6 12 -5 -2.10 3.40 6 12 -5 -6.00 7.10 -6 12 -5 -5.60 2.90 6 12 5 2.30 7.20 -6 12 -5 -4.20 3.80 7 12 -5 85.79 8.20 7 12 -5 72.09 12.80 7 12 -5 77.69 16.40 -7 12 -5 87.29 9.60 -7 12 -5 87.09 8.20 7 12 5 94.79 15.20 8 12 -5 4.30 7.50 8 -12 5 4.90 4.10 -8 12 5 11.60 3.40 8 12 -5 13.90 4.10 8 12 -5 -1.70 8.90 -8 12 -5 11.70 3.70 -8 12 -5 3.80 5.00 8 12 5 11.80 8.90 8 -12 -5 -3.10 8.40 9 12 -5 18.00 3.90 9 12 -5 -0.30 9.80 9 -12 5 25.70 5.50 9 12 -5 12.00 8.70 -9 12 -5 18.30 5.90 9 12 5 13.30 9.40 9 12 5 19.20 4.90 -9 12 -5 15.30 5.90 9 -12 -5 12.30 8.30 10 12 -5 -3.60 10.10 10 12 -5 5.90 8.20 10 12 5 2.10 9.20 -10 12 -5 10.30 5.30 10 -12 -5 3.80 8.30 11 12 -5 30.20 10.00 11 12 -5 31.20 13.20 11 12 5 19.10 10.50 11 -12 -5 12.60 9.00 -11 12 -5 32.40 6.60 12 12 -5 11.70 8.40 12 12 -5 6.90 10.90 12 -12 -5 -9.50 7.60 12 -12 -5 8.20 11.60 12 12 5 10.60 9.70 -12 12 -5 9.80 5.00 13 12 -5 12.50 11.40 13 12 -5 1.80 7.00 13 -12 -5 21.80 8.90 13 -12 -5 -2.00 10.80 -13 12 -5 0.60 3.40 13 12 5 -7.60 7.30 14 12 -5 6.10 9.70 14 12 -5 9.70 4.50 14 -12 5 -4.90 7.00 14 -12 -5 -9.00 9.80 14 -12 -5 -2.20 6.80 15 12 -5 12.30 9.60 15 -12 5 15.00 8.70 15 -12 -5 27.30 12.40 15 -12 -5 30.10 10.60 16 -12 5 0.50 7.40 16 12 -5 2.90 7.00 16 -12 -5 -6.80 7.40 16 -12 -5 6.60 8.70 0 13 -5 303.07 19.70 0 13 5 273.97 29.60 0 13 -5 282.87 19.10 1 13 -5 4.70 3.70 -1 13 5 5.70 8.60 1 13 -5 17.80 7.50 1 13 -5 7.80 4.40 1 13 5 13.80 8.50 -1 13 -5 7.90 4.50 -1 13 -5 12.20 4.50 2 13 -5 16.70 8.00 2 13 -5 21.20 5.30 2 13 -5 16.30 4.60 -2 13 5 37.20 11.60 -2 13 -5 27.30 5.40 2 13 5 27.90 9.10 -2 13 -5 17.80 5.10 3 13 -5 6.20 3.30 -3 13 5 4.90 10.40 3 13 -5 -0.30 3.90 3 13 -5 9.30 7.30 3 13 -5 -8.30 6.10 -3 13 -5 5.90 4.30 -3 13 -5 -4.80 3.60 3 13 5 2.70 7.40 4 13 -5 140.29 14.50 4 13 -5 101.09 9.70 -4 13 5 84.19 19.80 4 13 -5 103.09 8.90 4 13 -5 121.29 16.10 -4 13 -5 109.19 10.30 4 13 5 90.59 17.80 -4 13 -5 108.09 9.90 5 13 -5 24.80 5.30 5 13 -5 15.50 3.80 5 13 -5 15.20 8.00 5 13 -5 18.00 9.90 -5 13 -5 8.90 4.60 -5 13 -5 17.50 5.50 5 13 5 10.90 8.20 6 13 -5 351.16 23.20 6 13 -5 388.76 28.20 6 13 -5 326.07 30.20 -6 13 -5 359.76 24.00 -6 13 -5 353.76 22.90 7 13 -5 143.89 11.70 7 13 -5 152.98 17.10 7 13 -5 134.69 19.90 -7 13 5 148.19 12.00 -7 13 -5 154.68 13.30 -7 13 -5 146.39 11.60 7 13 5 172.98 19.80 8 13 -5 37.40 6.20 8 -13 5 32.90 6.50 8 13 -5 47.90 13.30 -8 13 5 41.40 6.80 8 13 -5 38.60 10.20 -8 13 -5 46.50 6.10 8 -13 -5 35.80 9.80 -8 13 -5 44.20 7.90 8 13 5 32.10 11.60 9 13 -5 13.30 8.80 9 -13 5 14.70 5.20 9 13 -5 19.00 4.20 9 13 -5 1.20 10.10 9 13 5 7.20 9.30 9 -13 -5 9.60 8.60 -9 13 -5 7.90 3.80 -9 13 -5 0.80 5.00 10 13 -5 3.70 10.80 10 13 -5 6.20 8.40 10 13 5 4.70 9.20 -10 13 -5 8.00 5.60 10 -13 -5 1.90 8.30 11 13 -5 -3.00 7.30 11 13 -5 -2.80 10.60 -11 13 -5 6.60 5.40 11 -13 -5 -7.80 8.00 11 13 5 -4.50 9.20 12 13 -5 1.10 9.30 12 13 -5 9.50 19.90 12 13 5 3.70 12.20 -12 13 -5 6.70 6.90 13 13 -5 15.20 6.80 13 13 -5 -2.20 10.10 13 -13 -5 5.90 11.60 13 -13 -5 0.70 8.30 -13 13 -5 4.10 3.60 14 -13 5 0.90 7.80 14 13 -5 10.60 9.90 14 13 -5 17.80 9.40 14 -13 -5 47.70 13.80 14 -13 -5 16.50 8.30 15 -13 5 8.80 6.30 15 13 -5 6.20 9.50 15 -13 -5 -2.70 6.90 16 13 -5 20.40 8.50 16 -13 5 8.80 13.50 16 -13 -5 22.10 10.00 0 14 -5 0.10 4.10 0 14 -5 4.60 4.80 0 14 5 15.20 9.50 1 14 -5 90.89 9.60 -1 14 5 97.59 19.60 1 14 -5 90.09 8.90 -1 14 -5 95.79 9.80 1 14 5 90.89 17.20 -1 14 -5 87.29 9.20 2 14 -5 0.20 7.30 2 14 -5 -0.90 4.20 -2 14 5 -2.10 10.10 2 14 -5 2.60 3.60 -2 14 -5 -0.30 4.30 -2 14 -5 1.40 4.20 3 14 -5 86.79 8.50 3 14 -5 91.39 9.70 3 14 -5 81.29 15.60 -3 14 -5 85.89 9.30 3 14 5 93.69 16.10 -3 14 -5 93.59 9.70 4 14 -5 64.29 6.90 4 14 -5 78.39 14.80 4 14 -5 61.19 8.60 -4 14 -5 64.09 8.10 -4 14 -5 63.69 8.70 5 14 -5 101.19 18.10 5 14 -5 124.49 15.70 5 14 -5 103.39 10.40 5 14 -5 99.59 8.90 -5 14 -5 108.79 11.10 -5 14 -5 105.69 10.20 6 14 -5 39.10 6.90 6 14 -5 34.90 12.30 6 14 -5 50.89 11.50 -6 14 -5 35.70 7.60 -6 14 -5 40.90 6.60 -7 14 5 105.39 10.30 7 14 -5 93.29 18.40 7 14 -5 97.79 9.80 7 14 -5 110.89 15.50 -7 14 -5 101.49 9.40 -7 14 -5 98.09 11.00 -8 14 5 42.20 6.90 8 14 -5 45.30 6.80 8 -14 5 38.40 8.00 8 14 -5 38.60 10.80 8 14 -5 33.40 13.40 -8 14 -5 48.10 9.10 8 -14 -5 21.30 10.10 8 14 5 55.69 7.60 9 -14 5 -0.50 4.20 9 14 -5 2.00 8.40 9 14 -5 -3.30 3.70 9 14 -5 9.90 11.40 9 -14 -5 10.70 9.30 -9 14 -5 11.90 3.50 9 14 5 4.70 4.50 -9 14 -5 7.20 5.70 10 14 -5 -3.50 9.70 10 14 -5 -10.10 7.10 10 -14 -5 -1.60 7.90 -10 14 -5 -1.30 5.10 11 14 -5 8.60 8.00 11 14 -5 13.60 12.20 -11 14 -5 11.50 5.90 11 -14 -5 -1.80 8.00 12 14 -5 -6.60 6.20 12 14 -5 7.20 10.80 -12 14 -5 3.00 4.80 12 -14 -5 -1.90 7.70 12 -14 -5 -1.20 11.00 13 14 -5 6.30 5.60 13 14 -5 19.40 11.90 -13 14 -5 17.20 4.40 13 -14 -5 7.10 11.30 13 -14 -5 -7.60 7.00 14 14 -5 -3.70 8.80 14 -14 5 -3.90 7.10 14 -14 -5 -4.60 10.00 14 -14 -5 22.00 11.10 15 -14 5 3.50 6.40 15 14 -5 35.20 9.30 15 -14 -5 30.40 7.70 15 -14 -5 22.90 11.30 0 15 -5 29.90 6.20 0 15 5 26.10 10.90 0 15 -5 23.90 6.30 1 15 -5 6.00 5.30 1 15 -5 15.50 5.00 -1 15 5 5.40 9.10 1 15 5 21.10 10.10 -1 15 -5 15.80 5.40 -1 15 -5 23.50 6.10 2 15 -5 54.59 7.30 2 15 -5 49.20 8.40 -2 15 -5 59.09 8.10 -2 15 -5 51.99 8.00 2 15 5 21.00 11.90 3 15 -5 33.40 11.70 3 15 -5 24.50 6.50 3 15 -5 31.70 6.00 -3 15 -5 21.30 6.20 -3 15 -5 42.80 7.00 4 15 -5 265.07 19.10 4 15 -5 293.57 26.40 4 15 -5 250.57 17.70 -4 15 -5 281.37 19.20 -4 15 -5 252.07 19.50 5 15 -5 41.40 13.00 5 15 -5 57.79 6.80 5 15 -5 43.10 7.90 -5 15 -5 52.79 7.70 -5 15 -5 58.19 9.10 -6 15 5 48.40 10.40 6 15 -5 46.20 13.60 6 15 -5 35.40 7.00 -6 15 -5 33.90 7.60 7 15 -5 7.00 10.80 7 15 -5 -1.40 8.10 -7 15 5 1.70 4.60 7 15 -5 3.10 4.60 -7 15 -5 3.50 4.50 -7 15 -5 5.40 6.00 8 15 -5 10.30 4.60 8 -15 5 -2.40 5.10 8 15 -5 12.70 9.10 8 15 -5 23.20 13.20 -8 15 5 -0.70 4.10 8 15 5 -1.00 4.80 8 -15 -5 4.40 9.00 -8 15 -5 10.70 4.50 -8 15 -5 6.80 6.20 9 15 -5 0.80 4.00 9 15 -5 16.90 11.90 9 -15 5 11.10 4.90 9 15 -5 0.10 7.40 -9 15 -5 11.40 6.30 9 15 5 13.90 4.80 -9 15 -5 7.20 3.70 9 -15 -5 7.90 9.20 10 15 -5 8.30 8.30 10 15 -5 37.50 13.60 -10 15 -5 7.60 6.10 10 -15 -5 -2.30 8.30 11 15 -5 3.10 7.30 11 15 -5 3.90 11.80 11 -15 -5 7.20 8.30 -11 15 -5 0.50 5.10 12 15 -5 49.40 14.60 -12 15 -5 44.70 7.80 12 -15 -5 60.59 14.00 12 -15 -5 15.10 9.10 13 15 -5 -19.80 8.60 -13 15 5 3.00 4.40 13 -15 -5 4.90 10.00 -13 15 -5 -2.10 3.60 13 -15 -5 7.10 8.30 14 -15 5 6.00 7.90 14 15 -5 5.60 11.90 14 -15 -5 -7.10 5.80 14 -15 -5 15.50 12.60 15 -15 5 -2.80 9.10 15 15 -5 -3.50 6.60 15 -15 -5 7.90 8.80 15 -15 -5 -17.50 5.90 0 16 -5 1.20 5.20 0 16 -5 -2.10 4.40 1 16 -5 29.30 6.10 1 16 -5 24.00 7.10 -1 16 -5 22.70 6.30 -1 16 -5 20.10 6.70 2 16 -5 6.30 4.50 -2 16 -5 -5.30 8.30 3 16 -5 130.79 10.60 3 16 -5 100.89 11.60 -3 16 -5 107.29 11.60 -3 16 -5 122.79 11.70 4 16 -5 72.89 7.90 4 16 -5 82.89 17.00 4 16 -5 59.59 9.30 -4 16 -5 60.69 9.80 -4 16 -5 77.39 9.30 5 16 -5 142.99 20.60 -5 16 5 111.09 12.10 5 16 -5 86.79 9.00 5 16 -5 110.89 11.20 -5 16 -5 117.09 12.10 -5 16 -5 108.59 10.90 6 16 -5 6.30 11.80 6 16 -5 9.90 5.90 -6 16 5 4.50 6.00 -6 16 -5 5.20 4.90 -6 16 -5 12.10 6.60 7 16 -5 42.50 13.80 7 16 -5 32.20 6.90 -7 16 5 37.90 7.00 -7 16 -5 46.90 8.70 -7 16 -5 27.00 6.10 7 16 5 30.50 6.90 8 -16 5 21.20 6.20 8 16 -5 8.20 12.00 -8 16 5 7.10 4.60 8 16 -5 23.30 5.60 -8 16 -5 15.60 6.90 -8 16 -5 22.00 5.10 8 -16 -5 0.10 8.70 8 16 5 23.10 6.10 9 16 -5 13.40 4.50 9 16 -5 14.00 13.10 9 -16 -5 11.10 9.70 -9 16 -5 17.00 4.40 9 16 5 12.20 4.60 -9 16 -5 18.70 7.00 10 16 -5 -6.20 19.40 10 -16 -5 -3.90 13.90 11 16 -5 25.90 13.50 -11 16 -5 67.99 9.50 11 -16 -5 22.30 9.90 12 16 -5 2.20 10.30 -12 16 -5 2.50 4.00 12 -16 -5 7.90 8.00 12 -16 -5 2.10 10.80 -13 16 5 10.40 4.80 13 16 -5 23.70 11.30 -13 16 -5 17.80 4.30 13 -16 -5 2.70 10.10 13 -16 -5 5.50 9.80 14 -16 5 -1.60 6.90 14 16 -5 2.60 7.70 14 -16 -5 -0.20 5.80 14 -16 -5 -9.20 7.60 0 17 -5 32.20 7.00 0 17 -5 29.20 7.40 1 17 -5 29.10 7.20 1 17 -5 27.30 6.40 -1 17 -5 25.20 7.20 -1 17 -5 30.70 6.90 2 17 -5 36.40 7.80 2 17 -5 42.40 10.10 -2 17 -5 38.50 7.90 -2 17 -5 41.70 8.40 3 17 -5 3.70 5.90 -3 17 -5 5.60 5.80 -3 17 -5 8.00 6.00 4 17 -5 5.10 5.90 -4 17 5 10.30 7.00 4 17 -5 13.10 6.60 -4 17 -5 1.80 5.80 -4 17 -5 7.60 5.80 5 17 -5 0.10 6.10 -5 17 5 13.60 7.00 5 17 -5 3.00 3.90 5 17 -5 9.00 11.50 -5 17 -5 17.50 6.30 -5 17 -5 10.10 6.50 -6 17 5 35.50 8.00 6 17 -5 51.29 14.30 6 17 -5 42.20 7.80 -6 17 -5 38.40 7.20 6 17 5 42.00 8.20 -6 17 -5 52.29 9.60 7 17 -5 9.60 12.50 -7 17 5 4.00 5.40 7 17 -5 8.20 5.30 7 17 5 5.60 5.60 -7 17 -5 2.60 6.60 -7 17 -5 12.90 5.30 8 17 -5 38.20 6.80 -8 17 5 33.00 6.20 8 -17 5 39.00 7.40 8 17 -5 46.80 14.80 -8 17 -5 66.29 11.10 -8 17 -5 45.00 7.10 8 17 5 49.60 7.80 8 -17 -5 52.19 11.80 9 17 -5 10.80 5.70 9 17 -5 10.20 17.50 9 -17 -5 -6.80 9.40 -9 17 -5 -1.50 6.60 10 17 -5 36.40 15.10 -10 17 -5 57.99 9.80 10 -17 -5 28.70 10.60 11 17 -5 -3.10 11.00 -11 17 -5 2.10 5.30 11 -17 -5 4.80 8.10 -12 17 5 21.20 5.90 12 17 -5 25.20 11.60 12 -17 -5 16.00 7.90 -12 17 -5 25.60 6.70 12 -17 -5 21.20 10.90 -13 17 5 5.90 4.00 13 17 -5 12.20 10.00 13 -17 -5 3.90 7.20 -13 17 -5 8.60 4.00 13 -17 -5 14.80 9.20 14 -17 5 16.90 8.80 14 17 -5 15.50 9.30 14 -17 -5 10.70 8.20 14 -17 -5 -11.00 6.70 0 18 -5 0.80 5.90 0 18 -5 -2.10 5.00 1 18 -5 9.00 6.60 1 18 -5 26.90 6.60 -1 18 -5 22.90 6.90 -1 18 -5 24.70 7.70 2 18 -5 67.69 10.70 2 18 -5 40.20 7.80 -2 18 -5 59.49 10.10 -2 18 -5 61.69 10.00 3 18 -5 25.50 7.60 3 18 -5 27.50 6.10 -3 18 5 34.60 8.60 -3 18 -5 34.90 8.00 -3 18 -5 37.70 8.10 -4 18 5 0.60 6.90 4 18 -5 18.10 6.70 4 18 -5 5.40 4.10 -4 18 -5 15.00 6.70 4 18 5 1.60 2.90 -4 18 -5 5.90 6.40 5 18 -5 33.10 7.80 -5 18 5 22.80 7.70 -5 18 -5 46.60 8.50 5 18 5 24.70 7.70 -5 18 -5 25.50 8.00 -6 18 5 -8.20 5.10 6 18 -5 0.10 5.70 6 18 -5 -1.60 11.90 6 18 5 1.60 5.90 -6 18 -5 -2.70 5.00 -6 18 -5 -0.10 6.40 7 18 -5 3.40 12.60 7 18 -5 8.10 5.80 -7 18 5 11.20 6.00 -7 18 -5 13.70 5.70 7 18 5 5.30 5.50 -7 18 -5 12.60 7.50 8 18 -5 1.60 20.40 8 18 -5 -2.90 5.80 8 -18 5 0.90 8.80 8 -18 -5 -3.70 10.40 -8 18 -5 1.00 6.00 -8 18 -5 5.10 11.10 9 18 -5 23.10 5.60 9 18 -5 51.69 15.30 -9 18 -5 59.59 10.30 9 -18 -5 47.40 11.50 9 18 5 28.40 6.20 10 18 -5 0.20 11.40 -10 18 -5 4.40 6.20 10 -18 -5 5.30 8.60 11 18 -5 15.30 12.00 -11 18 -5 22.20 6.20 11 -18 -5 25.30 9.40 -12 18 5 5.30 5.10 12 18 -5 3.00 10.80 12 -18 -5 17.40 14.10 -12 18 -5 6.60 4.30 12 -18 -5 10.70 7.10 -13 18 5 41.40 8.60 13 -18 -5 35.10 10.50 13 -18 -5 30.40 8.30 -13 18 -5 44.90 5.70 0 19 -5 0.70 5.30 0 19 -5 -8.30 6.00 0 19 5 -7.70 6.80 1 19 -5 47.80 9.10 -1 19 5 58.29 10.50 1 19 -5 46.50 9.20 -1 19 -5 64.59 10.90 -1 19 -5 61.79 10.40 2 19 -5 76.39 9.50 -2 19 5 70.39 11.60 2 19 -5 73.49 11.30 2 19 5 67.49 11.20 -2 19 -5 80.49 11.50 -2 19 -5 70.09 10.90 3 19 -5 2.10 6.30 3 19 -5 8.60 4.80 -3 19 5 2.30 7.40 3 19 5 9.10 7.60 -3 19 -5 -1.50 6.00 -3 19 -5 8.50 6.90 4 19 -5 59.39 10.20 -4 19 5 77.69 11.60 4 19 -5 42.80 6.90 -4 19 -5 72.99 10.70 -4 19 -5 79.69 11.40 4 19 5 51.29 9.80 -5 19 5 30.90 8.50 5 19 -5 39.30 8.20 5 19 5 31.90 8.50 -5 19 -5 30.00 7.60 -5 19 -5 43.90 8.80 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17.60 10.30 15 9 -7 23.20 7.50 15 -9 7 17.10 7.60 15 -9 -7 32.30 12.30 15 -9 -7 10.60 8.90 16 9 -7 48.70 14.30 16 9 -7 51.99 9.10 16 -9 -7 30.30 9.80 16 -9 -7 51.19 13.70 17 9 -7 5.50 7.50 17 -9 -7 18.90 10.00 17 -9 -7 27.60 10.70 0 10 7 4.30 6.80 0 10 -7 0.80 4.30 0 10 -7 2.20 3.00 0 10 -7 1.60 4.20 -1 10 7 545.35 43.70 1 10 -7 493.45 34.20 1 10 -7 521.85 31.40 1 10 7 518.45 41.10 -1 10 -7 521.55 32.20 2 10 -7 309.57 19.40 -2 10 7 317.37 31.60 2 10 -7 292.97 23.00 2 10 -7 338.17 23.40 -2 10 -7 297.27 19.80 2 10 7 321.07 28.40 -2 -10 7 268.17 26.80 3 10 -7 277.17 21.60 3 10 -7 274.47 17.70 3 10 -7 269.97 17.10 -3 10 7 293.97 30.10 3 10 -7 269.97 24.10 -3 10 -7 256.97 17.70 -3 -10 7 220.38 33.20 -3 10 -7 271.77 17.40 3 10 7 248.38 24.70 4 10 -7 299.27 17.80 4 10 -7 275.37 18.10 4 10 -7 291.47 22.90 -4 10 7 297.87 31.60 4 10 -7 270.27 22.50 -4 10 -7 279.97 18.10 -4 10 -7 267.37 18.50 -4 -10 7 244.98 23.30 4 10 7 281.27 25.70 5 10 -7 7.10 6.80 -5 10 7 10.20 9.30 5 10 -7 9.50 2.90 5 10 -7 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313.37 20.50 -3 -11 7 286.37 28.20 3 11 7 309.27 29.20 -3 11 -7 313.67 20.90 -4 11 7 409.86 41.20 4 11 -7 440.56 31.80 4 11 -7 452.35 31.20 4 11 -7 456.35 26.70 4 11 -7 441.46 26.20 -4 11 -7 426.56 26.90 -4 -11 7 350.26 32.60 -4 11 -7 433.26 26.40 4 11 7 395.46 34.60 5 11 -7 60.19 6.90 -5 11 7 62.39 17.80 5 11 -7 40.60 10.10 5 11 -7 60.79 12.80 5 11 -7 56.19 5.90 -5 11 -7 56.19 6.70 -5 -11 7 51.29 9.90 -5 -11 7 72.49 11.60 -5 11 -7 47.40 7.30 5 11 7 44.40 11.40 6 11 -7 186.28 18.90 6 11 -7 191.38 20.30 6 11 -7 184.78 13.40 -6 11 7 220.28 28.90 6 11 -7 180.68 12.70 -6 11 -7 200.28 14.60 6 11 7 174.28 19.10 -6 11 -7 187.38 13.40 7 11 -7 282.77 18.40 7 11 -7 290.27 24.90 -7 11 7 296.07 35.00 7 11 -7 309.47 26.60 -7 11 -7 306.37 19.60 -7 11 -7 274.07 18.20 7 -11 -7 302.87 22.00 7 11 7 208.58 24.10 8 11 -7 85.99 15.90 8 11 -7 131.49 18.50 8 11 -7 101.59 8.70 -8 11 -7 114.49 10.50 8 11 7 111.99 16.40 -8 11 -7 86.09 8.40 8 -11 -7 98.89 19.30 9 11 -7 206.98 24.30 9 11 -7 222.48 15.50 9 11 -7 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9.40 9 12 -7 19.40 11.40 9 12 -7 14.70 3.60 9 -12 -7 13.80 8.70 -9 12 -7 13.80 5.80 -9 12 -7 15.40 4.00 10 12 -7 1.90 8.50 10 12 -7 -1.20 10.10 10 -12 -7 2.60 8.10 -10 12 -7 -1.30 4.20 11 12 -7 94.89 19.50 11 12 -7 66.09 14.70 11 -12 -7 66.59 14.60 11 -12 -7 93.59 17.20 -11 12 -7 85.99 9.70 12 12 -7 10.50 12.60 12 12 -7 27.00 14.10 12 -12 -7 2.40 10.80 -12 12 -7 0.30 5.60 12 -12 -7 3.00 10.90 13 12 -7 24.00 13.10 13 12 -7 41.50 9.80 -13 12 -7 21.60 5.40 13 -12 -7 34.20 13.00 13 -12 -7 26.20 10.70 14 -12 7 3.80 6.30 14 12 -7 23.60 7.70 14 12 -7 30.70 11.50 14 -12 -7 31.30 12.90 14 -12 -7 4.40 7.50 15 12 -7 108.09 22.20 15 12 -7 108.99 12.00 15 -12 -7 145.89 21.40 16 12 -7 6.30 7.70 16 -12 -7 -5.70 8.40 16 -12 -7 6.80 8.50 0 13 7 439.06 41.90 0 13 -7 462.55 28.70 0 13 -7 453.65 28.70 1 13 -7 69.79 8.50 1 13 -7 74.49 8.10 1 13 -7 69.39 12.30 -1 13 7 101.19 19.40 -1 13 -7 74.29 8.50 -1 13 -7 68.19 8.50 1 13 7 92.59 17.70 -2 13 7 28.20 12.10 2 13 -7 58.99 7.20 2 13 -7 57.19 11.10 2 13 -7 66.39 8.00 2 13 7 44.90 13.00 -2 13 -7 66.49 8.00 -2 13 -7 73.89 8.20 3 13 -7 171.18 13.80 3 13 -7 198.98 19.60 3 13 -7 229.48 19.40 -3 13 7 174.08 27.40 3 13 -7 169.58 13.00 -3 13 -7 176.38 13.40 3 13 7 134.79 21.60 -3 13 -7 166.28 13.80 4 13 -7 1421.16 83.09 -4 13 7 1406.46 102.99 4 13 -7 1529.45 82.89 4 13 -7 1452.45 88.99 4 13 7 1262.97 93.09 -4 13 -7 1450.65 83.59 -4 13 -7 1465.15 83.09 5 13 -7 40.70 11.30 5 13 -7 41.60 5.80 5 13 -7 44.10 6.80 5 13 -7 35.90 10.10 -5 13 7 5.70 11.70 -5 13 -7 38.60 6.90 -5 13 -7 39.00 6.60 5 13 7 11.00 9.70 6 13 -7 716.83 42.80 6 13 -7 683.43 42.00 6 13 -7 732.43 48.20 6 13 -7 690.53 50.19 -6 13 -7 719.63 43.60 -6 13 -7 708.83 42.50 7 13 -7 121.69 19.00 7 13 -7 119.39 16.80 7 13 -7 109.79 10.30 -7 13 -7 123.89 11.70 -7 13 -7 117.79 10.10 8 13 -7 20.90 11.50 8 13 -7 28.10 5.30 -8 13 7 23.10 5.50 8 13 -7 22.60 10.30 -8 13 -7 33.40 6.90 8 -13 -7 30.00 10.00 -8 13 -7 24.70 4.90 9 13 -7 72.69 15.70 9 13 -7 48.60 6.50 9 13 -7 66.79 14.90 -9 13 -7 68.59 9.50 9 -13 -7 51.39 11.90 -9 13 -7 48.40 6.80 10 13 -7 105.39 20.40 10 13 -7 88.59 15.60 10 -13 -7 79.69 15.90 -10 13 -7 90.89 10.40 11 13 -7 -4.10 7.60 11 13 -7 -16.60 9.60 11 -13 -7 2.60 8.60 -11 13 -7 4.10 4.80 11 -13 -7 15.30 11.10 12 13 -7 4.70 7.90 12 13 -7 -4.30 11.10 12 -13 -7 3.80 11.10 -12 13 -7 3.90 4.40 12 -13 -7 3.30 9.20 13 13 -7 10.10 11.50 13 13 -7 1.60 6.20 -13 13 -7 11.20 4.00 13 -13 -7 10.90 11.60 13 -13 -7 5.40 8.80 14 -13 7 91.69 20.00 14 13 -7 149.59 19.00 14 13 -7 103.19 12.60 14 -13 -7 138.89 19.80 15 13 -7 8.50 8.90 15 -13 7 7.40 5.60 15 -13 -7 9.60 9.50 15 -13 -7 -2.20 6.70 16 13 -7 85.89 13.20 16 -13 -7 99.29 14.60 0 14 -7 -1.50 4.10 0 14 -7 0.60 4.30 0 14 7 17.10 10.20 -1 14 7 11.80 12.10 1 14 -7 8.20 4.70 1 14 -7 5.60 4.70 -1 14 -7 5.00 4.80 1 14 7 10.40 10.50 -1 14 -7 4.50 4.60 2 14 -7 923.01 55.49 -2 14 7 911.31 73.39 2 14 -7 965.80 60.59 2 14 -7 958.60 55.19 -2 14 -7 918.51 55.39 -2 14 -7 944.91 55.69 2 14 7 867.21 68.69 3 14 -7 488.85 30.00 3 14 -7 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5.80 -5 15 -7 14.50 6.30 -5 15 -7 10.90 5.30 6 15 -7 7.20 4.90 6 15 -7 1.90 10.50 6 15 -7 -6.70 8.60 -6 15 -7 5.50 4.70 -6 15 -7 -1.30 5.50 7 15 -7 274.87 19.10 -7 15 7 249.08 19.30 7 15 -7 336.87 26.40 7 15 -7 287.57 28.50 -7 15 -7 281.07 20.60 -7 15 -7 239.38 18.30 8 15 -7 21.00 12.50 -8 15 7 6.80 5.00 8 15 -7 5.10 4.50 8 15 -7 21.70 10.20 -8 15 -7 21.20 4.80 -8 15 -7 11.70 6.30 8 -15 -7 14.60 10.10 9 15 -7 176.08 23.70 9 15 -7 162.68 19.10 9 15 -7 146.89 12.10 9 15 7 123.99 12.40 -9 15 -7 174.48 12.20 -9 15 -7 164.28 14.80 9 -15 -7 139.29 18.00 10 15 -7 70.59 16.60 10 15 -7 99.59 15.90 -10 15 -7 84.49 10.20 10 -15 -7 60.29 13.90 11 15 -7 -6.60 10.80 11 15 -7 1.10 7.10 11 -15 -7 7.20 10.80 11 -15 -7 4.80 9.80 -11 15 -7 -0.60 5.00 12 15 -7 117.39 14.20 12 15 -7 121.89 19.30 12 -15 -7 57.49 14.40 -12 15 -7 112.79 10.50 12 -15 -7 144.29 18.60 13 15 -7 137.39 20.40 13 -15 -7 176.08 19.10 -13 15 -7 147.59 10.90 13 -15 -7 82.69 15.20 14 15 -7 25.80 9.70 14 -15 7 18.30 7.70 14 -15 -7 17.30 7.70 14 -15 -7 29.00 10.20 15 15 -7 11.20 8.30 15 -15 -7 14.90 6.80 15 -15 -7 -2.40 7.30 0 16 -7 -2.80 5.20 1 16 -7 436.96 28.40 1 16 -7 423.66 28.60 -1 16 -7 444.26 28.80 -1 16 -7 423.46 28.40 2 16 -7 240.78 16.90 2 16 -7 222.28 17.60 -2 16 -7 221.08 17.70 -2 16 -7 227.08 17.70 3 16 -7 61.19 9.40 3 16 -7 88.49 17.00 3 16 -7 64.79 8.30 -3 16 -7 54.99 9.50 -3 16 -7 79.69 9.50 4 16 -7 25.40 5.50 4 16 -7 20.60 6.40 4 16 -7 20.00 11.10 -4 16 -7 23.50 6.90 -4 16 -7 28.60 6.50 5 16 -7 47.40 8.30 5 16 -7 38.10 13.40 5 16 -7 23.80 5.20 -5 16 -7 36.10 7.00 -5 16 -7 48.10 9.40 6 16 -7 11.80 5.70 6 16 -7 17.70 11.60 -6 16 -7 17.80 5.90 -6 16 -7 10.20 6.60 7 16 -7 9.10 5.30 7 16 -7 21.60 13.00 -7 16 7 11.70 5.80 -7 16 -7 9.50 5.10 -7 16 -7 2.70 6.60 -8 16 7 44.80 7.60 8 16 -7 50.89 7.70 8 16 -7 45.50 14.70 -8 16 -7 51.89 7.40 8 -16 -7 37.30 11.80 8 16 7 40.40 7.50 -8 16 -7 68.89 10.80 9 16 -7 94.49 20.10 9 16 -7 103.89 9.50 9 -16 -7 126.89 17.20 -9 16 -7 103.39 9.40 -9 16 -7 120.49 12.60 9 16 7 78.49 9.60 10 16 -7 24.40 13.20 10 -16 -7 19.40 10.80 -10 16 -7 30.90 7.40 11 16 -7 346.77 33.30 11 -16 -7 438.66 29.70 11 -16 -7 250.47 26.50 -11 16 -7 353.06 23.60 12 16 -7 25.80 11.50 12 -16 -7 38.10 11.50 12 -16 -7 12.70 9.00 -12 16 -7 38.10 6.80 13 16 -7 115.99 22.30 -13 16 7 81.99 9.00 -13 16 -7 102.19 8.10 13 -16 -7 109.09 20.20 13 -16 -7 60.69 12.00 14 -16 7 5.00 7.30 14 16 -7 10.10 8.30 14 -16 -7 20.10 9.40 14 -16 -7 4.20 6.80 0 17 -7 539.05 34.60 1 17 -7 1.80 5.10 1 17 -7 -3.90 5.70 -1 17 -7 -6.20 5.40 -1 17 -7 4.10 5.90 2 17 -7 153.08 13.40 2 17 -7 155.78 14.80 -2 17 -7 170.88 14.70 -2 17 -7 184.98 15.20 3 17 -7 60.39 9.80 3 17 -7 81.59 8.90 -3 17 -7 62.09 10.10 -3 17 -7 68.89 10.10 4 17 -7 -1.40 10.00 4 17 -7 -2.70 5.80 4 17 -7 4.90 4.20 -4 17 -7 0.80 5.90 -4 17 -7 6.90 5.70 5 17 -7 9.70 11.80 5 17 -7 0.70 3.50 5 17 -7 11.80 6.10 -5 17 -7 9.80 6.00 -5 17 -7 12.30 6.80 6 17 -7 73.89 16.50 6 17 -7 43.90 8.50 -6 17 7 66.29 10.10 -6 17 -7 53.29 10.10 -6 17 -7 69.29 8.60 7 17 -7 43.40 7.40 -7 17 7 54.49 8.50 7 17 -7 34.60 14.00 -7 17 -7 34.10 6.70 -7 17 -7 39.10 9.00 8 17 -7 0.50 4.50 -8 17 7 8.30 4.80 8 17 -7 -7.70 10.90 8 17 7 -6.90 4.40 -8 17 -7 9.10 6.80 8 -17 -7 11.30 10.00 -8 17 -7 6.00 4.30 9 17 -7 -1.70 4.10 9 17 -7 9.10 12.40 -9 17 -7 -2.10 6.00 -9 17 -7 -2.80 4.60 9 17 7 -2.40 3.70 9 -17 -7 2.80 9.20 10 17 -7 432.86 34.70 -10 17 -7 380.26 25.10 10 -17 -7 287.87 27.90 11 17 -7 4.80 10.70 11 -17 -7 -6.10 9.00 -11 17 -7 2.40 4.60 11 -17 -7 -2.90 8.70 12 17 -7 403.66 33.00 12 -17 -7 396.66 30.50 12 -17 -7 321.57 31.70 -12 17 -7 408.36 25.30 -13 17 7 7.40 4.00 13 17 -7 6.10 8.40 13 -17 -7 -9.20 6.00 13 -17 -7 9.40 8.50 -13 17 -7 0.40 3.90 14 17 -7 6.80 7.20 14 -17 7 5.80 6.80 14 -17 -7 -12.00 7.30 14 -17 -7 16.90 8.30 0 18 -7 -8.50 5.40 0 18 -7 -0.70 5.30 1 18 -7 156.08 15.30 1 18 -7 170.98 14.30 -1 18 -7 171.58 14.90 -1 18 -7 162.88 15.10 2 18 -7 193.38 16.70 2 18 -7 200.68 15.70 -2 18 -7 217.48 16.80 -2 18 -7 186.38 16.60 3 18 -7 79.79 11.30 3 18 -7 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4.20 11.80 12 -12 -8 3.90 10.60 13 12 -8 9.30 11.00 13 12 -8 17.20 8.70 13 -12 -8 5.20 11.00 13 -12 -8 16.00 10.30 14 -12 8 35.50 11.00 14 12 -8 47.60 10.00 14 12 -8 36.20 12.40 14 -12 -8 24.90 11.80 14 -12 -8 25.10 9.50 15 -12 8 18.30 6.70 15 12 -8 15.30 6.20 15 12 -8 17.20 10.20 15 -12 -8 3.20 12.70 15 -12 -8 11.90 8.10 16 12 -8 8.10 8.10 16 -12 -8 25.90 10.70 16 -12 -8 -1.20 6.80 0 13 -8 -4.10 4.00 0 13 8 9.50 9.00 0 13 -8 0.70 4.00 1 13 -8 209.88 18.60 1 13 -8 182.58 13.80 -1 13 8 191.88 27.30 1 13 -8 170.58 13.90 -1 13 -8 164.28 13.70 -1 13 -8 173.08 14.00 1 13 8 197.78 23.30 -2 13 8 40.80 14.60 2 13 -8 73.29 12.00 2 13 -8 63.69 8.20 2 13 -8 51.49 7.40 2 13 8 49.90 14.10 -2 13 -8 57.79 8.10 -2 13 -8 61.79 8.20 3 13 -8 303.17 20.20 3 13 -8 391.66 26.60 3 13 -8 288.17 25.90 -3 13 8 338.47 38.70 3 13 -8 312.97 20.70 3 13 8 226.58 29.40 -3 13 -8 298.17 20.80 -3 13 -8 296.77 20.40 -4 13 8 4.20 9.30 4 13 -8 15.10 8.90 4 13 -8 6.40 4.10 4 13 -8 15.30 8.90 4 13 -8 9.20 4.90 -4 13 -8 14.90 5.20 -4 13 -8 10.70 5.30 4 13 8 8.40 8.80 5 13 -8 330.37 20.80 5 13 -8 363.26 27.80 5 13 -8 289.17 27.90 5 13 -8 312.57 21.20 -5 13 -8 327.57 22.20 -5 13 -8 293.47 20.90 6 13 -8 23.60 4.70 6 13 -8 24.80 5.50 6 13 -8 21.30 12.50 6 13 -8 27.90 10.60 -6 13 -8 25.90 5.50 -6 13 -8 31.60 7.00 7 13 -8 14.50 9.30 7 13 -8 2.00 3.90 7 13 -8 1.30 9.90 -7 13 -8 9.30 5.70 -7 13 -8 10.10 4.30 -8 13 8 -4.30 4.00 8 13 -8 3.60 10.90 8 13 -8 -9.60 7.90 8 13 -8 2.80 4.10 -8 13 -8 7.40 3.80 -8 13 -8 -3.50 5.20 8 -13 -8 0.10 8.50 9 13 -8 12.10 11.70 9 13 -8 13.50 4.30 9 13 -8 23.40 11.00 -9 13 -8 20.10 6.10 -9 13 -8 14.30 4.20 9 -13 -8 26.30 10.10 10 13 -8 -0.10 10.30 10 13 -8 2.00 8.80 10 13 8 0.80 5.00 10 -13 -8 -2.70 9.60 10 -13 -8 3.40 9.80 -10 13 -8 2.20 5.00 11 13 -8 1.40 8.50 11 13 -8 10.00 11.70 11 -13 -8 8.70 9.60 11 -13 -8 12.70 10.80 -11 13 -8 7.20 5.00 12 13 -8 8.60 8.10 12 13 -8 3.20 11.00 12 -13 -8 5.10 9.90 12 -13 -8 8.40 11.60 -12 13 -8 12.30 4.60 13 13 -8 7.20 6.70 13 13 -8 25.50 12.00 -13 13 -8 0.30 3.60 13 -13 -8 8.60 11.20 13 -13 -8 1.20 8.90 14 -13 8 -7.60 6.10 14 13 -8 -7.70 4.90 14 13 -8 -10.00 8.50 14 -13 -8 4.50 7.30 14 -13 -8 8.00 9.60 15 13 -8 29.20 9.60 15 -13 8 6.60 6.20 15 -13 -8 13.20 7.50 15 -13 -8 25.10 10.10 0 14 8 77.99 21.90 0 14 -8 104.99 10.00 0 14 -8 95.69 10.20 -1 14 8 106.59 22.40 1 14 -8 119.69 11.30 1 14 -8 107.09 10.90 -1 14 -8 135.29 11.80 1 14 8 132.99 22.80 -1 14 -8 118.39 11.10 2 14 -8 43.00 7.20 2 14 -8 61.59 13.00 2 14 -8 43.00 8.00 -2 14 8 31.60 13.60 -2 14 -8 37.70 6.80 -2 14 -8 40.40 7.90 2 14 8 30.80 12.70 3 14 -8 177.58 13.60 3 14 -8 168.68 14.10 3 14 -8 180.28 20.40 3 14 8 148.79 23.70 -3 14 -8 183.08 14.00 -3 14 -8 180.48 14.40 4 14 -8 372.96 31.60 4 14 -8 393.76 24.40 4 14 -8 491.55 31.70 4 14 -8 353.16 24.90 -4 14 -8 368.56 24.70 4 14 8 378.36 36.40 -4 14 -8 323.47 26.70 5 14 -8 21.50 11.40 5 14 -8 14.60 9.70 5 14 -8 8.40 5.10 5 14 -8 7.20 4.20 -5 14 -8 19.40 6.30 5 14 8 42.30 13.10 -5 14 -8 11.20 5.20 6 14 -8 43.40 6.80 6 14 -8 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16 -8 29.00 8.20 -7 16 8 5.30 5.50 7 16 -8 7.60 11.60 7 16 -8 5.40 4.80 -7 16 -8 5.60 4.80 -7 16 -8 6.90 6.30 8 16 -8 2.00 11.40 -8 16 8 -1.00 3.90 8 16 -8 2.10 4.20 -8 16 -8 0.20 5.90 8 -16 -8 -1.70 9.30 -8 16 -8 6.70 4.10 9 16 -8 32.60 15.90 9 16 -8 25.90 12.30 9 -16 -8 22.10 11.20 -9 16 -8 33.30 7.90 10 16 -8 75.99 16.30 10 -16 -8 46.20 12.60 -10 16 -8 47.80 9.30 10 -16 -8 42.50 12.20 11 16 -8 -4.50 11.10 11 -16 -8 -4.10 8.90 11 -16 -8 1.50 9.60 -11 16 -8 3.80 5.10 12 16 -8 92.99 16.70 -12 16 -8 44.80 8.90 12 -16 -8 52.79 12.40 12 -16 -8 52.99 12.10 13 16 -8 3.20 9.40 13 -16 -8 9.90 9.10 13 -16 -8 -0.40 7.60 -13 16 -8 2.30 3.90 14 16 -8 12.60 8.60 14 -16 8 0.10 6.40 14 -16 -8 -2.10 5.80 14 -16 -8 6.60 8.00 0 17 -8 8.60 5.80 0 17 -8 0.20 5.70 1 17 -8 64.19 9.30 1 17 -8 57.39 10.00 -1 17 -8 64.29 10.10 -1 17 -8 59.39 9.90 2 17 -8 11.50 5.70 2 17 -8 15.60 6.80 -2 17 -8 10.40 6.60 -2 17 -8 8.10 6.20 3 17 -8 27.50 6.40 3 17 -8 35.40 7.50 -3 17 -8 35.00 7.20 -3 17 -8 26.00 7.30 4 17 -8 3.00 5.70 4 17 -8 7.50 4.20 4 17 -8 13.90 11.50 -4 17 -8 4.70 6.00 -4 17 -8 -5.10 5.40 5 17 -8 0.00 4.00 5 17 -8 12.50 11.80 5 17 -8 5.50 5.90 -5 17 -8 16.40 6.00 -5 17 -8 2.60 6.40 6 17 -8 39.70 14.40 6 17 -8 36.00 7.20 -6 17 8 23.70 7.30 -6 17 -8 36.20 7.00 -6 17 -8 33.80 8.40 7 17 -8 34.30 7.00 7 17 -8 10.40 12.50 -7 17 8 36.90 7.20 -7 17 -8 27.20 6.20 7 -17 -8 42.80 11.30 -7 17 -8 36.30 8.40 8 17 -8 -8.10 11.00 8 17 -8 -3.50 7.10 -8 17 -8 5.00 6.60 8 -17 -8 2.50 9.50 -8 17 -8 -11.40 6.10 8 17 8 5.20 8.10 9 17 -8 24.50 4.90 9 17 -8 5.90 12.60 9 17 8 5.80 4.40 9 -17 -8 0.70 9.20 -9 17 -8 11.20 6.70 10 17 -8 5.30 11.90 10 -17 -8 12.80 10.30 10 -17 -8 6.60 9.60 -10 17 -8 -1.40 5.30 11 17 -8 119.69 20.20 11 -17 -8 119.19 16.90 11 -17 -8 98.89 15.50 -11 17 -8 140.09 11.80 12 17 -8 7.00 10.40 -12 17 -8 1.10 3.60 12 -17 -8 5.00 10.50 12 -17 -8 12.90 12.60 -13 17 8 15.30 5.60 13 17 -8 12.80 9.40 13 -17 -8 2.50 6.30 13 -17 -8 24.20 9.00 0 18 -8 32.60 7.00 0 18 -8 17.50 7.20 1 18 -8 -0.20 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28.10 9.10 13 18 -8 -8.70 6.90 13 -18 -8 0.80 6.70 13 -18 -8 1.20 5.50 0 19 -8 0.50 6.00 0 19 -8 -1.10 6.10 1 19 -8 1.50 6.30 1 19 -8 2.10 5.40 -1 19 -8 -0.30 6.30 -1 19 -8 -4.30 5.70 2 19 -8 11.10 7.00 2 19 -8 14.80 5.90 -2 19 -8 18.80 7.40 -2 19 -8 9.90 7.30 3 19 -8 12.40 7.10 3 19 -8 5.60 4.90 -3 19 -8 10.30 6.80 -3 19 -8 2.10 6.40 -4 19 8 79.89 12.60 4 19 -8 72.99 10.80 4 19 -8 53.79 7.90 -4 19 -8 92.39 11.50 -4 19 -8 80.69 10.20 5 19 -8 57.19 9.80 -5 19 8 48.40 9.50 -5 19 -8 41.00 9.00 -5 19 -8 50.39 9.40 -6 19 8 -1.90 5.30 6 19 -8 8.30 5.70 6 19 8 1.00 5.70 -6 19 -8 0.20 5.00 -6 19 -8 -2.60 6.80 7 19 -8 10.60 5.60 -7 19 8 0.70 5.40 -7 19 -8 15.20 5.20 7 19 8 1.80 5.70 -7 19 -8 -0.90 6.40 7 -19 -8 16.40 9.70 -8 19 8 12.10 5.30 8 19 -8 20.70 5.30 8 -19 -8 18.50 9.60 8 19 8 12.20 4.70 -8 19 -8 28.70 8.00 -8 19 -8 35.50 5.90 9 -19 -8 2.50 8.50 -9 19 -8 10.90 6.20 9 19 8 -2.90 4.80 9 -19 -8 -2.00 7.50 10 -19 -8 -5.60 6.90 -10 19 -8 2.70 5.10 10 -19 -8 -1.60 7.00 -11 19 -8 8.40 4.50 11 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182.48 18.50 -9 8 -9 166.78 11.30 -9 8 -9 161.68 12.90 10 8 -9 34.20 11.10 10 8 -9 14.00 9.90 10 -8 -9 22.10 9.70 -10 8 -9 25.30 5.20 10 -8 -9 18.30 8.20 11 8 -9 323.17 30.40 11 8 -9 342.47 30.60 11 -8 -9 376.76 27.70 -11 8 -9 340.97 22.90 11 -8 -9 433.96 30.80 12 8 -9 -6.30 8.70 12 8 -9 9.80 10.20 12 -8 -9 2.60 8.40 12 -8 -9 7.40 10.70 13 8 -9 39.00 13.30 13 8 -9 34.70 12.10 13 -8 9 38.30 10.00 13 -8 -9 31.10 12.50 13 -8 -9 17.00 10.00 14 -8 9 -0.70 5.20 14 8 -9 -3.80 9.50 14 8 -9 4.50 8.00 14 -8 -9 -4.00 10.50 14 -8 -9 6.50 9.30 15 8 -9 17.90 7.60 15 8 -9 14.10 9.70 15 -8 -9 8.60 10.50 15 -8 -9 -1.70 8.20 16 8 -9 6.80 10.70 16 8 -9 1.40 5.40 16 -8 -9 -10.00 13.50 16 -8 -9 8.40 7.60 17 8 -9 -2.80 6.00 17 -8 -9 -8.20 7.80 17 -8 -9 -7.00 7.70 0 9 9 773.12 73.59 0 9 -9 821.12 47.30 0 9 -9 762.52 49.40 0 9 -9 846.32 53.49 1 9 -9 11.20 3.50 -1 9 9 -1.60 6.20 1 9 -9 3.60 5.40 1 9 -9 5.30 5.10 1 9 -9 7.10 3.50 -1 9 -9 9.30 3.80 -1 9 -9 7.10 3.40 1 9 9 4.30 7.30 2 9 -9 237.08 20.00 -2 9 9 281.77 29.70 2 9 -9 275.57 17.20 2 9 -9 247.38 20.90 2 9 -9 267.47 17.20 -2 9 -9 267.57 17.50 -2 9 -9 272.37 17.20 2 9 9 233.28 25.40 3 9 -9 56.89 6.60 3 9 -9 59.79 6.30 -3 9 9 43.70 13.40 3 9 -9 75.89 11.30 3 9 -9 64.19 10.80 -3 -9 9 57.59 13.10 -3 9 -9 62.79 6.50 -3 9 -9 69.89 7.10 3 9 9 72.19 13.40 -4 9 9 12.40 10.50 4 9 -9 22.90 4.40 4 9 -9 21.00 8.30 4 9 -9 30.60 4.40 4 9 -9 22.00 7.90 -4 9 -9 23.90 4.30 -4 -9 9 16.10 4.60 -4 -9 9 20.40 8.30 -4 9 -9 24.20 4.70 4 9 9 18.70 8.10 5 9 -9 2.40 7.10 5 9 -9 2.20 6.30 -5 9 9 7.10 9.70 5 9 -9 -4.60 2.50 5 9 -9 3.60 3.10 -5 -9 9 -4.30 5.40 -5 9 -9 5.50 3.30 -5 9 -9 -2.20 3.30 -5 -9 9 2.40 3.40 5 9 9 -4.50 5.20 -6 9 9 3.80 9.80 6 9 -9 10.90 8.30 6 9 -9 6.00 3.10 6 9 -9 5.50 3.30 6 9 -9 -9.20 6.00 -6 -9 9 5.80 4.10 -6 9 -9 3.50 3.80 6 9 9 9.10 6.50 -6 9 -9 7.40 3.50 6 -9 -9 4.70 5.20 -7 9 9 90.39 19.30 7 9 -9 70.39 14.10 7 9 -9 69.09 6.80 7 9 -9 80.09 14.30 7 9 -9 85.49 7.20 -7 9 -9 85.79 7.20 7 -9 -9 89.79 10.80 7 9 9 80.99 12.90 -7 9 -9 75.29 8.50 8 9 -9 28.00 4.50 8 9 -9 21.10 9.90 -8 9 9 22.20 14.90 8 9 -9 29.20 10.60 -8 9 -9 30.80 6.00 8 -9 -9 33.70 9.00 -8 9 -9 31.90 4.90 8 -9 -9 32.20 7.70 9 9 -9 8.70 9.80 9 9 -9 6.90 9.50 9 -9 -9 2.40 6.50 9 -9 -9 8.40 8.20 -9 9 -9 10.70 3.00 -9 9 -9 19.20 5.00 10 9 -9 316.37 30.40 10 9 -9 290.87 29.30 10 -9 -9 350.56 26.50 -10 9 -9 328.67 22.40 10 -9 -9 421.36 29.00 11 9 -9 7.30 9.70 11 9 -9 1.10 10.20 11 -9 -9 1.60 9.90 11 -9 -9 5.90 8.50 -11 9 -9 0.80 3.40 12 9 -9 177.88 22.50 12 9 -9 209.38 25.10 -12 9 -9 222.88 15.00 12 -9 -9 183.38 20.60 12 -9 -9 245.48 24.50 13 9 -9 1.90 8.90 13 9 -9 10.00 11.00 13 -9 -9 11.70 12.70 13 -9 -9 19.20 10.00 14 9 -9 6.10 10.50 14 9 -9 5.20 8.10 14 -9 9 9.00 5.70 14 -9 -9 8.50 11.20 14 -9 -9 6.70 9.40 15 9 -9 10.80 7.30 15 9 -9 -3.80 8.00 15 -9 -9 15.90 9.50 15 -9 -9 10.70 11.30 16 9 -9 3.50 7.90 16 9 -9 6.90 5.00 16 -9 -9 6.30 7.70 16 -9 -9 1.80 8.60 17 9 -9 -4.50 5.70 17 -9 -9 4.90 8.70 17 -9 -9 -8.00 6.10 0 10 -9 -1.60 4.00 0 10 -9 1.10 3.30 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17.30 13.90 7 10 -9 12.90 3.20 7 10 -9 8.70 8.50 7 10 -9 19.70 9.00 -7 10 9 -7.40 11.20 7 10 -9 12.90 3.80 -7 10 -9 14.90 5.00 -7 10 -9 11.30 3.80 7 -10 -9 10.50 6.90 7 10 9 -10.00 7.30 8 10 -9 200.38 22.90 8 10 -9 195.68 24.10 8 10 -9 222.18 15.00 -8 10 -9 226.98 16.40 8 -10 -9 228.88 19.00 -8 10 -9 234.38 15.20 9 10 -9 40.80 12.20 9 10 -9 42.40 12.30 9 -10 -9 70.19 14.00 -9 10 -9 69.99 8.30 -9 10 -9 39.80 5.80 9 -10 -9 66.39 11.50 10 10 -9 10.40 10.60 10 10 -9 21.00 11.70 10 -10 -9 16.20 9.30 -10 10 -9 28.20 5.80 10 -10 -9 23.60 11.00 11 10 -9 359.66 32.10 11 10 -9 372.66 33.80 11 -10 -9 381.86 30.00 -11 10 -9 376.76 24.80 11 -10 -9 415.26 31.30 12 10 -9 4.60 9.30 12 10 -9 16.50 12.00 -12 10 -9 10.90 4.40 12 -10 -9 16.90 11.30 12 -10 -9 13.20 9.90 13 10 -9 10.30 9.10 13 10 -9 31.40 12.00 13 -10 -9 35.90 13.20 13 -10 -9 31.40 11.30 14 10 -9 50.99 13.10 14 10 -9 27.40 9.30 14 -10 9 22.40 6.80 14 -10 -9 79.19 16.80 14 -10 -9 41.90 12.40 15 10 -9 8.10 6.70 15 10 -9 -0.10 8.50 15 -10 -9 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11 -9 175.68 20.50 -6 11 9 205.58 30.30 6 11 -9 179.18 20.30 6 11 -9 219.48 14.00 -6 11 -9 180.88 14.50 -6 11 -9 207.58 13.90 6 11 9 133.49 20.10 7 11 -9 165.78 12.10 7 11 -9 149.09 21.10 7 11 -9 120.89 13.60 7 11 -9 154.68 20.30 -7 11 -9 175.28 12.30 -7 11 -9 178.78 13.50 8 11 -9 38.50 5.90 8 11 -9 47.80 11.90 8 11 -9 55.49 13.00 8 -11 -9 38.40 9.50 -8 11 -9 38.30 7.80 -8 11 -9 43.30 6.10 9 11 -9 92.39 17.60 9 11 -9 113.29 20.10 9 11 -9 101.79 9.10 -9 11 -9 111.99 11.00 -9 11 -9 123.89 9.40 9 -11 -9 154.18 16.70 9 -11 -9 104.79 15.30 10 11 -9 73.39 16.10 10 11 -9 78.39 17.20 10 -11 -9 90.79 15.00 -10 11 -9 83.19 9.90 10 -11 -9 123.89 16.90 11 11 -9 6.50 11.30 11 11 -9 1.00 8.60 -11 11 -9 1.40 4.50 11 -11 -9 -3.50 9.00 11 -11 -9 10.50 9.60 12 11 -9 99.09 24.00 12 11 -9 70.99 22.30 -12 11 -9 86.69 12.90 12 -11 -9 94.49 18.30 12 -11 -9 83.79 18.70 13 11 -9 45.10 12.10 13 11 -9 81.59 17.30 13 -11 -9 83.09 16.80 13 -11 -9 64.79 14.50 14 -11 9 20.50 11.10 14 11 -9 17.20 7.50 14 11 -9 14.70 11.10 14 -11 -9 6.20 8.60 14 -11 -9 6.40 11.40 15 11 -9 -2.50 5.10 15 11 -9 4.90 10.90 15 -11 -9 1.00 7.90 15 -11 -9 6.50 10.10 16 11 -9 23.50 8.60 16 -11 -9 41.30 11.60 16 -11 -9 26.90 8.60 0 12 -9 0.60 3.90 0 12 -9 -1.60 3.90 0 12 9 -0.20 7.70 1 12 -9 17.20 5.20 -1 12 9 28.90 12.20 1 12 -9 34.50 6.30 1 12 -9 22.60 7.30 1 12 9 20.30 9.80 -1 12 -9 34.80 6.40 -1 12 -9 29.00 5.70 2 12 -9 0.90 4.00 2 12 -9 4.30 8.00 2 12 -9 0.90 5.70 2 12 -9 0.60 3.50 -2 12 9 5.70 9.40 -2 12 -9 2.90 4.20 -2 12 -9 2.20 4.30 2 12 9 -14.20 5.90 3 12 -9 37.70 9.90 3 12 -9 45.60 7.40 3 12 -9 50.09 6.40 -3 12 9 33.20 13.00 3 12 -9 48.40 10.90 -3 12 -9 36.80 7.00 -3 12 -9 49.40 7.50 3 12 9 26.00 10.40 -4 12 9 16.90 11.50 4 12 -9 23.00 5.30 4 12 -9 26.50 5.00 4 12 -9 29.90 9.70 4 12 -9 17.40 9.30 4 12 9 19.50 9.30 -4 12 -9 19.30 5.50 -4 12 -9 21.30 4.90 5 12 -9 468.05 27.40 5 12 -9 427.46 27.60 -5 12 9 500.45 48.30 5 12 -9 477.45 34.00 5 12 -9 424.96 34.30 -5 12 -9 437.86 27.50 5 12 9 379.86 37.30 -5 12 -9 419.16 28.40 6 12 -9 38.90 6.00 6 12 -9 38.80 11.90 6 12 -9 38.20 11.30 6 12 -9 38.70 6.20 6 12 9 10.10 12.40 -6 12 -9 45.50 8.10 -6 12 -9 39.30 6.70 7 12 -9 374.36 24.90 7 12 -9 398.26 33.50 7 12 -9 388.86 32.00 7 -12 -9 431.36 29.30 -7 12 -9 388.76 24.90 -7 12 -9 388.26 26.10 8 12 -9 14.80 4.20 8 12 -9 -2.10 9.40 8 12 -9 9.90 9.50 -8 12 -9 12.70 4.50 8 -12 -9 11.30 8.20 -8 12 -9 15.00 5.70 9 12 -9 28.30 5.00 9 12 -9 24.60 10.90 9 12 -9 26.80 12.50 -9 12 -9 38.90 5.80 9 -12 -9 43.00 11.20 9 -12 -9 41.40 10.80 -9 12 -9 31.00 6.70 10 12 -9 15.90 12.40 10 12 -9 16.90 11.10 10 -12 -9 19.30 10.50 -10 12 -9 17.90 5.90 10 -12 -9 10.80 9.30 11 12 -9 6.30 11.50 11 12 -9 7.30 10.10 11 -12 -9 17.20 10.70 -11 12 -9 25.60 5.70 11 -12 -9 7.90 10.50 12 12 -9 24.10 10.50 12 12 -9 10.40 11.80 -12 12 -9 26.60 5.30 12 -12 -9 10.70 10.90 12 -12 -9 18.80 11.00 13 12 -9 11.50 11.70 13 12 -9 23.10 9.10 13 -12 -9 11.30 10.50 13 -12 -9 12.40 11.70 14 -12 9 13.90 7.20 14 12 -9 1.70 8.90 14 12 -9 3.80 9.30 14 -12 -9 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24.20 6.70 1 6 -12 80.29 11.60 1 6 -12 106.49 8.50 1 6 -12 65.49 11.00 1 6 -12 95.29 8.20 -1 6 12 120.99 17.20 -1 -6 -12 104.59 7.60 -1 6 -12 113.59 11.80 -1 -6 12 114.69 12.80 1 6 12 107.99 16.60 -1 6 -12 111.29 8.70 1 -6 -12 80.19 8.50 1 -6 -12 108.99 7.90 -1 6 -12 111.99 8.40 2 6 -12 6.40 3.10 2 6 -12 3.40 5.70 2 6 -12 2.80 3.10 -2 6 12 0.90 8.10 -2 -6 -12 4.80 2.50 2 6 -12 0.80 3.70 2 6 12 11.50 7.70 2 -6 -12 1.30 2.70 -2 6 -12 5.30 3.00 -2 6 -12 4.30 3.60 2 -6 -12 1.90 3.40 -2 -6 12 -0.70 3.90 -3 6 12 24.50 10.40 3 6 -12 31.60 5.10 3 6 -12 21.50 6.20 3 6 -12 29.60 5.00 3 6 -12 31.50 8.60 -3 -6 -12 27.50 3.90 -3 6 -12 24.00 4.50 -3 -6 12 22.90 6.50 3 -6 -12 25.90 5.30 3 -6 -12 32.80 6.60 3 -6 -12 30.50 4.40 3 6 12 19.60 9.00 -3 6 -12 23.70 4.80 -4 -6 -12 22.30 3.60 -4 6 12 12.70 9.00 4 6 -12 25.70 4.70 4 6 -12 26.20 4.60 4 6 -12 25.90 8.50 4 6 -12 27.80 10.70 -4 6 -12 22.80 4.30 4 6 12 32.50 10.00 4 -6 -12 14.90 5.40 -4 6 -12 21.90 4.60 4 -6 -12 34.60 4.90 4 -6 -12 31.10 6.10 -4 -6 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34.00 6.70 2 7 -12 39.40 5.60 2 7 -12 29.50 6.80 -2 7 12 19.50 9.90 2 7 -12 41.10 5.70 2 7 -12 28.20 8.30 2 -7 -12 32.50 5.90 2 -7 -12 40.30 4.80 2 7 12 24.60 9.60 -2 7 -12 30.60 5.90 -2 -7 12 37.30 7.90 -2 7 -12 34.10 5.50 3 7 -12 17.30 4.30 3 7 -12 16.00 7.70 -3 7 12 20.70 9.80 3 7 -12 24.10 6.50 -3 -7 -12 14.80 3.10 3 7 -12 19.20 4.30 3 -7 -12 24.10 4.60 3 7 12 29.60 9.90 -3 -7 12 31.40 7.10 -3 7 -12 18.20 4.70 3 -7 -12 9.30 4.60 -3 7 -12 17.80 4.10 -4 -7 -12 79.99 6.60 -4 7 12 91.19 18.40 4 7 -12 80.89 7.80 4 7 -12 66.89 10.50 4 7 -12 75.19 13.30 4 7 -12 86.49 7.70 4 -7 -12 91.59 7.80 4 -7 -12 85.09 9.80 4 7 12 101.29 15.40 -4 7 -12 88.89 7.80 4 -7 -12 76.09 9.10 -4 -7 12 92.99 11.70 -4 7 -12 96.89 8.80 5 7 -12 6.20 3.40 5 7 -12 5.50 3.40 5 7 -12 11.50 8.00 -5 7 12 21.40 10.60 5 7 -12 15.20 6.70 -5 -7 -12 5.50 2.10 -5 7 -12 10.10 3.80 5 -7 -12 7.60 5.30 -5 -7 12 5.20 5.30 5 -7 -12 8.50 5.20 5 -7 -12 5.70 3.70 -5 7 -12 4.40 3.80 5 7 12 3.80 6.30 -6 -7 -12 7.20 2.10 6 7 -12 14.30 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10.30 13 -7 -12 -4.50 8.70 14 7 -12 5.80 9.30 14 7 -12 9.00 9.90 14 -7 -12 6.70 9.70 14 -7 -12 13.10 11.20 15 7 -12 -11.90 7.00 15 7 -12 -5.10 6.60 15 -7 -12 3.70 10.20 15 -7 -12 12.30 10.20 16 7 -12 -2.50 7.10 16 7 -12 0.80 6.10 16 -7 -12 7.10 9.00 16 -7 -12 7.10 7.90 0 8 -12 43.70 6.10 0 8 -12 32.40 8.40 0 8 12 37.90 11.80 0 -8 -12 29.90 4.50 0 8 -12 37.50 6.10 -1 -8 -12 0.50 2.40 1 8 -12 7.70 4.90 1 8 -12 -1.30 5.80 -1 8 12 -2.90 7.00 1 8 -12 0.00 3.30 1 8 -12 1.20 3.10 -1 8 -12 1.10 3.60 -1 8 -12 0.00 3.70 1 8 12 4.00 6.90 1 -8 -12 3.20 2.80 1 -8 -12 6.00 3.70 -2 8 12 2.90 7.70 -2 -8 -12 2.80 2.50 2 8 -12 -3.50 5.30 2 8 -12 4.50 3.50 2 8 -12 1.20 4.20 2 8 -12 1.20 3.60 -2 -8 12 2.60 4.40 2 8 12 0.10 6.10 -2 8 -12 -1.50 3.50 2 -8 -12 1.90 3.40 2 -8 -12 0.60 2.90 -2 8 -12 2.80 3.60 -3 8 12 3.10 8.50 3 8 -12 6.30 7.40 3 8 -12 8.10 6.80 3 8 -12 1.10 3.70 -3 -8 -12 4.60 2.60 3 8 -12 8.90 4.00 -3 -8 12 14.30 4.80 -3 8 -12 8.00 4.20 3 -8 -12 8.00 3.40 3 8 12 -5.00 6.60 3 -8 -12 13.10 4.50 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3.50 6.70 9 8 -12 -5.30 8.30 9 8 -12 -2.00 9.10 -9 8 -12 4.60 3.00 -9 8 -12 3.40 4.30 9 -8 -12 -2.80 6.80 9 -8 -12 11.60 8.90 10 8 -12 21.60 12.10 10 8 -12 22.80 11.30 -10 8 -12 26.80 5.30 10 -8 -12 30.10 11.30 10 -8 -12 14.80 8.90 11 8 -12 5.90 10.50 11 8 -12 2.70 10.00 11 -8 -12 4.10 9.60 -11 8 -12 -2.00 3.20 11 -8 -12 5.60 8.70 12 8 -12 -3.90 9.40 12 8 -12 0.10 9.80 12 -8 -12 -4.90 8.50 12 -8 -12 5.40 10.60 13 8 -12 0.10 9.60 13 8 -12 -5.10 8.60 13 -8 -12 -1.50 8.80 13 -8 -12 -4.80 10.40 14 8 -12 7.90 9.70 14 8 -12 5.70 8.40 14 -8 -12 10.70 9.10 14 -8 -12 1.30 9.70 15 8 -12 0.40 8.50 15 8 -12 -8.00 8.60 15 -8 -12 10.00 10.50 15 -8 -12 7.20 9.30 16 8 -12 15.60 8.40 16 8 -12 6.40 5.50 16 -8 -12 18.40 8.60 16 -8 -12 7.40 8.60 0 9 -12 4.30 4.00 0 9 -12 -7.00 4.20 0 9 -12 6.90 6.70 0 9 12 13.90 8.20 0 9 -12 2.60 3.70 0 -9 -12 -0.50 2.80 -1 9 12 27.40 11.60 1 9 -12 29.80 8.60 1 9 -12 13.60 4.50 1 9 -12 16.60 5.70 -1 -9 -12 20.00 3.80 1 9 -12 17.10 4.80 1 -9 -12 24.40 4.90 -1 9 -12 37.20 6.00 -1 9 -12 17.30 4.70 1 9 12 18.90 9.00 1 -9 -12 19.80 4.20 2 9 -12 4.00 4.00 -2 -9 -12 6.40 2.90 2 9 -12 4.30 3.90 -2 9 12 6.70 8.30 2 9 -12 2.90 6.70 2 9 -12 3.50 5.10 -2 9 -12 7.40 4.00 2 9 12 9.00 9.10 -2 9 -12 6.00 4.40 2 -9 -12 9.00 3.40 3 9 -12 5.40 3.80 3 9 -12 0.40 5.50 3 9 -12 7.30 4.10 -3 9 12 -1.40 9.40 3 9 -12 -1.20 7.00 -3 -9 12 0.00 3.80 -3 9 -12 2.10 4.30 3 9 12 6.50 7.70 -3 9 -12 7.80 4.10 3 -9 -12 5.60 5.10 4 9 -12 31.70 8.70 4 9 -12 40.70 6.20 -4 9 12 48.40 15.10 4 9 -12 33.90 10.20 4 9 -12 40.20 6.30 4 -9 -12 39.20 7.00 -4 9 -12 42.70 6.30 4 9 12 24.90 10.40 -4 -9 12 34.40 7.50 -4 9 -12 44.30 7.30 5 9 -12 4.80 6.80 5 9 -12 10.90 8.90 5 9 -12 17.60 4.50 5 9 -12 11.00 4.20 -5 9 12 19.70 10.60 5 -9 -12 10.20 5.70 -5 9 -12 8.30 4.80 -5 -9 12 13.00 6.90 5 -9 -12 8.30 5.90 -5 9 -12 17.90 4.40 5 9 12 13.30 8.30 6 9 -12 5.40 3.70 6 9 -12 11.30 9.40 6 9 -12 13.20 8.40 6 9 -12 6.90 3.80 -6 9 12 8.80 11.60 -6 9 -12 5.70 3.90 6 -9 -12 8.30 6.20 6 9 12 -2.50 9.30 6 -9 -12 2.50 5.90 -6 9 -12 7.60 4.70 7 9 -12 15.40 4.10 7 9 -12 7.70 9.80 7 9 -12 8.00 3.60 7 9 12 16.30 11.90 7 -9 -12 7.90 7.00 -7 9 -12 19.80 5.30 -7 9 -12 7.30 3.90 7 -9 -12 25.20 7.60 8 9 -12 14.00 3.80 8 9 -12 1.30 3.00 8 9 -12 2.50 9.00 8 9 -12 -6.30 8.40 8 -9 -12 2.10 7.80 -8 9 -12 9.10 3.70 -8 9 -12 -1.40 4.20 8 -9 -12 4.90 7.20 9 9 -12 15.20 10.20 9 9 -12 -2.40 9.00 -9 9 -12 4.10 4.50 9 -9 -12 6.40 8.70 9 -9 -12 8.20 8.20 10 9 -12 10.50 10.70 10 9 -12 -8.00 8.70 10 -9 -12 7.60 9.80 -10 9 -12 6.30 4.30 10 -9 -12 -1.00 7.90 11 9 -12 27.20 12.20 11 9 -12 6.40 10.80 11 -9 -12 13.50 10.70 -11 9 -12 4.60 4.20 11 -9 -12 6.00 8.90 12 9 -12 2.00 9.70 12 9 -12 -0.60 10.00 12 -9 -12 9.20 10.90 12 -9 -12 3.90 9.70 13 9 -12 0.70 10.30 13 9 -12 -6.00 8.30 13 -9 -12 5.60 9.40 13 -9 -12 3.50 10.50 14 9 -12 -1.20 7.30 14 9 -12 -5.40 9.00 14 -9 -12 -11.60 8.60 14 -9 -12 1.00 8.80 15 9 -12 16.80 10.10 15 9 -12 7.80 6.00 15 -9 -12 5.80 8.10 15 -9 -12 -11.90 9.20 16 9 -12 8.10 8.00 16 9 -12 5.10 6.70 16 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21.00 4.80 5 -10 -12 19.60 6.90 -5 -10 12 2.30 6.90 5 -10 -12 12.00 5.70 6 10 -12 2.40 8.20 6 10 -12 5.30 3.90 6 10 -12 10.90 9.40 6 10 -12 9.10 4.00 6 10 12 31.10 12.00 -6 10 -12 9.00 4.20 -6 10 -12 6.50 5.60 6 -10 -12 3.90 6.10 7 10 -12 24.80 10.50 7 10 -12 16.10 4.20 7 10 -12 9.40 10.20 7 10 -12 22.10 4.70 -7 10 -12 24.60 6.30 7 -10 -12 19.00 8.00 7 -10 -12 17.90 8.00 -7 10 -12 25.90 5.10 8 10 -12 13.70 10.60 8 10 -12 10.00 4.00 8 10 -12 8.40 10.00 8 -10 -12 2.80 7.80 -8 10 -12 12.10 4.10 8 -10 -12 12.50 8.00 -8 10 -12 5.50 5.00 9 10 -12 -5.10 5.40 9 10 -12 -0.30 9.60 9 10 -12 -4.40 10.00 9 -10 -12 7.40 9.00 -9 10 -12 4.10 4.70 9 -10 -12 9.30 8.50 -9 10 -12 2.50 3.20 10 10 -12 17.80 11.40 10 10 -12 28.00 12.20 10 -10 -12 29.40 10.70 -10 10 -12 14.20 5.50 10 -10 -12 9.90 10.30 11 10 -12 1.90 10.10 11 10 -12 1.50 9.80 -11 10 -12 1.80 3.70 11 -10 -12 -5.10 8.70 11 -10 -12 -2.90 9.70 12 10 -12 20.20 11.00 12 10 -12 32.00 13.40 -12 10 -12 1.10 3.50 12 -10 -12 1.40 10.30 12 -10 -12 15.60 10.80 13 10 -12 6.20 10.40 13 10 -12 -5.60 7.30 13 -10 -12 -3.70 9.00 13 -10 -12 4.60 10.70 14 10 -12 -2.50 8.90 14 10 -12 1.70 7.10 14 -10 -12 2.50 9.30 14 -10 -12 -3.90 9.20 15 10 -12 -8.70 7.50 15 10 -12 4.00 6.10 15 -10 -12 -5.90 8.20 15 -10 -12 2.40 8.50 0 11 -12 3.70 4.60 0 11 -12 7.50 4.50 1 11 -12 88.19 13.90 -1 11 12 32.80 13.80 1 11 -12 50.49 7.90 1 11 -12 61.99 10.40 1 11 -12 57.79 7.70 1 11 12 46.30 14.50 1 -11 -12 57.29 10.40 -1 11 -12 60.19 8.10 -1 11 -12 60.29 8.00 -2 11 12 93.09 20.40 2 11 -12 62.69 11.80 2 11 -12 75.59 8.90 2 11 -12 84.69 8.80 2 11 -12 105.69 14.80 -2 11 -12 84.89 9.70 -2 11 -12 90.79 9.10 2 11 12 67.99 17.90 2 -11 -12 72.79 8.30 3 11 -12 0.80 7.70 3 11 -12 2.10 4.20 3 11 -12 -4.50 4.20 -3 11 12 -0.60 11.20 3 11 -12 -12.80 6.00 -3 11 -12 0.50 4.10 -3 11 -12 1.30 4.60 3 -11 -12 3.00 4.30 -3 -11 12 1.80 5.50 4 11 -12 3.60 4.00 4 11 -12 0.10 7.20 4 11 -12 5.80 8.60 4 11 -12 -0.30 4.20 4 -11 -12 11.80 5.30 4 11 12 2.80 14.60 -4 11 -12 9.50 4.50 -4 11 -12 1.60 4.90 -4 -11 12 -1.60 5.10 5 11 -12 19.90 5.40 5 11 -12 23.80 9.70 5 11 -12 24.50 5.20 5 11 -12 18.40 10.50 5 11 12 15.30 12.10 -5 11 -12 19.60 5.20 5 -11 -12 28.10 7.10 6 11 -12 10.50 4.40 6 11 -12 9.90 9.80 6 11 -12 11.00 4.60 6 11 -12 12.10 9.10 6 11 12 14.90 12.70 -6 11 -12 12.20 5.80 6 -11 -12 9.50 7.10 -6 11 -12 15.60 5.90 6 -11 -12 11.50 7.70 7 11 -12 -0.10 3.90 7 11 -12 13.70 3.90 7 11 -12 -9.40 8.90 7 11 -12 5.90 9.60 -7 11 -12 9.90 4.50 7 -11 -12 5.70 7.50 7 -11 -12 8.70 7.80 -7 11 -12 2.70 5.50 8 11 -12 4.00 9.50 8 11 -12 4.40 3.70 8 11 -12 4.40 10.10 8 -11 -12 3.70 7.80 -8 11 -12 0.10 4.90 -8 11 -12 -1.40 3.60 8 -11 -12 -5.90 7.20 9 11 -12 6.40 10.10 9 11 -12 10.70 4.20 9 11 -12 3.60 9.90 9 -11 -12 6.10 8.80 9 -11 -12 6.70 8.60 -9 11 -12 1.50 3.30 -9 11 -12 -3.80 4.20 10 11 -12 24.40 12.20 10 11 -12 25.60 12.20 10 -11 -12 18.20 10.00 -10 11 -12 13.70 5.80 10 -11 -12 15.40 10.40 11 11 -12 35.90 15.20 11 11 -12 83.49 26.50 -11 11 -12 36.70 7.30 12 11 -12 -10.70 9.90 12 11 -12 4.40 9.20 12 -11 -12 -1.60 9.70 12 -11 -12 5.80 11.00 -12 11 -12 1.30 3.30 13 11 -12 -11.40 9.00 13 11 -12 7.50 8.50 13 -11 -12 -5.60 8.60 13 -11 -12 -9.70 9.20 14 11 -12 -9.90 7.60 14 11 -12 7.10 6.80 14 -11 -12 -13.10 7.50 14 -11 -12 -9.00 8.20 15 11 -12 1.30 5.70 15 11 -12 -2.00 6.70 15 -11 -12 -4.30 7.30 15 -11 -12 1.70 7.40 0 12 12 159.68 23.90 0 12 -12 177.48 13.80 0 12 -12 168.28 13.60 -1 12 12 40.80 13.90 1 12 -12 37.00 8.50 1 12 -12 32.90 6.70 1 12 -12 41.70 7.80 1 12 12 41.80 13.00 -1 12 -12 45.10 8.10 -1 12 -12 41.90 7.50 2 12 -12 18.60 5.50 2 12 -12 13.10 9.10 2 12 -12 9.10 5.40 2 12 -12 13.00 7.40 2 12 12 50.09 14.40 -2 12 -12 5.60 5.40 2 -12 -12 11.80 4.10 -2 12 -12 11.30 5.40 3 12 -12 19.50 5.70 3 12 -12 16.80 5.40 3 12 -12 21.10 9.80 3 12 -12 23.70 8.80 -3 -12 12 17.30 5.50 -3 12 -12 11.60 5.80 3 -12 -12 11.10 4.90 3 12 12 11.70 11.40 -3 12 -12 15.90 5.30 4 12 -12 14.70 10.20 4 12 -12 7.80 5.00 4 12 -12 3.60 4.40 4 12 -12 9.20 8.60 -4 12 -12 8.70 6.60 -4 12 -12 2.50 5.20 4 -12 -12 4.20 5.20 5 12 -12 3.70 4.70 5 12 -12 -3.70 3.80 5 12 -12 -4.20 8.50 -5 12 -12 2.30 5.40 5 12 12 9.40 14.70 -5 12 -12 -1.20 4.30 5 -12 -12 7.80 6.30 6 12 -12 48.30 7.10 6 12 -12 36.30 12.10 6 12 -12 43.50 6.70 6 12 -12 38.40 12.20 6 -12 -12 34.90 9.00 -6 12 -12 53.89 7.10 6 -12 -12 42.50 9.70 -6 12 -12 33.60 7.40 7 12 -12 25.90 11.70 7 12 -12 22.10 5.20 7 12 -12 19.20 11.30 7 12 -12 8.10 3.90 7 -12 -12 24.30 8.80 -7 12 -12 27.20 5.50 -7 12 -12 10.80 6.20 7 -12 -12 22.10 9.40 8 12 -12 -1.50 3.70 8 12 -12 7.40 10.10 8 12 -12 -2.10 9.90 8 -12 -12 11.40 8.60 -8 12 -12 -4.70 5.10 -8 12 -12 0.90 3.60 8 -12 -12 -0.30 7.70 9 12 -12 18.00 4.70 9 12 -12 18.00 12.50 9 12 -12 33.20 12.40 -9 12 -12 18.10 4.50 -9 12 -12 24.30 6.50 9 -12 -12 36.20 10.60 9 -12 -12 20.70 9.90 10 12 -12 13.50 11.90 10 12 -12 25.40 12.10 -10 12 -12 10.80 6.60 10 -12 -12 5.90 9.50 10 -12 -12 26.90 10.90 11 12 -12 19.50 12.10 11 12 -12 -2.60 9.30 11 -12 -12 9.30 10.20 -11 12 -12 3.00 4.60 11 -12 -12 4.60 10.40 12 12 -12 3.80 9.30 12 12 -12 -0.70 9.80 12 -12 -12 7.90 10.50 12 -12 -12 -2.70 10.20 -12 12 -12 -0.10 3.10 13 12 -12 -1.00 6.80 13 12 -12 -6.30 8.80 13 -12 -12 0.90 9.30 13 -12 -12 0.50 9.00 14 12 -12 2.60 7.90 14 12 -12 -1.40 5.30 14 -12 -12 8.10 8.50 14 -12 -12 0.50 9.20 15 12 -12 -5.70 4.90 15 12 -12 -2.10 7.00 15 -12 -12 -0.10 7.30 15 -12 -12 1.20 7.30 0 13 -12 0.30 5.40 0 13 -12 6.20 7.50 1 13 -12 147.19 12.80 1 13 -12 143.09 14.10 -1 13 -12 135.69 12.90 2 13 -12 5.00 5.00 2 13 -12 4.70 5.20 2 13 -12 6.50 6.60 2 -13 -12 0.80 3.80 -2 13 -12 2.50 5.10 -2 13 -12 3.60 5.40 3 13 -12 14.60 8.00 3 13 -12 4.60 4.90 3 13 -12 1.30 5.20 3 13 -12 -4.10 9.10 3 -13 -12 5.60 4.90 -3 13 -12 0.90 4.90 -3 13 -12 0.40 5.30 -3 -13 12 12.70 8.60 4 13 -12 5.50 13.30 4 13 -12 -5.80 4.60 4 13 -12 -5.30 9.50 4 13 -12 6.20 5.10 -4 13 -12 -0.90 5.20 -4 13 -12 0.70 4.90 4 -13 -12 -1.40 5.40 5 13 -12 1.40 6.20 5 13 -12 5.20 10.70 5 13 -12 10.30 5.20 5 13 -12 19.40 10.90 -5 13 -12 4.30 5.70 -5 13 -12 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1.00 5.70 6 1 -22 8.60 5.40 6 1 -22 -0.90 6.90 6 -1 -22 -6.20 6.00 6 -1 -22 3.60 5.70 -6 1 -22 11.00 4.30 -6 1 -22 3.60 4.80 6 -1 -22 -1.00 5.10 7 1 -22 120.09 10.80 -7 -1 -22 97.89 8.70 7 1 -22 86.69 15.90 7 1 -22 80.89 12.60 7 -1 -22 127.99 10.60 -7 1 -22 117.19 9.30 7 -1 -22 100.89 15.70 7 -1 -22 84.29 12.30 -7 1 -22 104.99 10.00 8 1 -22 -7.60 6.90 8 1 -22 7.70 6.90 8 1 -22 4.20 4.50 8 -1 -22 -2.00 6.40 -8 1 -22 2.30 2.80 8 -1 -22 9.00 4.80 8 -1 -22 -0.50 8.30 9 1 -22 25.20 5.30 9 1 -22 26.50 9.40 9 1 -22 24.90 8.30 9 -1 -22 21.20 7.70 9 -1 -22 33.70 10.80 10 1 -22 -7.20 6.00 10 1 -22 7.00 7.70 10 -1 -22 -2.90 5.50 10 -1 -22 4.70 7.70 11 1 -22 56.59 10.00 11 1 -22 20.70 9.90 11 -1 -22 25.20 8.30 11 -1 -22 19.30 8.70 12 1 -22 -2.60 6.10 12 1 -22 -9.30 5.50 12 -1 -22 11.40 7.40 12 -1 -22 -6.20 6.00 0 -2 -22 140.59 12.90 0 -2 -22 141.89 12.70 0 2 -22 174.18 13.90 0 2 -22 167.48 13.60 1 2 -22 5.40 5.40 -1 -2 -22 10.40 5.20 -1 -2 -22 11.30 5.80 1 2 -22 3.40 5.60 -1 2 -22 15.80 5.90 1 -2 -22 7.40 5.30 1 -2 -22 2.80 5.50 -1 2 -22 20.80 6.10 2 2 -22 69.79 9.60 2 2 -22 72.79 10.40 2 2 -22 60.59 9.40 -2 -2 -22 67.59 8.70 -2 -2 -22 76.39 9.40 -2 2 -22 76.89 9.40 2 -2 -22 74.99 9.00 -2 2 -22 69.49 9.40 2 -2 -22 76.79 9.30 3 2 -22 0.20 5.70 3 2 -22 3.30 5.30 3 2 -22 0.30 5.00 -3 -2 -22 2.50 5.50 -3 -2 -22 0.00 4.20 -3 2 -22 1.90 5.10 -3 2 -22 7.70 5.80 3 -2 -22 1.60 5.00 3 -2 -22 4.50 5.10 -4 -2 -22 17.20 6.20 4 2 -22 16.60 5.90 4 2 -22 12.10 7.70 -4 -2 -22 17.30 5.00 4 2 -22 30.60 6.20 4 -2 -22 25.50 6.00 4 -2 -22 11.70 6.20 4 -2 -22 22.30 6.10 -4 2 -22 17.60 5.60 -4 2 -22 21.90 6.10 5 2 -22 5.40 7.90 -5 -2 -22 -3.40 3.70 -5 -2 -22 5.30 5.30 5 2 -22 -2.10 4.70 5 2 -22 1.60 5.10 5 -2 -22 9.50 6.30 -5 2 -22 2.80 4.60 -5 2 -22 0.30 5.00 5 -2 -22 3.70 5.20 5 -2 -22 0.60 5.50 -6 -2 -22 113.09 9.80 6 2 -22 89.49 13.70 6 2 -22 150.18 11.90 6 2 -22 133.69 10.90 6 2 -22 124.29 16.60 6 -2 -22 113.39 13.30 6 -2 -22 89.29 14.70 -6 2 -22 115.99 10.50 6 -2 -22 125.59 11.80 -6 2 -22 140.59 11.50 7 2 -22 10.00 4.30 7 2 -22 5.00 4.80 -7 -2 -22 7.70 3.00 7 2 -22 -3.20 6.30 7 2 -22 0.10 8.40 7 -2 -22 9.30 8.10 7 -2 -22 4.20 5.10 -7 2 -22 1.00 4.40 -7 2 -22 7.60 3.90 7 -2 -22 -4.90 5.90 8 2 -22 36.00 9.60 8 2 -22 39.80 6.80 8 2 -22 31.50 10.80 8 -2 -22 36.30 10.30 -8 2 -22 46.20 6.70 8 -2 -22 36.20 7.20 8 -2 -22 46.20 9.40 -8 2 -22 28.80 5.30 9 2 -22 5.40 4.20 9 2 -22 0.00 8.00 9 2 -22 5.90 6.80 9 -2 -22 1.00 5.90 9 -2 -22 -2.70 6.40 10 2 -22 17.70 8.60 10 2 -22 25.60 9.60 10 -2 -22 27.00 8.80 10 -2 -22 7.60 7.60 11 2 -22 4.30 6.20 11 2 -22 3.20 7.60 11 -2 -22 -0.30 7.30 11 -2 -22 -1.70 5.80 12 2 -22 -0.20 6.90 12 2 -22 6.00 6.90 12 -2 -22 15.00 6.90 12 -2 -22 -2.70 5.10 0 3 -22 1.30 5.30 0 3 -22 4.70 5.50 0 -3 -22 -2.50 4.60 0 -3 -22 -5.60 5.00 1 3 -22 107.99 11.30 -1 -3 -22 110.69 11.10 1 3 -22 101.99 10.90 -1 -3 -22 112.59 10.40 -1 3 -22 94.99 10.70 1 -3 -22 102.79 10.60 1 -3 -22 79.99 10.10 -1 3 -22 107.09 11.50 -2 -3 -22 -0.30 4.60 2 3 -22 5.40 5.60 -2 -3 -22 2.60 5.40 2 3 -22 1.00 5.50 2 3 -22 9.50 5.70 -2 3 -22 -2.40 5.00 2 -3 -22 -0.50 5.50 2 -3 -22 7.80 5.20 -2 3 -22 2.50 5.40 3 3 -22 27.00 6.50 -3 -3 -22 33.40 5.90 3 3 -22 48.50 8.20 -3 -3 -22 38.30 7.20 3 3 -22 28.00 8.50 -3 3 -22 18.00 6.10 3 -3 -22 28.70 6.50 -3 3 -22 19.00 6.50 4 3 -22 -1.90 4.60 4 3 -22 -3.00 6.60 4 3 -22 4.70 5.30 -4 -3 -22 1.50 4.20 -4 3 -22 -5.70 5.00 4 -3 -22 7.80 5.40 -4 3 -22 -1.50 4.90 5 3 -22 104.79 9.90 5 3 -22 75.09 9.10 -5 -3 -22 81.79 8.10 5 3 -22 86.59 13.70 -5 3 -22 72.59 9.50 5 -3 -22 51.79 11.00 -5 3 -22 98.99 9.10 5 -3 -22 58.89 10.40 5 -3 -22 86.89 9.40 6 3 -22 0.00 4.90 6 3 -22 3.20 5.20 -6 -3 -22 4.50 4.30 6 3 -22 -12.60 6.40 -6 3 -22 -5.50 4.60 6 -3 -22 3.80 8.80 6 -3 -22 -0.40 7.40 6 -3 -22 0.10 5.10 -6 3 -22 0.30 4.60 7 3 -22 66.59 7.90 7 3 -22 82.59 9.30 7 3 -22 63.29 11.60 7 3 -22 74.89 15.60 -7 -3 -22 75.79 6.70 7 -3 -22 82.59 9.20 7 -3 -22 43.30 10.90 -7 3 -22 86.89 8.70 -7 3 -22 80.59 7.90 7 -3 -22 55.49 11.40 8 3 -22 5.30 4.40 8 3 -22 -4.60 6.30 8 3 -22 3.60 9.10 -8 3 -22 4.90 3.30 8 -3 -22 7.10 7.60 8 -3 -22 12.00 7.30 -8 3 -22 4.70 4.00 9 3 -22 27.60 8.20 9 3 -22 16.20 4.80 9 3 -22 37.80 11.20 -9 3 -22 25.10 4.90 9 -3 -22 19.80 7.60 9 -3 -22 26.90 8.80 10 3 -22 3.20 8.80 10 3 -22 -15.80 7.20 10 -3 -22 17.10 7.50 10 -3 -22 13.80 6.90 11 3 -22 22.90 6.90 11 3 -22 30.50 9.40 11 -3 -22 10.30 6.50 11 -3 -22 14.20 7.70 12 3 -22 2.00 6.70 12 3 -22 -7.10 7.90 12 -3 -22 9.20 7.40 12 -3 -22 -2.10 6.10 0 -4 -22 102.29 10.00 0 4 -22 98.59 11.10 0 4 -22 99.49 10.50 1 4 -22 1.90 5.80 -1 -4 -22 6.20 5.00 1 4 -22 0.90 5.50 -1 4 -22 5.00 5.70 -1 4 -22 -3.20 5.10 1 -4 -22 1.60 5.00 2 4 -22 15.90 6.40 -2 -4 -22 21.20 5.50 2 4 -22 21.50 7.80 2 4 -22 16.40 6.10 -2 4 -22 13.80 6.20 2 -4 -22 19.30 5.80 -2 4 -22 20.60 6.50 3 4 -22 3.40 7.50 -3 -4 -22 4.50 4.50 3 4 -22 11.00 5.70 3 4 -22 7.20 5.50 -3 4 -22 1.30 5.20 -3 4 -22 4.90 6.00 3 -4 -22 6.60 5.40 -4 -4 -22 51.09 7.10 4 4 -22 34.40 7.00 4 4 -22 42.10 10.20 4 4 -22 53.39 8.60 4 -4 -22 48.10 7.90 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76.59 13.70 7 5 -22 96.79 16.60 7 -5 -22 84.09 12.80 -7 5 -22 96.89 9.40 -7 5 -22 98.79 9.50 7 -5 -22 76.89 12.00 8 5 -22 17.50 10.90 8 5 -22 7.70 4.30 8 5 -22 8.80 3.50 8 5 -22 4.50 6.50 8 -5 -22 -0.30 6.50 8 -5 -22 14.90 6.70 -8 5 -22 12.90 4.30 -8 5 -22 11.20 4.00 9 5 -22 37.20 9.30 9 5 -22 25.20 5.50 9 5 -22 39.50 11.30 -9 5 -22 46.50 6.00 -9 5 -22 38.90 5.80 9 -5 -22 24.50 8.00 9 -5 -22 27.70 8.80 10 5 -22 8.90 8.10 10 5 -22 0.90 5.80 10 -5 -22 8.80 7.20 10 -5 -22 -2.20 6.80 11 5 -22 21.70 6.40 11 5 -22 27.10 9.40 11 -5 -22 7.80 6.20 11 -5 -22 2.40 5.70 12 5 -22 -0.70 6.10 12 5 -22 3.90 6.60 12 -5 -22 11.40 8.40 12 -5 -22 7.80 6.50 0 6 -22 196.38 15.90 0 6 -22 203.18 16.20 0 -6 -22 199.48 14.90 -1 -6 -22 12.80 5.00 1 6 -22 5.40 6.20 1 6 -22 -0.80 5.50 -1 6 -22 8.50 5.70 1 -6 -22 6.20 5.30 -1 6 -22 7.80 6.00 2 6 -22 66.79 9.80 2 6 -22 73.29 9.30 -2 -6 -22 72.59 8.60 2 -6 -22 60.29 8.90 -2 6 -22 59.49 9.50 -2 6 -22 72.29 10.00 -3 -6 -22 6.30 4.50 3 6 -22 -0.30 5.50 3 6 -22 9.60 5.80 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33.20 6.00 7 7 -22 50.09 7.30 7 7 -22 42.80 11.80 -7 7 -22 53.79 7.10 7 -7 -22 26.60 8.00 -7 7 -22 40.00 6.90 8 7 -22 25.20 5.00 8 7 -22 22.50 11.20 -8 7 -22 26.70 5.00 8 -7 -22 17.60 6.80 8 -7 -22 27.30 7.80 -8 7 -22 31.20 5.40 9 7 -22 11.80 8.50 9 7 -22 32.60 10.30 9 -7 -22 41.30 8.00 -9 7 -22 16.10 3.80 -9 7 -22 14.90 4.00 9 -7 -22 55.99 9.70 10 7 -22 -0.80 6.90 10 7 -22 -15.80 7.80 10 -7 -22 10.20 6.10 10 -7 -22 -0.40 5.90 11 7 -22 18.60 8.20 11 7 -22 5.60 6.70 11 -7 -22 14.50 6.60 11 -7 -22 -2.50 8.00 12 7 -22 -9.60 5.30 12 -7 -22 1.50 5.00 0 8 -22 32.30 7.20 0 8 -22 26.70 7.20 0 -8 -22 25.90 6.00 -1 -8 -22 -0.30 4.30 1 8 -22 1.40 5.90 1 8 -22 2.40 5.90 -1 8 -22 2.20 6.00 1 -8 -22 1.50 5.00 -1 8 -22 0.40 6.00 -2 -8 -22 89.69 9.10 2 8 -22 81.49 10.90 2 8 -22 86.79 10.90 -2 8 -22 107.09 11.20 -2 8 -22 93.49 10.90 2 -8 -22 77.29 9.80 3 8 -22 9.60 6.00 -3 -8 -22 8.10 5.00 3 8 -22 14.70 6.20 -3 8 -22 21.50 7.50 -3 8 -22 15.50 6.40 4 8 -22 50.49 8.30 4 8 -22 68.99 14.60 4 8 -22 64.59 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5.00 4 9 -22 5.40 9.10 -4 9 -22 0.80 5.80 -4 9 -22 4.10 5.30 4 -9 -22 -7.30 4.50 5 9 -22 47.60 6.80 5 9 -22 23.30 5.90 5 9 -22 42.10 12.40 -5 9 -22 28.70 7.00 -5 9 -22 25.70 6.30 5 -9 -22 10.50 5.90 6 9 -22 -3.30 3.80 6 9 -22 0.50 3.80 6 9 -22 -5.60 8.70 -6 9 -22 -1.50 4.30 6 -9 -22 0.10 4.80 -6 9 -22 -1.90 5.20 7 9 -22 12.30 4.30 7 9 -22 13.70 4.40 7 9 -22 4.00 9.50 -7 9 -22 8.30 4.90 -7 9 -22 14.90 4.70 7 -9 -22 12.90 5.80 8 9 -22 5.10 8.00 8 9 -22 4.20 3.40 8 -9 -22 -7.20 4.80 -8 9 -22 7.90 3.90 -8 9 -22 2.70 4.10 9 9 -22 49.70 12.60 -9 9 -22 66.39 7.10 9 -9 -22 31.80 7.60 -9 9 -22 34.70 5.20 10 9 -22 14.40 8.10 10 -9 -22 11.00 6.20 11 9 -22 26.50 8.70 11 -9 -22 3.80 7.90 0 10 -22 17.30 6.80 0 10 -22 21.20 7.00 1 10 -22 10.00 6.30 1 10 -22 6.30 6.10 -1 10 -22 -4.60 5.80 -1 10 -22 6.20 6.40 2 10 -22 61.49 9.60 2 10 -22 82.89 10.40 -2 10 -22 82.09 10.30 -2 10 -22 69.69 10.30 3 10 -22 5.70 5.70 3 10 -22 -5.00 5.50 -3 10 -22 11.00 6.50 -3 10 -22 -3.80 5.30 3 -10 -22 1.80 5.00 4 10 -22 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0.00 3 9 26 -3.86 0.00 4 9 26 2.09 0.00 5 9 26 0.00 0.00 6 9 26 0.30 0.00 0 10 26 2.30 0.00 1 10 26 2.28 0.00 2 10 26 5.36 0.00 3 10 26 -1.18 0.00 4 10 26 1.98 0.00 5 10 26 -1.04 0.00 6 10 26 1.55 0.00 1 11 26 -3.79 0.00 2 11 26 -1.72 0.00 3 11 26 -3.57 0.00 4 11 26 0.53 0.00 5 11 26 -1.07 0.00 0 12 26 2.20 0.00 1 12 26 1.95 0.00 2 12 26 3.69 0.00 3 12 26 1.23 0.00 4 12 26 0.73 0.00 1 13 26 -2.09 0.00 2 13 26 -1.49 0.00 1 0 27 -0.66 0.00 3 0 27 1.27 0.00 5 0 27 3.77 0.00 0 1 27 -0.26 0.00 1 1 27 1.89 0.00 2 1 27 1.32 0.00 3 1 27 -1.07 0.00 4 1 27 -2.76 0.00 5 1 27 1.10 0.00 6 1 27 -0.45 0.00 7 1 27 -2.05 0.00 1 2 27 -0.63 0.00 2 2 27 -1.18 0.00 3 2 27 0.05 0.00 4 2 27 0.80 0.00 5 2 27 2.13 0.00 6 2 27 -2.23 0.00 7 2 27 -4.57 0.00 0 3 27 -0.93 0.00 1 3 27 2.17 0.00 2 3 27 0.87 0.00 3 3 27 0.15 0.00 4 3 27 -3.76 0.00 5 3 27 0.33 0.00 6 3 27 3.61 0.00 7 3 27 -1.25 0.00 1 4 27 0.83 0.00 2 4 27 -2.31 0.00 3 4 27 1.13 0.00 4 4 27 1.49 0.00 5 4 27 0.60 0.00 6 4 27 1.27 0.00 7 4 27 -4.28 0.00 0 5 27 -2.06 0.00 1 5 27 0.44 0.00 2 5 27 0.79 0.00 3 5 27 -0.29 0.00 4 5 27 -0.68 0.00 5 5 27 -1.56 0.00 6 5 27 1.79 0.00 7 5 27 0.00 0.00 1 6 27 0.04 0.00 2 6 27 0.48 0.00 3 6 27 0.69 0.00 4 6 27 0.37 0.00 5 6 27 -0.29 0.00 6 6 27 0.54 0.00 0 7 27 -1.65 0.00 1 7 27 -1.08 0.00 2 7 27 -0.81 0.00 3 7 27 0.83 0.00 4 7 27 -1.74 0.00 5 7 27 -1.50 0.00 6 7 27 2.03 0.00 1 8 27 1.85 0.00 2 8 27 0.36 0.00 3 8 27 2.16 0.00 4 8 27 0.01 0.00 5 8 27 -1.28 0.00 6 8 27 3.50 0.00 0 9 27 -0.51 0.00 1 9 27 -0.81 0.00 2 9 27 -1.92 0.00 3 9 27 0.02 0.00 4 9 27 0.60 0.00 5 9 27 -0.42 0.00 1 10 27 -0.50 0.00 2 10 27 0.47 0.00 3 10 27 1.82 0.00 4 10 27 -0.87 0.00 0 11 27 1.56 0.00 1 11 27 0.17 0.00 2 11 27 -0.74 0.00 3 11 27 -0.24 0.00 0 0 28 3.87 0.00 2 0 28 -0.71 0.00 4 0 28 3.81 0.00 6 0 28 -0.77 0.00 1 1 28 -1.64 0.00 2 1 28 1.04 0.00 3 1 28 -0.83 0.00 4 1 28 -0.03 0.00 5 1 28 -4.08 0.00 6 1 28 -0.32 0.00 0 2 28 1.59 0.00 1 2 28 -1.76 0.00 2 2 28 0.54 0.00 3 2 28 -0.70 0.00 4 2 28 2.33 0.00 5 2 28 1.08 0.00 6 2 28 0.83 0.00 1 3 28 -0.94 0.00 2 3 28 0.69 0.00 3 3 28 0.07 0.00 4 3 28 -1.15 0.00 5 3 28 -1.30 0.00 6 3 28 1.47 0.00 0 4 28 0.73 0.00 1 4 28 -0.21 0.00 2 4 28 0.50 0.00 3 4 28 2.20 0.00 4 4 28 1.12 0.00 5 4 28 -1.83 0.00 6 4 28 -0.61 0.00 1 5 28 -1.87 0.00 2 5 28 -1.23 0.00 3 5 28 -1.47 0.00 4 5 28 -0.85 0.00 5 5 28 -1.41 0.00 6 5 28 1.77 0.00 0 6 28 4.25 0.00 1 6 28 0.71 0.00 2 6 28 1.63 0.00 3 6 28 1.50 0.00 4 6 28 2.19 0.00 5 6 28 -0.27 0.00 1 7 28 -2.55 0.00 2 7 28 -2.27 0.00 3 7 28 -1.85 0.00 4 7 28 1.55 0.00 0 8 28 1.56 0.00 1 8 28 1.10 0.00 2 8 28 1.31 0.00 3 8 28 -0.99 0.00 4 8 28 3.97 0.00 1 9 28 -0.88 0.00 2 9 28 0.53 0.00 1 0 29 -2.18 0.00 3 0 29 -2.43 0.00 5 0 29 1.53 0.00 0 1 29 0.82 0.00 1 1 29 0.08 0.00 2 1 29 3.03 0.00 3 1 29 -0.31 0.00 4 1 29 -0.39 0.00 5 1 29 0.84 0.00 1 2 29 -1.45 0.00 2 2 29 0.03 0.00 3 2 29 0.00 0.00 4 2 29 -0.52 0.00 0 3 29 2.04 0.00 1 3 29 1.12 0.00 2 3 29 -0.93 0.00 3 3 29 1.43 0.00 4 3 29 -1.86 0.00 1 4 29 0.30 0.00 2 4 29 -2.32 0.00 3 4 29 1.60 0.00 4 4 29 -0.42 0.00 0 5 29 -0.01 0.00 1 5 29 0.87 0.00 2 5 29 -1.51 0.00 3 5 29 0.30 0.00 1 6 29 0.01 0.00 2 6 29 0.53 0.00 0 7 29 0.20 0.00 1 7 29 -0.35 0.00 0 0 30 0.85 0.00 1 1 30 1.11 0.00 0 2 30 -0.69 0.00 18 0 0 3.99 0.00 18 1 0 -5.09 0.00 19 1 0 2.56 0.00 0 2 0 295.96 0.00 18 2 0 -4.19 0.00 19 2 0 3.15 0.00 4 3 0 30.80 0.00 18 3 0 3.61 0.00 19 3 0 3.06 0.00 18 4 0 -6.00 0.00 19 4 0 -0.67 0.00 18 7 0 -6.05 0.00 18 8 0 -5.22 0.00 18 9 0 -2.69 0.00 0 12 0 -1.30 0.00 1 12 0 0.25 0.00 1 13 0 2.09 0.00 6 20 0 -3.55 0.00 4 21 0 3.27 0.00 12 21 0 1.59 0.00 11 22 0 -2.23 0.00 10 23 0 1.57 0.00 7 25 0 -0.48 0.00 5 26 0 1.19 0.00 19 0 1 -0.45 0.00 0 1 1 -218.57 0.00 18 1 1 -1.09 0.00 19 1 1 2.84 0.00 18 2 1 -4.03 0.00 19 2 1 -1.20 0.00 18 3 1 -2.53 0.00 19 3 1 -3.78 0.00 18 8 1 -1.48 0.00 18 9 1 -0.14 0.00 4 21 1 -4.13 0.00 12 21 1 -6.76 0.00 11 22 1 3.36 0.00 10 23 1 1.74 0.00 7 25 1 -2.13 0.00 5 26 1 0.48 0.00 0 27 1 4.60 0.00 19 1 2 3.56 0.00 19 2 2 -0.23 0.00 19 3 2 1.24 0.00 18 9 2 -9.74 0.00 12 21 2 1.17 0.00 11 22 2 -3.54 0.00 10 23 2 2.13 0.00 7 25 2 1.20 0.00 5 26 2 -1.14 0.00 19 0 3 -3.39 0.00 19 1 3 4.63 0.00 19 2 3 -2.21 0.00 19 3 3 -1.32 0.00 18 9 3 1.41 0.00 17 12 3 -1.19 0.00 7 25 3 -2.96 0.00 0 0 4 225.85 0.00 19 1 4 4.58 0.00 17 12 4 -5.94 0.00 14 18 4 0.84 0.00 4 26 4 1.61 0.00 18 8 5 -0.47 0.00 16 14 5 0.18 0.00 15 16 5 -1.09 0.00 8 24 5 -0.11 0.00 4 26 5 2.63 0.00 17 11 6 -2.07 0.00 15 16 6 0.97 0.00 13 19 6 2.59 0.00 6 25 6 1.08 0.00 3 26 6 -1.90 0.00 18 7 7 -1.25 0.00 12 20 7 1.01 0.00 10 22 7 -1.73 0.00 9 23 7 -0.91 0.00 2 26 7 1.03 0.00 18 6 8 4.18 0.00 17 10 8 0.80 0.00 16 13 8 -0.16 0.00 15 15 8 4.12 0.00 14 17 8 -2.39 0.00 7 24 8 2.35 0.00 5 25 8 -2.14 0.00 0 26 8 1.11 0.00 1 26 8 -0.40 0.00 18 4 9 0.45 0.00 18 5 9 -0.18 0.00 13 18 9 -0.41 0.00 8 23 9 1.82 0.00 4 25 9 0.92 0.00 18 0 10 2.72 0.00 18 1 10 3.14 0.00 18 2 10 -1.14 0.00 18 3 10 0.39 0.00 16 12 10 -0.38 0.00 15 14 10 0.50 0.00 14 16 10 -1.27 0.00 12 19 10 2.47 0.00 9 22 10 -0.32 0.00 6 24 10 -0.11 0.00 3 25 10 -0.52 0.00 16 11 11 -0.51 0.00 7 23 11 1.97 0.00 5 24 11 -1.02 0.00 0 25 11 -1.69 0.00 1 25 11 0.98 0.00 2 25 11 1.00 0.00 13 5 12 -2.87 0.00 17 6 12 -2.67 0.00 16 10 12 -0.29 0.00 15 13 12 -4.96 0.00 14 15 12 3.00 0.00 12 18 12 1.40 0.00 8 22 12 1.10 0.00 4 24 12 -2.40 0.00 17 4 13 -4.53 0.00 16 9 13 0.17 0.00 15 12 13 1.09 0.00 13 16 13 0.63 0.00 3 24 13 0.49 0.00 17 1 14 -1.01 0.00 16 8 14 0.21 0.00 15 11 14 1.38 0.00 12 17 14 -1.67 0.00 8 21 14 1.00 0.00 16 6 15 -1.12 0.00 15 10 15 0.70 0.00 12 16 15 1.50 0.00 3 23 15 -0.22 0.00 16 4 16 -0.77 0.00 15 9 16 -0.07 0.00 10 18 16 0.48 0.00 9 19 16 0.18 0.00 8 20 16 -1.61 0.00 11 2 17 1.47 0.00 15 7 17 -0.60 0.00 11 16 17 -1.40 0.00 7 20 17 -2.73 0.00 5 21 17 -3.07 0.00 2 22 17 1.43 0.00 15 5 18 1.99 0.00 14 9 18 2.60 0.00 11 15 18 1.22 0.00 6 20 18 1.32 0.00 4 21 18 -0.79 0.00 14 7 19 -2.72 0.00 13 10 19 3.68 0.00 11 14 19 -1.78 0.00 0 21 19 -2.09 0.00 1 21 19 -2.12 0.00 14 4 20 0.18 0.00 14 5 20 -0.62 0.00 12 11 20 0.02 0.00 11 13 20 1.89 0.00 5 19 20 0.06 0.00 1 20 20 -1.65 0.00 2 20 20 -0.44 0.00 13 6 21 -2.67 0.00 1 11 21 -4.42 0.00 5 18 21 -1.57 0.00 2 19 21 -1.83 0.00 3 19 21 -0.45 0.00 13 1 22 2.64 0.00 13 2 22 -0.76 0.00 13 3 22 1.24 0.00 2 9 22 1.58 0.00 11 10 22 -0.22 0.00 10 12 22 -1.44 0.00 5 17 22 -0.36 0.00 3 18 22 -1.25 0.00 12 4 23 0.03 0.00 12 5 23 0.95 0.00 11 8 23 -1.87 0.00 9 12 23 -1.01 0.00 5 16 23 1.01 0.00 3 17 23 -0.73 0.00 0 4 24 -2.91 0.00 11 5 24 -0.67 0.00 10 8 24 -0.19 0.00 9 10 24 0.80 0.00 8 12 24 0.33 0.00 7 13 24 -0.43 0.00 6 14 24 0.66 0.00 2 16 24 0.56 0.00 10 5 25 3.01 0.00 10 6 25 -1.19 0.00 9 8 25 1.14 0.00 8 9 25 0.24 0.00 8 10 25 1.88 0.00 4 14 25 -2.27 0.00 0 15 25 -0.35 0.00 1 15 25 -0.49 0.00 2 15 25 -3.05 0.00 8 0 26 3.56 0.00 8 1 26 2.49 0.00 9 1 26 -1.41 0.00 9 2 26 -0.66 0.00 9 3 26 0.63 0.00 9 4 26 2.33 0.00 9 5 26 -1.11 0.00 8 6 26 -1.25 0.00 8 7 26 1.93 0.00 8 8 26 -1.06 0.00 7 9 26 -1.11 0.00 6 11 26 0.60 0.00 3 13 26 -1.42 0.00 7 0 27 -1.20 0.00 8 1 27 2.61 0.00 8 2 27 5.76 0.00 8 3 27 2.22 0.00 8 4 27 0.73 0.00 7 6 27 -2.84 0.00 7 7 27 -1.64 0.00 5 10 27 -3.30 0.00 1 12 27 -0.53 0.00 7 1 28 3.71 0.00 7 2 28 -0.47 0.00 7 3 28 0.04 0.00 6 6 28 -0.71 0.00 5 7 28 -1.98 0.00 3 9 28 -3.62 0.00 0 10 28 0.45 0.00 1 10 28 -0.59 0.00 5 2 29 1.07 0.00 5 3 29 -0.45 0.00 4 5 29 0.83 0.00 3 6 29 0.62 0.00 2 7 29 0.32 0.00 2 0 30 -2.64 0.00 2 1 30 0.14 0.00 1 2 30 -0.42 0.00 2 2 30 -1.18 0.00 1 3 30 0.37 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 201118) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.500 0.500 237 97 ' ' 2 0.000 0.500 0.000 435 264 ' ' 3 0.500 0.000 0.500 436 264 ' ' 4 0.500 1.000 0.000 237 97 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 0 2 0 3.775 4 3 0 12.109 0 1 1 2.527 0 0 4 6.737 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL 1_a P n n m R = 0.07 CELL 14.4962 20.3758 22.8688 90.00 90.00 90.00 SPGR Pnnm # Solvent Accessible Volume = 1333 # Electrons Found in S.A.V. = 721 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.965 0.625 0.011 ! 3.23 eA-3 Q102 0.256 0.031-0.001 ! 3.19 eA-3 Q103 0.593 0.453 0.502 ! 3.18 eA-3 C104 0.368 0.984 0.450 ! 2.68 eA-3 C105 0.803 0.576 0.817 ! 2.52 eA-3 Q106 0.206 0.469 0.496 ! 2.43 eA-3 Q107 0.363 0.096 0.465 ! 2.30 eA-3 Q108 0.127 0.561 0.042 ! 2.24 eA-3 C109 0.109 0.313 0.500 ! 2.22 eA-3 C110 0.359 0.078 0.497 ! 2.17 eA-3 Q111 0.496 0.062 0.415 ! 2.08 eA-3 Q112 0.337 0.935 0.632 ! 2.05 eA-3 C113 0.186 0.528 0.222 ! 2.01 eA-3 Q114 0.388 0.391 0.502 ! 2.00 eA-3 Q115 0.316 0.503 0.220 ! 2.00 eA-3 Q116 0.337 0.062 0.002 ! 1.99 eA-3 Q117 1.000 0.999 0.016 ! 1.89 eA-3 Q118 0.957 0.375 0.501 ! 1.85 eA-3 Q119 0.768 0.172-0.002 ! 1.69 eA-3 Q120 0.441 0.062 0.000 ! 1.67 eA-3 C121 0.417 0.094 0.500 ! 1.62 eA-3 C122 0.488 0.078 0.502 ! 1.61 eA-3 C123 0.096 0.547 0.003 ! 1.61 eA-3 Q124 0.112 0.547 0.216 ! 1.60 eA-3 Q125 0.998 0.237 0.276 ! 1.59 eA-3 Q126 0.611 0.125 0.003 ! 1.56 eA-3 Q127 0.343 0.375 0.501 ! 1.54 eA-3 C128 0.526 0.031 0.500 ! 1.50 eA-3 Q129 0.051 0.533 0.207 ! 1.50 eA-3 Q130 0.064 0.562 0.056 ! 1.47 eA-3 C131 0.574 0.048 0.475 ! 1.47 eA-3 Q132 0.124 0.453 0.501 ! 1.46 eA-3 C133 0.550 0.109 0.002 ! 1.43 eA-3 C134 0.107 0.500-0.005 ! 1.40 eA-3 Q135 0.884 0.156 0.001 ! 1.40 eA-3 Q136 0.406 0.626 0.942 ! 1.39 eA-3 Q137 0.588 0.621 0.644 ! 1.39 eA-3 Q138 0.490 0.093 0.545 ! 1.39 eA-3 Q139 1.000 0.998 0.570 ! 1.38 eA-3 C140 0.826 0.687 0.506 ! 1.38 eA-3 Q141 0.388 0.922 0.001 ! 1.36 eA-3 Q142 0.797 0.047 0.004 ! 1.35 eA-3 Q143 0.394 0.016-0.002 ! 1.35 eA-3 C144 0.952 0.578 0.003 ! 1.34 eA-3 Q145 0.384 0.063 0.977 ! 1.33 eA-3 Q146 0.408 0.139 0.646 ! 1.32 eA-3 Q147 0.305 0.991 0.284 ! 1.31 eA-3 C148 0.958 0.469-0.001 ! 1.31 eA-3 Q149 0.487 0.017 0.043 ! 1.31 eA-3 Q150 0.925 0.388 0.325 ! 1.30 eA-3 Q151 0.059 0.562 0.116 ! 1.27 eA-3 C152 0.023 0.469 0.499 ! 1.26 eA-3 Q153 0.923 0.657 0.314 ! 1.25 eA-3 Q154 0.858 0.641 0.001 ! 1.21 eA-3 Q155 0.873 0.171 0.025 ! 1.21 eA-3 Q156 0.718 0.016 0.504 ! 1.21 eA-3 Q157 0.646 0.020 0.262 ! 1.20 eA-3 Q158 0.026 0.529 0.072 ! 1.20 eA-3 Q159 0.986 0.474 0.180 ! 1.20 eA-3 Q160 0.302 0.266 0.498 ! 1.19 eA-3 Q161 0.232 0.392 0.088 ! 1.19 eA-3 Q162 0.801 0.437-0.003 ! 1.18 eA-3 C163 0.570 0.219-0.003 ! 1.17 eA-3 Q164 0.077 0.519 0.159 ! 1.17 eA-3 Q165 0.337 0.547 0.498 ! 1.17 eA-3 Q166 0.276 0.876 0.854 ! 1.16 eA-3 Q167 0.359 0.234 0.497 ! 1.15 eA-3 Q168 0.824 0.594 0.902 ! 1.15 eA-3 Q169 0.753 0.390 0.355 ! 1.14 eA-3 C170 0.454 0.979 0.547 ! 1.14 eA-3 C171 1.002 0.347 0.462 ! 1.14 eA-3 Q172 0.495 0.206 0.590 ! 1.14 eA-3 Q173 0.939 0.326 0.017 ! 1.14 eA-3 Q174 0.207 0.376 0.101 ! 1.12 eA-3 Q175 0.301 0.219 0.497 ! 1.11 eA-3 Q176 0.591 0.328 0.367 ! 1.11 eA-3 Q177 0.843 0.312 0.979 ! 1.11 eA-3 Q178 0.876 0.359 0.502 ! 1.10 eA-3 Q179 0.689 0.125 0.004 ! 1.09 eA-3 C180 0.070 0.342 0.481 ! 1.09 eA-3 Q181 0.177 0.203 0.501 ! 1.09 eA-3 Q182 0.953 0.549 0.362 ! 1.08 eA-3 Q183 0.886 0.624 0.172 ! 1.08 eA-3 Q184 0.040 0.452 0.680 ! 1.08 eA-3 Q185 1.000 0.500 0.102 ! 1.08 eA-3 Q186 0.508 0.965 0.204 ! 1.07 eA-3 Q187 0.298 0.828 0.499 ! 1.06 eA-3 Q188 0.582 0.048 0.437 ! 1.05 eA-3 Q189 0.986 0.528 0.575 ! 1.05 eA-3 C190 1.000 0.500 0.031 ! 1.05 eA-3 Q191 0.579 0.047 0.682 ! 1.04 eA-3 Q192 0.389 0.093 0.583 ! 1.04 eA-3 Q193 0.550 0.015 0.394 ! 1.04 eA-3 Q194 0.625 0.892 0.322 ! 1.04 eA-3 Q195 0.468 0.171 0.034 ! 1.03 eA-3 C196 0.132 0.422 0.005 ! 1.03 eA-3 Q197 0.513 0.453 0.498 ! 1.03 eA-3 Q198 0.326 0.244 0.520 ! 1.03 eA-3 Q199 0.785 0.125-0.002 ! 1.03 eA-3 ) ; _shelx_fab_checksum 525 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x, y, -z' 'x-1/2, -y-1/2, z-1/2' '-x-1/2, y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Gd1 Gd 0.40692(3) 0.61957(2) 0.64667(2) 0.02777(13) Uani 1 1 d . U . . . Gd2 Gd 0.000000 1.000000 0.27363(2) 0.02858(15) Uani 1 2 d S TU P . . Gd3 Gd 0.633376 0.460896 0.500000 0.027 Uani 0.0826 1 d . U P A -1 O1W O 0.684846 0.573606 0.500000 0.049(5) Uani 0.0826(7) 1 d S U P A -1 O2W O 0.469826 0.440187 0.500000 0.033(7) Uani 0.0826(7) 1 d S U P A -1 O3W O 0.797565 0.441502 0.503986 0.022(3) Uani 0.0826(7) 1 d S U P A -1 Gd4 Gd 0.681773 0.455367 0.500000 0.027 Uani 0.1674(7) 1 d S U P A -2 O4W O 0.8248(18) 0.4289(13) 0.5562(10) 0.022(3) Uani 0.1674(7) 1 d . U P A -2 O5W O 0.517835 0.481284 0.500000 0.047(5) Uani 0.1674(7) 1 d S U P A -2 O6W O 0.735783 0.566936 0.500000 0.049(5) Uani 0.1674(7) 1 d S U P A -2 P1_1 P 0.62472(12) 0.53154(8) 0.64066(7) 0.0232(3) Uani 1 1 d . U . . . O1_1 O 0.5496(3) 0.5804(2) 0.6247(2) 0.0280(10) Uani 1 1 d . U . . . O2_1 O 0.6030(3) 0.4916(2) 0.69590(19) 0.0247(9) Uani 1 1 d . U . . . O3_1 O 0.6399(3) 0.4791(2) 0.59353(19) 0.0262(9) Uani 1 1 d . U . . . O4_1 O 1.2416(4) 0.6104(3) 0.6637(3) 0.0437(13) Uani 1 1 d . U . . . O5_1 O 1.3064(3) 0.7034(2) 0.6879(2) 0.0366(12) Uani 1 1 d . U . . . O6_1 O 1.0956(3) 0.9032(3) 0.7056(2) 0.0348(11) Uani 1 1 d . U . . . O7_1 O 0.9714(4) 0.8829(2) 0.7574(2) 0.0289(10) Uani 1 1 d . U . . . C1_1 C 0.7302(3) 0.5775(2) 0.6531(3) 0.0253(12) Uani 1 1 d DG U . . . C2_1 C 0.8125(5) 0.54519(19) 0.6653(7) 0.032(3) Uani 0.59(3) 1 d DG U P B 1 H2_1 H 0.814373 0.499571 0.665616 0.039 Uiso 0.59(3) 1 calc R U P B 1 C3_1 C 0.8919(4) 0.5811(3) 0.6769(7) 0.035(3) Uani 0.59(3) 1 d DG U P B 1 H3_1 H 0.946986 0.559501 0.684957 0.042 Uiso 0.59(3) 1 calc R U P B 1 C4_1 C 0.8891(3) 0.6493(3) 0.6763(3) 0.0326(15) Uani 1 1 d DG U . B . C5_1 C 0.8068(5) 0.68156(19) 0.6642(7) 0.034(3) Uani 0.59(3) 1 d DG U P B 1 H5_1 H 0.804929 0.727184 0.663860 0.040 Uiso 0.59(3) 1 calc R U P B 1 C6_1 C 0.7274(4) 0.6457(2) 0.6526(7) 0.033(3) Uani 0.59(3) 1 d DG U P B 1 H6_1 H 0.672315 0.667255 0.644518 0.040 Uiso 0.59(3) 1 calc R U P B 1 C2A_1 C 0.8146(10) 0.5518(9) 0.6414(13) 0.036(4) Uani 0.41(3) 1 d D U P B 2 H2A_1 H 0.818269 0.509716 0.625773 0.043 Uiso 0.41(3) 1 calc R U P B 2 C3A_1 C 0.8957(11) 0.5861(9) 0.6520(14) 0.040(4) Uani 0.41(3) 1 d D U P B 2 H3A_1 H 0.952853 0.567842 0.643217 0.048 Uiso 0.41(3) 1 calc R U P B 2 C5A_1 C 0.8039(10) 0.6751(9) 0.6861(13) 0.035(4) Uani 0.41(3) 1 d D U P B 2 H5A_1 H 0.799116 0.717716 0.700345 0.042 Uiso 0.41(3) 1 calc R U P B 2 C6A_1 C 0.7242(11) 0.6398(9) 0.6753(13) 0.035(4) Uani 0.41(3) 1 d D U P B 2 H6A_1 H 0.666846 0.658286 0.683053 0.042 Uiso 0.41(3) 1 calc R U P B 2 C7_1 C 0.9749(5) 0.6889(3) 0.6877(3) 0.0327(15) Uani 1 1 d . U . . . C8_1 C 1.0625(5) 0.6622(3) 0.6790(3) 0.0336(15) Uani 1 1 d . U . . . H8_1 H 1.068109 0.618726 0.667233 0.040 Uiso 1 1 calc R U . . . C9_1 C 1.1421(5) 0.6999(3) 0.6877(3) 0.0292(14) Uani 1 1 d . U . . . C10_1 C 1.1347(5) 0.7652(3) 0.7031(3) 0.0286(14) Uani 1 1 d . U . . . H10_1 H 1.187279 0.790820 0.707631 0.034 Uiso 1 1 calc R U . . . C11_1 C 1.0479(5) 0.7919(3) 0.7117(3) 0.0273(13) Uani 1 1 d . U . . . C12_1 C 0.9700(5) 0.7548(3) 0.7063(3) 0.0300(14) Uani 1 1 d . U . . . H12_1 H 0.912952 0.773178 0.715074 0.036 Uiso 1 1 calc R U . . . C13_1 C 1.2355(5) 0.6696(3) 0.6800(3) 0.0314(14) Uani 1 1 d . U . . . C14_1 C 1.0395(5) 0.8626(3) 0.7262(3) 0.0266(13) Uani 1 1 d . U . . . P1_2 P 0.3706(2) 0.69564(13) 0.500000 0.0367(6) Uani 1 2 d S TU P D . O1_2 O 0.3671(4) 0.6517(3) 0.5537(2) 0.0439(13) Uani 1 1 d . U . . . O2_2 O 0.4533(7) 0.7401(5) 0.500000 0.061(2) Uani 1 2 d S TU P . . O3_2 O -0.0876(5) 0.9551(3) 0.3451(3) 0.0546(17) Uani 1 1 d . U . . . O4_2 O -0.2256(9) 0.9541(12) 0.3906(6) 0.077(6) Uani 0.56(3) 1 d D U P C 1 O4A_2 O -0.1917(18) 1.0058(13) 0.4004(8) 0.081(8) Uani 0.44(3) 1 d D U P C 2 C1_2 C 0.2658(7) 0.7470(5) 0.500000 0.046(2) Uani 1 2 d GS TU P . . C2_2 C 0.2018(8) 0.7466(6) 0.5450(3) 0.073(5) Uani 0.5 1 d G U P D -1 H2_2 H 0.209537 0.718299 0.576497 0.088 Uiso 0.5 1 calc R U P D -1 C3_2 C 0.1260(8) 0.7883(7) 0.5431(5) 0.070(5) Uani 0.5 1 d G U P D -1 H3_2 H 0.082748 0.786906 0.573056 0.084 Uiso 0.5 1 calc R U P D -1 C4_2 C 0.1142(7) 0.8306(6) 0.4989(6) 0.060(3) Uani 1 2 d G TU P D . C5_2 C 0.1782(8) 0.8310(5) 0.4506(5) 0.049(4) Uani 0.5 1 d G U P D -1 H5_2 H 0.168975 0.858662 0.418823 0.058 Uiso 0.5 1 calc R U P D -1 C6_2 C 0.2540(7) 0.7892(5) 0.4525(2) 0.045(3) Uani 0.5 1 d G U P D -1 H6_2 H 0.296745 0.789409 0.422205 0.054 Uiso 0.5 1 calc R U P D -1 C7_2 C 0.0308(10) 0.8745(7) 0.500000 0.051(3) Uani 1 2 d S TU P . . C8_2 C -0.0083(7) 0.8964(5) 0.4477(4) 0.055(2) Uani 1 1 d . U . . . H8_2 H 0.018980 0.884953 0.412384 0.066 Uiso 1 1 calc R U . . . C10_2 C -0.1273(10) 0.9520(7) 0.500000 0.050(3) Uani 1 2 d S TU P . . H10_2 H -0.182273 0.975573 0.499999 0.060 Uiso 1 2 calc R U P . . C11_2 C -0.1321(8) 0.9557(6) 0.3926(4) 0.075(3) Uani 1 1 d D U . . . C9_2 C -0.0875(6) 0.9350(5) 0.4477(4) 0.052(2) Uani 1 1 d . U . . . C1_3 C 0.483500 0.774000 0.652500 0.050 Uani 0.6025 1 d D U P E 1 H1_3 H 0.422029 0.784203 0.659768 0.060 Uiso 0.602(13) 1 calc R U P E 1 O1_3 O 0.4983(16) 0.7169(11) 0.6459(8) 0.042(3) Uani 0.602(13) 1 d D U P E 1 N1_3 N 0.5369(12) 0.8231(8) 0.6513(8) 0.088(4) Uani 0.602(13) 1 d D U P E 1 C2_3 C 0.6391(13) 0.8077(14) 0.6418(13) 0.108(6) Uani 0.602(13) 1 d D U P E 1 H2A_3 H 0.650117 0.762148 0.649769 0.161 Uiso 0.602(13) 1 calc R U P E 1 H2AB_3 H 0.675723 0.834150 0.667663 0.161 Uiso 0.602(13) 1 calc R U P E 1 H2AC_3 H 0.655477 0.817234 0.602032 0.161 Uiso 0.602(13) 1 calc R U P E 1 C3_3 C 0.515(3) 0.8963(11) 0.6494(16) 0.155(10) Uani 0.602(13) 1 d D U P E 1 H3A_3 H 0.515066 0.911009 0.609530 0.233 Uiso 0.602(13) 1 calc R U P E 1 H3AB_3 H 0.561243 0.919960 0.671002 0.233 Uiso 0.602(13) 1 calc R U P E 1 H3AC_3 H 0.455697 0.903983 0.666484 0.233 Uiso 0.602(13) 1 calc R U P E 1 C1_4 C 0.5506(18) 0.7351(12) 0.6034(13) 0.087(4) Uani 0.398(13) 1 d D U P E 2 H1_4 H 0.564882 0.705844 0.573549 0.104 Uiso 0.398(13) 1 calc R U P E 2 O1_4 O 0.490(3) 0.7183(14) 0.6352(15) 0.051(4) Uani 0.398(13) 1 d D U P E 2 N1_4 N 0.5990(18) 0.7875(13) 0.6044(12) 0.102(5) Uani 0.398(13) 1 d D U P E 2 C2_4 C 0.669(3) 0.802(2) 0.5556(18) 0.144(11) Uani 0.398(13) 1 d D U P E 2 H2A_4 H 0.698776 0.842876 0.563213 0.216 Uiso 0.398(13) 1 calc R U P E 2 H2AB_4 H 0.713803 0.767349 0.554267 0.216 Uiso 0.398(13) 1 calc R U P E 2 H2AC_4 H 0.637060 0.804105 0.518767 0.216 Uiso 0.398(13) 1 calc R U P E 2 C3_4 C 0.587(3) 0.8416(19) 0.6508(19) 0.116(8) Uani 0.398(13) 1 d D U P E 2 H3A_4 H 0.630661 0.876342 0.643291 0.174 Uiso 0.398(13) 1 calc R U P E 2 H3AB_4 H 0.525807 0.858709 0.649185 0.174 Uiso 0.398(13) 1 calc R U P E 2 H3AC_4 H 0.598799 0.823605 0.688936 0.174 Uiso 0.398(13) 1 calc R U P E 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Gd1 0.0247(2) 0.02056(18) 0.0381(2) -0.00112(13) -0.00135(14) 0.00166(13) Gd2 0.0319(3) 0.0239(2) 0.0300(2) 0.000 0.000 0.0044(2) Gd3 0.027 0.027 0.027 0.000 0.000 0.000 O1W 0.082(12) 0.034(6) 0.030(7) 0.009(9) -0.001(14) -0.015(7) O2W 0.019(8) 0.042(18) 0.039(18) 0.00(4) -0.001(19) 0.021(10) O3W 0.021(5) 0.031(7) 0.013(6) 0.002(6) -0.001(5) -0.018(5) Gd4 0.027 0.027 0.027 0.000 0.000 0.000 O4W 0.021(5) 0.031(7) 0.013(6) 0.002(6) -0.001(5) -0.018(5) O5W 0.035(7) 0.077(14) 0.030(8) 0.001(18) -0.001(10) 0.006(8) O6W 0.082(12) 0.034(6) 0.030(7) 0.009(9) -0.001(14) -0.015(7) P1_1 0.0187(8) 0.0161(7) 0.0347(8) 0.0009(6) 0.0014(7) 0.0011(6) O1_1 0.021(2) 0.022(2) 0.042(2) 0.0017(19) 0.001(2) 0.0011(18) O2_1 0.024(2) 0.022(2) 0.029(2) 0.0011(17) 0.0031(18) -0.0026(18) O3_1 0.030(3) 0.020(2) 0.029(2) -0.0006(17) 0.0047(19) 0.0012(18) O4_1 0.027(3) 0.024(2) 0.080(4) -0.007(3) 0.003(3) 0.001(2) O5_1 0.023(2) 0.026(2) 0.061(3) -0.012(2) -0.004(2) 0.000(2) O6_1 0.028(3) 0.023(2) 0.053(3) -0.003(2) 0.003(2) -0.001(2) O7_1 0.032(3) 0.022(2) 0.033(2) -0.0076(18) 0.006(2) 0.0027(19) C1_1 0.023(3) 0.017(3) 0.036(3) 0.000(2) 0.005(3) -0.003(2) C2_1 0.028(5) 0.020(4) 0.048(8) 0.005(5) -0.012(5) 0.001(4) C3_1 0.029(5) 0.020(4) 0.056(8) 0.002(5) -0.008(6) 0.000(4) C4_1 0.021(3) 0.025(3) 0.052(4) -0.007(3) 0.003(3) -0.003(2) C5_1 0.025(5) 0.018(4) 0.058(9) 0.006(5) 0.003(6) -0.007(4) C6_1 0.021(5) 0.017(4) 0.060(9) 0.004(5) 0.006(6) -0.001(4) C2A_1 0.026(5) 0.024(6) 0.058(10) -0.008(7) -0.009(7) 0.001(5) C3A_1 0.027(6) 0.026(6) 0.066(10) -0.010(7) -0.006(7) 0.004(5) C5A_1 0.026(5) 0.020(6) 0.058(10) -0.007(6) 0.007(7) -0.003(5) C6A_1 0.019(6) 0.029(6) 0.057(10) -0.010(6) 0.015(7) -0.005(5) C7_1 0.026(3) 0.018(3) 0.053(4) -0.005(3) 0.003(3) -0.004(2) C8_1 0.029(3) 0.021(3) 0.051(4) -0.011(3) 0.006(3) 0.000(3) C9_1 0.020(3) 0.022(3) 0.046(4) -0.003(3) 0.002(3) 0.002(2) C10_1 0.024(3) 0.024(3) 0.038(3) -0.004(3) 0.001(3) 0.003(3) C11_1 0.028(3) 0.020(3) 0.034(3) -0.002(2) 0.009(3) -0.005(2) C12_1 0.026(3) 0.021(3) 0.043(4) -0.007(3) 0.008(3) 0.000(2) C13_1 0.028(3) 0.019(3) 0.047(4) -0.005(3) 0.004(3) 0.001(3) C14_1 0.024(3) 0.020(3) 0.035(3) -0.007(2) -0.004(3) 0.003(2) P1_2 0.0479(17) 0.0268(12) 0.0353(13) 0.000 0.000 0.0038(12) O1_2 0.052(4) 0.047(3) 0.033(2) 0.006(2) -0.003(2) 0.013(3) O2_2 0.060(5) 0.045(5) 0.078(6) 0.000 0.000 -0.011(4) O3_2 0.072(5) 0.047(4) 0.045(3) 0.014(3) 0.025(3) 0.016(3) O4_2 0.051(6) 0.136(17) 0.045(7) 0.015(9) 0.004(5) 0.013(9) O4A_2 0.073(14) 0.119(17) 0.052(9) 0.025(10) 0.014(8) 0.056(12) C1_2 0.063(6) 0.039(5) 0.037(5) 0.000 0.000 0.017(5) C2_2 0.075(10) 0.090(11) 0.055(8) 0.034(8) 0.019(7) 0.034(8) C3_2 0.070(10) 0.096(12) 0.042(8) 0.017(7) 0.009(7) 0.035(8) C4_2 0.065(7) 0.074(8) 0.042(6) 0.000 0.000 0.032(6) C5_2 0.060(9) 0.051(8) 0.035(7) 0.009(6) 0.003(6) 0.021(7) C6_2 0.061(9) 0.043(8) 0.030(6) 0.004(5) 0.004(6) 0.015(6) C7_2 0.045(6) 0.069(8) 0.041(5) 0.000 0.000 0.014(5) C8_2 0.056(5) 0.066(6) 0.042(4) 0.009(4) 0.013(4) 0.021(4) C10_2 0.046(7) 0.056(7) 0.047(5) 0.000 0.000 0.008(6) C11_2 0.060(5) 0.114(8) 0.051(4) 0.034(5) 0.018(4) 0.040(6) C9_2 0.043(5) 0.066(6) 0.046(4) 0.014(4) 0.010(3) 0.013(4) C1_3 0.050 0.050 0.050 0.000 0.000 0.000 O1_3 0.034(6) 0.034(3) 0.059(7) 0.004(5) 0.010(5) -0.007(4) N1_3 0.081(7) 0.052(5) 0.133(10) 0.000(7) 0.014(8) -0.017(5) C2_3 0.065(7) 0.107(13) 0.151(15) 0.020(13) -0.024(11) -0.014(8) C3_3 0.17(2) 0.057(6) 0.24(3) -0.028(15) 0.01(2) 0.004(10) C1_4 0.077(8) 0.073(8) 0.110(9) 0.005(7) 0.015(7) -0.021(7) O1_4 0.059(9) 0.015(5) 0.078(10) -0.012(7) 0.004(7) -0.005(5) N1_4 0.092(10) 0.084(9) 0.131(10) 0.005(8) 0.016(9) -0.034(7) C2_4 0.12(2) 0.15(2) 0.16(2) 0.035(18) 0.040(16) -0.038(18) C3_4 0.096(17) 0.090(14) 0.162(16) -0.015(12) -0.010(15) -0.014(14) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0137 0.0067 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Gd Gd -3.4578 11.1283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0241 0.0134 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0389 0.0241 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2543 0.3332 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1_1 Gd1 O1_2 97.13(19) . . ? O1_1 Gd1 O1_4 79.2(11) . . ? O1_2 Gd1 O1_4 77.4(8) . . ? O1_1 Gd1 O7_1 80.75(18) . 4_466 ? O1_2 Gd1 O7_1 162.8(2) . 4_466 ? O1_1 Gd1 O1_3 77.6(7) . . ? O1_2 Gd1 O1_3 84.0(5) . . ? O7_1 Gd1 O1_3 78.9(5) 4_466 . ? O1_1 Gd1 O5_1 151.19(17) . 1_455 ? O1_2 Gd1 O5_1 90.45(19) . 1_455 ? O7_1 Gd1 O5_1 83.89(18) 4_466 1_455 ? O1_3 Gd1 O5_1 75.6(7) . 1_455 ? O1_1 Gd1 O4_1 154.69(17) . 1_455 ? O1_2 Gd1 O4_1 85.5(2) . 1_455 ? O7_1 Gd1 O4_1 103.7(2) 4_466 1_455 ? O1_3 Gd1 O4_1 127.7(7) . 1_455 ? O5_1 Gd1 O4_1 53.35(17) 1_455 1_455 ? O1_1 Gd1 O3_1 81.61(17) . 2_665 ? O1_2 Gd1 O3_1 72.82(18) . 2_665 ? O7_1 Gd1 O3_1 123.25(15) 4_466 2_665 ? O1_3 Gd1 O3_1 146.5(6) . 2_665 ? O5_1 Gd1 O3_1 127.09(16) 1_455 2_665 ? O4_1 Gd1 O3_1 75.12(17) 1_455 2_665 ? O1_1 Gd1 O2_1 80.56(16) . 2_665 ? O1_2 Gd1 O2_1 130.64(18) . 2_665 ? O7_1 Gd1 O2_1 66.08(15) 4_466 2_665 ? O1_3 Gd1 O2_1 141.1(5) . 2_665 ? O5_1 Gd1 O2_1 114.93(17) 1_455 2_665 ? O4_1 Gd1 O2_1 78.75(17) 1_455 2_665 ? O3_1 Gd1 O2_1 57.99(14) 2_665 2_665 ? O1_1 Gd1 C13_1 176.7(2) . 1_455 ? O1_2 Gd1 C13_1 85.7(2) . 1_455 ? O7_1 Gd1 C13_1 96.1(2) 4_466 1_455 ? O1_3 Gd1 C13_1 101.1(7) . 1_455 ? O5_1 Gd1 C13_1 26.58(18) 1_455 1_455 ? O4_1 Gd1 C13_1 26.92(17) 1_455 1_455 ? O3_1 Gd1 C13_1 100.88(19) 2_665 1_455 ? O2_1 Gd1 C13_1 98.90(18) 2_665 1_455 ? O1_1 Gd1 P1_1 77.14(12) . 2_665 ? O1_2 Gd1 P1_1 101.73(16) . 2_665 ? O7_1 Gd1 P1_1 94.43(11) 4_466 2_665 ? O1_3 Gd1 P1_1 154.6(7) . 2_665 ? O5_1 Gd1 P1_1 128.48(13) 1_455 2_665 ? O4_1 Gd1 P1_1 77.68(13) 1_455 2_665 ? O3_1 Gd1 P1_1 28.92(11) 2_665 2_665 ? O2_1 Gd1 P1_1 29.29(10) 2_665 2_665 ? C13_1 Gd1 P1_1 103.99(14) 1_455 2_665 ? O1_1 Gd1 Gd2 69.01(12) . 7_676 ? O1_2 Gd1 Gd2 157.56(15) . 7_676 ? O7_1 Gd1 Gd2 36.09(11) 4_466 7_676 ? O1_3 Gd1 Gd2 108.8(5) . 7_676 ? O5_1 Gd1 Gd2 110.26(13) 1_455 7_676 ? O4_1 Gd1 Gd2 99.71(15) 1_455 7_676 ? O3_1 Gd1 Gd2 87.35(10) 2_665 7_676 ? O2_1 Gd1 Gd2 32.53(10) 2_665 7_676 ? C13_1 Gd1 Gd2 108.83(15) 1_455 7_676 ? P1_1 Gd1 Gd2 58.86(3) 2_665 7_676 ? O3_2 Gd2 O3_2 87.5(4) 2_575 . ? O3_2 Gd2 O2_1 160.3(2) 2_575 8_665 ? O3_2 Gd2 O2_1 99.3(2) . 8_665 ? O3_2 Gd2 O2_1 99.3(2) 2_575 7_575 ? O3_2 Gd2 O2_1 160.3(2) . 7_575 ? O2_1 Gd2 O2_1 80.4(2) 8_665 7_575 ? O3_2 Gd2 O6_1 81.5(2) 2_575 5_676 ? O3_2 Gd2 O6_1 82.4(2) . 5_676 ? O2_1 Gd2 O6_1 81.08(17) 8_665 5_676 ? O2_1 Gd2 O6_1 116.77(17) 7_575 5_676 ? O3_2 Gd2 O6_1 82.4(2) 2_575 6_456 ? O3_2 Gd2 O6_1 81.5(2) . 6_456 ? O2_1 Gd2 O6_1 116.77(17) 8_665 6_456 ? O2_1 Gd2 O6_1 81.08(17) 7_575 6_456 ? O6_1 Gd2 O6_1 157.7(3) 5_676 6_456 ? O3_2 Gd2 O7_1 132.7(2) 2_575 6_456 ? O3_2 Gd2 O7_1 74.3(2) . 6_456 ? O2_1 Gd2 O7_1 67.05(15) 8_665 6_456 ? O2_1 Gd2 O7_1 87.71(16) 7_575 6_456 ? O6_1 Gd2 O7_1 136.10(17) 5_676 6_456 ? O6_1 Gd2 O7_1 52.28(16) 6_456 6_456 ? O3_2 Gd2 O7_1 74.3(2) 2_575 5_676 ? O3_2 Gd2 O7_1 132.7(2) . 5_676 ? O2_1 Gd2 O7_1 87.71(16) 8_665 5_676 ? O2_1 Gd2 O7_1 67.05(15) 7_575 5_676 ? O6_1 Gd2 O7_1 52.28(16) 5_676 5_676 ? O6_1 Gd2 O7_1 136.10(17) 6_456 5_676 ? O7_1 Gd2 O7_1 147.3(2) 6_456 5_676 ? O3_2 Gd2 C14_1 106.4(2) 2_575 6_456 ? O3_2 Gd2 C14_1 73.5(2) . 6_456 ? O2_1 Gd2 C14_1 93.28(18) 8_665 6_456 ? O2_1 Gd2 C14_1 86.80(17) 7_575 6_456 ? O6_1 Gd2 C14_1 154.07(19) 5_676 6_456 ? O6_1 Gd2 C14_1 25.88(19) 6_456 6_456 ? O7_1 Gd2 C14_1 26.75(18) 6_456 6_456 ? O7_1 Gd2 C14_1 153.32(17) 5_676 6_456 ? O3_2 Gd2 C14_1 73.5(2) 2_575 5_676 ? O3_2 Gd2 C14_1 106.4(2) . 5_676 ? O2_1 Gd2 C14_1 86.80(17) 8_665 5_676 ? O2_1 Gd2 C14_1 93.28(18) 7_575 5_676 ? O6_1 Gd2 C14_1 25.88(19) 5_676 5_676 ? O6_1 Gd2 C14_1 154.07(19) 6_456 5_676 ? O7_1 Gd2 C14_1 153.32(17) 6_456 5_676 ? O7_1 Gd2 C14_1 26.75(18) 5_676 5_676 ? C14_1 Gd2 C14_1 179.9(3) 6_456 5_676 ? O3_2 Gd2 Gd1 162.61(16) 2_575 7_575 ? O3_2 Gd2 Gd1 95.06(19) . 7_575 ? O2_1 Gd2 Gd1 35.83(11) 8_665 7_575 ? O2_1 Gd2 Gd1 73.05(11) 7_575 7_575 ? O6_1 Gd2 Gd1 115.88(13) 5_676 7_575 ? O6_1 Gd2 Gd1 80.94(13) 6_456 7_575 ? O7_1 Gd2 Gd1 33.83(10) 6_456 7_575 ? O7_1 Gd2 Gd1 115.12(11) 5_676 7_575 ? C14_1 Gd2 Gd1 58.31(14) 6_456 7_575 ? C14_1 Gd2 Gd1 121.78(13) 5_676 7_575 ? O3_2 Gd2 Gd1 95.06(19) 2_575 8_665 ? O3_2 Gd2 Gd1 162.61(16) . 8_665 ? O2_1 Gd2 Gd1 73.05(11) 8_665 8_665 ? O2_1 Gd2 Gd1 35.83(11) 7_575 8_665 ? O6_1 Gd2 Gd1 80.94(13) 5_676 8_665 ? O6_1 Gd2 Gd1 115.88(13) 6_456 8_665 ? O7_1 Gd2 Gd1 115.12(11) 6_456 8_665 ? O7_1 Gd2 Gd1 33.83(10) 5_676 8_665 ? C14_1 Gd2 Gd1 121.78(13) 6_456 8_665 ? C14_1 Gd2 Gd1 58.31(14) 5_676 8_665 ? Gd1 Gd2 Gd1 87.615(14) 7_575 8_665 ? O3_1 Gd3 O2W 94.17(13) . . ? O3_1 Gd3 O3W 87.02(13) . . ? O2W Gd3 O3W 160.4 . . ? O3_1 Gd3 O1W 79.86(12) . . ? O2W Gd3 O1W 118.1 . . ? O3W Gd3 O1W 81.4 . . ? O3_1 Gd4 O6W 83.44(11) . . ? O3_1 Gd4 O5W 72.15(12) . . ? O6W Gd4 O5W 96.476(2) . . ? O3_1 Gd4 O4W 77.5(6) . . ? O6W Gd4 O4W 86.2(6) . . ? O5W Gd4 O4W 149.0(5) . . ? O1_1 P1_1 O3_1 113.0(3) . . ? O1_1 P1_1 O2_1 113.4(3) . . ? O3_1 P1_1 O2_1 103.8(3) . . ? O1_1 P1_1 C1_1 107.7(3) . . ? O3_1 P1_1 C1_1 110.4(3) . . ? O2_1 P1_1 C1_1 108.5(3) . . ? O1_1 P1_1 Gd1 123.5(2) . 2_665 ? O3_1 P1_1 Gd1 50.50(17) . 2_665 ? O2_1 P1_1 Gd1 53.83(17) . 2_665 ? C1_1 P1_1 Gd1 128.79(19) . 2_665 ? P1_1 O1_1 Gd1 146.0(3) . . ? P1_1 O2_1 Gd2 136.1(3) . 7_676 ? P1_1 O2_1 Gd1 96.9(2) . 2_665 ? Gd2 O2_1 Gd1 111.64(17) 7_676 2_665 ? P1_1 O3_1 Gd3 143.6(3) . . ? P1_1 O3_1 Gd4 147.9(3) . . ? P1_1 O3_1 Gd1 100.6(2) . 2_665 ? Gd3 O3_1 Gd1 109.66(18) . 2_665 ? C13_1 O4_1 Gd1 92.4(4) . 1_655 ? C13_1 O5_1 Gd1 92.8(4) . 1_655 ? C14_1 O6_1 Gd2 95.2(4) . 5_676 ? C14_1 O7_1 Gd1 143.5(5) . 4_566 ? C14_1 O7_1 Gd2 91.3(4) . 5_676 ? Gd1 O7_1 Gd2 110.08(17) 4_566 5_676 ? C2A_1 C1_1 C6A_1 119.2(10) . . ? C2_1 C1_1 C6_1 120.0 . . ? C2A_1 C1_1 P1_1 121.9(8) . . ? C6A_1 C1_1 P1_1 118.9(8) . . ? C2_1 C1_1 P1_1 120.7(3) . . ? C6_1 C1_1 P1_1 119.3(3) . . ? C1_1 C2_1 C3_1 120.0 . . ? C1_1 C2_1 H2_1 120.0 . . ? C3_1 C2_1 H2_1 120.0 . . ? C2_1 C3_1 C4_1 120.0 . . ? C2_1 C3_1 H3_1 120.0 . . ? C4_1 C3_1 H3_1 120.0 . . ? C5_1 C4_1 C3_1 120.0 . . ? C5A_1 C4_1 C3A_1 118.8(10) . . ? C5A_1 C4_1 C7_1 121.0(8) . . ? C5_1 C4_1 C7_1 119.3(5) . . ? C3_1 C4_1 C7_1 120.7(5) . . ? C3A_1 C4_1 C7_1 120.2(8) . . ? C6_1 C5_1 C4_1 120.0 . . ? C6_1 C5_1 H5_1 120.0 . . ? C4_1 C5_1 H5_1 120.0 . . ? C5_1 C6_1 C1_1 120.0 . . ? C5_1 C6_1 H6_1 120.0 . . ? C1_1 C6_1 H6_1 120.0 . . ? C1_1 C2A_1 C3A_1 122.3(14) . . ? C1_1 C2A_1 H2A_1 118.9 . . ? C3A_1 C2A_1 H2A_1 118.9 . . ? C2A_1 C3A_1 C4_1 118.2(14) . . ? C2A_1 C3A_1 H3A_1 120.9 . . ? C4_1 C3A_1 H3A_1 120.9 . . ? C4_1 C5A_1 C6A_1 121.9(14) . . ? C4_1 C5A_1 H5A_1 119.1 . . ? C6A_1 C5A_1 H5A_1 119.1 . . ? C1_1 C6A_1 C5A_1 119.7(14) . . ? C1_1 C6A_1 H6A_1 120.2 . . ? C5A_1 C6A_1 H6A_1 120.2 . . ? C8_1 C7_1 C12_1 117.3(7) . . ? C8_1 C7_1 C4_1 121.3(6) . . ? C12_1 C7_1 C4_1 121.4(6) . . ? C7_1 C8_1 C9_1 121.1(6) . . ? C7_1 C8_1 H8_1 119.5 . . ? C9_1 C8_1 H8_1 119.5 . . ? C10_1 C9_1 C8_1 120.1(6) . . ? C10_1 C9_1 C13_1 119.8(6) . . ? C8_1 C9_1 C13_1 120.1(6) . . ? C9_1 C10_1 C11_1 119.1(7) . . ? C9_1 C10_1 H10_1 120.5 . . ? C11_1 C10_1 H10_1 120.5 . . ? C12_1 C11_1 C10_1 121.4(6) . . ? C12_1 C11_1 C14_1 119.4(7) . . ? C10_1 C11_1 C14_1 119.3(6) . . ? C11_1 C12_1 C7_1 120.9(7) . . ? C11_1 C12_1 H12_1 119.5 . . ? C7_1 C12_1 H12_1 119.5 . . ? O5_1 C13_1 O4_1 120.7(7) . . ? O5_1 C13_1 C9_1 119.9(6) . . ? O4_1 C13_1 C9_1 119.4(6) . . ? O5_1 C13_1 Gd1 60.6(4) . 1_655 ? O4_1 C13_1 Gd1 60.6(4) . 1_655 ? C9_1 C13_1 Gd1 170.7(5) . 1_655 ? O6_1 C14_1 O7_1 119.6(6) . . ? O6_1 C14_1 C11_1 120.3(6) . . ? O7_1 C14_1 C11_1 120.0(6) . . ? O6_1 C14_1 Gd2 58.9(4) . 5_676 ? O7_1 C14_1 Gd2 62.0(3) . 5_676 ? C11_1 C14_1 Gd2 165.5(5) . 5_676 ? O2_2 P1_2 O1_2 112.4(3) . . ? O2_2 P1_2 O1_2 112.4(3) . 6_556 ? O1_2 P1_2 O1_2 107.7(5) . 6_556 ? O2_2 P1_2 C1_2 108.4(6) . . ? O1_2 P1_2 C1_2 107.9(3) . . ? O1_2 P1_2 C1_2 107.9(3) 6_556 . ? P1_2 O1_2 Gd1 155.0(4) . . ? C11_2 O3_2 Gd2 154.6(8) . . ? C2_2 C1_2 C6_2 120.0 . . ? C2_2 C1_2 P1_2 123.2(4) . . ? C6_2 C1_2 P1_2 116.8(4) . . ? C1_2 C2_2 C3_2 120.1 . . ? C1_2 C2_2 H2_2 119.9 . . ? C3_2 C2_2 H2_2 119.9 . . ? C2_2 C3_2 C4_2 121.2 . . ? C2_2 C3_2 H3_2 119.4 . . ? C4_2 C3_2 H3_2 119.4 . . ? C4_2 C4_2 C5_2 140.0(2) 6_556 . ? C4_2 C4_2 C3_2 40.95(6) 6_556 . ? C5_2 C4_2 C3_2 120.0 . . ? C4_2 C4_2 C7_2 89.1(9) 6_556 . ? C5_2 C4_2 C7_2 121.8(8) . . ? C3_2 C4_2 C7_2 118.2(8) . . ? C4_2 C5_2 C6_2 118.7 . . ? C4_2 C5_2 H5_2 120.6 . . ? C6_2 C5_2 H5_2 120.6 . . ? C5_2 C6_2 C1_2 119.9 . . ? C5_2 C6_2 H6_2 120.1 . . ? C1_2 C6_2 H6_2 120.1 . . ? C8_2 C7_2 C8_2 117.8(12) 6_556 . ? C8_2 C7_2 C4_2 122.1(8) 6_556 . ? C8_2 C7_2 C4_2 120.1(8) . . ? C8_2 C7_2 C4_2 120.1(8) 6_556 6_556 ? C8_2 C7_2 C4_2 122.1(8) . 6_556 ? C4_2 C7_2 C4_2 1.9(11) . 6_556 ? C9_2 C8_2 C7_2 121.1(9) . . ? C9_2 C8_2 H8_2 119.4 . . ? C7_2 C8_2 H8_2 119.4 . . ? C9_2 C10_2 C9_2 121.3(13) 6_556 . ? C9_2 C10_2 H10_2 119.4 6_556 . ? C9_2 C10_2 H10_2 119.4 . . ? O3_2 C11_2 O4A_2 116.7(11) . . ? O3_2 C11_2 O4_2 118.8(10) . . ? O3_2 C11_2 C9_2 120.4(9) . . ? O4A_2 C11_2 C9_2 112.5(12) . . ? O4_2 C11_2 C9_2 117.3(9) . . ? C10_2 C9_2 C8_2 119.2(9) . . ? C10_2 C9_2 C11_2 119.1(9) . . ? C8_2 C9_2 C11_2 121.6(8) . . ? O1_3 C1_3 N1_3 131.2(12) . . ? O1_3 C1_3 H1_3 114.4 . . ? N1_3 C1_3 H1_3 114.4 . . ? C1_3 O1_3 Gd1 135.3(16) . . ? C1_3 N1_3 C3_3 130.4(18) . . ? C1_3 N1_3 C2_3 115.6(14) . . ? C3_3 N1_3 C2_3 113.4(18) . . ? N1_3 C2_3 H2A_3 109.5 . . ? N1_3 C2_3 H2AB_3 109.5 . . ? H2A_3 C2_3 H2AB_3 109.5 . . ? N1_3 C2_3 H2AC_3 109.5 . . ? H2A_3 C2_3 H2AC_3 109.5 . . ? H2AB_3 C2_3 H2AC_3 109.5 . . ? N1_3 C3_3 H3A_3 109.5 . . ? N1_3 C3_3 H3AB_3 109.5 . . ? H3A_3 C3_3 H3AB_3 109.5 . . ? N1_3 C3_3 H3AC_3 109.5 . . ? H3A_3 C3_3 H3AC_3 109.5 . . ? H3AB_3 C3_3 H3AC_3 109.5 . . ? O1_4 C1_4 N1_4 129(3) . . ? O1_4 C1_4 H1_4 115.3 . . ? N1_4 C1_4 H1_4 115.3 . . ? C1_4 O1_4 Gd1 134(3) . . ? C1_4 N1_4 C2_4 121(2) . . ? C1_4 N1_4 C3_4 123(2) . . ? C2_4 N1_4 C3_4 116(2) . . ? N1_4 C2_4 H2A_4 109.5 . . ? N1_4 C2_4 H2AB_4 109.5 . . ? H2A_4 C2_4 H2AB_4 109.5 . . ? N1_4 C2_4 H2AC_4 109.5 . . ? H2A_4 C2_4 H2AC_4 109.5 . . ? H2AB_4 C2_4 H2AC_4 109.5 . . ? N1_4 C3_4 H3A_4 109.5 . . ? N1_4 C3_4 H3AB_4 109.5 . . ? H3A_4 C3_4 H3AB_4 109.5 . . ? N1_4 C3_4 H3AC_4 109.5 . . ? H3A_4 C3_4 H3AC_4 109.5 . . ? H3AB_4 C3_4 H3AC_4 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Gd1 O1_1 2.272(5) . ? Gd1 O1_2 2.297(5) . ? Gd1 O1_4 2.36(2) . ? Gd1 O7_1 2.385(5) 4_466 ? Gd1 O1_3 2.385(15) . ? Gd1 O5_1 2.434(5) 1_455 ? Gd1 O4_1 2.435(6) 1_455 ? Gd1 O3_1 2.446(4) 2_665 ? Gd1 O2_1 2.533(4) 2_665 ? Gd1 C13_1 2.792(7) 1_455 ? Gd1 P1_1 3.1159(16) 2_665 ? Gd1 Gd2 4.0232(5) 7_676 ? Gd2 O3_2 2.263(6) 2_575 ? Gd2 O3_2 2.263(6) . ? Gd2 O2_1 2.328(4) 8_665 ? Gd2 O2_1 2.328(4) 7_575 ? Gd2 O6_1 2.457(5) 5_676 ? Gd2 O6_1 2.457(5) 6_456 ? Gd2 O7_1 2.523(5) 6_456 ? Gd2 O7_1 2.523(5) 5_676 ? Gd2 C14_1 2.858(6) 6_456 ? Gd2 C14_1 2.858(6) 5_676 ? Gd3 O3_1 2.173(4) . ? Gd3 O2W 2.4081 . ? Gd3 O3W 2.4144 . ? Gd3 O1W 2.4147 . ? Gd4 O3_1 2.275(4) . ? Gd4 O6W 2.40434(9) . ? Gd4 O5W 2.43445(9) . ? Gd4 O4W 2.50(3) . ? P1_1 O1_1 1.521(5) . ? P1_1 O3_1 1.533(5) . ? P1_1 O2_1 1.535(5) . ? P1_1 C1_1 1.815(4) . ? O4_1 C13_1 1.265(8) . ? O5_1 C13_1 1.251(9) . ? O6_1 C14_1 1.253(9) . ? O7_1 C14_1 1.287(8) . ? C1_1 C2A_1 1.358(15) . ? C1_1 C6A_1 1.370(15) . ? C1_1 C2_1 1.3900 . ? C1_1 C6_1 1.3900 . ? C2_1 C3_1 1.3900 . ? C2_1 H2_1 0.9300 . ? C3_1 C4_1 1.3900 . ? C3_1 H3_1 0.9300 . ? C4_1 C5A_1 1.361(15) . ? C4_1 C5_1 1.3900 . ? C4_1 C3A_1 1.405(15) . ? C4_1 C7_1 1.505(8) . ? C5_1 C6_1 1.3900 . ? C5_1 H5_1 0.9300 . ? C6_1 H6_1 0.9300 . ? C2A_1 C3A_1 1.390(16) . ? C2A_1 H2A_1 0.9300 . ? C3A_1 H3A_1 0.9300 . ? C5A_1 C6A_1 1.383(16) . ? C5A_1 H5A_1 0.9300 . ? C6A_1 H6A_1 0.9300 . ? C7_1 C8_1 1.395(10) . ? C7_1 C12_1 1.411(9) . ? C8_1 C9_1 1.400(10) . ? C8_1 H8_1 0.9300 . ? C9_1 C10_1 1.379(9) . ? C9_1 C13_1 1.499(10) . ? C10_1 C11_1 1.385(10) . ? C10_1 H10_1 0.9300 . ? C11_1 C12_1 1.365(10) . ? C11_1 C14_1 1.483(9) . ? C12_1 H12_1 0.9300 . ? P1_2 O2_2 1.503(10) . ? P1_2 O1_2 1.522(5) . ? P1_2 O1_2 1.522(5) 6_556 ? P1_2 C1_2 1.845(7) . ? O3_2 C11_2 1.263(11) . ? O4_2 C11_2 1.357(15) . ? O4A_2 C11_2 1.350(16) . ? C1_2 C2_2 1.3847 . ? C1_2 C6_2 1.3954 . ? C2_2 C3_2 1.3900 . ? C2_2 H2_2 0.9300 . ? C3_2 C4_2 1.3377 . ? C3_2 H3_2 0.9300 . ? C4_2 C4_2 0.05(3) 6_556 ? C4_2 C5_2 1.4422 . ? C4_2 C7_2 1.505(15) . ? C5_2 C6_2 1.3900 . ? C5_2 H5_2 0.9300 . ? C6_2 H6_2 0.9300 . ? C7_2 C8_2 1.396(11) 6_556 ? C7_2 C8_2 1.396(11) . ? C8_2 C9_2 1.391(13) . ? C8_2 H8_2 0.9300 . ? C10_2 C9_2 1.373(11) 6_556 ? C10_2 C9_2 1.373(11) . ? C10_2 H10_2 0.9300 . ? C11_2 C9_2 1.478(13) . ? C1_3 O1_3 1.19(3) . ? C1_3 N1_3 1.266(16) . ? C1_3 H1_3 0.9300 . ? N1_3 C3_3 1.52(2) . ? N1_3 C2_3 1.53(2) . ? C2_3 H2A_3 0.9600 . ? C2_3 H2AB_3 0.9600 . ? C2_3 H2AC_3 0.9600 . ? C3_3 H3A_3 0.9600 . ? C3_3 H3AB_3 0.9600 . ? C3_3 H3AC_3 0.9600 . ? C1_4 O1_4 1.19(3) . ? C1_4 N1_4 1.28(2) . ? C1_4 H1_4 0.9300 . ? N1_4 C2_4 1.53(2) . ? N1_4 C3_4 1.54(2) . ? C2_4 H2A_4 0.9600 . ? C2_4 H2AB_4 0.9600 . ? C2_4 H2AC_4 0.9600 . ? C3_4 H3A_4 0.9600 . ? C3_4 H3AB_4 0.9600 . ? C3_4 H3AC_4 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O3_1 P1_1 O1_1 Gd1 113.7(5) . . . . ? O2_1 P1_1 O1_1 Gd1 -4.1(6) . . . . ? C1_1 P1_1 O1_1 Gd1 -124.1(5) . . . . ? Gd1 P1_1 O1_1 Gd1 56.9(6) 2_665 . . . ? O1_1 P1_1 O2_1 Gd2 -16.0(5) . . . 7_676 ? O3_1 P1_1 O2_1 Gd2 -139.0(4) . . . 7_676 ? C1_1 P1_1 O2_1 Gd2 103.5(4) . . . 7_676 ? Gd1 P1_1 O2_1 Gd2 -131.4(4) 2_665 . . 7_676 ? O1_1 P1_1 O2_1 Gd1 115.4(2) . . . 2_665 ? O3_1 P1_1 O2_1 Gd1 -7.6(3) . . . 2_665 ? C1_1 P1_1 O2_1 Gd1 -125.0(2) . . . 2_665 ? O1_1 P1_1 O3_1 Gd3 30.8(6) . . . . ? O2_1 P1_1 O3_1 Gd3 154.0(5) . . . . ? C1_1 P1_1 O3_1 Gd3 -89.9(5) . . . . ? Gd1 P1_1 O3_1 Gd3 146.1(6) 2_665 . . . ? O1_1 P1_1 O3_1 Gd4 62.5(6) . . . . ? O2_1 P1_1 O3_1 Gd4 -174.2(5) . . . . ? C1_1 P1_1 O3_1 Gd4 -58.1(6) . . . . ? Gd1 P1_1 O3_1 Gd4 177.8(7) 2_665 . . . ? O1_1 P1_1 O3_1 Gd1 -115.3(2) . . . 2_665 ? O2_1 P1_1 O3_1 Gd1 7.9(3) . . . 2_665 ? C1_1 P1_1 O3_1 Gd1 124.0(2) . . . 2_665 ? O1_1 P1_1 C1_1 C2A_1 -148.6(16) . . . . ? O3_1 P1_1 C1_1 C2A_1 -24.9(16) . . . . ? O2_1 P1_1 C1_1 C2A_1 88.3(16) . . . . ? Gd1 P1_1 C1_1 C2A_1 30.3(16) 2_665 . . . ? O1_1 P1_1 C1_1 C6A_1 31.6(15) . . . . ? O3_1 P1_1 C1_1 C6A_1 155.4(15) . . . . ? O2_1 P1_1 C1_1 C6A_1 -91.5(15) . . . . ? Gd1 P1_1 C1_1 C6A_1 -149.5(15) 2_665 . . . ? O1_1 P1_1 C1_1 C2_1 -176.3(8) . . . . ? O3_1 P1_1 C1_1 C2_1 -52.5(8) . . . . ? O2_1 P1_1 C1_1 C2_1 60.6(8) . . . . ? Gd1 P1_1 C1_1 C2_1 2.6(9) 2_665 . . . ? O1_1 P1_1 C1_1 C6_1 6.1(8) . . . . ? O3_1 P1_1 C1_1 C6_1 129.8(8) . . . . ? O2_1 P1_1 C1_1 C6_1 -117.0(8) . . . . ? Gd1 P1_1 C1_1 C6_1 -175.0(8) 2_665 . . . ? C6_1 C1_1 C2_1 C3_1 0.0 . . . . ? P1_1 C1_1 C2_1 C3_1 -177.6(4) . . . . ? C1_1 C2_1 C3_1 C4_1 0.0 . . . . ? C2_1 C3_1 C4_1 C5_1 0.0 . . . . ? C2_1 C3_1 C4_1 C7_1 -178.9(6) . . . . ? C3_1 C4_1 C5_1 C6_1 0.0 . . . . ? C7_1 C4_1 C5_1 C6_1 178.9(6) . . . . ? C4_1 C5_1 C6_1 C1_1 0.0 . . . . ? C2_1 C1_1 C6_1 C5_1 0.0 . . . . ? P1_1 C1_1 C6_1 C5_1 177.7(4) . . . . ? C6A_1 C1_1 C2A_1 C3A_1 1(3) . . . . ? P1_1 C1_1 C2A_1 C3A_1 -178.6(16) . . . . ? C1_1 C2A_1 C3A_1 C4_1 1(3) . . . . ? C5A_1 C4_1 C3A_1 C2A_1 -3(3) . . . . ? C7_1 C4_1 C3A_1 C2A_1 -179.0(16) . . . . ? C3A_1 C4_1 C5A_1 C6A_1 3(3) . . . . ? C7_1 C4_1 C5A_1 C6A_1 179.3(17) . . . . ? C2A_1 C1_1 C6A_1 C5A_1 -1(3) . . . . ? P1_1 C1_1 C6A_1 C5A_1 178.9(16) . . . . ? C4_1 C5A_1 C6A_1 C1_1 -1(3) . . . . ? C5A_1 C4_1 C7_1 C8_1 178.6(16) . . . . ? C5_1 C4_1 C7_1 C8_1 -156.3(10) . . . . ? C3_1 C4_1 C7_1 C8_1 22.6(12) . . . . ? C3A_1 C4_1 C7_1 C8_1 -5.2(18) . . . . ? C5A_1 C4_1 C7_1 C12_1 -2.8(18) . . . . ? C5_1 C4_1 C7_1 C12_1 22.3(12) . . . . ? C3_1 C4_1 C7_1 C12_1 -158.8(10) . . . . ? C3A_1 C4_1 C7_1 C12_1 173.3(16) . . . . ? C12_1 C7_1 C8_1 C9_1 -0.9(11) . . . . ? C4_1 C7_1 C8_1 C9_1 177.8(7) . . . . ? C7_1 C8_1 C9_1 C10_1 -2.3(11) . . . . ? C7_1 C8_1 C9_1 C13_1 178.0(7) . . . . ? C8_1 C9_1 C10_1 C11_1 2.2(11) . . . . ? C13_1 C9_1 C10_1 C11_1 -178.1(6) . . . . ? C9_1 C10_1 C11_1 C12_1 1.2(10) . . . . ? C9_1 C10_1 C11_1 C14_1 -177.9(6) . . . . ? C10_1 C11_1 C12_1 C7_1 -4.5(11) . . . . ? C14_1 C11_1 C12_1 C7_1 174.5(7) . . . . ? C8_1 C7_1 C12_1 C11_1 4.3(11) . . . . ? C4_1 C7_1 C12_1 C11_1 -174.4(7) . . . . ? Gd1 O5_1 C13_1 O4_1 8.4(8) 1_655 . . . ? Gd1 O5_1 C13_1 C9_1 -169.3(6) 1_655 . . . ? Gd1 O4_1 C13_1 O5_1 -8.4(8) 1_655 . . . ? Gd1 O4_1 C13_1 C9_1 169.3(6) 1_655 . . . ? C10_1 C9_1 C13_1 O5_1 0.4(11) . . . . ? C8_1 C9_1 C13_1 O5_1 -179.9(7) . . . . ? C10_1 C9_1 C13_1 O4_1 -177.3(7) . . . . ? C8_1 C9_1 C13_1 O4_1 2.4(11) . . . . ? Gd2 O6_1 C14_1 O7_1 -12.9(7) 5_676 . . . ? Gd2 O6_1 C14_1 C11_1 163.1(6) 5_676 . . . ? Gd1 O7_1 C14_1 O6_1 -114.9(7) 4_566 . . . ? Gd2 O7_1 C14_1 O6_1 12.5(7) 5_676 . . . ? Gd1 O7_1 C14_1 C11_1 69.1(10) 4_566 . . . ? Gd2 O7_1 C14_1 C11_1 -163.6(6) 5_676 . . . ? Gd1 O7_1 C14_1 Gd2 -127.4(7) 4_566 . . 5_676 ? C12_1 C11_1 C14_1 O6_1 -145.7(7) . . . . ? C10_1 C11_1 C14_1 O6_1 33.3(10) . . . . ? C12_1 C11_1 C14_1 O7_1 30.3(10) . . . . ? C10_1 C11_1 C14_1 O7_1 -150.7(7) . . . . ? C12_1 C11_1 C14_1 Gd2 -63(2) . . . 5_676 ? C10_1 C11_1 C14_1 Gd2 115.6(19) . . . 5_676 ? O2_2 P1_2 O1_2 Gd1 16.5(10) . . . . ? O1_2 P1_2 O1_2 Gd1 140.8(6) 6_556 . . . ? C1_2 P1_2 O1_2 Gd1 -102.9(9) . . . . ? O2_2 P1_2 C1_2 C2_2 -117.4(7) . . . . ? O1_2 P1_2 C1_2 C2_2 4.5(8) . . . . ? O1_2 P1_2 C1_2 C2_2 120.6(7) 6_556 . . . ? O2_2 P1_2 C1_2 C6_2 60.6(6) . . . . ? O1_2 P1_2 C1_2 C6_2 -177.4(6) . . . . ? O1_2 P1_2 C1_2 C6_2 -61.3(7) 6_556 . . . ? C6_2 C1_2 C2_2 C3_2 -0.3 . . . . ? P1_2 C1_2 C2_2 C3_2 177.7(8) . . . . ? C1_2 C2_2 C3_2 C4_2 -1.5 . . . . ? C2_2 C3_2 C4_2 C4_2 -129.98(18) . . . 6_556 ? C2_2 C3_2 C4_2 C5_2 3.2 . . . . ? C2_2 C3_2 C4_2 C7_2 -179.7(13) . . . . ? C4_2 C4_2 C5_2 C6_2 44.91(8) 6_556 . . . ? C3_2 C4_2 C5_2 C6_2 -3.1 . . . . ? C7_2 C4_2 C5_2 C6_2 179.8(13) . . . . ? C4_2 C5_2 C6_2 C1_2 1.3 . . . . ? C2_2 C1_2 C6_2 C5_2 0.3 . . . . ? P1_2 C1_2 C6_2 C5_2 -177.8(8) . . . . ? C4_2 C4_2 C7_2 C8_2 1.0(14) 6_556 . . 6_556 ? C5_2 C4_2 C7_2 C8_2 -151.9(12) . . . 6_556 ? C3_2 C4_2 C7_2 C8_2 31.0(18) . . . 6_556 ? C4_2 C4_2 C7_2 C8_2 179(51) 6_556 . . . ? C5_2 C4_2 C7_2 C8_2 26.1(19) . . . . ? C3_2 C4_2 C7_2 C8_2 -151.0(11) . . . . ? C5_2 C4_2 C7_2 C4_2 -152.9(6) . . . 6_556 ? C3_2 C4_2 C7_2 C4_2 30.0(8) . . . 6_556 ? C8_2 C7_2 C8_2 C9_2 -4(2) 6_556 . . . ? C4_2 C7_2 C8_2 C9_2 177.6(12) . . . . ? C4_2 C7_2 C8_2 C9_2 177.6(12) 6_556 . . . ? Gd2 O3_2 C11_2 O4A_2 48(3) . . . . ? Gd2 O3_2 C11_2 O4_2 107(2) . . . . ? Gd2 O3_2 C11_2 C9_2 -94.4(17) . . . . ? C9_2 C10_2 C9_2 C8_2 4(2) 6_556 . . . ? C9_2 C10_2 C9_2 C11_2 -178.7(10) 6_556 . . . ? C7_2 C8_2 C9_2 C10_2 0.4(19) . . . . ? C7_2 C8_2 C9_2 C11_2 -176.9(12) . . . . ? O3_2 C11_2 C9_2 C10_2 162.9(12) . . . . ? O4A_2 C11_2 C9_2 C10_2 19(2) . . . . ? O4_2 C11_2 C9_2 C10_2 -38(2) . . . . ? O3_2 C11_2 C9_2 C8_2 -19.8(19) . . . . ? O4A_2 C11_2 C9_2 C8_2 -163.7(18) . . . . ? O4_2 C11_2 C9_2 C8_2 138.9(15) . . . . ? N1_3 C1_3 O1_3 Gd1 -179.9(14) . . . . ? O1_3 C1_3 N1_3 C3_3 168(2) . . . . ? O1_3 C1_3 N1_3 C2_3 -2(2) . . . . ? N1_4 C1_4 O1_4 Gd1 -171(3) . . . . ? O1_4 C1_4 N1_4 C2_4 -175(3) . . . . ? O1_4 C1_4 N1_4 C3_4 1(3) . . . . ?