#------------------------------------------------------------------------------ #$Date: 2021-04-28 04:49:41 +0300 (Wed, 28 Apr 2021) $ #$Revision: 264608 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/72/7707204.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7707204 loop_ _publ_author_name 'Gao, Liuzhou' 'Zhang, Hanyin' 'Liu, Xueting' 'Wang, Guoqiang' 'Li, Shuhua' _publ_section_title ; Mechanistic Insights into the Dearomative Diborylation of Pyrazines: A Radical or non-Radical Process? ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT00921D _journal_year 2021 _chemical_formula_moiety 'C20 H30 B2 N2 O4' _chemical_formula_sum 'C20 H30 B2 N2 O4' _chemical_formula_weight 384.08 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _audit_block_doi 10.5517/ccdc.csd.cc27jt9x _audit_creation_date 2021-01-29 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6226) ; _audit_update_record ; 2021-03-20 deposited with the CCDC. 2021-04-27 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 107.916(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 15.7142(11) _cell_length_b 11.0458(8) _cell_length_c 12.8792(9) _cell_measurement_reflns_used 9888 _cell_measurement_temperature 190.0 _cell_measurement_theta_max 54.002 _cell_measurement_theta_min 2.571 _cell_volume 2127.1(3) _computing_cell_refinement 'SAINT v8.37A (Bruker, 2015)' _computing_data_reduction 'SAINT v8.37A (Bruker, 2015)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'olex2.solve 1.3 (Bourhis et al., 2015)' _diffrn_ambient_temperature 190.0 _diffrn_measured_fraction_theta_full 0.984 _diffrn_measured_fraction_theta_max 0.984 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type GaK\a _diffrn_radiation_wavelength 1.34139 _diffrn_reflns_av_R_equivalents 0.0480 _diffrn_reflns_av_unetI/netI 0.0382 _diffrn_reflns_Laue_measured_fraction_full 0.984 _diffrn_reflns_Laue_measured_fraction_max 0.984 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 17293 _diffrn_reflns_point_group_measured_fraction_full 0.984 _diffrn_reflns_point_group_measured_fraction_max 0.984 _diffrn_reflns_theta_full 53.594 _diffrn_reflns_theta_max 54.003 _diffrn_reflns_theta_min 2.571 _diffrn_source_current 2.86 _diffrn_source_power 0.1993706 _diffrn_source_voltage 69.71 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.415 _exptl_absorpt_correction_T_max 0.7506 _exptl_absorpt_correction_T_min 0.5651 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1639 before and 0.1005 after correction. The Ratio of minimum to maximum transmission is 0.7529. The \l/2 correction factor is Not present. ; _exptl_crystal_colour red _exptl_crystal_colour_primary red _exptl_crystal_density_diffrn 1.199 _exptl_crystal_description block _exptl_crystal_F_000 824 _exptl_crystal_size_max 0.21 _exptl_crystal_size_mid 0.17 _exptl_crystal_size_min 0.13 _refine_diff_density_max 0.216 _refine_diff_density_min -0.259 _refine_diff_density_rms 0.057 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.061 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 261 _refine_ls_number_reflns 3843 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.061 _refine_ls_R_factor_all 0.0466 _refine_ls_R_factor_gt 0.0424 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0659P)^2^+0.4140P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1152 _refine_ls_wR_factor_ref 0.1199 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3466 _reflns_number_total 3843 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt00921d2.cif _cod_data_source_block w_a _cod_database_code 7707204 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.948 _shelx_estimated_absorpt_t_min 0.918 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C1(H1), C2(H2), C5(H5), C6(H6), C7(H7), C8(H8) 2.b Idealised Me refined as rotating group: C10(H10A,H10B,H10C), C11(H11A,H11B,H11C), C13(H13A,H13B,H13C), C14(H14A,H14B, H14C), C16(H16A,H16B,H16C), C17(H17A,H17B,H17C), C19(H19A,H19B,H19C), C20(H20A, H20B,H20C) ; _shelx_res_file ; TITL W_a.res in P2(1)/c w_a.res created by SHELXL-2018/3 at 21:58:33 on 29-Jan-2021 REM Old TITL W in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.135, Rweak 0.003, Alpha 0.034, Orientation as input REM Formula found by SHELXT: C22 N2 O4 CELL 1.34139 15.7142 11.0458 12.8792 90 107.916 90 ZERR 4 0.0011 0.0008 0.0009 0 0.003 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H B N O DISP B 0.007 0.0029 26.6 DISP C 0.0137 0.0067 57.1 DISP H 0 0 0.6 DISP N 0.0241 0.0134 109.9 DISP O 0.0389 0.0241 193.4 UNIT 80 120 8 8 16 L.S. 10 PLAN 4 SIZE 0.13 0.17 0.21 TEMP -83.15 CONF LIST 6 fmap 2 MORE -1 BOND $H ACTA REM REM REM WGHT 0.065900 0.414000 FVAR 1.18693 B1 3 0.643374 0.049323 0.755211 11.00000 0.02589 0.02170 = 0.02820 -0.00209 0.00998 -0.00120 B2 3 0.850079 0.694740 0.732623 11.00000 0.02677 0.02087 = 0.02949 0.00086 0.00810 0.00015 C1 1 0.758217 0.190227 0.865999 11.00000 0.02606 0.02337 = 0.02444 0.00230 0.00549 0.00007 AFIX 43 H1 2 0.772428 0.133517 0.924277 11.00000 -1.20000 AFIX 0 C2 1 0.799240 0.297611 0.882283 11.00000 0.02783 0.02353 = 0.02406 -0.00005 0.00448 -0.00150 AFIX 43 H2 2 0.840786 0.315262 0.951591 11.00000 -1.20000 AFIX 0 C3 1 0.781711 0.388230 0.796185 11.00000 0.02184 0.02131 = 0.02445 -0.00159 0.00702 -0.00014 C4 1 0.719682 0.350224 0.691631 11.00000 0.02160 0.02191 = 0.02480 -0.00105 0.00725 0.00087 C5 1 0.680172 0.241015 0.679899 11.00000 0.02507 0.02303 = 0.02406 -0.00127 0.00552 -0.00115 AFIX 43 H5 2 0.640636 0.219195 0.610435 11.00000 -1.20000 AFIX 0 C6 1 0.819788 0.498524 0.808036 11.00000 0.02776 0.02130 = 0.02391 0.00034 0.00495 -0.00065 AFIX 43 H6 2 0.859291 0.520796 0.877386 11.00000 -1.20000 AFIX 0 C7 1 0.743561 0.546991 0.620688 11.00000 0.02829 0.02509 = 0.02568 0.00419 0.00433 0.00016 AFIX 43 H7 2 0.730769 0.602379 0.561446 11.00000 -1.20000 AFIX 0 C8 1 0.703878 0.438832 0.604427 11.00000 0.02705 0.02611 = 0.02431 0.00017 0.00401 -0.00152 AFIX 43 H8 2 0.664419 0.419343 0.534273 11.00000 -1.20000 AFIX 0 C9 1 0.942746 0.849417 0.808946 11.00000 0.03179 0.01895 = 0.03166 0.00099 0.00724 -0.00420 C10 1 1.042915 0.865480 0.854168 11.00000 0.03472 0.03610 = 0.04031 -0.00126 0.00507 -0.00811 AFIX 137 H10A 2 1.062284 0.849961 0.932902 11.00000 -1.50000 H10B 2 1.058802 0.948482 0.840579 11.00000 -1.50000 H10C 2 1.072609 0.808413 0.818344 11.00000 -1.50000 AFIX 0 C11 1 0.895834 0.923224 0.874427 11.00000 0.04633 0.03020 = 0.03906 -0.00467 0.01409 -0.00061 AFIX 137 H11A 2 0.831096 0.910740 0.844980 11.00000 -1.50000 H11B 2 0.909482 1.009236 0.869695 11.00000 -1.50000 H11C 2 0.916623 0.897370 0.950901 11.00000 -1.50000 AFIX 0 C12 1 0.902656 0.867881 0.682932 11.00000 0.03397 0.02244 = 0.03317 0.00163 0.00762 -0.00776 C13 1 0.965087 0.828073 0.620329 11.00000 0.04747 0.04921 = 0.03899 -0.00526 0.01769 -0.01239 AFIX 137 H13A 2 0.989456 0.747973 0.645913 11.00000 -1.50000 H13B 2 1.014169 0.886380 0.632254 11.00000 -1.50000 H13C 2 0.932042 0.824101 0.542302 11.00000 -1.50000 AFIX 0 C14 1 0.866291 0.993449 0.648070 11.00000 0.06210 0.02690 = 0.04347 0.01001 0.00761 -0.00374 AFIX 137 H14A 2 0.838004 0.994971 0.568825 11.00000 -1.50000 H14B 2 0.915374 1.052207 0.668306 11.00000 -1.50000 H14C 2 0.821965 1.014414 0.684521 11.00000 -1.50000 AFIX 0 C15 1 0.585041 -0.122060 0.801334 11.00000 0.03108 0.02463 = 0.03107 -0.00170 0.00885 -0.01053 C16 1 0.525692 -0.082922 0.868200 11.00000 0.03810 0.04821 = 0.03312 -0.00523 0.01492 -0.01358 AFIX 137 H16A 2 0.559471 -0.087092 0.945988 11.00000 -1.50000 H16B 2 0.473704 -0.136731 0.852863 11.00000 -1.50000 H16C 2 0.505485 0.000390 0.849029 11.00000 -1.50000 AFIX 0 C17 1 0.618140 -0.250318 0.829524 11.00000 0.05540 0.02629 = 0.04511 0.00512 0.01205 -0.00761 AFIX 137 H17A 2 0.661476 -0.270529 0.791400 11.00000 -1.50000 H17B 2 0.567490 -0.306475 0.806955 11.00000 -1.50000 H17C 2 0.646873 -0.256953 0.908462 11.00000 -1.50000 AFIX 0 C18 1 0.542650 -0.096514 0.676420 11.00000 0.03604 0.02235 = 0.03002 -0.00325 0.01057 -0.01037 C19 1 0.441575 -0.103244 0.634852 11.00000 0.03828 0.04095 = 0.03657 -0.00268 0.00510 -0.01490 AFIX 137 H19A 2 0.416280 -0.046482 0.675931 11.00000 -1.50000 H19B 2 0.422237 -0.185701 0.644469 11.00000 -1.50000 H19C 2 0.420776 -0.081906 0.557246 11.00000 -1.50000 AFIX 0 C20 1 0.583098 -0.171160 0.604528 11.00000 0.06330 0.03379 = 0.03817 -0.00925 0.02240 -0.00714 AFIX 137 H20A 2 0.561593 -0.140733 0.529481 11.00000 -1.50000 H20B 2 0.565383 -0.256053 0.605993 11.00000 -1.50000 H20C 2 0.648438 -0.164894 0.631685 11.00000 -1.50000 AFIX 0 N1 4 0.695014 0.157227 0.766677 11.00000 0.02642 0.02086 = 0.02695 -0.00011 0.00616 -0.00269 N2 4 0.803318 0.582621 0.721305 11.00000 0.02911 0.02136 = 0.02660 0.00160 0.00507 -0.00205 O1 5 0.662488 -0.040977 0.831400 11.00000 0.02743 0.02430 = 0.03072 0.00189 0.00603 -0.00645 O2 5 0.569464 0.029177 0.667136 11.00000 0.03150 0.02352 = 0.02948 0.00083 0.00579 -0.00751 O3 5 0.921445 0.721988 0.821767 11.00000 0.03181 0.01964 = 0.03086 0.00286 0.00428 -0.00382 O4 5 0.827914 0.782733 0.654327 11.00000 0.03070 0.02392 = 0.03312 0.00545 0.00238 -0.00504 HKLF 4 REM W_a.res in P2(1)/c REM wR2 = 0.1199, GooF = S = 1.061, Restrained GooF = 1.061 for all data REM R1 = 0.0424 for 3466 Fo > 4sig(Fo) and 0.0466 for all 3843 data REM 261 parameters refined using 0 restraints END WGHT 0.0659 0.4140 REM Highest difference peak 0.216, deepest hole -0.259, 1-sigma level 0.057 Q1 1 1.0000 1.0000 1.0000 10.50000 0.05 0.22 Q2 1 1.0057 0.7356 0.9021 11.00000 0.05 0.18 Q3 1 0.8865 0.9280 0.6611 11.00000 0.05 0.18 Q4 1 0.7328 0.2788 0.6468 11.00000 0.05 0.17 ; _shelx_res_checksum 86670 _shelx_hkl_file ; 0 0 5 0.80 0.40 0 0 5 0.70 0.80 0 0 5 -0.80 0.80 0 0 -5 1.20 0.30 0 0 -5 3.60 1.50 0 0 -5 0.10 1.10 0 0 -7 0.40 1.90 0 0 7 -0.50 1.20 0 0 7 -1.80 0.80 0 0 -7 -1.00 1.40 0 0 7 0.30 0.40 0 0 8 57.59 3.90 0 0 -8 65.09 6.10 0 0 8 67.49 4.70 0 0 8 69.19 5.20 0 0 -9 1.70 2.50 0 0 9 1.80 1.90 0 0 9 0.80 1.30 0 0 10 2.20 2.30 0 0 10 2.00 1.60 0 0 -10 -1.30 3.20 0 0 11 0.60 3.00 0 0 11 0.60 1.70 0 0 -11 -1.20 2.10 0 0 12 19.80 2.90 0 0 -12 16.00 3.20 0 0 12 13.40 4.00 0 0 13 -1.70 2.00 0 0 -13 0.60 3.50 0 0 13 6.80 5.50 0 0 14 538.35 33.90 0 -1 0 0.60 0.20 0 -1 0 0.20 0.10 0 1 -1 326.97 20.90 0 1 -1 352.86 20.80 0 1 -2 532.25 29.00 0 -1 -2 406.76 29.40 0 1 -3 25.80 1.50 0 1 -3 26.00 1.90 0 1 3 23.50 2.40 0 -1 -3 21.80 1.90 0 -1 3 23.60 1.70 0 -1 3 21.90 1.50 0 -1 -4 2391.36 146.59 0 1 -5 572.34 34.10 0 1 -5 546.75 34.00 0 1 5 548.35 33.50 0 1 5 496.45 33.50 0 -1 5 528.05 33.50 0 -1 -5 556.34 33.30 0 -1 5 570.54 33.70 0 -1 5 543.35 33.40 0 1 6 2160.18 126.09 0 1 -6 1896.21 126.79 0 1 -6 2068.49 126.89 0 1 6 1972.50 126.09 0 -1 6 2106.29 126.19 0 -1 -6 1963.20 125.79 0 -1 -6 2074.69 126.59 0 -1 6 2304.77 126.39 0 1 7 178.48 11.60 0 1 -7 204.88 12.80 0 1 7 181.58 11.60 0 1 7 173.38 11.30 0 -1 -7 159.88 11.10 0 -1 7 195.78 12.10 0 -1 7 178.88 11.30 0 -1 -7 187.68 12.40 0 -1 -7 188.28 11.10 0 -1 7 177.38 11.70 0 1 8 618.34 37.10 0 1 8 615.34 37.00 0 1 -8 574.14 38.20 0 -1 8 624.74 37.50 0 -1 8 601.44 37.10 0 -1 -8 556.04 37.80 0 1 -9 1274.77 83.39 0 1 9 1314.07 82.09 0 1 9 1380.16 81.99 0 -1 9 1313.77 81.99 0 -1 -9 1347.97 81.79 0 -1 -9 1385.66 83.09 0 1 10 2694.83 161.48 0 1 -10 2506.55 163.28 0 1 10 2670.93 161.68 0 -1 -10 2566.04 161.28 0 -1 10 2771.02 161.48 0 1 11 496.35 32.10 0 1 11 504.35 31.70 0 1 -11 472.45 34.30 0 -1 11 489.55 34.10 0 -1 11 529.05 31.70 0 -1 -11 521.75 31.70 0 1 12 679.83 44.60 0 1 -12 687.53 43.90 0 1 12 707.23 43.90 0 -1 12 743.43 44.00 0 1 -13 8.30 3.20 0 1 13 4.10 4.50 0 1 13 8.60 2.70 0 -1 13 6.50 2.40 0 1 14 45.10 5.00 0 -1 -14 52.59 9.00 0 -1 14 36.50 4.30 0 2 0 9.60 1.30 0 2 0 9.70 0.90 0 -2 0 6.20 0.80 0 -2 0 7.50 0.90 0 2 -2 6.90 0.70 0 2 -2 9.50 1.40 0 2 -2 9.00 0.90 0 2 2 7.10 0.70 0 -2 2 6.50 0.70 0 -2 -2 6.90 0.80 0 2 4 8.20 1.10 0 2 4 8.90 1.00 0 2 -4 7.10 1.60 0 2 4 9.40 0.90 0 2 4 7.80 1.90 0 2 -4 9.20 0.80 0 -2 4 9.00 1.00 0 -2 -4 11.10 1.00 0 2 6 2.50 0.30 0 2 6 2.40 0.90 0 2 -6 1.50 1.70 0 2 6 2.70 0.90 0 2 6 2.30 1.00 0 2 6 2.00 0.50 0 -2 -6 1.80 0.50 0 -2 6 1.40 1.90 0 -2 6 1.70 1.00 0 -2 6 2.60 0.60 0 -2 -6 1.50 1.20 0 2 -7 1775.72 119.69 0 2 -7 2001.70 118.49 0 2 7 2022.60 117.29 0 2 7 1762.82 117.09 0 -2 -7 1785.12 116.99 0 -2 7 2169.08 118.09 0 -2 7 1834.12 117.39 0 -2 7 2033.50 117.49 0 2 8 34.20 2.80 0 2 -8 32.70 4.80 0 2 8 31.30 2.90 0 2 -8 21.80 4.10 0 -2 8 30.40 2.80 0 -2 -8 32.10 3.10 0 -2 -8 30.20 3.90 0 -2 8 25.70 2.20 0 -2 8 24.80 4.70 0 -2 -8 26.30 2.10 0 -2 -8 28.00 2.20 0 2 9 424.36 26.80 0 2 -9 429.96 28.70 0 2 9 423.26 26.70 0 -2 -9 398.66 27.40 0 -2 9 440.16 26.80 0 -2 9 444.06 28.80 0 2 10 20.90 2.60 0 -2 10 5.70 7.70 0 -2 10 17.10 2.50 0 2 -11 576.74 42.80 0 2 11 655.43 40.30 0 2 11 657.33 40.00 0 -2 11 662.23 40.10 0 -2 11 648.44 43.30 0 2 -12 1.90 2.40 0 2 12 2.10 2.70 0 2 12 1.20 2.20 0 -2 12 -3.00 1.70 0 -2 -12 4.60 5.30 0 2 13 11.00 2.70 0 2 -13 5.50 2.70 0 2 13 -0.90 3.60 0 -2 -13 8.30 6.80 0 -2 13 5.60 2.30 0 2 14 10.20 2.70 0 2 -14 12.30 6.70 0 -2 14 12.30 2.80 0 3 0 -0.20 0.40 0 3 0 2.20 0.80 0 -3 0 0.00 0.40 0 -3 0 0.20 0.40 0 3 -1 1013.20 61.69 0 3 1 998.00 61.39 0 3 2 1191.68 72.49 0 3 -3 130.49 8.50 0 3 3 115.09 7.40 0 3 3 120.19 7.70 0 3 -3 123.29 7.60 0 3 -3 119.29 7.80 0 -3 -3 122.99 7.60 0 -3 3 132.79 7.50 0 -3 3 103.29 7.90 0 3 -4 1684.83 90.49 0 3 4 1375.76 89.49 0 -3 4 1408.46 89.69 0 -3 4 1465.85 89.69 0 -3 -4 1562.64 89.59 0 -3 -4 1316.27 90.19 0 3 5 3315.07 223.08 0 3 5 3377.56 221.78 0 -3 5 4013.30 222.08 0 -3 5 3878.51 222.78 0 3 6 3897.11 246.18 0 3 6 3956.50 247.08 0 -3 6 3971.50 247.08 0 -3 6 3918.01 246.38 0 -3 -6 3874.51 246.08 0 -3 -6 4663.23 247.28 0 3 -7 802.92 46.40 0 3 7 673.43 44.20 0 3 7 667.63 45.00 0 3 7 758.12 44.70 0 3 -7 836.42 46.00 0 3 7 725.93 44.70 0 -3 -7 665.23 44.50 0 -3 7 730.83 44.90 0 -3 7 699.73 44.60 0 3 -8 322.57 21.70 0 3 8 302.17 19.70 0 3 8 317.37 19.80 0 -3 8 330.87 20.00 0 -3 8 305.07 19.60 0 -3 -8 340.77 21.50 0 -3 8 279.37 22.00 0 3 9 94.49 6.90 0 3 -9 96.69 9.50 0 3 9 98.09 7.00 0 -3 -9 106.59 9.50 0 -3 9 97.69 7.10 0 3 -10 224.48 18.60 0 3 10 247.88 16.00 0 3 10 246.88 15.80 0 -3 -10 229.08 18.20 0 -3 10 263.67 16.00 0 3 11 62.29 5.70 0 3 -11 81.49 11.20 0 3 11 68.39 6.10 0 -3 11 71.49 5.90 0 -3 -11 79.69 10.10 0 3 12 51.09 5.20 0 3 12 57.39 5.90 0 -3 -12 61.49 9.50 0 -3 12 52.49 5.40 0 3 -13 145.59 10.30 0 3 13 130.39 10.90 0 -3 -13 128.69 16.30 0 -3 13 144.69 10.00 0 -3 14 4.30 2.10 0 4 0 118.99 7.70 0 4 0 108.59 7.20 0 4 0 124.19 7.90 0 -4 0 120.19 7.60 0 -4 0 118.99 7.50 0 4 1 94.89 6.30 0 4 -1 100.29 6.40 0 4 1 97.29 6.40 0 4 -1 101.09 6.80 0 4 -1 92.09 5.90 0 4 1 82.99 5.90 0 -4 1 93.99 6.50 0 -4 1 100.89 6.20 0 -4 1 101.29 6.30 0 -4 -1 98.89 6.20 0 4 2 12.80 3.50 0 4 2 23.40 1.80 0 4 -2 26.30 3.00 0 4 -2 19.00 1.90 0 4 2 20.80 1.40 0 4 2 21.20 1.80 0 -4 -2 21.30 1.80 0 -4 2 22.40 1.70 0 -4 2 22.00 2.50 0 4 3 37.50 2.90 0 4 -3 37.90 4.00 0 4 3 38.60 2.40 0 4 -3 37.30 3.00 0 -4 3 31.80 2.90 0 -4 3 40.70 2.70 0 -4 -3 41.20 2.80 0 -4 3 41.60 2.90 0 -4 3 30.90 3.00 0 -4 -3 37.10 4.80 0 4 -4 1939.31 118.09 0 -4 4 1884.71 117.89 0 -4 -4 1947.21 118.79 0 -4 4 1957.30 118.49 0 4 5 54.19 3.60 0 4 -5 51.19 4.20 0 4 5 53.99 3.20 0 4 5 49.40 3.70 0 4 -5 53.59 5.30 0 -4 5 52.29 3.80 0 -4 5 54.09 3.50 0 -4 -5 50.09 3.70 0 -4 5 54.09 4.00 0 -4 -5 37.20 5.60 0 4 6 1505.55 109.89 0 4 6 1761.42 108.39 0 4 -6 1743.93 109.09 0 4 6 1861.81 108.39 0 4 -6 1811.92 109.89 0 -4 -6 1620.24 108.29 0 -4 -6 1829.52 109.69 0 -4 6 1860.01 108.49 0 -4 6 1988.00 108.19 0 -4 6 1781.12 108.59 0 4 7 70.89 6.50 0 4 -7 78.39 7.30 0 4 7 64.39 5.20 0 4 -7 77.79 7.40 0 4 7 79.39 5.30 0 4 7 75.19 4.60 0 -4 -7 59.59 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115.29 7.20 -1 2 7 106.99 7.30 -1 2 7 105.29 6.80 1 -2 -7 105.59 6.90 -1 -2 7 119.79 9.10 1 -2 -7 108.09 7.40 1 -2 -7 104.69 8.20 -1 -2 7 114.09 7.40 -1 -2 7 103.39 7.20 1 2 -6 64.49 5.50 1 2 -6 60.09 5.00 -1 2 6 54.59 4.00 -1 2 6 50.59 4.50 -1 2 6 50.89 3.50 -1 2 6 62.49 3.90 -1 -2 6 55.49 3.90 1 -2 -6 65.79 4.70 1 -2 -6 56.29 4.10 1 -2 -6 59.29 3.80 -1 -2 6 46.60 5.60 -1 -2 6 55.59 4.10 1 2 -5 314.37 20.00 1 2 -5 335.57 19.70 -1 2 5 267.57 19.90 -1 -2 5 300.17 19.10 1 -2 -5 325.37 19.40 -1 -2 5 286.97 19.10 1 -2 -5 295.77 18.90 -1 -2 5 342.07 19.90 -1 2 4 122.79 10.50 -1 2 4 135.59 9.40 1 2 -4 167.18 9.90 1 2 -4 159.18 10.30 1 -2 -4 146.79 9.30 -1 -2 4 162.98 9.20 -1 -2 4 158.78 9.60 1 -2 -4 158.18 9.80 -1 -2 4 141.49 9.50 -1 2 3 9.90 1.00 1 2 -3 10.60 1.20 1 2 -3 8.30 1.60 -1 2 3 9.30 2.20 -1 -2 3 8.50 1.00 -1 -2 3 10.30 0.80 1 -2 -3 7.40 2.50 1 -2 -3 9.40 0.90 1 2 -2 141.19 8.00 -1 2 2 135.79 8.00 -1 2 2 126.99 7.70 1 2 -2 115.99 8.30 -1 -2 2 115.59 8.10 -1 -2 2 118.09 7.70 -1 -2 2 123.99 7.90 1 -2 -2 118.09 7.70 1 2 -1 18.20 1.60 -1 2 1 20.80 1.60 -1 2 1 21.50 1.50 1 2 -1 21.40 2.30 1 -2 -1 23.20 1.50 -1 -2 1 18.80 2.00 -1 -2 1 22.60 1.70 1 2 2 1723.23 105.89 1 2 3 136.29 9.30 -1 2 -3 162.08 9.90 -1 2 -3 166.08 9.30 -1 2 -3 151.68 9.50 1 2 3 150.68 9.30 1 -2 3 144.89 9.50 1 -2 3 145.09 9.40 1 -2 3 141.49 9.60 1 -2 3 155.38 9.30 1 2 4 1956.30 125.39 1 2 4 2006.80 124.79 -1 -2 -4 2003.20 124.69 1 -2 4 2000.60 125.49 1 -2 4 2276.37 124.99 1 2 5 144.99 9.40 1 2 5 135.09 8.90 -1 2 -5 146.29 10.10 1 2 5 145.99 9.20 -1 2 -5 155.68 9.00 1 2 5 138.19 9.00 -1 2 -5 155.08 9.50 1 2 5 135.29 9.20 -1 -2 -5 148.59 9.10 1 -2 5 140.29 9.10 1 -2 5 144.89 9.50 1 -2 5 152.28 10.10 -1 -2 -5 150.78 9.30 1 2 6 2762.32 181.58 -1 2 -6 3134.99 182.18 -1 -2 -6 3012.50 181.78 1 -2 6 2926.41 181.78 1 -2 6 3197.88 182.28 -1 -2 -6 2860.01 181.38 1 2 7 92.19 6.50 1 2 7 104.09 6.70 -1 2 -7 114.49 8.10 -1 2 -7 97.99 7.50 1 -2 7 108.99 8.00 1 -2 7 91.79 6.80 -1 -2 -7 94.29 6.20 -1 -2 -7 92.39 6.40 1 -2 7 91.39 6.20 -1 2 -8 31.90 5.00 1 2 8 27.40 2.90 1 2 8 33.20 3.20 1 -2 8 30.60 5.40 -1 -2 -8 26.00 3.10 -1 -2 -8 29.30 4.10 1 -2 8 36.20 3.10 -1 -2 -8 29.60 2.40 -1 -2 -8 29.00 2.40 1 2 9 223.58 14.80 1 2 9 222.48 15.00 -1 2 -9 230.08 16.70 1 -2 9 229.88 14.90 1 -2 9 251.77 17.80 1 2 10 906.31 55.19 -1 2 -10 776.62 56.79 1 2 10 920.51 54.89 1 -2 10 884.71 57.29 1 -2 10 951.30 55.09 -1 2 -11 145.49 15.00 1 2 11 155.88 11.20 1 2 11 158.08 10.50 1 -2 11 163.68 10.60 1 -2 11 107.69 15.30 1 2 12 136.49 9.90 1 2 12 130.99 10.60 1 -2 12 130.09 11.40 -1 -2 -12 168.28 14.00 1 2 13 4.80 4.00 -1 2 -13 7.40 2.90 1 2 13 6.60 2.70 1 -2 13 7.50 2.30 -1 -2 -13 8.90 7.50 1 2 14 11.30 2.70 -1 2 -14 22.20 4.10 1 -2 14 21.50 2.90 1 3 -14 3.00 2.90 1 -3 -14 -11.40 15.50 -1 -3 14 2.40 2.20 -1 3 13 -0.40 3.30 1 3 -13 4.90 2.60 1 -3 -13 -1.50 7.30 -1 -3 13 0.10 2.10 1 3 -12 24.60 3.50 -1 3 12 22.20 3.50 -1 3 12 19.70 3.20 -1 -3 12 24.40 3.20 1 -3 -12 23.30 7.30 1 3 -11 36.80 7.20 -1 3 11 50.49 5.00 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4.00 1 3 -4 615.34 36.20 -1 3 4 562.74 35.20 -1 3 4 583.24 35.30 1 3 -4 630.44 35.70 -1 -3 4 617.34 35.10 -1 -3 4 482.05 35.60 1 -3 -4 537.55 36.00 -1 -3 4 562.84 35.40 1 -3 -4 580.04 35.20 -1 3 3 210.28 14.30 -1 3 3 241.38 14.70 1 3 -3 243.98 14.90 1 3 -3 232.68 15.30 -1 -3 3 239.18 14.50 -1 -3 3 248.78 14.80 1 -3 -3 234.08 14.60 -1 3 2 166.68 10.50 1 3 -2 179.28 11.10 1 3 -2 166.68 11.00 -1 3 2 161.68 10.20 -1 -3 2 159.28 10.60 1 -3 -2 164.98 10.40 -1 -3 2 174.78 10.40 -1 3 1 251.67 15.60 1 3 -1 261.37 15.80 -1 3 1 272.57 15.70 1 3 -1 258.87 16.10 -1 -3 1 214.48 15.80 -1 -3 1 250.77 15.70 1 -3 -1 260.27 15.60 -1 -3 1 253.67 15.60 1 3 0 9.60 1.10 -1 3 0 10.10 1.00 -1 3 0 9.80 1.00 -1 -3 0 9.50 1.00 -1 -3 0 9.10 1.30 -1 -3 0 8.10 1.10 1 3 1 61.09 4.30 1 3 1 71.69 4.50 -1 3 -1 62.29 4.70 -1 3 -1 70.19 4.20 -1 3 -1 64.49 4.30 1 -3 1 68.59 4.30 1 -3 1 60.69 4.20 -1 -3 -1 56.59 4.40 -1 -3 -1 69.29 4.20 1 3 2 552.54 35.50 -1 3 -2 667.83 35.70 -1 3 -2 568.84 35.80 -1 3 -2 594.84 36.20 1 3 2 540.65 35.80 -1 -3 -2 617.74 35.80 1 -3 2 532.95 35.90 1 -3 2 594.44 35.80 1 3 3 178.08 11.30 1 3 3 176.18 11.30 -1 3 -3 162.68 11.40 1 3 3 203.78 11.10 -1 3 -3 186.08 11.30 -1 3 -3 186.58 12.00 1 -3 3 154.78 11.50 1 -3 3 180.08 11.40 1 -3 3 179.28 11.50 1 -3 3 199.68 11.20 -1 -3 -3 187.88 11.30 1 3 4 30.70 2.20 1 3 4 27.50 1.70 -1 3 -4 30.60 2.30 -1 3 -4 26.40 3.30 -1 3 -4 31.40 2.00 1 3 4 25.10 2.10 1 3 4 25.00 2.00 1 -3 4 25.80 2.00 1 -3 4 20.30 3.80 1 -3 4 25.40 2.10 1 -3 4 24.20 2.60 1 3 5 287.67 18.60 -1 3 -5 326.47 19.80 1 3 5 291.67 18.30 -1 3 -5 330.57 19.00 1 3 5 312.97 18.70 -1 3 -5 288.07 18.40 1 3 5 279.47 18.50 1 -3 5 300.07 20.10 1 -3 5 289.67 18.60 -1 -3 -5 297.97 18.60 1 -3 5 329.37 18.90 -1 -3 -5 295.77 19.70 1 -3 5 285.27 18.50 -1 3 -6 280.97 20.30 1 3 6 334.07 19.20 1 3 6 284.77 19.60 -1 3 -6 340.67 19.80 1 3 6 302.67 19.00 1 3 6 290.57 18.80 1 3 6 297.47 19.20 -1 -3 -6 312.97 19.10 1 -3 6 298.67 19.10 1 -3 6 318.17 19.50 1 -3 6 341.27 21.10 1 3 7 423.36 25.00 -1 3 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-4 10 96.49 6.80 1 -4 -10 90.79 10.70 -1 4 9 38.20 3.60 -1 4 9 37.10 3.50 1 4 -9 41.70 7.00 1 -4 -9 33.70 6.20 -1 -4 9 39.20 3.70 -1 4 8 49.50 4.30 -1 4 8 54.49 3.40 -1 4 8 54.79 4.10 1 4 -8 53.49 7.00 -1 -4 8 55.89 4.40 1 -4 -8 54.39 7.40 1 4 -7 437.46 26.80 -1 4 7 408.86 24.20 -1 4 7 366.26 24.70 -1 4 7 377.26 26.30 1 4 -7 368.96 25.80 -1 4 7 403.26 24.60 1 -4 -7 423.36 26.60 -1 -4 7 400.26 25.60 -1 4 6 19.40 4.10 -1 4 6 22.80 1.40 1 4 -6 19.20 3.30 1 4 -6 17.90 2.90 -1 4 6 22.00 2.10 -1 4 6 21.40 1.90 -1 -4 6 20.60 1.50 -1 -4 6 23.20 2.30 -1 -4 6 18.50 2.00 1 -4 -6 22.30 2.10 1 -4 -6 26.70 4.50 -1 4 5 229.68 13.20 1 4 -5 206.98 16.30 -1 4 5 225.98 13.50 1 4 -5 219.28 14.10 -1 4 5 176.38 16.40 -1 4 5 207.68 13.60 1 -4 -5 209.38 15.10 -1 -4 5 240.98 13.70 1 4 -4 27.10 2.50 1 4 -4 31.30 3.90 -1 4 4 25.80 1.60 -1 4 4 15.00 4.00 -1 4 4 24.90 2.10 -1 -4 4 25.40 1.90 1 -4 -4 25.50 2.10 -1 -4 4 24.80 2.20 -1 -4 4 23.30 2.40 1 -4 -4 23.80 4.00 1 4 -2 5.60 0.50 -1 4 2 6.40 0.50 -1 4 2 6.20 1.10 1 4 -2 5.80 1.70 1 4 -2 6.40 1.20 -1 4 2 6.70 0.90 -1 4 2 2.50 2.60 1 -4 -2 7.60 0.90 -1 -4 2 6.10 0.80 -1 -4 2 6.10 1.10 1 -4 -2 9.40 2.60 -1 -4 2 5.50 1.10 -1 4 0 9.00 0.60 -1 4 0 7.40 1.20 1 4 0 9.20 1.50 1 4 0 9.20 0.70 -1 4 0 9.40 1.20 1 4 0 8.30 1.20 -1 4 0 10.80 1.30 1 -4 0 9.20 1.10 1 -4 0 9.70 2.00 -1 -4 0 10.00 1.20 -1 -4 0 9.10 1.20 -1 4 -1 492.05 28.70 1 4 1 447.76 28.50 -1 4 -1 476.15 29.20 -1 4 -1 490.85 29.00 1 4 1 420.06 28.90 -1 4 -1 437.46 28.50 -1 -4 -1 446.16 28.80 -1 -4 -1 542.45 28.80 1 -4 1 480.05 28.90 1 -4 1 450.15 28.70 -1 4 -2 113.29 7.30 -1 4 -2 116.89 7.90 1 4 2 115.49 7.80 1 4 2 118.69 7.40 -1 4 -2 134.29 7.70 -1 4 -2 122.69 8.30 1 -4 2 113.59 8.00 1 -4 2 113.99 8.00 1 -4 2 121.99 7.60 1 -4 2 130.49 7.80 -1 -4 -2 120.69 7.70 -1 4 -4 6.30 2.00 -1 4 -4 7.60 1.50 1 4 4 8.60 1.10 1 4 4 3.50 2.40 1 4 4 6.90 0.60 -1 4 -4 8.80 1.10 1 4 4 5.60 1.10 1 4 4 6.00 1.10 1 -4 4 7.00 0.90 1 -4 4 6.10 1.50 1 -4 4 5.60 1.10 -1 -4 -4 4.30 3.10 1 4 5 1949.20 125.09 1 4 5 1949.90 125.19 -1 4 -5 2323.87 126.59 1 -4 5 1998.90 124.99 -1 -4 -5 2085.49 126.49 1 -4 5 1993.10 125.19 1 -4 5 2146.69 125.69 -1 -4 -5 1991.20 125.19 1 4 6 260.47 19.10 1 4 6 323.17 17.90 1 4 6 256.37 17.70 -1 4 -6 318.27 19.50 -1 4 -6 278.47 18.40 1 4 6 298.07 17.40 1 -4 6 289.37 18.10 -1 -4 -6 278.77 19.20 1 -4 6 272.77 17.60 1 -4 6 273.07 17.80 -1 4 -7 41.50 5.40 1 4 7 34.30 2.20 1 4 7 31.50 2.90 1 4 7 30.80 3.60 1 4 7 34.20 3.00 -1 -4 -7 49.00 6.10 1 -4 7 34.70 3.30 1 4 8 86.09 6.00 -1 4 -8 87.89 8.70 1 4 8 78.19 5.90 1 -4 8 83.49 6.20 -1 -4 -8 76.19 9.00 1 4 9 92.79 7.20 -1 4 -9 105.99 10.30 -1 -4 -9 90.19 10.60 1 -4 9 105.19 7.40 1 4 10 153.48 10.50 1 4 10 146.39 10.10 -1 4 -10 140.99 13.90 1 -4 10 155.18 10.40 -1 -4 -10 142.49 14.30 1 4 11 160.88 11.40 1 4 11 147.89 10.90 1 -4 11 172.98 11.20 -1 -4 -11 161.28 16.30 1 4 12 340.87 22.40 1 -4 12 343.37 22.10 1 4 13 89.69 8.00 -1 4 -13 81.59 7.30 1 -4 13 89.39 7.00 -1 5 13 97.39 8.10 1 5 -13 86.29 7.70 -1 -5 13 93.69 7.20 -1 5 12 121.89 9.30 -1 -5 12 132.69 9.10 1 -5 -12 115.29 16.10 -1 5 11 32.20 3.90 1 -5 -11 33.50 8.40 -1 -5 11 39.10 4.10 -1 5 10 302.47 19.50 1 5 -10 280.37 23.00 -1 -5 10 315.37 19.60 1 -5 -10 316.67 23.30 -1 5 9 583.54 37.00 -1 5 9 620.34 37.70 1 5 -9 619.04 40.90 -1 -5 9 640.34 37.90 1 -5 -9 572.24 40.30 -1 5 8 324.97 19.80 -1 5 8 314.87 20.40 -1 -5 8 337.27 20.70 1 -5 -8 322.87 23.10 -1 5 7 344.67 21.60 1 5 -7 378.36 24.50 -1 5 7 360.46 22.10 -1 -5 7 364.96 22.30 1 -5 -7 317.27 24.20 1 5 -6 118.59 9.90 -1 5 6 121.79 7.20 -1 5 6 124.79 7.70 1 5 -6 110.39 8.70 -1 -5 6 115.09 7.90 -1 -5 6 112.69 7.40 1 5 -5 290.37 18.00 -1 5 5 274.27 16.80 1 5 -5 301.17 19.00 -1 5 5 285.37 17.10 -1 -5 5 274.77 17.30 -1 -5 5 245.18 17.00 -1 -5 5 258.27 17.40 1 -5 -5 281.67 19.10 -1 5 4 767.52 47.20 1 5 -4 718.13 46.60 1 5 -4 811.82 48.40 1 5 -4 754.62 47.50 -1 -5 4 758.52 46.80 1 -5 -4 825.92 48.50 -1 -5 4 692.53 47.50 -1 -5 4 812.92 47.00 1 5 -3 1398.86 85.59 -1 5 3 1360.16 84.79 1 5 -3 1358.66 84.99 -1 -5 3 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132.09 11.40 4 -6 6 124.19 9.20 4 6 7 4.30 2.10 -4 6 -7 5.80 3.90 4 -6 7 15.30 2.70 4 6 8 7.50 2.40 -4 6 -8 8.80 4.70 4 -6 8 7.40 2.40 4 6 9 147.09 10.80 4 -6 9 154.68 10.80 4 6 10 10.00 2.90 4 -6 10 11.00 2.60 4 6 11 131.89 9.90 4 -6 11 128.49 9.40 4 7 -13 116.49 9.30 4 7 -12 4.10 2.70 4 -7 -12 -3.70 8.00 -4 -7 12 2.60 2.50 4 7 -11 -0.20 2.50 -4 7 11 0.60 0.50 -4 7 11 1.80 1.70 -4 -7 11 2.00 2.40 4 -7 -11 6.90 6.70 4 7 -10 15.00 3.10 -4 7 10 15.30 1.30 -4 7 10 17.80 2.50 -4 -7 10 18.60 3.00 4 -7 -10 23.80 7.30 4 7 -9 190.08 18.30 -4 7 9 206.38 12.40 -4 7 9 196.08 13.00 -4 -7 9 210.78 13.40 4 -7 -9 198.38 17.50 -4 7 8 35.00 2.30 -4 7 8 34.50 3.20 4 7 -8 45.80 8.00 4 -7 -8 28.60 6.80 -4 7 7 208.08 12.80 4 7 -7 234.98 17.90 -4 7 7 207.58 13.30 -4 -7 7 198.48 13.50 4 -7 -7 202.88 16.90 -4 7 6 119.29 7.20 4 7 -6 113.89 12.00 4 -7 -6 110.69 11.50 -4 7 5 7.80 0.70 4 7 -5 8.30 3.80 4 -7 -5 8.20 4.60 4 7 -4 124.79 11.00 -4 7 4 127.79 7.40 4 7 -4 114.49 7.40 4 -7 -4 105.49 10.20 4 7 -3 173.58 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47.20 -4 7 -4 682.13 44.40 4 7 4 742.13 45.10 4 7 4 744.03 44.50 4 -7 4 722.83 45.50 4 -7 4 716.43 45.60 4 7 5 382.56 22.60 -4 7 -5 388.56 25.90 4 7 5 385.46 23.40 -4 7 -5 341.57 22.50 4 -7 5 357.16 23.70 -4 7 -6 2966.10 185.58 4 7 6 3028.90 183.08 4 -7 6 3000.20 183.38 -4 7 -7 244.58 20.40 4 7 7 265.67 17.10 4 -7 7 271.17 17.30 4 7 8 636.14 40.00 4 -7 8 641.34 40.10 4 7 9 20.90 3.40 4 -7 9 19.80 3.00 4 7 10 70.29 6.30 4 -7 10 72.09 6.10 4 7 11 14.00 4.80 4 -7 11 21.60 4.30 4 8 -12 6.20 2.80 4 8 -11 -2.50 2.60 -4 8 11 -0.20 0.50 -4 8 11 2.60 1.80 4 -8 -11 0.80 7.50 -4 8 10 23.80 1.70 4 8 -10 22.00 3.60 -4 8 10 21.80 3.00 4 -8 -10 29.70 8.00 -4 8 9 103.09 6.50 4 8 -9 121.29 8.50 -4 8 9 102.19 7.30 4 -8 -9 90.49 12.40 4 8 -8 11.90 5.30 -4 8 8 16.70 2.20 -4 8 8 20.60 1.40 4 -8 -8 24.60 6.90 -4 8 7 47.40 3.70 -4 8 7 42.90 2.80 4 8 -7 32.60 7.30 4 -8 -7 42.40 7.30 4 8 -6 2022.40 131.79 4 -8 -6 2180.48 130.79 4 8 -5 113.99 12.20 -4 8 5 123.29 7.60 4 -8 -5 129.69 11.60 4 8 -4 3792.92 226.88 4 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1706.23 102.19 -8 5 -5 1750.12 103.99 8 -5 5 1629.64 102.69 8 5 6 4.60 2.30 -8 5 -6 4.00 4.00 8 -5 6 7.90 2.80 8 5 7 33.20 4.40 8 -5 7 26.40 3.80 8 5 8 11.10 3.30 8 -5 8 7.60 2.50 8 5 9 30.40 4.50 8 -5 9 27.90 3.70 8 5 10 52.09 6.00 8 -5 10 40.40 4.70 8 6 -13 27.00 4.70 8 -6 -13 21.00 7.30 8 6 -12 16.00 3.90 8 -6 -12 11.60 6.70 8 6 -11 54.89 6.30 8 -6 -11 51.59 9.60 8 6 -10 3.20 3.00 8 -6 -10 3.00 5.90 8 6 -9 454.75 40.70 8 6 -9 635.54 35.80 -8 6 9 569.24 34.10 8 -6 -9 579.14 39.20 8 -6 -9 546.35 36.20 8 6 -8 5.40 5.00 8 6 -8 0.00 2.60 -8 6 8 -0.20 1.30 8 -6 -8 10.90 4.30 8 -6 -8 3.10 5.90 -8 6 7 1701.93 103.09 8 6 -7 1701.13 108.09 8 6 -7 1744.53 104.29 8 -6 -7 1533.05 104.69 8 -6 -7 1806.12 107.29 -8 6 6 3.30 1.30 8 6 -6 4.30 4.40 -8 6 6 4.70 0.50 8 -6 -6 5.60 5.10 -8 -6 6 0.00 1.30 8 -6 -6 8.10 3.90 8 6 -5 235.58 14.60 -8 6 5 224.18 13.40 8 6 -5 216.88 18.20 -8 6 5 201.08 14.00 8 -6 -5 205.98 15.40 8 -6 -5 226.38 17.30 8 6 -4 1.00 3.70 8 6 -4 -0.10 2.10 -8 6 4 0.90 0.30 -8 6 4 0.60 1.10 8 -6 -4 -3.60 3.90 8 -6 -4 4.50 3.20 8 6 -3 363.56 25.10 8 6 -3 321.67 20.70 8 6 -3 330.97 21.40 -8 6 3 350.06 20.40 8 -6 -3 356.86 22.00 8 -6 -3 336.97 23.30 8 -6 -3 266.97 23.20 -8 6 2 2.20 0.40 -8 6 2 4.60 1.80 8 6 -2 3.70 1.10 8 6 -2 3.90 4.70 8 -6 -2 1.00 2.50 8 -6 -2 5.70 3.50 8 -6 -2 5.50 4.10 -8 6 1 73.29 4.30 -8 6 1 62.59 5.20 8 6 -1 73.09 10.70 8 6 -1 67.69 4.90 8 -6 -1 68.29 6.30 8 -6 -1 69.89 7.10 8 -6 -1 59.49 8.00 -8 6 0 2.80 1.20 8 6 0 7.30 1.50 -8 6 0 3.80 0.50 8 -6 0 1.60 2.50 8 -6 0 1.80 3.30 -8 6 -1 82.89 5.00 8 6 1 80.49 5.80 -8 6 -1 73.39 5.90 8 -6 1 87.19 7.30 8 6 2 45.50 4.10 8 -6 2 45.30 5.00 8 -6 2 56.19 6.20 -8 6 -3 2.30 0.40 -8 6 -3 -0.60 3.10 8 6 3 0.20 1.50 8 -6 3 2.30 2.30 8 -6 3 3.80 2.90 -8 6 -4 107.89 6.80 -8 6 -4 111.49 10.50 8 6 4 118.59 8.20 8 -6 4 97.49 8.90 8 -6 4 112.79 8.30 8 6 5 1.00 2.00 -8 6 -5 0.00 0.30 -8 6 -5 1.80 4.60 8 -6 5 -0.30 2.30 8 6 6 46.90 5.10 8 -6 6 44.70 5.20 8 6 7 292.07 19.30 8 -6 7 286.97 19.20 8 6 8 14.40 3.40 8 -6 8 10.00 2.80 8 6 9 25.70 4.00 8 -6 9 26.20 3.40 8 7 -12 94.69 8.60 8 -7 -12 102.19 12.70 8 7 -11 112.19 9.50 8 -7 -11 121.19 14.00 -8 7 10 2.20 0.50 8 7 -10 2.20 3.00 8 -7 -10 2.40 6.00 8 7 -9 235.38 16.20 -8 7 9 241.28 14.50 8 -7 -9 222.88 19.90 8 7 -8 1251.37 81.29 -8 7 8 1390.66 75.29 8 -7 -8 1080.39 76.69 8 -7 -8 1207.88 79.59 8 7 -7 1603.34 105.79 8 7 -7 1621.64 101.59 -8 7 7 1801.22 100.49 8 -7 -7 1629.04 101.69 8 -7 -7 1584.14 104.29 -8 7 6 940.61 55.59 8 7 -6 837.82 60.39 8 7 -6 915.41 56.69 8 -7 -6 965.90 56.99 8 -7 -6 893.11 59.29 8 7 -5 69.79 8.10 8 7 -5 71.59 10.80 -8 7 5 64.69 4.20 8 -7 -5 76.89 9.00 8 7 -4 457.75 32.80 -8 7 4 482.25 28.00 8 7 -4 467.35 29.00 8 7 -4 421.16 28.30 8 -7 -4 524.45 31.70 8 -7 -4 404.26 31.20 8 7 -3 1053.69 66.69 -8 7 3 1113.29 66.29 8 7 -3 1100.79 71.09 8 -7 -3 1093.19 69.09 8 7 -2 769.52 49.20 8 7 -2 795.82 53.69 -8 7 2 817.42 48.80 8 -7 -2 824.92 51.39 8 7 -1 196.98 12.80 8 7 -1 193.88 18.60 -8 7 1 194.88 12.30 8 -7 -1 214.08 15.40 8 -7 -1 209.88 14.80 -8 7 0 34.50 2.30 8 7 0 44.30 3.90 8 -7 0 25.60 4.90 8 -7 0 29.80 4.60 -8 7 -1 287.37 17.60 8 7 1 289.17 18.30 8 -7 1 285.07 19.50 8 -7 1 288.87 19.90 -8 7 -2 312.47 19.50 8 7 2 321.27 20.30 -8 7 -2 329.57 22.40 8 -7 2 316.17 21.60 8 -7 2 319.27 21.30 8 7 3 390.66 24.40 -8 7 -3 365.96 23.40 -8 7 -3 367.66 26.40 8 -7 3 398.26 25.40 8 -7 3 402.86 25.10 8 7 4 30.10 3.70 -8 7 -4 20.20 1.50 8 -7 4 27.80 3.70 8 -7 4 18.60 3.70 8 7 5 65.69 5.80 -8 7 -5 61.79 3.90 8 -7 5 62.49 6.10 8 7 6 5.60 2.30 8 -7 6 5.90 2.60 8 7 7 3.90 2.30 8 -7 7 5.30 2.30 8 7 8 102.89 8.30 8 -7 8 98.09 7.80 8 -8 -12 226.48 18.70 8 8 -11 6.70 3.50 -8 8 11 3.00 0.70 8 -8 -11 6.80 6.00 -8 8 10 43.00 2.80 8 8 -10 45.60 5.70 8 -8 -10 56.09 9.10 8 8 -9 6.60 3.10 -8 8 9 10.70 0.90 8 -8 -9 4.10 5.50 -8 8 8 70.09 4.50 -8 8 8 71.59 5.10 8 8 -8 68.09 6.90 8 -8 -8 90.59 10.50 8 8 -7 20.80 3.80 -8 8 7 22.40 1.60 8 8 -7 15.80 7.80 8 -8 -7 27.00 6.50 8 8 -6 201.68 26.80 -8 8 6 173.88 10.80 8 8 -6 171.48 12.30 8 -8 -6 173.18 15.20 8 8 -5 14.50 3.30 8 8 -5 8.30 6.20 -8 8 5 14.70 1.10 8 -8 -5 13.10 5.90 8 -8 -5 18.20 5.40 8 8 -4 26.10 7.20 -8 8 4 40.90 2.50 8 8 -4 35.90 3.30 8 -8 -4 39.90 6.40 8 -8 -4 29.60 6.60 -8 8 3 5.60 3.20 -8 8 3 7.50 0.70 8 8 -3 12.20 2.70 8 8 -3 9.50 6.60 8 -8 -3 10.20 4.50 8 -8 -3 9.70 4.90 8 8 -2 794.62 49.10 8 8 -2 761.52 54.09 -8 8 2 859.81 48.60 -8 8 2 741.93 50.39 8 -8 -2 761.12 51.19 8 -8 -2 863.11 51.29 -8 8 1 7.50 3.60 8 8 -1 7.50 1.60 -8 8 1 4.50 0.60 8 -8 -1 7.70 3.90 8 -8 -1 5.60 3.20 8 8 0 105.39 7.30 -8 8 0 106.39 6.40 -8 8 0 95.39 9.50 8 -8 0 109.89 9.10 8 -8 0 99.49 9.30 -8 8 -1 -0.50 3.50 -8 8 -1 0.20 0.40 8 8 1 2.00 1.40 8 -8 1 -0.80 2.40 8 8 2 106.09 7.70 -8 8 -2 104.89 6.60 8 -8 2 108.79 8.90 8 -8 2 106.49 8.50 -8 8 -3 42.90 2.70 -8 8 -3 35.30 6.00 8 8 3 45.50 4.30 8 -8 3 41.90 4.80 8 -8 3 45.40 5.30 8 8 4 29.20 3.90 -8 8 -4 32.10 2.10 8 -8 4 29.30 4.20 8 8 5 144.89 10.20 8 -8 5 138.99 10.50 8 8 6 7.80 2.70 8 -8 6 -1.80 2.20 8 8 7 2.50 2.50 8 -8 7 3.30 2.00 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52.69 5.90 10 4 0 109.29 7.40 -10 4 0 97.49 7.20 -10 4 0 107.59 6.40 10 -4 0 97.59 8.50 10 -4 0 101.09 10.40 10 -4 0 99.79 8.40 -10 -4 0 102.89 7.50 -10 4 -1 9.80 0.80 10 4 1 5.70 1.90 -10 4 -1 5.50 1.40 10 -4 1 6.40 2.70 10 -4 1 7.80 3.70 10 -4 1 9.10 2.70 -10 -4 -1 11.20 2.30 10 4 2 1514.75 94.49 -10 4 -2 1495.25 93.49 10 -4 2 1650.93 94.89 10 -4 2 1490.65 95.59 10 4 3 7.30 2.40 -10 4 -3 10.60 0.80 10 -4 3 9.80 3.40 10 -4 3 7.60 2.30 -10 4 -4 2458.85 150.98 10 4 4 2500.45 152.28 10 -4 4 2491.65 152.78 -10 4 -5 0.00 3.50 10 4 5 1.00 2.70 -10 4 -5 0.70 0.40 10 -4 5 0.70 2.60 10 4 6 1035.50 64.09 -10 4 -6 1021.60 62.39 10 -4 6 1018.90 63.89 10 4 7 57.89 6.80 10 -4 7 67.69 6.00 10 4 8 0.90 3.30 10 -4 8 0.50 1.90 10 4 9 7.80 3.70 10 -4 9 8.40 2.30 10 5 -13 27.00 5.00 10 5 -13 32.30 6.90 10 -5 -13 39.30 9.00 10 5 -12 34.20 6.70 10 5 -12 45.20 6.00 10 -5 -12 38.10 9.20 10 5 -11 124.29 10.50 10 -5 -11 135.19 12.80 10 -5 -11 129.29 14.90 10 5 -10 155.08 11.60 -10 5 10 146.89 8.90 10 -5 -10 128.89 15.10 10 -5 -10 137.29 13.30 10 5 -9 380.46 24.00 10 5 -9 342.27 29.70 -10 5 9 369.16 21.90 10 -5 -9 352.86 27.30 10 -5 -9 336.67 24.90 10 5 -8 423.96 26.00 -10 5 8 415.16 24.10 10 5 -8 379.76 31.00 10 -5 -8 340.77 26.80 10 -5 -8 400.96 29.10 10 5 -7 137.49 11.20 10 5 -7 118.89 15.40 -10 5 7 140.59 8.40 10 5 -7 135.09 10.60 10 -5 -7 131.99 12.10 10 -5 -7 149.79 13.80 10 5 -6 192.98 13.30 10 5 -6 166.18 17.60 -10 5 6 194.38 11.30 -10 -5 6 169.48 11.80 10 -5 -6 196.88 14.50 10 -5 -6 188.18 15.90 -10 5 5 360.76 25.30 -10 5 5 403.76 24.60 10 5 -5 406.86 26.30 10 5 -5 352.56 30.30 10 -5 -5 428.76 27.10 10 -5 -5 431.16 28.60 -10 -5 5 448.36 25.60 -10 5 4 393.66 27.10 10 5 -4 446.76 28.00 10 5 -4 410.36 32.40 -10 5 4 462.45 26.40 10 -5 -4 453.45 29.80 -10 5 3 489.45 32.40 -10 5 3 539.45 31.80 10 5 -3 543.25 38.30 10 5 -3 508.95 33.30 10 -5 -3 476.25 35.80 -10 -5 3 514.45 32.60 10 -5 -3 588.04 35.10 10 5 -2 64.39 5.10 10 5 -2 72.09 7.50 10 -5 -2 58.19 8.60 10 -5 -2 84.39 11.30 -10 -5 2 68.29 5.60 10 -5 -2 74.29 7.00 10 5 -1 284.77 18.10 -10 5 1 296.17 17.40 -10 5 1 286.17 19.20 10 -5 -1 296.77 21.00 10 -5 -1 295.97 19.80 10 -5 -1 240.18 18.90 -10 -5 1 290.27 18.50 10 5 0 713.43 46.20 -10 5 0 733.33 45.50 10 -5 0 759.12 46.90 10 -5 0 736.03 47.30 10 -5 0 809.02 48.50 10 5 1 1933.11 121.79 -10 5 -1 1904.81 120.99 10 -5 1 1947.31 122.49 10 -5 1 2190.28 123.59 -10 5 -2 592.34 36.50 10 5 2 610.64 37.50 10 -5 2 563.64 37.90 10 -5 2 632.94 38.90 10 5 3 276.37 18.30 -10 5 -3 263.07 17.00 10 -5 3 281.77 18.40 10 -5 3 301.07 19.50 10 5 4 109.09 8.40 -10 5 -4 102.19 6.60 10 -5 4 117.59 9.20 -10 5 -5 315.77 19.60 10 5 5 316.97 21.30 10 -5 5 336.27 21.70 10 5 6 421.26 27.70 10 -5 6 428.46 27.60 10 5 7 72.79 7.10 10 -5 7 66.49 6.20 10 5 8 14.30 3.50 10 -5 8 21.10 3.10 10 6 -13 209.38 16.30 10 6 -13 244.68 18.10 10 6 -12 43.50 7.40 10 6 -12 37.90 5.30 10 -6 -12 30.90 8.40 10 6 -11 30.80 5.00 10 -6 -11 29.70 8.40 10 6 -10 68.79 7.40 10 -6 -10 56.89 9.80 10 6 -9 2467.65 150.48 -10 6 9 2498.45 148.89 10 -6 -9 2548.74 153.68 10 -6 -9 2280.47 150.68 10 6 -8 5.60 7.70 10 6 -8 9.30 3.70 -10 6 8 11.70 1.00 10 -6 -8 12.70 6.70 10 -6 -8 2.60 4.60 10 6 -7 2260.77 152.38 10 6 -7 2527.65 147.69 10 -6 -7 2476.15 148.09 10 -6 -7 2338.67 150.18 10 6 -6 12.40 7.20 -10 6 6 5.40 0.60 10 6 -6 7.90 3.20 10 -6 -6 4.70 4.00 10 -6 -6 10.10 5.70 10 6 -5 84.19 13.40 -10 6 5 87.59 5.20 10 6 -5 81.39 7.70 10 -6 -5 80.49 8.50 10 -6 -5 69.39 9.90 -10 6 4 58.09 3.50 10 6 -4 47.50 9.50 10 6 -4 49.00 6.20 10 -6 -4 49.99 8.40 10 -6 -4 62.09 8.50 10 -6 -4 57.79 6.80 10 6 -3 843.42 51.69 -10 6 3 867.31 50.29 10 6 -3 803.72 56.69 10 -6 -3 850.91 53.29 10 -6 -3 745.43 53.59 -10 6 2 33.20 2.20 10 6 -2 34.30 3.40 10 -6 -2 30.90 4.40 10 -6 -2 36.60 5.70 10 -6 -2 27.90 6.20 -10 6 1 169.38 10.30 10 6 -1 160.28 11.10 10 -6 -1 167.88 14.00 10 -6 -1 176.78 12.90 -10 6 0 205.68 12.40 10 6 0 196.38 13.20 10 -6 0 188.28 15.50 10 -6 0 214.18 14.70 10 6 1 804.02 51.19 -10 6 -1 825.42 50.39 10 -6 1 858.21 52.89 10 -6 1 828.22 52.09 -10 6 -2 110.19 6.80 10 6 2 110.29 8.20 10 -6 2 111.59 8.70 10 -6 2 109.59 9.60 10 6 3 4.20 2.40 -10 6 -3 5.00 3.70 -10 6 -3 5.80 0.60 10 -6 3 1.60 3.10 10 -6 3 3.90 2.30 10 6 4 64.19 5.90 -10 6 -4 62.59 3.90 10 -6 4 60.39 6.40 10 6 5 3.40 2.50 10 -6 5 -0.90 2.40 10 6 6 21.90 3.70 10 -6 6 25.10 3.80 10 6 7 217.38 15.20 10 -6 7 215.28 14.70 10 6 8 22.40 4.40 10 -6 8 21.90 4.20 10 7 -12 80.09 9.70 10 7 -12 75.89 7.90 10 -7 -12 69.09 10.80 10 7 -11 140.19 10.80 -10 7 11 123.29 7.90 10 -7 -11 133.49 14.10 10 7 -10 219.18 15.00 -10 7 10 202.58 12.50 10 -7 -10 183.18 18.20 -10 7 9 93.89 5.90 10 7 -9 93.89 8.80 10 -7 -9 99.19 11.10 10 -7 -9 96.39 12.10 -10 7 8 55.39 3.60 10 7 -8 57.59 6.70 10 -7 -8 60.39 6.60 10 -7 -8 72.69 10.20 10 7 -7 17.50 9.00 10 7 -7 8.70 3.80 -10 7 7 13.10 1.10 10 -7 -7 4.50 5.40 10 -7 -7 17.50 4.40 -10 7 6 179.48 10.90 10 7 -6 172.28 13.00 10 -7 -6 168.28 15.30 10 -7 -6 185.08 13.30 -10 7 5 106.99 6.70 10 7 -5 117.19 9.30 10 7 -5 94.39 14.60 10 -7 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1.70 0.50 10 8 4 2.00 2.30 10 -8 4 0.70 2.40 10 8 5 5.90 2.70 10 -8 5 9.20 2.50 10 8 6 4.50 2.80 10 -8 6 3.80 3.30 10 9 -10 23.30 4.70 -10 9 10 26.10 1.80 10 -9 -10 30.90 14.70 10 -9 -10 28.00 6.20 -10 9 9 246.38 14.30 10 9 -9 223.18 16.50 10 -9 -9 245.88 26.70 10 -9 -9 211.58 18.20 10 9 -8 183.08 14.20 -10 9 8 197.58 11.80 10 -9 -8 213.58 16.30 10 -9 -8 156.58 17.70 10 9 -7 330.57 22.60 -10 9 7 320.17 21.00 -10 9 7 330.47 20.60 10 -9 -7 378.16 24.60 10 -9 -7 345.27 25.50 10 -9 -6 16.90 5.30 10 -9 -6 15.20 6.70 -10 9 5 35.40 2.50 10 -9 -5 49.30 7.80 10 -9 -5 47.20 6.90 -10 9 4 108.79 7.10 10 -9 -4 126.99 10.60 10 -9 -4 122.49 11.60 -10 9 3 181.38 11.30 10 -9 -3 196.48 14.40 10 -9 -3 171.58 17.10 -10 9 2 147.99 8.90 10 -9 -2 135.29 12.30 10 -9 -2 144.49 11.80 -10 9 1 12.50 1.10 10 9 -1 17.30 3.00 10 -9 -1 12.70 3.80 10 -9 -1 15.80 4.40 -10 9 0 3.20 0.50 10 9 0 3.40 1.90 10 -9 0 0.40 3.10 10 -9 0 2.40 2.60 10 9 1 21.10 2.90 -10 9 -1 18.00 1.40 10 -9 1 19.50 3.50 10 -9 1 21.60 4.00 10 9 2 120.29 9.10 -10 9 -2 126.79 7.70 10 -9 2 126.99 9.60 10 -9 2 128.69 9.80 10 9 3 30.50 4.30 -10 9 -3 34.20 2.20 10 -9 3 38.30 4.40 10 9 4 70.59 6.20 10 -9 4 71.79 6.40 10 9 5 6.40 2.40 10 -9 5 14.10 2.80 -10 10 8 4.40 0.90 10 -10 -8 6.90 5.80 -10 10 7 21.60 3.00 -10 10 7 19.20 1.40 10 -10 -7 12.90 4.90 -10 10 6 1.00 0.40 10 -10 -6 1.30 3.70 -10 10 5 4.80 0.60 10 -10 -5 2.90 3.70 10 -10 -5 -0.50 5.90 -10 10 4 12.50 1.00 10 -10 -4 15.10 5.10 10 -10 -4 12.20 4.00 -10 10 3 97.99 6.10 10 -10 -3 89.99 9.90 10 -10 -3 105.49 9.10 -10 10 2 12.30 1.10 10 -10 -2 7.60 4.10 10 -10 -2 14.20 3.60 -10 10 1 114.89 7.00 10 10 -1 103.89 8.20 10 -10 -1 117.59 9.70 10 -10 -1 121.29 9.30 -10 10 0 0.30 0.40 10 10 0 2.10 1.90 10 -10 0 2.10 2.50 10 -10 0 2.90 3.50 -10 10 -1 207.18 12.40 10 10 1 189.38 13.50 10 -10 1 215.28 14.20 10 -10 1 199.48 14.20 -10 10 -2 2.70 0.60 10 10 2 0.30 2.10 10 -10 2 0.80 3.60 -10 10 -3 1099.69 65.49 10 10 3 1056.09 66.59 10 -10 3 1072.59 66.59 -10 11 5 121.39 7.90 10 -11 -5 148.59 12.30 -10 11 4 98.69 6.30 10 -11 -4 110.19 9.00 -10 11 3 99.39 6.20 10 -11 -3 100.19 8.60 -10 11 2 42.10 2.70 10 -11 -2 39.50 5.20 -10 11 1 3.20 0.50 10 -11 -1 1.80 2.30 -10 11 0 34.50 2.30 10 11 0 33.10 4.40 10 -11 0 41.10 5.60 11 0 -14 20.50 5.90 11 0 -14 19.90 7.30 11 0 -13 -0.50 5.90 11 0 -13 1.70 4.90 11 0 -12 33.30 9.80 11 0 -12 25.50 11.70 11 0 -11 0.80 4.50 11 0 -11 -1.10 5.00 11 0 -10 178.98 15.40 11 0 -10 168.18 14.00 11 0 -9 4.10 5.10 11 0 -9 1.40 4.20 11 0 -8 75.89 9.10 11 0 -8 50.79 6.80 -11 0 8 61.19 3.80 -11 0 7 0.20 1.00 11 0 -7 1.90 4.30 11 0 -7 -1.40 3.40 -11 0 7 0.10 0.20 11 0 -6 32.40 5.20 -11 0 6 34.30 2.90 11 0 -6 24.80 5.60 -11 0 5 1.00 1.00 11 0 -5 1.60 3.70 11 0 -5 -0.20 3.70 -11 0 4 142.99 9.20 11 0 -4 130.89 11.40 11 0 -4 147.59 11.60 -11 0 3 1.20 0.90 11 0 -3 -2.70 2.80 11 0 -3 -0.90 3.40 11 0 -2 39.20 5.60 11 0 -2 42.00 6.50 -11 0 2 45.40 3.60 11 0 -2 38.70 5.50 11 0 -2 49.90 6.10 11 0 -1 4.50 3.70 11 0 -1 -2.80 2.80 -11 0 1 0.10 1.00 11 0 -1 0.10 3.10 11 0 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134.39 18.00 11 1 8 26.90 3.40 11 1 8 38.20 7.40 11 -1 8 36.80 4.10 11 -1 8 30.40 16.60 11 1 9 -1.50 9.70 11 1 9 1.00 2.20 11 -1 9 -1.60 3.00 11 -1 9 5.20 15.80 11 2 -14 415.86 29.60 11 -2 -14 470.95 33.00 11 2 -13 12.00 6.50 11 2 -13 7.50 4.80 11 -2 -13 7.80 7.10 11 -2 -13 14.40 5.90 11 2 -12 5.90 5.30 11 2 -12 4.80 4.50 11 -2 -12 7.70 6.60 11 -2 -12 1.70 5.30 11 2 -11 7.40 5.20 11 2 -11 2.60 4.30 11 -2 -11 2.40 5.30 11 -2 -11 4.20 6.20 11 2 -10 52.19 14.10 11 2 -10 59.09 7.10 11 2 -10 40.00 7.30 11 -2 -10 76.09 10.40 11 -2 -10 60.29 7.80 11 2 -9 7.60 4.20 11 2 -9 4.10 8.20 -11 2 9 2.90 0.40 11 2 -9 1.70 4.20 11 -2 -9 7.90 4.80 11 -2 -9 7.90 6.00 11 2 -8 305.07 25.40 -11 2 8 279.57 16.60 11 2 -8 263.97 19.90 -11 2 8 247.08 17.20 11 2 -8 276.07 19.00 11 -2 -8 264.17 19.70 11 -2 -8 296.87 21.50 11 2 -7 1.10 3.70 -11 2 7 2.10 0.40 -11 2 7 0.20 1.20 11 2 -7 3.80 6.50 11 2 -7 2.10 3.40 -11 -2 7 -0.50 1.00 11 -2 -7 3.60 4.60 11 -2 -7 -3.00 4.00 11 2 -6 635.34 39.70 -11 2 6 646.44 37.70 11 2 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622.64 43.50 11 4 -4 54.59 6.80 -11 4 4 65.69 3.70 -11 4 4 55.79 4.70 11 -4 -4 52.59 6.80 11 -4 -4 46.20 7.10 -11 -4 4 55.29 4.50 11 4 -3 20.60 4.40 -11 4 3 20.90 2.80 -11 4 3 24.00 1.50 11 -4 -3 25.50 6.10 11 -4 -3 20.50 4.80 -11 -4 3 19.50 2.50 11 4 -2 44.70 4.40 -11 4 2 52.99 4.70 11 4 -2 43.90 5.60 -11 4 2 51.99 3.10 -11 -4 2 46.70 4.40 11 -4 -2 48.20 5.90 11 -4 -2 44.40 7.70 -11 4 1 22.10 1.50 11 4 -1 25.20 3.30 11 4 -1 26.30 4.20 11 -4 -1 21.30 4.10 11 -4 -1 29.50 6.80 11 -4 -1 22.50 5.50 -11 4 0 134.19 8.10 11 4 0 123.29 9.30 11 -4 0 148.89 10.40 11 -4 0 134.89 11.80 11 -4 0 127.39 10.20 11 4 1 1303.07 85.69 -11 4 -1 1395.46 84.69 11 -4 1 1548.95 87.49 11 -4 1 1341.07 86.09 11 4 2 426.16 29.30 -11 4 -2 470.05 28.10 11 -4 2 465.05 30.60 11 -4 2 483.35 29.50 11 4 3 1202.18 76.69 -11 4 -3 1221.48 75.39 11 -4 3 1218.38 76.49 11 -4 3 1324.57 77.59 11 4 4 164.58 12.80 -11 4 -4 188.28 11.10 11 -4 4 186.08 13.30 -11 4 -5 28.70 1.80 11 4 5 18.80 3.60 11 -4 5 24.50 3.90 11 4 6 2.80 3.20 11 -4 6 3.80 2.40 11 4 7 163.68 13.10 11 -4 7 185.58 12.50 11 4 8 12.70 4.20 11 -4 8 16.40 2.80 11 5 -13 -1.10 4.20 11 -5 -13 -0.30 6.50 11 5 -12 -3.10 3.90 11 5 -12 -0.50 5.20 11 -5 -12 -3.20 6.70 11 -5 -12 2.10 6.60 11 5 -11 123.89 12.60 11 5 -11 140.59 11.20 11 -5 -11 113.49 12.70 11 -5 -11 131.19 14.70 11 5 -10 28.00 8.20 -11 5 10 23.80 1.60 11 5 -10 26.20 6.30 11 -5 -10 25.40 6.50 11 5 -9 635.24 49.50 11 5 -9 545.85 34.50 11 5 -9 508.25 35.20 -11 5 9 525.95 32.30 11 -5 -9 474.85 35.10 11 -5 -9 544.65 37.70 -11 5 8 203.88 11.80 11 5 -8 206.38 14.50 11 5 -8 152.38 25.60 11 -5 -8 160.58 15.20 11 -5 -8 192.78 17.40 -11 5 7 113.59 7.00 11 5 -7 106.19 9.90 11 5 -7 98.39 16.10 11 -5 -7 120.59 11.20 11 -5 -7 124.19 12.90 -11 5 6 0.30 0.40 11 5 -6 -1.90 3.40 11 5 -6 3.80 5.80 11 -5 -6 -4.50 4.10 11 -5 -6 -2.00 4.50 11 5 -5 385.16 26.10 -11 5 5 415.96 24.10 11 5 -5 389.46 31.80 11 -5 -5 407.26 26.80 11 -5 -5 367.56 27.90 11 5 -4 345.67 26.30 -11 5 4 396.66 22.90 11 5 -4 343.87 30.60 11 -5 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6 10 208.58 13.60 11 6 -10 219.18 17.60 11 6 -10 232.58 16.30 11 -6 -10 241.38 16.90 11 -6 -10 230.48 19.70 -11 6 9 0.00 0.40 11 6 -9 1.30 5.10 11 6 -9 -1.20 4.90 11 -6 -9 2.90 5.20 -11 6 8 1401.86 87.99 11 6 -8 1448.56 89.89 11 -6 -8 1513.45 92.79 11 -6 -8 1434.96 90.19 11 6 -7 0.50 3.40 -11 6 7 1.40 0.50 11 6 -7 5.80 8.90 11 -6 -7 3.70 4.30 11 -6 -7 3.40 5.80 -11 6 6 302.17 18.60 11 6 -6 295.27 20.70 11 6 -6 276.07 26.90 11 -6 -6 346.07 21.50 11 -6 -6 301.47 22.90 -11 6 5 24.90 1.60 11 6 -5 17.80 4.40 11 6 -5 15.40 7.90 11 -6 -5 23.70 4.90 11 -6 -5 17.40 5.60 11 6 -4 316.47 21.70 -11 6 4 334.97 19.60 11 6 -4 280.97 28.10 11 -6 -4 299.47 24.00 11 -6 -4 346.87 23.50 11 -6 -4 327.67 21.90 -11 6 3 23.30 1.60 11 -6 -3 21.10 5.00 11 -6 -3 19.40 4.30 11 -6 -3 27.60 6.70 11 6 -2 0.40 1.70 11 -6 -2 6.90 3.60 11 -6 -2 -0.20 3.10 11 -6 -2 1.80 4.50 11 6 -1 3.90 1.90 -11 6 1 4.60 0.60 11 -6 -1 -1.00 2.80 11 -6 -1 2.70 4.30 11 -6 -1 4.00 3.00 -11 6 0 651.13 38.20 11 6 0 598.34 39.10 11 -6 0 689.13 41.40 11 -6 0 581.14 40.10 11 6 1 0.40 1.90 11 -6 1 0.90 2.50 11 -6 1 19.30 4.30 11 6 2 80.19 6.70 -11 6 -2 80.99 5.00 11 -6 2 91.79 8.40 11 -6 2 75.99 6.90 11 6 3 5.40 2.40 -11 6 -3 5.90 0.60 11 -6 3 6.40 2.50 11 -6 3 5.00 3.00 -11 6 -4 65.89 4.10 11 6 4 66.09 6.30 11 -6 4 62.49 6.70 -11 6 -5 1.60 0.40 11 6 5 0.50 2.50 11 -6 5 0.80 2.40 11 6 6 5.20 3.00 11 -6 6 8.00 2.60 11 6 7 10.60 3.40 11 -6 7 14.30 2.80 -11 7 11 0.30 0.50 11 7 -11 6.90 7.50 11 7 -11 -1.30 3.60 11 -7 -11 -2.90 6.20 11 7 -10 23.80 5.10 -11 7 10 18.10 1.40 11 -7 -10 24.50 7.50 -11 7 9 11.50 1.00 11 7 -9 10.20 4.00 11 -7 -9 10.60 4.40 11 -7 -9 11.00 6.70 11 7 -8 33.90 5.80 -11 7 8 40.80 2.60 11 -7 -8 40.20 8.00 11 -7 -8 48.80 8.40 -11 7 7 2.40 0.50 11 7 -7 2.40 3.70 11 -7 -7 4.80 5.20 11 -7 -7 1.10 3.70 11 7 -6 40.10 5.70 11 7 -6 32.30 13.50 -11 7 6 36.40 2.40 11 -7 -6 39.80 7.40 11 -7 -6 30.20 7.80 11 -7 -6 42.80 5.50 11 7 -5 4.90 4.10 11 7 -5 4.80 8.50 -11 7 5 4.20 0.60 11 -7 -5 8.00 4.80 11 -7 -5 6.20 3.50 11 -7 -5 1.00 5.40 11 7 -4 163.28 24.20 -11 7 4 170.28 10.20 11 -7 -4 159.18 13.80 11 -7 -4 124.59 14.70 11 -7 -4 188.98 12.60 -11 7 3 3.40 0.50 11 -7 -3 2.00 4.90 11 -7 -3 5.40 3.30 11 -7 -3 1.90 3.80 11 7 -2 76.69 6.40 -11 7 2 92.29 5.30 11 -7 -2 84.39 9.70 11 -7 -2 73.89 8.10 -11 7 1 1.20 0.40 11 7 -1 1.50 1.90 11 -7 -1 1.40 3.80 11 -7 -1 11.90 3.50 11 7 0 172.28 12.40 -11 7 0 190.48 11.30 11 -7 0 187.28 14.30 11 -7 0 187.88 13.50 -11 7 -1 13.20 1.00 11 7 1 7.60 2.40 11 -7 1 11.10 3.90 11 -7 1 14.20 3.50 11 7 2 229.18 16.70 -11 7 -2 262.67 15.20 11 7 3 0.40 2.30 -11 7 -3 0.00 0.40 11 -7 3 1.90 2.10 11 -7 3 1.50 2.80 11 7 4 12.30 3.10 -11 7 -4 12.80 1.00 11 -7 4 10.50 3.00 11 7 5 150.08 11.50 11 -7 5 165.48 11.50 11 7 6 12.20 3.20 11 -7 6 14.70 3.00 -11 8 10 5.10 0.70 11 8 -10 3.60 3.90 11 -8 -10 2.70 5.30 -11 8 9 158.58 10.00 11 8 -9 153.88 12.70 11 -8 -9 188.28 15.70 11 8 -8 -2.30 3.70 -11 8 8 0.20 0.40 11 -8 -8 4.40 5.00 11 -8 -8 -1.90 6.60 -11 8 7 116.79 7.10 11 8 -7 114.49 10.20 11 -8 -7 114.59 13.70 11 -8 -7 107.49 12.00 -11 8 6 4.20 0.50 11 8 -6 11.80 6.30 11 -8 -6 6.00 4.50 11 -8 -6 2.90 5.70 -11 8 4 15.50 1.20 11 -8 -4 13.00 4.80 11 -8 -4 13.10 5.30 11 -8 -3 2235.08 142.89 11 -8 -3 2367.26 142.69 -11 8 2 26.40 1.80 11 -8 -2 27.30 4.80 11 -8 -2 19.40 5.00 -11 8 1 92.29 5.50 11 8 -1 81.39 6.80 11 -8 -1 91.99 9.70 -11 8 0 7.70 0.80 11 -8 0 10.20 3.20 11 -8 0 10.90 3.80 11 8 1 612.14 43.00 -11 8 -1 681.03 42.10 11 -8 1 725.03 43.90 11 -8 1 762.02 44.40 -11 8 -2 9.30 0.80 11 8 2 8.80 2.50 11 -8 2 7.70 2.60 11 -8 2 11.40 3.30 11 8 3 260.37 17.90 -11 8 -3 289.77 16.60 11 -8 3 257.47 18.30 11 8 4 -0.50 2.10 11 -8 4 -3.20 2.20 11 8 5 2.00 3.10 11 -8 5 1.70 3.50 11 9 -9 60.89 6.50 -11 9 9 43.80 3.10 11 -9 -9 52.09 9.60 11 -9 -9 43.50 7.10 -11 9 8 23.10 1.60 11 -9 -8 14.60 8.50 11 -9 -8 27.70 6.20 -11 9 7 2.30 1.40 11 9 -7 -8.50 5.20 11 -9 -7 4.10 7.20 11 -9 -7 14.40 4.90 -11 9 6 15.40 1.20 11 -9 -6 18.90 5.30 11 -9 -6 16.90 6.20 -11 9 5 16.00 1.20 11 -9 -5 13.60 5.60 11 -9 -5 15.30 4.70 -11 9 4 -0.40 0.40 11 -9 -4 5.50 4.60 11 -9 -4 1.50 3.50 -11 9 3 213.78 12.90 11 -9 -3 189.08 16.00 11 -9 -3 224.38 15.80 -11 9 2 183.88 11.00 11 -9 -2 173.38 13.50 11 -9 -2 174.48 13.90 -11 9 1 41.50 2.70 11 9 -1 37.50 4.50 11 -9 -1 43.90 5.60 11 -9 -1 39.30 5.60 11 9 0 83.09 7.20 -11 9 0 93.79 5.80 11 -9 0 101.59 8.70 11 -9 0 99.19 8.00 -11 9 -1 135.19 8.20 11 9 1 122.09 9.60 11 -9 1 143.69 10.20 11 -9 1 134.79 10.50 11 9 2 28.90 4.10 -11 9 -2 28.70 1.90 11 -9 2 24.10 3.90 11 -9 2 32.50 4.30 11 9 3 99.79 8.20 -11 9 -3 112.19 6.60 11 -9 3 105.29 8.40 -11 10 7 14.60 1.20 -11 10 6 131.09 7.80 11 -10 -6 106.59 10.90 11 -10 -6 143.09 13.30 -11 10 5 1.10 0.40 11 -10 -5 7.50 8.80 11 -10 -5 0.20 3.60 -11 10 4 52.99 3.50 11 -10 -4 52.89 6.70 11 -10 -4 69.59 7.80 -11 10 3 7.30 0.70 11 -10 -3 5.60 4.60 11 -10 -3 14.70 3.90 -11 10 2 1.80 0.50 11 -10 -2 6.20 3.80 11 -10 -2 2.30 3.10 -11 10 1 1.10 0.40 11 -10 -1 2.60 2.70 11 -10 -1 1.60 3.50 -11 10 0 44.50 2.80 11 10 0 39.20 4.80 11 -10 0 47.10 5.00 -11 10 -1 42.60 2.70 11 10 1 35.90 4.60 11 -10 1 46.50 4.80 11 -10 1 30.10 4.30 12 0 -14 4.10 6.10 12 0 -14 5.30 5.30 12 0 -13 -2.00 5.30 12 0 -13 -3.70 6.10 12 0 -12 69.39 10.40 12 0 -12 89.19 10.50 12 0 -11 3.40 5.70 12 0 -11 -0.30 4.60 12 0 -10 6.90 6.00 12 0 -10 2.60 4.80 12 0 -9 -3.80 4.60 12 0 -9 1.40 4.60 -12 0 8 414.96 23.70 12 0 -8 363.36 26.40 12 0 -8 366.86 27.50 -12 0 7 0.30 0.30 12 0 -7 1.10 4.70 -12 0 7 1.30 1.20 12 0 -7 -0.50 4.00 12 0 -6 123.89 11.80 -12 0 6 120.59 8.30 12 0 -6 134.69 11.30 12 0 -5 -2.30 3.90 12 0 -5 -2.70 3.60 -12 0 5 -1.30 1.30 12 0 -4 282.67 19.50 12 0 -4 265.17 19.50 12 0 -3 -3.30 3.00 -12 0 3 1.50 1.10 12 0 -3 1.60 3.80 12 0 -2 362.96 27.70 12 0 -2 451.65 28.50 12 0 -2 436.86 29.50 12 0 -2 452.15 27.70 -12 0 2 445.36 26.80 -12 0 1 2.10 1.30 12 0 -1 -3.20 3.00 12 0 -1 4.70 3.70 12 0 -1 2.10 3.60 12 0 -1 -1.40 2.20 12 0 0 99.49 9.50 12 0 0 102.79 9.40 12 0 1 -3.50 2.80 12 0 1 1.20 2.50 12 0 1 0.60 3.80 12 0 2 150.28 12.10 12 0 2 141.29 11.10 12 0 3 6.10 4.20 12 0 3 -2.10 2.30 12 0 4 723.93 41.50 12 0 4 581.64 42.30 12 0 5 2.70 6.10 12 0 5 -1.20 2.20 12 0 6 931.51 54.09 12 0 6 794.82 56.59 -12 0 -7 -0.50 0.40 12 0 7 -10.30 10.10 12 0 7 0.00 2.00 12 0 8 115.59 17.90 12 0 8 115.69 10.00 12 1 -14 25.70 5.90 12 1 -14 24.60 7.10 12 -1 -14 25.00 8.10 12 1 -13 106.19 11.60 12 1 -13 130.49 13.60 12 -1 -13 114.09 13.80 12 -1 -13 99.69 12.00 12 1 -12 49.20 8.70 12 1 -12 64.69 8.10 12 -1 -12 55.09 9.40 12 -1 -12 71.69 8.90 12 1 -11 224.48 17.10 12 1 -11 235.58 18.80 12 -1 -11 196.78 18.90 12 -1 -11 217.28 17.60 12 1 -10 2.00 4.50 12 1 -10 -2.00 4.90 12 -1 -10 -0.90 5.00 12 -1 -10 7.10 5.90 12 1 -9 12.50 5.90 12 -1 -9 8.50 5.80 12 -1 -9 11.00 5.50 -12 1 8 133.99 7.50 12 1 -8 115.79 12.00 12 1 -8 125.19 11.10 12 -1 -8 141.19 11.90 12 -1 -8 109.99 12.80 -12 -1 8 109.29 7.50 -12 1 7 203.98 12.70 12 1 -7 196.68 14.90 -12 1 7 190.68 11.80 12 -1 -7 200.98 16.20 -12 -1 7 173.98 12.30 12 -1 -7 194.48 15.10 12 1 -6 465.35 28.80 12 1 -6 410.76 29.10 -12 1 6 428.76 26.10 -12 1 6 388.06 26.90 12 -1 -6 500.35 29.20 12 -1 -6 442.36 30.40 -12 -1 6 394.56 26.60 -12 1 5 1.30 1.40 12 1 -5 7.40 4.50 12 1 -5 4.50 3.90 12 -1 -5 8.50 4.50 12 -1 -5 0.70 3.80 -12 1 4 66.39 5.10 12 1 -4 69.89 7.80 12 1 -4 68.69 7.80 12 -1 -4 65.79 8.00 12 1 -3 31.00 6.30 12 1 -3 31.00 5.40 -12 1 3 33.50 3.30 12 -1 -3 51.49 6.10 12 -1 -3 31.40 6.10 -12 -1 3 30.00 3.20 12 1 -2 17.10 4.10 -12 1 2 21.20 2.70 12 1 -2 22.50 5.00 12 1 -2 20.10 4.80 -12 -1 2 21.10 2.70 12 -1 -2 17.90 5.00 12 -1 -2 22.60 4.10 12 -1 -2 17.30 5.50 12 1 -1 -0.30 2.80 -12 1 1 0.80 1.30 12 1 -1 -3.70 3.20 12 1 -1 -1.30 3.40 -12 -1 1 3.40 1.40 12 -1 -1 5.00 4.10 12 -1 -1 0.60 2.30 12 1 0 40.20 5.60 12 1 0 51.49 5.70 12 1 0 52.79 6.10 12 -1 0 32.80 5.90 12 -1 0 46.30 6.20 12 -1 0 51.69 5.80 12 1 1 11.80 3.70 12 1 1 13.90 3.60 12 1 1 20.70 4.30 12 -1 1 9.30 3.20 12 -1 1 5.40 5.10 12 -1 1 12.40 4.00 12 1 2 17.70 3.40 12 1 2 14.90 3.70 12 -1 2 22.50 4.40 12 -1 2 27.20 7.70 12 1 3 12.10 2.80 12 1 3 9.90 3.60 12 -1 3 7.20 3.00 12 -1 3 8.80 8.10 12 1 4 80.69 8.40 12 1 4 82.09 6.70 12 -1 4 83.99 7.30 12 -1 4 56.39 10.80 12 1 5 1.10 3.40 12 1 5 -0.60 2.00 12 -1 5 3.90 10.70 12 -1 5 -0.20 2.30 12 1 6 159.18 13.90 -12 1 -6 163.48 10.20 12 1 6 170.38 11.50 12 -1 6 173.48 11.90 12 1 7 18.40 2.80 12 1 7 26.20 7.20 12 -1 7 20.60 16.80 12 -1 7 17.50 2.90 12 1 8 12.00 9.20 12 1 8 36.30 4.30 12 -1 8 40.60 5.50 12 -1 8 31.60 18.00 12 2 -14 47.60 7.10 12 2 -14 49.30 11.50 12 -2 -14 29.20 8.50 12 2 -13 33.40 7.60 12 2 -13 25.10 5.90 12 -2 -13 25.30 8.20 12 -2 -13 27.10 7.10 12 2 -12 -3.40 5.60 12 2 -12 -5.30 4.50 12 -2 -12 -1.50 5.50 12 -2 -12 -0.10 6.60 12 2 -11 26.20 6.60 12 -2 -11 37.00 9.50 12 -2 -11 23.60 11.10 12 2 -10 -3.20 10.10 12 2 -10 -4.60 4.90 -12 2 10 0.00 0.30 12 2 -10 3.00 4.50 12 -2 -10 -3.50 5.00 12 -2 -10 -0.20 5.60 -12 2 9 110.79 6.70 12 2 -9 112.39 11.60 12 2 -9 116.69 10.50 12 2 -9 83.29 15.40 12 -2 -9 113.29 11.20 12 -2 -9 106.59 12.90 12 2 -8 3.40 8.50 -12 2 8 2.90 0.40 12 2 -8 0.40 4.70 12 2 -8 2.50 4.20 12 -2 -8 7.60 5.20 12 -2 -8 4.90 5.50 12 2 -7 93.29 10.70 -12 2 7 84.59 6.40 12 2 -7 88.79 8.90 -12 2 7 93.59 5.40 12 -2 -7 74.99 10.70 -12 -2 7 74.39 7.00 12 -2 -7 90.99 10.10 -12 2 6 1.70 0.40 12 2 -6 1.80 4.50 -12 2 6 2.10 1.40 12 2 -6 0.90 4.00 12 -2 -6 2.30 4.60 12 -2 -6 -3.10 4.20 12 2 -5 2197.98 124.89 -12 2 5 1825.72 123.09 -12 -2 5 2071.29 123.39 12 -2 -5 1985.60 124.99 12 2 -4 38.30 5.60 -12 2 4 29.20 1.80 -12 2 4 24.00 3.00 -12 -2 4 26.20 3.10 12 -2 -4 26.60 5.60 12 -2 -4 18.20 5.00 12 2 -3 508.35 33.50 12 2 -3 533.35 33.00 -12 2 3 474.85 31.20 12 -2 -3 514.95 33.10 12 -2 -3 503.65 34.50 12 -2 -3 514.65 33.10 -12 -2 3 479.85 31.20 12 2 -2 125.19 11.00 -12 2 2 127.59 8.90 12 2 -2 149.59 11.60 12 2 -2 119.29 9.80 12 -2 -2 133.89 10.50 12 -2 -2 152.68 11.30 -12 -2 2 123.09 8.80 12 -2 -2 137.09 12.80 12 2 -1 305.77 21.50 12 2 -1 307.67 20.80 12 2 -1 314.77 21.50 12 -2 -1 346.67 21.80 12 -2 -1 314.97 21.10 12 -2 -1 328.97 22.90 12 2 0 33.80 4.70 12 2 0 29.70 4.50 12 2 0 35.90 4.40 12 -2 0 33.90 6.00 12 -2 0 32.00 4.30 12 -2 0 32.30 4.70 12 2 1 60.09 6.30 12 2 1 61.19 6.00 12 2 1 61.19 6.20 12 -2 1 60.59 5.50 12 -2 1 65.29 9.00 12 -2 1 69.49 6.30 12 -2 1 73.19 7.50 12 2 2 20.90 3.10 12 2 2 11.30 3.00 12 -2 2 22.00 8.90 12 -2 2 15.20 4.20 12 2 3 130.09 10.10 12 2 3 122.39 9.00 12 -2 3 129.39 10.20 12 -2 3 101.19 15.20 12 2 4 15.30 3.70 -12 2 -4 21.60 1.50 12 2 4 26.70 3.20 12 -2 4 14.70 13.80 12 -2 4 23.80 4.00 12 2 5 0.90 2.10 -12 2 -5 0.40 0.30 12 2 5 0.10 4.90 12 2 6 2.00 2.10 12 2 6 1.50 3.60 -12 2 -6 0.90 0.40 12 -2 6 1.80 2.30 12 -2 6 4.80 16.50 12 2 7 105.59 8.00 12 -2 7 121.89 8.40 12 -2 7 50.99 17.30 12 2 8 3.60 5.50 12 3 -13 126.29 11.70 12 3 -13 128.19 13.60 12 -3 -13 118.39 13.20 12 -3 -13 136.59 15.30 12 3 -12 16.90 6.50 12 3 -12 18.30 5.10 12 -3 -12 14.60 7.20 12 -3 -12 9.80 6.30 12 3 -11 2.10 5.00 12 3 -11 1.80 4.50 12 -3 -11 7.20 6.60 12 -3 -11 0.90 5.40 12 3 -10 254.37 18.50 12 3 -10 246.68 19.60 12 -3 -10 264.77 21.40 12 -3 -10 248.08 19.40 12 3 -9 87.29 9.30 12 3 -9 88.49 15.40 -12 3 9 86.59 5.40 12 3 -9 84.49 10.20 12 -3 -9 86.39 10.10 12 -3 -9 96.19 12.30 -12 3 8 93.29 5.90 12 3 -8 95.79 9.80 12 3 -8 111.59 17.00 12 3 -8 87.59 10.30 12 -3 -8 92.29 10.80 12 -3 -8 106.19 12.00 -12 3 7 19.50 1.30 12 3 -7 15.60 4.60 12 3 -7 12.80 8.10 12 3 -7 15.40 6.80 12 -3 -7 13.60 5.30 12 -3 -7 15.10 5.90 12 3 -6 695.03 43.50 -12 3 6 733.33 41.30 12 3 -6 595.14 48.70 12 -3 -6 748.73 45.40 12 -3 -6 704.13 44.20 -12 -3 6 594.74 41.80 -12 3 5 44.30 2.90 12 3 -5 46.20 6.30 12 -3 -5 48.40 7.80 12 -3 -5 48.00 7.00 -12 -3 5 45.90 4.00 12 3 -4 727.33 52.99 12 3 -4 899.41 55.39 -12 3 4 883.51 50.69 -12 -3 4 823.92 51.29 12 -3 -4 812.12 53.59 12 -3 -4 856.71 53.29 12 3 -3 218.68 16.40 12 3 -3 229.78 16.90 -12 3 3 233.98 13.90 12 -3 -3 242.28 17.00 12 -3 -3 202.88 18.30 12 3 -2 48.50 6.00 12 3 -2 39.70 5.00 -12 3 2 41.30 2.60 12 -3 -2 40.80 5.70 12 -3 -2 25.60 6.40 -12 3 1 248.18 14.60 12 3 -1 229.78 16.70 12 3 -1 229.88 15.90 12 -3 -1 269.27 18.50 12 -3 -1 224.58 16.70 12 3 0 -0.20 2.50 -12 3 0 8.00 0.70 12 3 0 8.00 3.10 12 3 0 11.20 3.20 12 -3 0 7.00 2.70 12 -3 0 9.30 4.30 12 -3 0 10.10 3.40 12 3 1 39.40 4.60 -12 3 -1 34.20 2.20 12 -3 1 34.80 4.40 12 -3 1 32.00 4.30 12 -3 1 26.00 5.10 12 3 2 2.80 2.80 12 3 2 -3.90 2.20 -12 3 -2 1.30 0.40 12 -3 2 0.80 1.90 12 -3 2 -2.50 3.10 12 3 3 37.00 5.00 -12 3 -3 40.70 2.60 12 -3 3 43.40 5.60 12 3 4 100.79 8.70 -12 3 -4 101.29 6.30 12 -3 4 101.09 8.70 -12 3 -5 46.60 3.00 12 -3 5 44.50 5.40 -12 3 -6 20.20 1.30 12 3 6 11.50 3.60 12 -3 6 16.80 3.30 12 3 7 42.20 5.90 12 -3 7 37.00 4.60 12 4 -13 7.80 4.60 12 4 -13 4.40 6.60 12 -4 -13 9.70 6.80 12 -4 -13 4.90 7.40 12 4 -12 186.38 14.70 12 4 -12 182.88 16.10 12 -4 -12 165.38 15.90 12 -4 -12 219.88 18.80 12 4 -11 18.70 5.10 12 4 -11 15.30 5.90 12 -4 -11 18.20 6.00 12 -4 -11 32.90 8.30 -12 4 10 28.00 1.90 12 4 -10 24.20 8.00 12 4 -10 32.70 6.90 12 -4 -10 37.70 7.50 12 4 -9 9.60 5.10 -12 4 9 10.60 0.90 12 4 -9 15.20 4.70 12 4 -9 10.90 14.70 12 -4 -9 7.90 6.30 12 -4 -9 12.70 5.60 12 4 -8 434.96 39.60 12 4 -8 473.75 30.60 -12 4 8 483.45 28.20 12 -4 -8 452.05 31.30 12 -4 -8 442.56 32.80 -12 4 7 105.19 6.50 12 4 -7 105.49 10.10 12 -4 -7 106.19 12.10 12 -4 -7 108.29 11.20 12 4 -6 2371.36 137.99 12 4 -6 2101.19 143.49 12 -4 -6 2132.09 139.39 12 -4 -6 2325.57 138.49 -12 4 5 116.09 7.00 12 4 -5 102.69 10.30 12 -4 -5 108.09 10.90 12 -4 -5 113.39 11.50 12 4 -4 1143.29 74.59 -12 4 4 1224.88 72.59 12 -4 -4 1212.88 75.69 12 -4 -4 1189.68 74.89 -12 4 3 75.19 4.80 12 -4 -3 80.99 8.50 12 -4 -3 79.39 8.60 12 -4 -3 92.39 10.50 12 4 -2 101.69 9.70 12 4 -2 99.69 8.10 -12 4 2 111.49 6.70 12 -4 -2 119.79 9.80 12 -4 -2 109.49 9.60 12 -4 -2 113.39 11.70 -12 4 1 17.20 1.30 12 4 -1 20.50 3.20 12 -4 -1 14.60 3.80 12 -4 -1 13.20 3.80 12 -4 -1 15.70 5.20 -12 4 0 1458.25 86.99 12 4 0 1313.47 87.99 12 -4 0 1568.94 88.69 12 -4 0 1426.36 88.69 12 -4 0 1389.96 89.89 12 4 1 254.07 18.00 -12 4 -1 277.37 16.60 12 -4 1 304.77 19.90 12 -4 1 260.77 18.20 -12 4 -2 941.51 56.99 12 4 2 916.21 58.29 12 -4 2 959.30 59.39 12 -4 2 928.21 58.19 -12 4 -3 530.95 32.70 12 4 3 491.25 34.20 12 -4 3 597.24 35.10 -12 4 -4 123.89 8.10 12 4 4 159.88 12.70 12 4 5 39.70 5.30 -12 4 -5 28.60 1.90 12 -4 5 23.30 3.90 12 4 6 15.60 4.00 12 -4 6 16.30 3.10 12 4 7 17.10 4.30 12 -4 7 11.10 2.70 12 5 -13 19.50 6.80 12 5 -12 179.58 16.30 12 5 -12 187.88 14.70 12 -5 -12 167.18 19.80 12 -5 -12 203.98 18.40 12 5 -11 900.51 53.99 12 5 -11 819.92 54.79 12 -5 -11 779.22 53.99 12 -5 -11 887.81 56.89 -12 5 10 1104.09 70.69 12 5 -10 1285.17 73.29 12 5 -10 1096.99 73.59 12 -5 -10 1144.19 73.39 12 -5 -10 1197.18 75.89 12 5 -9 769.72 49.50 -12 5 9 763.82 47.20 12 -5 -9 842.02 53.09 12 -5 -9 740.63 49.99 -12 5 8 583.74 35.20 12 5 -8 506.95 47.70 12 5 -8 589.54 37.60 12 -5 -8 548.85 38.10 12 -5 -8 644.84 40.60 12 5 -7 46.90 11.70 -12 5 7 43.70 2.80 12 5 -7 43.20 6.00 12 -5 -7 40.70 7.20 12 -5 -7 48.70 8.60 -12 5 6 34.40 2.20 12 5 -6 30.10 10.70 12 5 -6 31.10 5.50 12 -5 -6 24.70 6.70 12 -5 -6 37.70 6.40 12 5 -5 556.64 46.90 12 5 -5 600.24 40.90 -12 5 5 646.54 38.70 12 -5 -5 654.83 41.30 12 -5 -5 713.23 42.80 -12 5 4 175.48 10.20 12 5 -4 159.58 13.10 12 -5 -4 153.68 13.20 12 -5 -4 173.18 14.30 12 -5 -4 152.48 15.10 -12 5 3 73.29 4.40 12 5 -3 69.89 8.30 12 -5 -3 67.29 8.40 12 -5 -3 66.59 9.40 12 -5 -3 63.59 7.90 12 5 -2 1.80 3.90 12 5 -2 5.20 3.20 -12 5 2 10.20 0.90 12 -5 -2 11.90 5.60 12 -5 -2 7.20 3.60 12 -5 -2 5.50 3.30 12 5 -1 6.70 2.30 -12 5 1 7.60 0.70 12 -5 -1 3.60 3.20 12 -5 -1 3.60 3.10 12 -5 -1 4.00 4.30 -12 5 0 8.10 0.80 12 5 0 8.90 2.60 12 -5 0 9.30 4.50 12 -5 0 6.30 3.00 12 5 1 4.00 2.40 -12 5 -1 3.80 0.50 12 -5 1 8.10 2.80 12 -5 1 6.60 4.00 -12 5 -2 89.69 5.40 12 5 2 81.89 7.40 12 -5 2 89.19 7.30 12 -5 2 85.89 8.60 -12 5 -3 90.59 5.80 12 5 3 94.99 8.00 12 -5 3 105.09 9.10 12 5 4 380.36 26.30 -12 5 -4 408.76 24.60 12 -5 4 422.66 26.70 -12 5 -5 379.46 23.50 12 5 5 379.36 25.40 12 -5 5 400.16 25.30 12 5 6 150.28 12.50 12 -5 6 190.18 12.20 12 6 -12 17.70 4.70 12 6 -12 18.20 7.70 12 -6 -12 27.10 7.60 12 6 -11 629.84 40.60 12 6 -11 685.43 43.50 12 -6 -11 545.55 41.00 12 -6 -11 665.13 43.80 12 6 -10 65.09 7.70 12 6 -10 13.90 12.00 -12 6 10 52.99 3.30 12 -6 -10 47.20 8.80 12 -6 -10 47.10 6.90 -12 6 9 51.69 3.40 12 6 -9 55.19 6.90 12 -6 -9 53.89 6.90 12 -6 -9 58.99 9.50 -12 6 8 5.90 0.60 12 6 -8 11.30 5.30 12 -6 -8 7.50 5.20 -12 6 7 139.59 8.90 12 6 -7 143.79 11.90 12 -6 -7 157.48 12.40 12 -6 -7 144.79 13.80 -12 6 6 0.70 0.40 12 6 -6 5.70 4.20 12 6 -6 -3.30 9.30 12 -6 -6 -1.40 5.00 12 -6 -6 4.50 4.30 12 6 -5 146.59 24.30 -12 6 5 172.28 10.00 12 6 -5 147.49 13.00 12 -6 -5 168.88 14.50 12 -6 -5 148.09 15.60 12 -6 -5 166.58 13.00 -12 6 4 0.80 0.40 12 6 -4 7.00 4.10 12 -6 -4 2.30 5.70 12 -6 -4 4.00 3.70 12 -6 -4 1.00 3.80 -12 6 3 238.48 14.50 12 -6 -3 190.98 18.60 12 -6 -3 273.67 16.90 12 -6 -3 235.38 17.70 -12 6 2 73.49 4.50 12 -6 -2 72.79 9.50 12 -6 -2 70.19 7.70 12 -6 -2 65.79 7.20 12 6 -1 176.88 13.10 -12 6 1 200.18 12.00 12 -6 -1 202.18 15.80 12 -6 -1 206.68 14.50 -12 6 0 25.20 1.80 12 6 0 30.10 3.70 12 -6 0 29.40 5.50 12 -6 0 25.10 4.20 12 6 1 59.39 5.90 -12 6 -1 70.09 4.20 12 -6 1 62.69 7.80 12 -6 1 67.79 6.40 -12 6 -2 34.60 2.30 12 6 2 30.90 4.60 -12 6 -3 452.25 27.40 12 6 3 432.06 28.90 12 -6 3 466.65 29.60 12 6 4 3.00 2.60 12 -6 4 2.60 2.60 12 6 5 4.10 2.80 12 -6 5 3.70 2.50 12 6 6 49.70 6.50 12 -6 6 36.20 4.60 -12 7 11 0.00 0.50 12 7 -11 4.90 6.40 12 -7 -11 -4.70 5.30 -12 7 10 2.30 0.50 12 7 -10 0.70 4.10 12 -7 -10 3.60 6.20 -12 7 9 17.00 1.30 12 7 -9 16.40 4.80 12 -7 -9 25.30 5.00 12 -7 -9 21.60 7.10 12 7 -8 2.20 3.90 12 -7 -8 2.20 3.90 12 -7 -8 1.70 5.50 -12 7 7 7.40 0.70 12 7 -7 3.80 4.00 12 -7 -7 5.00 6.40 12 -7 -7 5.30 5.00 12 -7 -7 3.60 3.70 12 7 -6 49.70 6.50 12 -7 -6 46.20 6.80 -12 7 5 50.39 3.10 12 -7 -5 44.10 5.60 12 -7 -5 32.90 7.50 12 -7 -5 49.99 7.50 -12 7 4 324.87 20.20 12 -7 -4 319.57 23.40 12 -7 -4 292.97 24.30 12 -7 -4 377.76 22.30 -12 7 3 159.88 10.00 12 -7 -3 179.48 13.40 12 -7 -3 151.18 14.50 -12 7 2 404.56 24.60 12 -7 -2 385.76 27.90 12 -7 -2 414.76 27.20 12 7 -1 145.29 10.70 -12 7 1 157.28 9.40 12 -7 -1 158.48 13.20 12 -7 -1 151.68 11.80 -12 7 0 111.69 7.10 12 7 0 114.09 8.50 -12 7 -1 114.39 7.10 12 7 1 105.89 8.50 12 -7 1 125.59 9.20 12 -7 1 113.79 10.00 12 7 2 52.09 5.50 -12 7 -2 54.29 3.50 12 -7 2 59.69 5.70 12 -7 2 59.59 6.60 12 7 3 57.39 6.20 -12 7 -3 62.99 3.90 12 -7 3 60.79 6.60 -12 7 -4 59.59 3.60 12 7 4 54.59 6.10 12 -7 4 49.99 5.70 12 7 5 7.60 4.50 12 -7 5 9.60 2.80 -12 8 10 174.78 10.60 12 8 -10 166.38 13.60 12 -8 -10 179.68 17.50 -12 8 9 0.40 0.40 12 8 -9 -1.50 4.30 12 -8 -9 2.80 5.20 12 -8 -9 -3.10 7.00 12 8 -8 1.80 4.60 -12 8 8 0.30 0.40 12 -8 -8 7.10 6.70 12 -8 -8 0.20 4.60 -12 8 7 2.90 0.50 12 8 -7 2.70 4.90 12 -8 -7 4.70 6.20 12 -8 -7 1.90 4.30 -12 8 6 206.48 13.10 12 -8 -6 210.38 18.20 12 -8 -6 235.98 17.20 -12 8 5 0.40 0.40 12 -8 -5 0.40 3.80 12 -8 -5 -0.60 5.30 -12 8 4 82.09 5.00 12 -8 -4 70.29 8.40 12 -8 -4 77.59 10.10 -12 8 3 5.90 0.70 12 -8 -3 0.40 4.50 12 -8 -3 8.90 3.70 -12 8 2 1.20 0.40 12 -8 -2 1.60 3.20 12 -8 -2 2.10 4.20 12 8 -1 30.50 3.90 -12 8 1 29.80 2.00 12 -8 -1 26.90 4.40 12 -8 -1 26.20 4.80 12 8 0 8.40 2.60 -12 8 0 8.50 0.80 12 -8 0 9.90 3.10 12 -8 0 8.20 3.90 12 8 1 19.60 3.20 -12 8 -1 23.00 1.50 12 -8 1 17.60 3.90 12 -8 1 20.40 3.50 12 8 2 5.10 2.50 -12 8 -2 3.30 0.50 12 -8 2 4.00 2.10 12 -8 2 5.10 2.80 -12 8 -3 17.40 1.30 12 8 3 11.10 3.00 12 -8 3 16.60 3.20 12 8 4 35.10 4.40 12 -8 4 39.30 5.60 12 9 -8 -4.70 8.00 -12 9 8 0.50 0.50 12 -9 -8 3.30 6.90 12 -9 -8 2.30 4.10 -12 9 7 58.49 3.60 12 -9 -7 59.29 7.70 12 -9 -7 47.90 8.30 -12 9 6 0.20 0.40 12 -9 -6 0.50 3.80 12 -9 -6 -9.50 5.10 -12 9 5 12.50 1.10 12 -9 -5 14.80 4.70 12 -9 -5 14.60 5.50 -12 9 4 0.60 0.40 12 -9 -4 -0.20 4.60 12 -9 -4 -2.60 2.90 -12 9 3 4.30 0.50 12 -9 -3 6.20 4.30 12 -9 -3 5.90 3.20 -12 9 2 5.40 0.60 12 -9 -2 6.10 4.10 12 -9 -2 7.00 3.50 -12 9 1 0.40 0.40 12 -9 -1 0.50 3.30 12 -9 -1 -1.60 2.50 -12 9 0 11.10 0.90 12 9 0 7.40 3.80 12 -9 0 11.40 2.90 12 -9 0 8.70 3.60 -12 9 -1 9.50 0.80 12 9 1 9.70 4.40 12 -9 1 10.30 2.90 12 -9 1 7.00 3.00 12 9 2 7.00 2.80 -12 9 -2 6.40 0.60 12 -9 2 2.60 3.40 -12 10 5 9.50 0.80 12 -10 -5 4.30 5.20 12 -10 -5 7.40 3.70 -12 10 4 3.60 0.50 12 -10 -4 2.60 3.00 12 -10 -4 5.00 4.60 -12 10 3 0.50 0.40 12 -10 -3 0.20 4.00 12 -10 -3 1.30 2.70 -12 10 2 36.10 2.30 12 -10 -2 31.20 4.80 12 -10 -2 36.10 5.00 12 -10 -1 -1.60 3.40 12 -10 -1 -1.10 2.40 13 0 -14 4.80 8.60 13 0 -13 -1.60 6.00 13 0 -13 1.20 5.70 13 0 -12 42.60 7.30 13 0 -12 54.49 9.60 13 0 -11 1.00 5.40 13 0 -11 0.80 6.20 13 0 -10 61.99 9.70 13 0 -10 58.19 8.30 13 0 -9 5.40 5.80 -13 0 9 0.10 0.20 13 0 -9 -3.30 4.80 13 0 -8 7.50 5.00 -13 0 8 6.40 0.60 13 0 -8 4.40 5.30 13 0 -7 -1.90 4.40 -13 0 7 0.30 0.30 13 0 -7 5.10 5.10 13 0 -6 15.40 5.20 13 0 -6 9.60 4.80 13 0 -5 -1.20 4.30 13 0 -5 3.80 4.20 13 0 -4 167.88 13.10 13 0 -4 163.98 13.70 13 0 -3 -6.10 3.10 13 0 -3 -2.10 4.10 13 0 -3 3.30 5.00 13 0 -2 21.30 5.60 13 0 -2 21.70 4.90 13 0 -1 1.40 3.90 13 0 -1 -0.10 3.40 13 0 -1 2.20 4.10 13 0 0 177.38 12.40 13 0 0 177.88 13.30 13 0 0 144.39 13.50 13 0 1 3.50 3.20 13 0 1 -1.70 5.20 13 0 1 0.60 2.60 13 0 2 18.90 6.20 13 0 2 20.80 3.70 13 0 3 -2.00 2.30 13 0 3 7.20 6.60 13 0 4 165.98 11.80 13 0 4 156.98 19.10 13 0 5 -2.00 2.10 13 0 5 -2.30 9.70 13 0 6 6.40 2.30 13 0 6 0.10 11.50 13 0 7 1.30 3.00 13 0 7 -5.20 14.40 13 1 -13 59.59 8.30 13 1 -13 57.99 9.70 13 -1 -13 49.50 8.30 13 -1 -13 68.49 10.90 13 1 -12 394.46 27.70 13 1 -12 401.96 29.50 13 -1 -12 414.56 30.00 13 -1 -12 377.06 27.90 13 1 -11 96.49 12.40 13 1 -11 93.99 11.10 13 -1 -11 88.39 11.20 13 -1 -11 114.39 12.90 13 1 -10 53.09 9.00 13 1 -10 45.40 7.20 13 -1 -10 42.80 7.30 13 -1 -10 41.60 8.40 13 1 -9 15.50 5.60 13 1 -9 26.10 6.90 13 -1 -9 20.30 5.90 13 -1 -9 17.90 6.70 -13 1 8 36.50 2.30 13 1 -8 34.40 7.40 13 1 -8 40.90 6.70 -13 -1 8 35.50 2.30 13 -1 -8 35.80 7.90 13 -1 -8 40.10 7.20 13 1 -7 4.30 5.00 13 1 -7 1.40 4.60 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1192.78 74.79 14 0 -3 6.20 5.20 14 0 -3 -0.90 4.40 14 0 -3 7.90 3.60 14 0 -2 237.08 17.80 14 0 -2 219.78 16.80 14 0 -1 1.40 3.60 14 0 -1 -0.10 3.20 14 0 0 5.00 4.80 14 0 0 1.20 3.50 14 0 0 -3.10 2.80 14 0 1 -0.50 2.90 14 0 1 0.30 2.70 14 0 1 -1.90 6.30 14 0 2 0.00 8.00 14 0 2 9.80 3.20 14 0 3 -1.50 2.60 14 0 3 -5.40 9.80 14 0 4 193.58 13.20 14 0 4 168.48 22.30 14 0 5 13.30 13.60 14 0 6 99.09 7.20 -14 0 -6 87.29 5.60 14 1 -13 28.80 6.90 14 1 -13 36.40 9.10 14 -1 -13 49.00 7.90 14 -1 -13 40.30 9.40 14 1 -12 1.10 6.80 14 1 -12 2.00 5.30 14 -1 -12 2.50 5.50 14 -1 -12 11.30 6.60 14 1 -11 147.19 14.00 14 1 -11 156.68 15.30 14 -1 -11 113.99 15.10 14 -1 -11 167.18 14.50 14 1 -10 2.30 5.20 14 1 -10 6.30 6.40 14 -1 -10 8.30 6.50 14 -1 -10 7.60 5.90 14 1 -9 2.00 4.90 14 1 -9 5.60 6.20 14 -1 -9 4.60 6.00 14 -1 -9 0.50 5.80 -14 1 8 179.68 10.70 14 1 -8 178.48 15.10 14 1 -8 167.58 15.60 -14 -1 8 174.18 10.60 14 -1 -8 157.88 15.40 14 -1 -8 173.58 15.20 14 1 -7 506.95 36.70 14 1 -7 582.34 36.90 -14 1 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9.70 14 1 5 6.60 9.10 14 1 5 6.60 2.50 14 -1 5 -2.10 14.30 14 -1 5 13.30 2.90 -14 1 -6 42.10 2.60 14 1 6 39.60 4.80 14 1 6 35.00 13.00 14 -1 6 40.20 5.50 14 -1 6 16.70 15.20 14 2 -13 90.49 11.20 14 2 -13 122.19 13.70 14 -2 -13 75.29 10.50 14 -2 -13 130.09 15.60 14 2 -12 17.50 7.30 14 2 -12 20.40 6.00 14 -2 -12 18.30 7.60 14 -2 -12 17.90 6.50 14 2 -11 287.97 23.00 14 2 -11 289.47 21.60 14 -2 -11 290.57 22.00 14 -2 -11 297.87 23.50 14 2 -10 -2.20 6.10 -14 2 10 0.00 0.30 14 2 -10 4.50 5.10 14 -2 -10 3.10 5.70 14 -2 -10 -8.70 5.50 14 2 -9 108.29 12.80 -14 2 9 112.29 6.80 14 2 -9 108.99 11.50 14 -2 -9 100.29 12.10 14 -2 -9 114.49 13.20 14 2 -8 14.30 5.90 14 2 -8 9.20 5.20 -14 2 8 5.60 0.50 14 -2 -8 -1.10 5.20 -14 -2 8 3.80 0.40 14 -2 -8 7.80 5.30 14 2 -7 58.49 8.20 -14 2 7 69.59 4.20 14 -2 -7 57.59 8.70 14 -2 -7 71.29 9.00 14 2 -6 10.50 7.80 14 2 -6 32.00 6.20 -14 2 6 25.50 1.70 14 -2 -6 22.10 6.10 14 -2 -6 27.40 6.40 -14 2 5 512.25 29.00 14 2 -5 432.76 32.60 14 2 -5 480.25 32.10 14 -2 -5 469.45 32.20 14 -2 -5 461.25 32.00 14 2 -4 -3.60 4.30 -14 2 4 0.90 0.40 14 2 -4 1.50 4.90 14 -2 -4 -1.70 4.50 14 -2 -4 -1.60 3.80 14 -2 -4 -0.40 5.40 14 2 -3 370.46 26.40 -14 2 3 395.26 23.40 14 2 -3 382.26 26.30 14 -2 -3 375.46 25.70 14 -2 -3 396.56 26.30 14 -2 -3 372.16 27.70 -14 2 2 90.89 5.60 14 2 -2 93.79 9.20 14 2 -2 95.19 9.40 14 -2 -2 99.59 10.90 14 -2 -2 80.69 9.00 14 -2 -2 80.89 7.80 14 2 -1 17.70 4.90 14 2 -1 23.10 4.80 14 2 -1 24.80 4.50 -14 2 1 28.60 1.80 14 -2 -1 23.20 4.40 14 -2 -1 26.80 5.70 14 2 0 52.59 6.10 -14 2 0 47.90 3.10 14 2 0 52.19 5.60 14 2 0 44.20 6.00 14 -2 0 45.90 6.50 14 -2 0 56.99 6.30 14 2 1 130.89 11.50 -14 2 -1 175.58 10.00 14 2 1 165.68 13.00 14 -2 1 180.58 13.10 14 2 2 7.20 4.30 -14 2 -2 7.00 0.70 14 -2 2 4.40 3.20 -14 2 -3 278.67 16.70 14 2 3 237.48 19.40 14 -2 3 299.57 18.90 -14 2 -4 87.69 5.20 14 2 4 68.09 9.70 14 -2 4 82.39 7.30 -14 2 -5 19.90 1.40 14 2 5 6.10 5.80 14 -2 5 20.80 3.40 14 -2 6 30.00 4.90 14 3 -12 57.09 9.70 14 3 -12 77.99 9.00 14 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1 196.68 11.40 14 -3 -1 186.88 15.40 14 -3 -1 189.38 13.90 14 -3 -1 183.28 13.30 14 3 0 1097.59 70.59 -14 3 0 1147.89 68.99 14 -3 0 1188.98 71.89 14 -3 0 1102.39 70.19 14 -3 0 1138.89 70.69 -14 3 -1 44.30 2.80 14 3 1 44.50 6.40 14 -3 1 41.60 6.00 14 3 2 164.28 14.70 -14 3 -2 152.88 9.50 14 -3 2 151.78 12.30 14 3 3 81.29 9.20 -14 3 -3 109.19 6.40 14 -3 3 108.09 9.00 14 3 4 35.70 5.50 -14 3 -4 37.30 2.50 14 -3 4 48.40 5.40 14 3 5 115.49 10.60 -14 3 -5 116.79 7.10 14 -3 5 108.99 8.90 14 4 -12 386.06 26.10 14 4 -12 364.66 28.00 14 -4 -12 366.06 26.30 14 -4 -12 371.66 28.10 14 4 -11 55.19 10.00 14 4 -11 47.90 7.10 14 -4 -11 60.79 8.40 14 -4 -11 51.09 9.30 -14 4 10 740.33 45.90 14 4 -10 788.12 49.00 14 -4 -10 810.12 50.99 14 -4 -10 687.73 48.80 -14 4 9 2.60 0.50 14 4 -9 2.40 5.00 14 -4 -9 3.00 6.00 14 -4 -9 1.30 5.40 14 -4 -8 245.78 22.90 14 -4 -8 304.17 25.20 -14 4 7 84.59 5.10 14 4 -7 72.79 9.00 14 -4 -7 87.49 10.40 14 -4 -7 75.59 10.30 14 4 -6 29.00 6.00 -14 4 6 30.70 2.00 14 -4 -6 29.80 6.90 14 -4 -6 31.10 6.50 14 4 -5 -5.30 4.30 -14 4 5 0.90 0.40 14 -4 -5 -1.50 5.50 14 -4 -5 2.70 4.60 14 -4 -5 -0.50 4.60 -14 4 4 167.58 10.20 14 4 -4 147.69 13.70 14 -4 -4 168.28 13.70 14 -4 -4 175.58 13.50 14 -4 -4 162.98 15.60 -14 4 3 15.30 1.10 14 4 -3 14.80 4.90 14 -4 -3 10.90 4.20 14 -4 -3 9.40 5.70 14 -4 -3 7.20 4.30 14 4 -2 -1.40 3.50 -14 4 2 6.60 0.70 14 -4 -2 11.00 5.10 14 -4 -2 4.20 3.50 14 -4 -2 3.00 3.30 14 4 -1 1.10 3.60 -14 4 1 8.90 0.80 14 -4 -1 7.80 3.20 14 -4 -1 5.30 4.50 14 -4 -1 11.80 3.70 -14 4 0 23.00 1.60 14 4 0 22.50 4.10 14 -4 0 20.80 3.60 14 -4 0 25.60 5.30 -14 4 -1 30.40 2.40 14 -4 1 40.80 5.70 14 4 2 71.59 7.80 -14 4 -2 88.39 5.30 14 -4 2 91.29 8.50 14 4 3 14.70 4.00 -14 4 -3 13.50 1.10 14 -4 3 9.10 3.20 14 4 4 6.20 3.50 -14 4 -4 4.10 0.50 14 -4 4 5.30 2.70 14 4 5 3.20 6.40 -14 4 -5 1.90 0.50 14 -4 5 1.70 2.30 14 5 -11 -4.00 4.20 14 -5 -11 -5.90 5.20 14 -5 -11 -0.70 7.20 14 5 -10 -0.50 4.70 -14 5 10 1.00 0.40 14 -5 -10 -1.30 5.20 14 -5 -10 2.40 5.50 14 5 -9 218.78 16.90 -14 5 9 202.28 13.10 14 -5 -9 231.68 16.90 14 -5 -9 223.68 18.90 -14 5 8 6.50 0.70 14 5 -8 6.00 5.20 14 -5 -8 8.80 5.10 14 -5 -8 2.60 5.30 -14 5 7 118.79 7.40 14 5 -7 120.19 11.70 14 -5 -7 129.59 11.60 14 -5 -7 114.79 12.50 14 5 -6 7.10 5.00 -14 5 6 12.70 1.10 14 -5 -6 15.60 8.20 14 5 -5 42.70 6.80 -14 5 5 53.39 3.40 14 -5 -5 59.79 7.50 14 -5 -5 59.49 8.10 14 -5 -5 48.70 9.00 14 5 -4 1.40 4.60 -14 5 4 6.50 0.60 14 -5 -4 5.10 4.10 14 -5 -4 4.80 5.70 14 -5 -4 8.80 4.00 -14 5 3 79.69 5.10 14 -5 -3 84.09 8.30 14 -5 -3 91.39 10.80 14 -5 -3 80.39 8.40 -14 5 2 19.60 1.50 14 -5 -2 23.40 5.60 14 -5 -2 17.50 4.00 14 -5 -2 21.50 4.40 -14 5 1 1.10 0.60 14 -5 -1 0.00 3.20 14 5 0 2.70 4.40 -14 5 0 6.00 0.60 14 -5 0 3.20 2.50 14 -5 0 5.60 3.90 -14 5 -1 0.70 0.40 14 5 1 0.10 3.00 14 -5 1 2.30 2.20 14 -5 1 1.80 3.40 14 5 2 5.50 3.00 -14 5 -2 3.60 0.50 14 -5 2 7.70 3.20 -14 5 -3 129.89 8.00 14 5 3 126.89 10.40 14 -5 3 135.29 10.40 -14 5 -4 177.08 10.40 14 5 4 143.89 13.00 14 -5 4 175.98 12.20 14 6 -10 4.20 5.00 -14 6 10 1.10 0.60 14 -6 -10 -1.40 5.50 14 6 -9 28.00 6.20 -14 6 9 16.50 1.30 14 -6 -9 24.20 5.10 14 -6 -9 25.60 6.70 -14 6 8 9.90 0.80 14 6 -8 8.50 5.10 14 -6 -8 6.10 4.40 14 -6 -8 9.70 6.60 14 -6 -8 6.10 5.20 14 6 -7 30.10 6.10 -14 6 7 39.40 2.40 14 -6 -7 34.40 6.90 14 -6 -7 28.10 7.90 14 -6 -7 32.10 5.80 14 6 -6 4.10 5.00 -14 6 6 1.40 0.50 14 -6 -6 1.10 4.40 14 -6 -6 -4.00 5.70 14 -6 -6 3.80 3.90 -14 6 5 319.37 19.40 14 6 -5 304.47 22.30 14 -6 -5 325.07 21.80 14 -6 -5 307.17 22.90 14 -6 -5 332.77 24.70 -14 6 4 -0.80 0.40 14 6 -4 -0.80 6.10 14 -6 -4 -1.70 3.50 14 -6 -4 0.00 3.40 14 -6 -4 1.20 5.10 -14 6 3 35.30 2.40 14 -6 -3 39.30 5.80 14 -6 -3 47.80 5.50 14 -6 -3 29.30 6.20 -14 6 2 0.60 0.40 14 -6 -2 3.40 3.30 14 -6 -2 -1.50 3.90 -14 6 1 11.60 0.90 14 -6 -1 10.80 4.40 14 -6 -1 11.40 3.40 14 6 0 49.60 6.80 -14 6 0 63.39 3.90 14 -6 0 60.49 7.80 14 -6 0 68.19 6.30 -14 6 -1 644.14 38.50 14 6 1 562.94 39.90 14 -6 1 646.64 39.80 14 -6 1 678.43 41.00 14 6 2 21.40 4.10 -14 6 -2 31.80 2.10 14 -6 2 47.80 5.80 14 -6 3 579.54 37.00 14 7 -9 2.90 6.00 14 -7 -9 8.70 6.40 14 -7 -9 11.60 4.20 14 -7 -9 2.70 5.10 -14 7 8 1.30 0.40 14 7 -8 0.30 5.20 14 -7 -8 3.50 3.70 14 -7 -8 -6.90 5.50 14 -7 -8 0.00 4.70 -14 7 7 3.10 0.50 14 7 -7 2.10 5.70 14 -7 -7 8.10 3.70 14 -7 -7 3.70 6.10 14 -7 -7 0.90 4.20 14 7 -6 4.10 5.90 -14 7 6 3.20 0.50 14 -7 -6 7.40 5.90 14 -7 -6 0.80 4.20 14 -7 -6 3.50 3.50 -14 7 5 53.29 3.40 14 -7 -5 55.89 7.60 14 -7 -5 58.19 6.60 14 -7 -5 46.30 8.40 -14 7 4 312.47 18.50 14 -7 -4 279.87 21.20 14 -7 -4 307.67 22.40 -14 7 3 103.39 6.50 14 -7 -3 100.99 11.00 14 -7 -3 107.69 9.50 -14 7 2 190.68 11.80 14 -7 -2 181.28 14.00 14 -7 -2 217.48 15.80 -14 7 1 12.50 1.00 14 -7 -1 6.60 3.90 14 -7 -1 9.20 3.30 -14 7 0 129.09 8.10 14 -7 0 127.99 9.80 14 -7 0 139.79 11.10 -14 7 -1 21.00 1.50 14 -7 1 13.00 3.70 14 -7 1 23.40 3.60 14 7 2 260.17 18.80 -14 7 -2 300.07 17.20 14 -7 2 273.47 18.90 -14 8 8 90.09 5.40 14 -8 -8 65.99 10.40 -14 8 7 0.50 0.40 14 -8 -7 -4.50 3.50 14 -8 -7 6.60 7.50 -14 8 6 30.20 2.00 14 -8 -6 27.20 5.60 14 -8 -6 20.30 6.20 -14 8 5 2.80 0.50 14 -8 -5 6.00 3.80 14 -8 -5 2.00 5.00 -14 8 4 35.00 2.40 14 -8 -4 39.60 5.50 14 -8 -4 36.40 6.50 -14 8 3 25.90 1.80 14 -8 -3 30.40 5.40 14 -8 -3 23.00 4.40 -14 8 2 116.79 6.90 14 -8 -2 104.29 10.20 14 -8 -2 105.99 9.20 -14 8 1 4.00 0.60 14 -8 -1 6.50 2.70 14 -8 -1 -0.40 3.20 -14 8 0 9.60 0.80 14 -8 0 8.10 3.20 14 -8 0 5.00 2.40 15 0 -12 12.10 6.10 15 0 -12 19.00 6.90 15 0 -11 -3.70 6.30 15 0 -11 -1.50 5.20 15 0 -10 13.50 6.10 15 0 -10 16.40 7.20 15 0 -9 -4.20 5.30 15 0 -9 4.60 5.60 -15 0 8 36.20 2.30 15 0 -8 31.60 7.20 15 0 -8 41.40 8.00 15 0 -7 9.00 5.60 15 0 -7 1.80 4.90 -15 0 7 0.70 0.40 15 0 -6 53.89 8.10 -15 0 6 68.29 4.20 15 0 -5 -0.10 5.40 15 0 -5 3.70 4.90 15 0 -5 -4.60 4.40 15 0 -4 9.60 5.00 15 0 -4 10.70 5.50 15 0 -3 -4.60 4.30 15 0 -3 4.70 4.50 15 0 -2 74.29 8.30 15 0 -2 64.49 8.60 15 0 -1 -1.60 3.20 15 0 -1 2.20 3.60 15 0 0 92.79 8.30 15 0 0 96.39 8.90 15 0 1 4.10 4.50 15 0 2 22.70 11.40 15 0 2 37.00 4.60 15 0 3 -1.30 12.40 15 0 3 6.00 2.70 15 0 4 142.09 10.20 15 0 5 -6.70 18.00 -15 0 -5 0.30 0.40 15 0 5 -2.00 2.20 15 1 -12 4.90 7.60 15 1 -12 0.20 5.30 15 -1 -12 5.90 6.20 15 -1 -12 4.60 6.70 15 1 -11 7.70 6.80 15 1 -11 10.30 6.10 15 -1 -11 4.60 6.80 15 -1 -11 11.80 6.10 15 1 -10 1.90 5.10 15 1 -10 3.50 6.50 15 -1 -10 2.30 5.60 15 -1 -10 -5.10 5.60 15 1 -9 1.00 5.10 15 1 -9 1.20 6.20 -15 1 9 0.70 0.40 15 -1 -9 -2.70 5.10 15 -1 -9 -1.30 5.70 -15 -1 9 0.10 0.30 15 1 -8 -3.40 5.80 15 -1 -8 -0.20 5.60 15 -1 -8 1.50 8.60 15 1 -7 33.00 6.80 -15 1 7 39.40 2.50 15 -1 -7 29.20 6.70 -15 -1 7 39.00 2.50 15 -1 -7 37.50 7.40 15 1 -6 61.39 8.30 -15 1 6 61.29 3.80 15 -1 -6 59.79 8.30 15 -1 -6 56.99 8.10 15 1 -5 130.59 14.00 15 1 -5 149.09 13.30 -15 1 5 149.29 8.70 15 -1 -5 137.39 14.80 15 -1 -5 125.19 12.90 15 -1 -5 137.09 12.30 15 1 -4 170.98 15.50 15 1 -4 178.88 15.00 -15 1 4 182.88 11.10 15 -1 -4 170.38 16.00 15 -1 -4 199.18 14.90 15 1 -3 172.08 14.70 15 1 -3 188.28 15.20 15 -1 -3 192.78 15.90 15 -1 -3 184.78 14.50 15 1 -2 260.87 18.80 15 1 -2 261.97 19.20 15 -1 -2 254.77 18.70 15 -1 -2 288.97 20.30 15 1 -1 148.49 11.60 15 1 -1 155.38 12.10 15 -1 -1 147.49 12.70 15 -1 -1 145.39 11.70 15 1 0 71.39 7.00 15 1 0 82.19 7.70 15 1 0 58.99 8.70 15 -1 0 75.49 8.10 15 -1 0 76.69 7.20 15 1 1 1.10 3.90 15 1 1 -3.90 11.10 15 -1 1 -0.30 3.00 15 1 2 56.49 10.70 15 1 2 59.49 6.10 15 -1 2 62.39 6.60 15 1 3 212.78 22.50 15 1 3 228.68 16.00 -15 1 -3 242.48 14.70 15 -1 3 260.97 16.60 -15 1 -4 222.58 13.00 15 1 4 187.18 15.10 15 1 4 192.98 22.90 15 -1 4 225.68 14.60 15 1 5 212.68 15.10 -15 1 -5 225.18 14.00 15 -1 5 249.48 15.30 15 2 -12 70.39 9.90 15 2 -12 86.49 9.80 15 -2 -12 60.79 9.50 15 -2 -12 86.79 10.00 15 2 -11 2.40 6.90 15 2 -11 5.20 5.10 15 -2 -11 4.80 6.80 15 -2 -11 -0.90 5.20 15 2 -10 20.00 6.50 15 2 -10 21.30 7.50 15 -2 -10 20.20 6.40 15 -2 -10 8.10 6.40 -15 2 9 0.40 0.40 15 2 -9 -1.50 4.90 15 2 -9 -2.20 6.50 15 -2 -9 1.10 5.60 15 -2 -9 2.80 5.40 15 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95.09 14.20 -15 2 -3 133.89 7.80 15 -2 3 126.39 10.00 15 2 4 10.20 8.60 -15 2 -4 23.50 1.60 15 -2 4 20.00 3.40 15 3 -12 7.00 7.80 15 3 -12 -7.50 8.30 15 -3 -12 4.30 6.00 15 -3 -12 7.70 8.00 15 3 -11 16.00 14.40 15 3 -11 25.40 6.50 15 -3 -11 14.10 7.40 15 -3 -11 22.90 6.80 -15 3 10 46.30 3.00 15 3 -10 49.80 7.50 15 -3 -10 41.40 8.90 15 -3 -10 55.69 8.50 15 3 -9 26.60 6.40 -15 3 9 26.40 1.80 15 -3 -9 38.30 7.80 15 -3 -9 28.20 6.50 15 3 -8 19.00 6.00 -15 3 8 19.30 1.40 15 -3 -8 27.60 7.30 15 -3 -8 17.30 6.30 15 3 -7 129.79 14.20 15 -3 -7 145.79 14.50 15 3 -6 3.50 6.00 15 3 -6 -0.90 4.70 -15 3 6 1.20 0.40 15 -3 -6 2.00 5.10 15 -3 -6 4.10 5.90 15 -3 -6 4.70 4.70 15 3 -5 7.60 5.10 15 3 -5 -3.00 5.50 15 -3 -5 2.60 4.50 15 -3 -5 1.40 6.20 15 -3 -5 5.80 4.60 15 3 -4 92.49 10.30 -15 3 4 96.39 5.70 15 -3 -4 92.59 9.30 15 -3 -4 82.09 11.30 15 -3 -4 81.19 9.30 15 3 -3 325.77 22.80 -15 3 3 331.57 20.00 15 -3 -3 325.37 22.70 15 -3 -3 316.47 22.30 15 -3 -3 343.27 24.50 15 3 -2 439.06 30.70 -15 3 2 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38.50 5.30 -16 7 3 2.80 0.60 16 -7 -3 2.10 2.70 17 0 -10 9.30 6.20 17 0 -10 6.20 7.10 -17 0 9 -0.80 0.60 17 0 -9 -1.30 5.00 -17 0 8 12.70 1.00 17 0 -8 13.60 7.00 17 0 -8 1.10 8.50 17 0 -8 7.90 5.60 -17 0 7 0.80 0.40 17 0 -7 -0.60 6.30 17 0 -7 3.20 5.40 17 0 -6 8.00 5.20 17 0 -6 12.80 5.90 -17 0 6 5.60 0.60 -17 0 5 0.20 0.40 17 0 -5 -1.30 4.90 17 0 -5 -0.60 4.30 -17 0 4 25.20 1.80 17 0 -4 27.50 5.70 17 0 -4 28.20 6.20 -17 0 3 4.30 0.60 17 0 -3 -2.10 4.20 17 0 -3 4.00 3.60 17 0 -2 10.90 4.20 17 0 -2 7.50 3.50 17 0 -1 5.80 3.70 17 0 -1 -0.50 3.00 17 0 0 2.30 3.20 17 0 1 2.10 5.30 -17 0 -1 0.50 0.40 -17 0 -2 17.70 1.70 17 0 2 24.40 3.60 17 1 -10 13.20 5.70 17 -1 -10 22.00 6.70 17 -1 -10 15.60 5.80 -17 1 9 35.80 2.20 17 1 -9 25.10 7.90 17 1 -9 34.30 6.90 17 -1 -9 24.80 6.40 17 -1 -9 25.30 6.90 17 1 -8 18.60 6.00 -17 1 8 15.40 1.10 17 1 -8 5.40 6.90 -17 -1 8 15.50 1.10 17 -1 -8 8.90 7.20 17 -1 -8 12.80 6.10 17 -1 -8 15.50 5.50 17 1 -7 11.90 6.80 -17 1 7 14.50 1.10 17 1 -7 10.20 5.40 17 -1 -7 20.50 6.00 17 -1 -7 13.10 6.70 -17 -1 7 13.90 1.10 17 -1 -7 15.80 6.00 17 1 -6 -1.90 4.90 -17 1 6 3.10 0.50 17 1 -6 8.30 5.90 -17 -1 6 2.50 0.40 17 -1 -6 5.30 5.10 17 -1 -6 0.20 8.10 17 -1 -6 1.90 5.90 -17 1 5 3.00 0.50 17 1 -5 4.50 4.50 17 1 -5 0.70 5.20 17 -1 -5 6.30 4.80 17 -1 -5 -0.80 5.00 17 1 -4 2.60 4.00 -17 1 4 2.00 0.50 17 1 -4 -1.00 4.80 17 -1 -4 5.50 5.10 17 -1 -4 5.10 4.00 -17 1 3 236.08 14.00 17 1 -3 210.38 16.50 17 1 -3 219.58 16.90 17 -1 -3 237.08 17.70 17 -1 -3 236.38 16.60 17 1 -2 1.00 3.30 -17 1 2 1.50 0.50 17 1 -2 -2.10 3.70 17 -1 -2 0.50 3.30 17 -1 -2 4.60 3.80 17 1 -1 45.20 5.50 17 1 -1 42.70 5.50 -17 1 1 51.99 3.20 17 -1 -1 58.19 7.00 -17 1 0 16.90 1.30 17 1 0 19.90 4.00 17 -1 0 18.00 3.90 17 1 1 41.20 4.90 -17 1 -1 49.50 3.00 17 -1 1 45.70 5.80 -17 1 -2 3.50 0.50 17 -1 2 1.00 2.50 17 2 -10 6.40 5.40 17 2 -10 7.30 8.30 17 -2 -10 9.30 5.80 17 -2 -10 11.70 5.70 17 2 -9 9.10 5.80 17 2 -9 6.20 9.90 -17 2 9 12.10 1.00 17 -2 -9 13.30 6.40 17 -2 -9 13.60 7.50 17 -2 -9 9.60 5.40 17 2 -8 65.39 9.70 17 2 -8 73.69 9.20 -17 2 8 63.69 3.90 17 -2 -8 74.19 10.00 17 -2 -8 44.80 9.10 -17 -2 8 62.69 3.90 17 -2 -8 49.80 7.80 17 2 -7 -2.30 5.00 17 2 -7 12.20 6.80 -17 2 7 2.00 0.40 17 -2 -7 1.30 4.70 17 -2 -7 -2.10 4.90 17 -2 -7 7.50 6.60 -17 -2 7 1.40 0.40 -17 2 6 7.20 0.70 17 2 -6 9.40 6.30 17 2 -6 10.50 5.50 17 -2 -6 10.30 6.70 17 -2 -6 7.90 4.60 -17 -2 6 8.60 0.70 17 -2 -6 6.20 5.00 -17 2 5 22.90 1.60 17 2 -5 18.60 6.10 17 2 -5 22.50 5.50 17 -2 -5 20.40 5.20 17 -2 -5 22.50 6.10 -17 2 4 290.57 17.30 17 2 -4 277.97 20.10 17 -2 -4 298.57 21.50 17 -2 -4 260.57 19.80 17 2 -3 31.00 5.10 -17 2 3 41.00 2.60 17 -2 -3 47.60 6.10 17 -2 -3 35.80 6.70 17 2 -2 710.73 47.20 -17 2 2 744.53 45.80 17 -2 -2 769.62 47.60 17 -2 -2 786.62 48.60 -17 2 1 6.40 0.60 17 -2 -1 9.40 4.00 -17 2 0 97.59 6.10 17 -2 0 99.19 9.00 -17 2 -1 101.09 6.30 17 -2 1 100.89 8.70 -17 3 9 2.50 0.50 17 3 -9 -1.00 5.50 17 -3 -9 5.40 4.90 17 -3 -9 4.70 6.20 -17 3 8 13.90 1.10 17 3 -8 12.10 5.80 17 -3 -8 12.50 5.70 -17 -3 8 13.90 1.20 17 -3 -8 12.80 6.90 17 -3 -8 20.10 5.80 17 3 -7 23.30 6.00 -17 3 7 25.60 1.70 17 -3 -7 34.50 6.20 17 -3 -7 26.90 5.90 17 -3 -7 21.00 6.80 -17 -3 7 24.40 1.70 -17 3 6 16.30 1.20 17 3 -6 10.00 5.20 17 -3 -6 20.60 5.20 17 -3 -6 18.00 6.70 17 -3 -6 12.80 4.90 17 3 -5 101.79 10.70 -17 3 5 105.79 6.40 17 -3 -5 100.39 11.80 17 -3 -5 93.79 9.50 17 -3 -5 105.99 10.00 17 3 -4 211.88 16.30 -17 3 4 230.88 13.50 17 -3 -4 230.18 16.20 17 -3 -4 199.48 15.50 17 -3 -4 223.78 17.80 17 3 -3 303.07 21.30 -17 3 3 324.47 19.30 17 -3 -3 325.27 22.90 17 -3 -3 304.07 21.30 -17 3 2 441.36 28.60 17 -3 -2 467.45 31.50 17 -3 -2 509.05 30.60 -17 3 1 272.47 16.80 17 -3 -1 279.57 19.60 17 -3 0 0.70 3.20 -17 4 9 1.40 0.40 17 -4 -9 -4.60 4.90 -17 4 8 12.70 1.30 17 4 -8 4.50 8.80 17 -4 -8 5.10 4.50 17 -4 -8 5.80 6.10 17 4 -7 35.80 6.80 -17 4 7 27.80 1.90 17 -4 -7 18.70 5.20 17 -4 -7 23.00 7.00 17 -4 -7 37.70 6.20 -17 4 6 8.20 0.70 17 4 -6 7.40 5.10 17 -4 -6 -0.30 5.50 17 -4 -6 15.40 4.70 17 -4 -6 1.70 3.80 -17 4 5 136.19 8.10 17 4 -5 112.49 11.70 17 -4 -5 140.79 11.00 17 -4 -5 136.19 12.90 17 -4 -5 117.89 10.90 -17 4 4 109.59 6.60 17 4 -4 109.79 10.60 17 -4 -4 99.89 9.40 17 -4 -4 111.39 11.60 17 -4 -4 100.19 9.40 -17 4 3 254.27 15.40 17 -4 -3 260.07 17.50 17 -4 -3 267.87 19.20 17 -4 -3 231.68 17.20 -17 4 2 38.80 2.70 17 -4 -2 50.89 6.60 17 -4 -2 48.80 6.60 -17 4 1 0.30 0.40 17 -4 -1 0.00 3.40 -17 4 0 33.20 2.20 17 -4 0 28.70 4.70 -17 5 7 0.30 0.60 17 5 -7 0.60 5.70 17 -5 -7 -0.90 4.50 17 -5 -7 4.30 6.10 17 -5 -7 6.70 4.30 -17 5 6 4.40 0.50 17 5 -6 -0.10 5.80 17 -5 -6 2.50 3.90 17 -5 -6 2.30 5.10 -17 5 5 11.30 1.00 17 -5 -5 14.20 5.90 17 -5 -5 13.10 3.90 -17 5 4 157.68 9.80 17 -5 -4 164.18 12.20 17 -5 -4 156.48 13.60 -17 5 3 26.30 1.80 17 -5 -3 32.60 5.90 17 -5 -3 23.30 4.20 -17 5 2 114.69 6.90 17 -5 -2 106.69 8.70 17 -5 -2 103.29 10.10 -17 5 1 1.40 0.60 17 -5 -1 3.90 3.10 -18 0 9 1.00 0.50 18 0 -9 -1.50 6.80 18 0 -8 335.67 31.40 -18 0 8 382.26 23.40 18 0 -8 416.16 26.90 18 0 -7 -0.90 4.50 18 0 -7 4.40 6.10 -18 0 7 1.00 0.40 -18 0 6 889.61 53.99 18 0 -6 879.61 56.59 18 0 -6 892.91 57.39 18 0 -5 -1.50 5.00 -18 0 5 0.10 0.40 18 0 -5 2.00 4.30 -18 0 4 322.07 20.10 18 0 -4 335.27 22.60 18 0 -4 337.47 23.10 18 0 -3 -1.30 4.00 -18 0 3 0.00 0.40 18 0 -3 3.10 3.30 18 0 -2 153.48 11.80 18 0 -2 165.58 15.00 -18 0 2 153.98 9.60 -18 0 1 0.60 0.40 18 0 -1 -1.10 3.40 -18 0 0 45.80 3.10 18 0 0 57.09 6.40 -18 1 9 22.70 1.60 18 1 -9 24.70 7.80 18 -1 -9 16.40 6.60 -18 1 8 5.40 0.60 18 1 -8 3.90 6.80 18 1 -8 5.70 4.90 18 -1 -8 6.20 5.00 -18 -1 8 5.70 0.60 18 -1 -8 8.90 6.80 -18 1 7 3.10 0.50 18 1 -7 0.70 4.50 18 -1 -7 6.80 5.00 18 -1 -7 -6.00 5.90 -18 1 6 157.98 9.60 18 1 -6 142.59 14.00 18 1 -6 161.98 13.40 -18 -1 6 155.08 9.60 18 -1 -6 156.38 13.10 18 -1 -6 162.58 14.70 -18 1 5 2.10 0.50 18 1 -5 4.40 5.00 18 1 -5 5.80 4.10 -18 -1 5 2.40 0.50 18 -1 -5 4.20 4.80 18 -1 -5 1.30 3.70 -18 1 4 14.60 1.10 18 1 -4 9.80 5.30 18 1 -4 7.90 4.20 18 -1 -4 11.80 4.00 -18 -1 4 14.50 1.10 18 -1 -4 9.30 4.80 18 1 -3 2.60 5.80 18 1 -3 -0.20 3.40 -18 1 3 1.00 0.40 18 -1 -3 -2.50 3.60 18 -1 -3 1.20 3.30 -18 1 2 43.30 2.60 18 1 -2 37.80 5.50 18 1 -2 31.20 6.20 18 -1 -2 41.60 5.70 18 -1 -2 36.30 4.90 -18 1 1 -0.10 0.40 18 1 -1 2.20 4.50 18 -1 -1 -4.80 3.40 18 2 -8 0.50 7.70 -18 2 8 5.00 0.60 18 -2 -8 6.40 5.90 -18 -2 8 5.90 0.60 18 -2 -8 3.60 4.30 18 2 -7 29.70 5.90 18 2 -7 39.70 9.10 -18 2 7 37.90 2.30 -18 -2 7 35.20 2.40 18 -2 -7 42.00 8.00 18 -2 -7 23.20 5.50 18 -2 -7 23.10 7.50 -18 2 6 12.90 1.10 18 2 -6 6.60 4.80 18 -2 -6 8.60 4.40 18 -2 -6 13.30 6.30 -18 -2 6 13.80 1.00 -18 2 5 0.30 0.40 18 2 -5 4.40 4.30 -18 -2 5 0.10 0.40 18 -2 -5 -2.40 3.70 18 -2 -5 -4.60 4.70 -18 2 4 27.70 1.90 18 -2 -4 28.90 6.00 18 -2 -4 21.30 4.40 -18 2 3 467.05 28.60 18 -2 -3 480.55 30.50 18 -2 -3 459.85 31.30 -18 2 2 2.30 0.50 18 -2 -2 -0.80 3.60 -18 2 1 713.53 41.80 18 -2 -1 650.03 44.20 -18 3 7 1.20 0.60 18 3 -7 3.20 5.00 18 -3 -7 2.50 4.80 18 -3 -7 0.70 5.70 18 -3 -7 2.30 4.20 -18 -3 7 1.50 0.40 -18 3 6 -0.20 0.40 18 3 -6 0.00 4.70 -18 -3 6 0.70 0.70 18 -3 -6 3.80 5.50 18 -3 -6 3.20 3.70 18 -3 -6 -0.10 4.70 18 3 -5 78.19 9.40 -18 3 5 84.99 5.30 18 -3 -5 98.99 10.70 18 -3 -5 86.29 8.50 18 3 -4 60.39 6.80 -18 3 4 67.99 4.20 18 -3 -4 63.09 7.80 18 -3 -4 67.19 7.30 -18 3 3 0.30 0.40 18 -3 -3 2.10 3.20 18 -3 -3 0.20 3.80 -18 3 2 0.00 0.40 18 4 -5 -0.40 4.70 18 -4 -5 0.70 4.00 -18 4 4 28.30 2.00 18 -4 -4 14.90 7.30 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 52628 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group B1 B 0.64337(9) 0.04932(11) 0.75521(11) 0.0249(3) Uani 1 1 d . . . . . B2 B 0.85008(9) 0.69474(11) 0.73262(11) 0.0258(3) Uani 1 1 d . . . . . C1 C 0.75822(7) 0.19023(10) 0.86600(9) 0.0251(3) Uani 1 1 d . . . . . H1 H 0.772428 0.133517 0.924277 0.030 Uiso 1 1 calc R U . . . C2 C 0.79924(7) 0.29761(10) 0.88228(9) 0.0259(3) Uani 1 1 d . . . . . H2 H 0.840786 0.315262 0.951591 0.031 Uiso 1 1 calc R U . . . C3 C 0.78171(7) 0.38823(9) 0.79619(9) 0.0226(3) Uani 1 1 d . . . . . C4 C 0.71968(7) 0.35022(9) 0.69163(9) 0.0227(3) Uani 1 1 d . . . . . C5 C 0.68017(7) 0.24101(10) 0.67990(9) 0.0245(3) Uani 1 1 d . . . . . H5 H 0.640636 0.219195 0.610435 0.029 Uiso 1 1 calc R U . . . C6 C 0.81979(7) 0.49852(10) 0.80804(9) 0.0250(3) Uani 1 1 d . . . . . H6 H 0.859291 0.520796 0.877386 0.030 Uiso 1 1 calc R U . . . C7 C 0.74356(8) 0.54699(10) 0.62069(9) 0.0273(3) Uani 1 1 d . . . . . H7 H 0.730769 0.602379 0.561446 0.033 Uiso 1 1 calc R U . . . C8 C 0.70388(8) 0.43883(10) 0.60443(9) 0.0267(3) Uani 1 1 d . . . . . H8 H 0.664419 0.419343 0.534273 0.032 Uiso 1 1 calc R U . . . C9 C 0.94275(8) 0.84942(10) 0.80895(10) 0.0280(3) Uani 1 1 d . . . . . C10 C 1.04292(9) 0.86548(12) 0.85417(11) 0.0385(3) Uani 1 1 d . . . . . H10A H 1.062284 0.849961 0.932902 0.058 Uiso 1 1 calc R U . . . H10B H 1.058802 0.948482 0.840579 0.058 Uiso 1 1 calc R U . . . H10C H 1.072609 0.808413 0.818344 0.058 Uiso 1 1 calc R U . . . C11 C 0.89583(10) 0.92322(11) 0.87443(11) 0.0383(3) Uani 1 1 d . . . . . H11A H 0.831096 0.910740 0.844980 0.057 Uiso 1 1 calc R U . . . H11B H 0.909482 1.009236 0.869695 0.057 Uiso 1 1 calc R U . . . H11C H 0.916623 0.897370 0.950901 0.057 Uiso 1 1 calc R U . . . C12 C 0.90266(8) 0.86788(10) 0.68293(10) 0.0305(3) Uani 1 1 d . . . . . C13 C 0.96509(10) 0.82807(14) 0.62033(12) 0.0442(3) Uani 1 1 d . . . . . H13A H 0.989456 0.747973 0.645913 0.066 Uiso 1 1 calc R U . . . H13B H 1.014169 0.886380 0.632254 0.066 Uiso 1 1 calc R U . . . H13C H 0.932042 0.824101 0.542302 0.066 Uiso 1 1 calc R U . . . C14 C 0.86629(11) 0.99345(12) 0.64807(12) 0.0461(4) Uani 1 1 d . . . . . H14A H 0.838004 0.994971 0.568825 0.069 Uiso 1 1 calc R U . . . H14B H 0.915374 1.052207 0.668306 0.069 Uiso 1 1 calc R U . . . H14C H 0.821965 1.014414 0.684521 0.069 Uiso 1 1 calc R U . . . C15 C 0.58504(8) -0.12206(10) 0.80133(10) 0.0291(3) Uani 1 1 d . . . . . C16 C 0.52569(9) -0.08292(13) 0.86820(11) 0.0389(3) Uani 1 1 d . . . . . H16A H 0.559471 -0.087092 0.945988 0.058 Uiso 1 1 calc R U . . . H16B H 0.473704 -0.136731 0.852863 0.058 Uiso 1 1 calc R U . . . H16C H 0.505485 0.000390 0.849029 0.058 Uiso 1 1 calc R U . . . C17 C 0.61814(10) -0.25032(11) 0.82952(12) 0.0430(4) Uani 1 1 d . . . . . H17A H 0.661476 -0.270529 0.791400 0.065 Uiso 1 1 calc R U . . . H17B H 0.567490 -0.306475 0.806955 0.065 Uiso 1 1 calc R U . . . H17C H 0.646873 -0.256953 0.908462 0.065 Uiso 1 1 calc R U . . . C18 C 0.54265(8) -0.09651(10) 0.67642(10) 0.0294(3) Uani 1 1 d . . . . . C19 C 0.44158(9) -0.10324(12) 0.63485(11) 0.0401(3) Uani 1 1 d . . . . . H19A H 0.416280 -0.046482 0.675931 0.060 Uiso 1 1 calc R U . . . H19B H 0.422237 -0.185701 0.644469 0.060 Uiso 1 1 calc R U . . . H19C H 0.420776 -0.081906 0.557246 0.060 Uiso 1 1 calc R U . . . C20 C 0.58310(11) -0.17116(12) 0.60453(11) 0.0435(4) Uani 1 1 d . . . . . H20A H 0.561593 -0.140733 0.529481 0.065 Uiso 1 1 calc R U . . . H20B H 0.565383 -0.256053 0.605993 0.065 Uiso 1 1 calc R U . . . H20C H 0.648438 -0.164894 0.631685 0.065 Uiso 1 1 calc R U . . . N1 N 0.69501(6) 0.15723(8) 0.76668(8) 0.0252(2) Uani 1 1 d . . . . . N2 N 0.80332(6) 0.58262(8) 0.72130(8) 0.0265(2) Uani 1 1 d . . . . . O1 O 0.66249(5) -0.04098(7) 0.83140(7) 0.0281(2) Uani 1 1 d . . . . . O2 O 0.56946(5) 0.02918(7) 0.66714(7) 0.0290(2) Uani 1 1 d . . . . . O3 O 0.92145(5) 0.72199(7) 0.82177(7) 0.0287(2) Uani 1 1 d . . . . . O4 O 0.82791(5) 0.78273(7) 0.65433(7) 0.0309(2) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 B1 0.0259(6) 0.0217(6) 0.0282(7) -0.0021(5) 0.0100(5) -0.0012(5) B2 0.0268(6) 0.0209(6) 0.0295(7) 0.0009(5) 0.0081(5) 0.0002(5) C1 0.0261(6) 0.0234(5) 0.0244(6) 0.0023(4) 0.0055(5) 0.0001(4) C2 0.0278(6) 0.0235(5) 0.0241(6) 0.0000(4) 0.0045(5) -0.0015(4) C3 0.0218(5) 0.0213(5) 0.0245(6) -0.0016(4) 0.0070(4) -0.0001(4) C4 0.0216(5) 0.0219(5) 0.0248(6) -0.0010(4) 0.0072(4) 0.0009(4) C5 0.0251(6) 0.0230(5) 0.0241(6) -0.0013(4) 0.0055(5) -0.0012(4) C6 0.0278(6) 0.0213(5) 0.0239(6) 0.0003(4) 0.0049(5) -0.0007(4) C7 0.0283(6) 0.0251(6) 0.0257(6) 0.0042(4) 0.0043(5) 0.0002(4) C8 0.0271(6) 0.0261(6) 0.0243(6) 0.0002(4) 0.0040(5) -0.0015(4) C9 0.0318(6) 0.0189(5) 0.0317(6) 0.0010(4) 0.0072(5) -0.0042(4) C10 0.0347(7) 0.0361(7) 0.0403(7) -0.0013(6) 0.0051(6) -0.0081(5) C11 0.0463(8) 0.0302(6) 0.0391(8) -0.0047(5) 0.0141(6) -0.0006(5) C12 0.0340(6) 0.0224(5) 0.0332(7) 0.0016(5) 0.0076(5) -0.0078(5) C13 0.0475(8) 0.0492(8) 0.0390(8) -0.0053(6) 0.0177(6) -0.0124(6) C14 0.0621(9) 0.0269(6) 0.0435(8) 0.0100(6) 0.0076(7) -0.0037(6) C15 0.0311(6) 0.0246(6) 0.0311(6) -0.0017(5) 0.0089(5) -0.0105(5) C16 0.0381(7) 0.0482(8) 0.0331(7) -0.0052(6) 0.0149(6) -0.0136(6) C17 0.0554(9) 0.0263(6) 0.0451(8) 0.0051(6) 0.0121(7) -0.0076(6) C18 0.0360(7) 0.0223(6) 0.0300(6) -0.0032(5) 0.0106(5) -0.0104(5) C19 0.0383(7) 0.0410(7) 0.0366(7) -0.0027(6) 0.0051(6) -0.0149(6) C20 0.0633(9) 0.0338(7) 0.0382(7) -0.0093(6) 0.0224(7) -0.0071(6) N1 0.0264(5) 0.0209(5) 0.0269(5) -0.0001(4) 0.0062(4) -0.0027(4) N2 0.0291(5) 0.0214(5) 0.0266(5) 0.0016(4) 0.0051(4) -0.0020(4) O1 0.0274(4) 0.0243(4) 0.0307(5) 0.0019(3) 0.0060(3) -0.0065(3) O2 0.0315(4) 0.0235(4) 0.0295(5) 0.0008(3) 0.0058(4) -0.0075(3) O3 0.0318(5) 0.0196(4) 0.0309(5) 0.0029(3) 0.0043(4) -0.0038(3) O4 0.0307(5) 0.0239(4) 0.0331(5) 0.0055(3) 0.0024(4) -0.0050(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0137 0.0067 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0070 0.0029 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0241 0.0134 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0389 0.0241 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 B1 N1 122.98(11) . . ? O1 B1 O2 114.80(10) . . ? O2 B1 N1 122.22(11) . . ? O3 B2 N2 122.73(11) . . ? O4 B2 N2 122.45(11) . . ? O4 B2 O3 114.81(10) . . ? C2 C1 H1 118.5 . . ? C2 C1 N1 123.05(10) . . ? N1 C1 H1 118.5 . . ? C1 C2 H2 119.3 . . ? C1 C2 C3 121.47(10) . . ? C3 C2 H2 119.3 . . ? C2 C3 C4 114.90(10) . . ? C6 C3 C2 124.26(10) . . ? C6 C3 C4 120.83(11) . . ? C5 C4 C3 121.07(11) . . ? C5 C4 C8 123.70(11) . . ? C8 C4 C3 115.23(10) . . ? C4 C5 H5 118.6 . . ? C4 C5 N1 122.72(10) . . ? N1 C5 H5 118.6 . . ? C3 C6 H6 118.7 . . ? C3 C6 N2 122.57(10) . . ? N2 C6 H6 118.7 . . ? C8 C7 H7 118.5 . . ? C8 C7 N2 122.96(10) . . ? N2 C7 H7 118.5 . . ? C4 C8 H8 119.3 . . ? C7 C8 C4 121.44(11) . . ? C7 C8 H8 119.3 . . ? C10 C9 C11 110.44(10) . . ? C10 C9 C12 115.09(10) . . ? C11 C9 C12 113.42(10) . . ? O3 C9 C10 108.40(9) . . ? O3 C9 C11 106.63(10) . . ? O3 C9 C12 102.06(8) . . ? C9 C10 H10A 109.5 . . ? C9 C10 H10B 109.5 . . ? C9 C10 H10C 109.5 . . ? H10A C10 H10B 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C9 C11 H11A 109.5 . . ? C9 C11 H11B 109.5 . . ? C9 C11 H11C 109.5 . . ? H11A C11 H11B 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C13 C12 C9 113.25(11) . . ? C13 C12 C14 110.81(12) . . ? C14 C12 C9 114.96(10) . . ? O4 C12 C9 102.35(9) . . ? O4 C12 C13 106.33(10) . . ? O4 C12 C14 108.31(10) . . ? C12 C13 H13A 109.5 . . ? C12 C13 H13B 109.5 . . ? C12 C13 H13C 109.5 . . ? H13A C13 H13B 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? C12 C14 H14A 109.5 . . ? C12 C14 H14B 109.5 . . ? C12 C14 H14C 109.5 . . ? H14A C14 H14B 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C16 C15 C17 110.91(11) . . ? C16 C15 C18 113.02(10) . . ? C17 C15 C18 114.90(10) . . ? O1 C15 C16 106.40(9) . . ? O1 C15 C17 108.22(10) . . ? O1 C15 C18 102.58(8) . . ? C15 C16 H16A 109.5 . . ? C15 C16 H16B 109.5 . . ? C15 C16 H16C 109.5 . . ? H16A C16 H16B 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C15 C17 H17A 109.5 . . ? C15 C17 H17B 109.5 . . ? C15 C17 H17C 109.5 . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C19 C18 C15 115.02(10) . . ? C19 C18 C20 110.39(11) . . ? C20 C18 C15 113.78(11) . . ? O2 C18 C15 102.26(8) . . ? O2 C18 C19 108.31(10) . . ? O2 C18 C20 106.25(9) . . ? C18 C19 H19A 109.5 . . ? C18 C19 H19B 109.5 . . ? C18 C19 H19C 109.5 . . ? H19A C19 H19B 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C18 C20 H20A 109.5 . . ? C18 C20 H20B 109.5 . . ? C18 C20 H20C 109.5 . . ? H20A C20 H20B 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C1 N1 B1 122.16(10) . . ? C1 N1 C5 116.64(9) . . ? C5 N1 B1 121.05(10) . . ? C6 N2 B2 121.80(10) . . ? C7 N2 B2 121.08(10) . . ? C7 N2 C6 116.96(9) . . ? B1 O1 C15 105.99(9) . . ? B1 O2 C18 106.15(9) . . ? B2 O3 C9 105.83(9) . . ? B2 O4 C12 105.62(9) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag B1 N1 1.4238(15) . ? B1 O1 1.3662(15) . ? B1 O2 1.3692(16) . ? B2 N2 1.4244(15) . ? B2 O3 1.3690(15) . ? B2 O4 1.3663(15) . ? C1 H1 0.9500 . ? C1 C2 1.3354(15) . ? C1 N1 1.4050(15) . ? C2 H2 0.9500 . ? C2 C3 1.4558(16) . ? C3 C4 1.4602(16) . ? C3 C6 1.3451(15) . ? C4 C5 1.3438(15) . ? C4 C8 1.4524(16) . ? C5 H5 0.9500 . ? C5 N1 1.4141(14) . ? C6 H6 0.9500 . ? C6 N2 1.4141(14) . ? C7 H7 0.9500 . ? C7 C8 1.3340(16) . ? C7 N2 1.4026(15) . ? C8 H8 0.9500 . ? C9 C10 1.5114(17) . ? C9 C11 1.5172(17) . ? C9 C12 1.5631(17) . ? C9 O3 1.4678(13) . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C12 C13 1.5141(19) . ? C12 C14 1.5146(17) . ? C12 O4 1.4607(13) . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 C16 1.5141(18) . ? C15 C17 1.5144(17) . ? C15 C18 1.5660(17) . ? C15 O1 1.4640(13) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 C19 1.5138(18) . ? C18 C20 1.5176(17) . ? C18 O2 1.4664(13) . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C1 C2 C3 C4 -2.43(16) . . . . ? C1 C2 C3 C6 178.93(11) . . . . ? C2 C1 N1 B1 -171.47(11) . . . . ? C2 C1 N1 C5 4.05(16) . . . . ? C2 C3 C4 C5 2.57(16) . . . . ? C2 C3 C4 C8 -178.27(9) . . . . ? C2 C3 C6 N2 177.81(10) . . . . ? C3 C4 C5 N1 0.58(17) . . . . ? C3 C4 C8 C7 -0.35(16) . . . . ? C3 C6 N2 B2 -174.42(11) . . . . ? C3 C6 N2 C7 0.94(16) . . . . ? C4 C3 C6 N2 -0.75(17) . . . . ? C4 C5 N1 B1 171.69(10) . . . . ? C4 C5 N1 C1 -3.88(16) . . . . ? C5 C4 C8 C7 178.79(11) . . . . ? C6 C3 C4 C5 -178.74(10) . . . . ? C6 C3 C4 C8 0.42(16) . . . . ? C8 C4 C5 N1 -178.51(10) . . . . ? C8 C7 N2 B2 174.52(11) . . . . ? C8 C7 N2 C6 -0.87(17) . . . . ? C9 C12 O4 B2 -25.87(11) . . . . ? C10 C9 C12 C13 33.14(14) . . . . ? C10 C9 C12 C14 -95.66(14) . . . . ? C10 C9 C12 O4 147.17(10) . . . . ? C10 C9 O3 B2 -145.27(11) . . . . ? C11 C9 C12 C13 161.68(10) . . . . ? C11 C9 C12 C14 32.88(15) . . . . ? C11 C9 C12 O4 -84.28(11) . . . . ? C11 C9 O3 B2 95.82(11) . . . . ? C12 C9 O3 B2 -23.39(12) . . . . ? C13 C12 O4 B2 93.16(12) . . . . ? C14 C12 O4 B2 -147.71(11) . . . . ? C15 C18 O2 B1 22.81(11) . . . . ? C16 C15 C18 C19 -31.24(14) . . . . ? C16 C15 C18 C20 -159.98(10) . . . . ? C16 C15 C18 O2 85.90(11) . . . . ? C16 C15 O1 B1 -95.26(11) . . . . ? C17 C15 C18 C19 97.44(13) . . . . ? C17 C15 C18 C20 -31.30(14) . . . . ? C17 C15 C18 O2 -145.42(10) . . . . ? C17 C15 O1 B1 145.49(10) . . . . ? C18 C15 O1 B1 23.65(11) . . . . ? C19 C18 O2 B1 144.66(10) . . . . ? C20 C18 O2 B1 -96.74(11) . . . . ? N1 B1 O1 C15 168.60(11) . . . . ? N1 B1 O2 C18 171.99(10) . . . . ? N1 C1 C2 C3 -0.89(18) . . . . ? N2 B2 O3 C9 -172.84(11) . . . . ? N2 B2 O4 C12 -166.62(11) . . . . ? N2 C7 C8 C4 0.61(18) . . . . ? O1 B1 N1 C1 -13.02(17) . . . . ? O1 B1 N1 C5 171.65(10) . . . . ? O1 B1 O2 C18 -9.02(13) . . . . ? O1 C15 C18 C19 -145.38(10) . . . . ? O1 C15 C18 C20 85.88(11) . . . . ? O1 C15 C18 O2 -28.24(11) . . . . ? O2 B1 N1 C1 165.89(10) . . . . ? O2 B1 N1 C5 -9.44(17) . . . . ? O2 B1 O1 C15 -10.38(13) . . . . ? O3 B2 N2 C6 8.77(18) . . . . ? O3 B2 N2 C7 -166.40(11) . . . . ? O3 B2 O4 C12 12.41(14) . . . . ? O3 C9 C12 C13 -84.03(11) . . . . ? O3 C9 C12 C14 147.18(11) . . . . ? O3 C9 C12 O4 30.01(11) . . . . ? O4 B2 N2 C6 -172.28(10) . . . . ? O4 B2 N2 C7 12.55(18) . . . . ? O4 B2 O3 C9 8.13(14) . . . . ?