Crystallography Open Database

Information card for entry 7707189

Preview

Coordinates	7707189.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H30 Na4.55 Nb12 O64.25 Ru5 V
Calculated formula	C30 H30 Na4.55 Nb12 O64.25 Ru5 V
Title of publication	Coordination capacity of Keggin anions as polytopic ligands: case study of [VNb<sub>12</sub>O<sub>40</sub>]<sup>15</sup>.
Authors of publication	Mukhacheva, Anna A.; Volcheck, Victoria V.; Sheven, Dmitry G.; Yanshole, Vadim V.; Kompankov, Nikolay B.; Haouas, Mohamed; Abramov, Pavel A.; Sokolov, Maxim N.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	20
Pages of publication	7078 - 7084
a	14.1141 ± 0.0007 Å
b	16.3111 ± 0.001 Å
c	22.4722 ± 0.0009 Å
α	92.167 ± 0.004°
β	93.075 ± 0.004°
γ	114.998 ± 0.005°
Cell volume	4671.6 ± 0.5 Å³
Cell temperature	140 ± 2 K
Ambient diffraction temperature	140 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1746
Residual factor for significantly intense reflections	0.0784
Weighted residual factors for significantly intense reflections	0.1625
Weighted residual factors for all reflections included in the refinement	0.1928
Goodness-of-fit parameter for all reflections included in the refinement	0.942
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
266035 (current)	2021-06-05	cif/ Updating files of 7707188, 7707189 Original log message: Adding full bibliography for 7707188--7707189.cif.	7707189.cif
264497	2021-04-24	cif/ Adding structures of 7707188, 7707189 via cif-deposit CGI script.	7707189.cif