#------------------------------------------------------------------------------ #$Date: 2021-04-28 04:53:10 +0300 (Wed, 28 Apr 2021) $ #$Revision: 264609 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/72/7707209.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7707209 loop_ _publ_author_name 'Tatarin, Sergei V.' 'Kalle, Paulina' 'Taydakov, Ilya V.' 'Varaksina, Evgenia' 'Korshunov, Vladislav M.' 'Bezzubov, Stanislav' _publ_section_title ; Sterically hindered phenanthroimidazole ligands drive structural flexibility and facile ligand exchange in cyclometalated iridium(III) complexes ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT00820J _journal_year 2021 _chemical_formula_moiety 'C108 H64 Cl6 Ir2 N8' _chemical_formula_sum 'C108 H64 Cl6 Ir2 N8' _chemical_formula_weight 2070.77 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _audit_creation_date 2020-12-22 _audit_creation_method ; Olex2 1.3 (compiled Nov 21 2019 18:26:39 for OlexSys, GUI svn.r6003) ; _audit_update_record ; 2020-12-23 deposited with the CCDC. 2021-04-27 downloaded from the CCDC. ; _cell_angle_alpha 69.415(2) _cell_angle_beta 64.151(2) _cell_angle_gamma 79.109(2) _cell_formula_units_Z 2 _cell_length_a 17.8595(11) _cell_length_b 18.4756(10) _cell_length_c 19.4513(11) _cell_measurement_reflns_used 9812 _cell_measurement_temperature 150.0 _cell_measurement_theta_max 26.39 _cell_measurement_theta_min 2.23 _cell_volume 5402.4(5) _computing_cell_refinement 'APEX3 v.2017.3_0 (Bruker AXS, 2017)' _computing_data_collection 'APEX3 v.2017.3_0 (Bruker AXS, 2017)' _computing_data_reduction 'SAINT v8.38A (Bruker AXS, 2016)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'olex2.solve 1.3 (Bourhis et al., 2015)' _diffrn_ambient_temperature 150.0 _diffrn_detector 'Bruker PHOTON III CMOS' _diffrn_detector_area_resol_mean 10.4 _diffrn_detector_type 'CMOS sensor' _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.988 _diffrn_measurement_device '3-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 Venture' _diffrn_measurement_method \w-scan _diffrn_radiation_monochromator 'focusing mirrors' _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0508 _diffrn_reflns_av_unetI/netI 0.0638 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.988 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 58725 _diffrn_reflns_point_group_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.988 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.427 _diffrn_reflns_theta_min 1.938 _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_type 'Incoatec I\mS microsource' _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 2.655 _exptl_absorpt_correction_T_max 0.7454 _exptl_absorpt_correction_T_min 0.5281 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0901 before and 0.0571 after correction. The Ratio of minimum to maximum transmission is 0.7085. The \l/2 correction factor is Not present. ; _exptl_crystal_colour yellow _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.273 _exptl_crystal_description plate _exptl_crystal_F_000 2048 _exptl_crystal_recrystallization_method 'Re-crystallisation from solvent: CH2Cl2' _exptl_crystal_size_max 0.35 _exptl_crystal_size_mid 0.20 _exptl_crystal_size_min 0.07 _refine_diff_density_max 3.935 _refine_diff_density_min -2.828 _refine_diff_density_rms 0.167 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.045 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 1117 _refine_ls_number_reflns 21930 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.045 _refine_ls_R_factor_all 0.0612 _refine_ls_R_factor_gt 0.0485 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0849P)^2^+1.6962P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1327 _refine_ls_wR_factor_ref 0.1405 _reflns_Friedel_coverage 0.000 _reflns_number_gt 17400 _reflns_number_total 21930 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt00820j2.cif _cod_data_source_block st242_dc _cod_depositor_comments ; The following automatic conversions were performed: data item '_diffrn_radiation_probe' value 'X-ray' was changed to 'x-ray' in accordance with the /home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 last updated on 2011-04-26. Automatic conversion script Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas ; _cod_database_code 7707209 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _computing.bruker_data_scaling 'SADABS V2012/1 (Bruker AXS Inc.)' _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Aromatic/amide H refined with riding coordinates: C00U(H00U), C014(H014), C015(H015), C018(H018), C01A(H01A), C01F(H01F), C01H(H01H), C01Q(H01Q), C01R(H01R), C01U(H01U), C01Z(H01Z), C024(H024), C025(H025), C028(H028), C029(H029), C02A(H02A), C02C(H02C), C02D(H02D), C02E(H02E), C02G(H02G), C02H(H02H), C02I(H02I), C02J(H02J), C02L(H02L), C02M(H02M), C02O(H02O), C02P(H02P), C02Q(H02Q), C02R(H02R), C02S(H02S), C02U(H02U), C02V(H02V), C02W(H02W), C02Y(H02Y), C02Z(H02Z), C030(H030), C031(H031), C032(H032), C033(H033), C034(H034), C035(H035), C036(H036), C037(H037), C038(H038), C039(H039), C03B(H03B), C03C(H03C), C03D(H03D), C03E(H03E), C03F(H03F), C03H(H03H), C03I(H03I), C03J(H03J), C03K(H03K), C03L(H03L), C03M(H03M), C03N(H03N), C03P(H03P), C03Q(H03Q), C03R(H03R), C03S(H03S), C03T(H03T), C03U(H03U), C03W(H03W) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL st242_dc_a.res in P-1 st242_dc.res created by SHELXL-2018/3 at 16:20:25 on 22-Dec-2020 REM Old TITL ST242_dc in P-1 REM SHELXT solution in P-1 REM R1 0.118, Rweak 0.006, Alpha 0.052, Orientation as input REM Formula found by SHELXT: C108 N22 Cl13 Ir2 CELL 0.71073 17.8595 18.4756 19.4513 69.415 64.151 79.109 ZERR 2 0.0011 0.001 0.0011 0.002 0.002 0.002 LATT 1 SFAC C H Cl Ir N UNIT 216 128 12 4 16 L.S. 8 PLAN 5 TEMP -123.15 CONF BOND $H list 4 MORE -1 ABIN fmap 2 53 acta OMIT 2 -2 3 OMIT 2 -2 4 OMIT 1 1 0 OMIT -3 0 3 OMIT 1 1 1 OMIT 2 -4 3 OMIT -2 1 0 OMIT 2 2 1 OMIT 3 0 5 OMIT -1 2 0 OMIT 3 2 1 OMIT 1 2 1 OMIT 3 3 2 OMIT 2 5 3 OMIT 1 5 2 OMIT 4 0 4 OMIT 2 1 1 REM REM REM WGHT 0.084900 1.696200 FVAR 0.14721 IR01 4 0.147362 0.699097 0.454166 11.00000 0.01701 0.01613 = 0.02118 -0.00709 -0.00935 -0.00067 IR02 4 0.367319 0.785986 0.324065 11.00000 0.01742 0.01831 = 0.02106 -0.00782 -0.00931 -0.00165 CL03 3 0.214594 0.827392 0.373307 11.00000 0.01787 0.01811 = 0.02836 -0.00765 -0.01082 -0.00035 CL04 3 0.299927 0.658274 0.408042 11.00000 0.01921 0.01742 = 0.02622 -0.00686 -0.00963 0.00046 CL05 3 0.051208 0.446849 0.744479 11.00000 0.05305 0.03163 = 0.02719 -0.00072 -0.01672 -0.01214 CL06 3 -0.149970 0.773239 0.396851 11.00000 0.03388 0.04433 = 0.06560 -0.02693 -0.03458 0.00623 CL07 3 0.674603 0.704648 0.089843 11.00000 0.03121 0.06307 = 0.04011 -0.02967 -0.00225 -0.00083 CL08 3 0.482158 1.075066 0.279150 11.00000 0.10940 0.03978 = 0.07694 -0.00959 -0.05587 -0.03196 N00I 5 0.356435 0.802557 0.218228 11.00000 0.02081 0.02100 = 0.02129 -0.00774 -0.00505 -0.00010 N00J 5 0.148874 0.655095 0.367711 11.00000 0.01813 0.01780 = 0.02302 -0.00651 -0.00956 -0.00182 N00L 5 0.399093 0.771533 0.420596 11.00000 0.01874 0.02255 = 0.02388 -0.00956 -0.01371 0.00276 N00N 5 0.160290 0.549509 0.333600 11.00000 0.02560 0.01970 = 0.03288 -0.01139 -0.01505 0.00184 N00P 5 0.121929 0.738392 0.551509 11.00000 0.01908 0.01578 = 0.02338 -0.00569 -0.00864 0.00008 N00Q 5 0.044123 0.820138 0.618942 11.00000 0.02505 0.02137 = 0.02648 -0.00843 -0.01167 0.00096 N00R 5 0.478803 0.702702 0.484214 11.00000 0.02489 0.02824 = 0.03019 -0.01592 -0.01696 0.00561 N00S 5 0.337045 0.885103 0.112615 11.00000 0.02278 0.03636 = 0.02300 -0.00425 -0.01085 -0.00717 C00T 1 0.033255 0.743742 0.472637 11.00000 0.01366 0.02406 = 0.02333 -0.00598 -0.00640 -0.00149 C00U 1 0.114408 0.459614 0.517735 11.00000 0.02788 0.02062 = 0.02767 -0.00763 -0.01202 -0.00509 AFIX 43 H00U 2 0.120287 0.425719 0.488415 11.00000 -1.20000 AFIX 0 C00V 1 0.462360 0.719677 0.418066 11.00000 0.01950 0.02059 = 0.03163 -0.01057 -0.01486 -0.00084 C00W 1 0.147933 0.678559 0.291864 11.00000 0.01501 0.02730 = 0.01880 -0.01098 -0.00732 -0.00230 C00X 1 0.005859 0.797085 0.517092 11.00000 0.01776 0.01908 = 0.02584 -0.00913 -0.01212 0.00256 C00Y 1 0.156839 0.612108 0.269396 11.00000 0.02116 0.03055 = 0.02648 -0.01229 -0.00977 -0.00446 C00Z 1 0.513034 0.700173 0.344079 11.00000 0.02422 0.02237 = 0.02835 -0.01060 -0.01355 -0.00247 C010 1 0.127158 0.753061 0.245753 11.00000 0.01896 0.02629 = 0.02097 -0.00365 -0.00731 -0.00484 C011 1 0.179425 0.468754 0.337429 11.00000 0.02751 0.02771 = 0.02857 -0.01305 -0.01114 -0.00340 C012 1 0.115922 0.591455 0.520865 11.00000 0.01632 0.02550 = 0.03010 -0.01693 -0.01188 0.00413 C013 1 0.153962 0.613727 0.196213 11.00000 0.02767 0.03345 = 0.02440 -0.01178 -0.01151 -0.00460 C014 1 0.111871 0.820012 0.268434 11.00000 0.02223 0.03669 = 0.02741 -0.00938 -0.00883 -0.00425 AFIX 43 H014 2 0.120993 0.818470 0.313542 11.00000 -1.20000 AFIX 0 C015 1 -0.018853 0.735397 0.438420 11.00000 0.01981 0.02311 = 0.02791 -0.00849 -0.01051 -0.00375 AFIX 43 H015 2 -0.004827 0.697784 0.411231 11.00000 -1.20000 AFIX 0 C016 1 0.057460 0.789343 0.559976 11.00000 0.02187 0.01922 = 0.01772 -0.00954 -0.00684 -0.00260 C017 1 0.150884 0.577802 0.393237 11.00000 0.01631 0.02254 = 0.03035 -0.01111 -0.01129 -0.00165 C018 1 -0.066947 0.844472 0.522478 11.00000 0.02299 0.02135 = 0.03157 -0.01194 -0.00948 -0.00113 AFIX 43 H018 2 -0.083318 0.880953 0.551305 11.00000 -1.20000 AFIX 0 C01A 1 0.090704 0.431245 0.600484 11.00000 0.02798 0.02184 = 0.03871 -0.00753 -0.01515 -0.00334 AFIX 43 H01A 2 0.082058 0.377703 0.628068 11.00000 -1.20000 AFIX 0 C01B 1 0.129601 0.538710 0.477782 11.00000 0.01388 0.02636 = 0.02947 -0.00998 -0.00958 -0.00185 C01C 1 0.113834 0.755648 0.177118 11.00000 0.02419 0.03229 = 0.02513 -0.00641 -0.01246 -0.01042 C01D 1 0.376632 0.792787 0.488614 11.00000 0.01832 0.02114 = 0.02702 -0.01133 -0.01281 -0.00217 C01E 1 0.351357 0.759646 0.173981 11.00000 0.01828 0.03504 = 0.02498 -0.01465 -0.00702 -0.00607 C01F 1 0.091321 0.561342 0.603766 11.00000 0.01956 0.02122 = 0.02743 -0.00921 -0.01137 -0.00288 AFIX 43 H01F 2 0.082260 0.594819 0.634450 11.00000 -1.20000 AFIX 0 C01G 1 0.148259 0.731836 0.611319 11.00000 0.01944 0.02279 = 0.01968 -0.00517 -0.00929 -0.00723 C01H 1 0.400978 0.625680 0.235037 11.00000 0.03084 0.03222 = 0.03105 -0.01764 -0.01072 -0.00494 AFIX 43 H01H 2 0.404908 0.641858 0.274579 11.00000 -1.20000 AFIX 0 C01I 1 0.374324 0.931937 0.202198 11.00000 0.01581 0.02415 = 0.02782 -0.00826 -0.00414 -0.00437 C01J 1 0.350491 0.875706 0.179250 11.00000 0.01970 0.02953 = 0.02129 -0.00402 -0.00830 -0.00472 C01K 1 0.336751 0.810688 0.109189 11.00000 0.02404 0.03582 = 0.02747 -0.00907 -0.01183 -0.00583 C01L 1 0.127107 0.685959 0.152950 11.00000 0.02911 0.03883 = 0.02420 -0.00885 -0.01100 -0.01120 C01M 1 0.332117 0.957765 0.053757 11.00000 0.02882 0.03664 = 0.02719 -0.00290 -0.01421 -0.00735 C01N 1 0.482461 0.742563 0.283072 11.00000 0.01769 0.02335 = 0.03123 -0.01489 -0.00875 -0.00192 C01O 1 0.213362 0.681128 0.706832 11.00000 0.02311 0.02054 = 0.03096 -0.00771 -0.01364 -0.00673 C01P 1 0.206328 0.677479 0.637971 11.00000 0.02333 0.02139 = 0.02377 -0.00589 -0.01127 -0.00571 C01Q 1 0.084002 0.887782 0.226901 11.00000 0.03798 0.03063 = 0.04159 -0.01591 -0.02095 -0.00075 AFIX 43 H01Q 2 0.072142 0.932232 0.244370 11.00000 -1.20000 AFIX 0 C01R 1 0.253993 0.435961 0.340964 11.00000 0.02993 0.03400 = 0.04018 -0.01675 -0.01268 0.00003 AFIX 43 H01R 2 0.292593 0.465798 0.339890 11.00000 -1.20000 AFIX 0 C01S 1 0.165205 0.737210 0.748610 11.00000 0.02465 0.03372 = 0.02922 -0.00648 -0.01179 -0.00993 C01T 1 0.543725 0.649327 0.498606 11.00000 0.02654 0.02788 = 0.03049 -0.01423 -0.02085 0.00868 C01U 1 -0.100363 0.841356 0.707830 11.00000 0.03392 0.02839 = 0.02831 -0.00941 -0.00419 -0.00225 AFIX 43 H01U 2 -0.105364 0.786951 0.731320 11.00000 -1.20000 AFIX 0 C01V 1 0.425797 0.749785 0.529457 11.00000 0.02471 0.02246 = 0.02775 -0.00945 -0.01064 -0.00411 C01W 1 -0.090025 0.782003 0.444655 11.00000 0.02606 0.02294 = 0.03611 -0.00581 -0.01866 -0.00768 C01X 1 0.108161 0.790723 0.720516 11.00000 0.02808 0.02843 = 0.02424 -0.00767 -0.01033 -0.00183 C01Y 1 0.366023 0.816987 0.629161 11.00000 0.03637 0.02567 = 0.02651 -0.00455 -0.01195 -0.01060 C01Z 1 0.379154 1.012092 0.165719 11.00000 0.03793 0.02394 = 0.03206 -0.00119 -0.01632 -0.00458 AFIX 43 H01Z 2 0.360178 1.036250 0.123937 11.00000 -1.20000 AFIX 0 C020 1 0.397963 0.895753 0.267537 11.00000 0.02014 0.02701 = 0.02316 -0.01042 -0.00711 -0.00128 C021 1 0.609404 0.700482 0.188777 11.00000 0.02761 0.02786 = 0.03257 -0.01411 -0.00578 -0.00373 C022 1 0.101231 0.782554 0.652729 11.00000 0.02649 0.01739 = 0.02485 -0.00419 -0.01057 -0.00534 C023 1 0.319701 0.853535 0.516299 11.00000 0.02481 0.02199 = 0.02699 -0.01093 -0.01015 -0.00328 C024 1 0.534215 0.742762 0.204751 11.00000 0.02526 0.03209 = 0.02634 -0.01572 -0.01076 -0.00606 AFIX 43 H024 2 0.517837 0.772046 0.162107 11.00000 -1.20000 AFIX 0 C025 1 0.122133 0.425862 0.341424 11.00000 0.03260 0.03150 = 0.03486 -0.00687 -0.01296 -0.01647 AFIX 43 H025 2 0.069655 0.448656 0.341836 11.00000 -1.20000 AFIX 0 C027 1 0.421386 0.757218 0.601942 11.00000 0.02273 0.02340 = 0.02995 -0.00896 -0.01472 -0.00597 C028 1 -0.160054 0.970669 0.695445 11.00000 0.04154 0.03352 = 0.04014 -0.01673 -0.01025 0.01148 AFIX 43 H028 2 -0.206690 1.004794 0.711584 11.00000 -1.20000 AFIX 0 C029 1 0.586520 0.654632 0.326294 11.00000 0.02867 0.03159 = 0.03974 -0.01900 -0.01902 0.00401 AFIX 43 H029 2 0.603761 0.624032 0.368015 11.00000 -1.20000 AFIX 0 C02A 1 -0.114999 0.836793 0.484377 11.00000 0.02715 0.02503 = 0.03960 -0.00750 -0.02072 0.00365 AFIX 43 H02A 2 -0.163734 0.868775 0.486005 11.00000 -1.20000 AFIX 0 C02B 1 0.080047 0.482580 0.641545 11.00000 0.02314 0.02626 = 0.02452 -0.00442 -0.01334 -0.00478 C02C 1 0.528712 0.571024 0.532968 11.00000 0.01919 0.02953 = 0.03354 -0.01064 -0.01453 -0.00254 AFIX 43 H02C 2 0.474984 0.553584 0.549546 11.00000 -1.20000 AFIX 0 C02D 1 0.591801 0.518693 0.542978 11.00000 0.03584 0.02060 = 0.04095 -0.00512 -0.02295 0.00129 AFIX 43 H02D 2 0.582106 0.464904 0.565870 11.00000 -1.20000 AFIX 0 C02E 1 0.141626 0.348996 0.344850 11.00000 0.05624 0.03148 = 0.03888 -0.01316 -0.00968 -0.01940 AFIX 43 H02E 2 0.103413 0.319037 0.345506 11.00000 -1.20000 AFIX 0 C02F 1 -0.024999 0.872561 0.646932 11.00000 0.03090 0.02241 = 0.02165 -0.01002 -0.01107 0.00128 C02G 1 0.250174 0.618998 0.604322 11.00000 0.01824 0.02714 = 0.02709 -0.00808 -0.01092 -0.00462 AFIX 43 H02G 2 0.244890 0.616449 0.558706 11.00000 -1.20000 AFIX 0 C02H 1 0.411866 1.057017 0.190486 11.00000 0.05459 0.02306 = 0.03869 -0.00408 -0.01678 -0.00955 AFIX 43 H02H 2 0.415419 1.111444 0.166144 11.00000 -1.20000 AFIX 0 C02I 1 0.669029 0.544704 0.519644 11.00000 0.03131 0.03110 = 0.06093 -0.01718 -0.02973 0.00741 AFIX 43 H02I 2 0.712692 0.508463 0.526249 11.00000 -1.20000 AFIX 0 C02J 1 0.469917 0.711812 0.643910 11.00000 0.03531 0.03098 = 0.04270 -0.00991 -0.02409 -0.00331 AFIX 43 H02J 2 0.506333 0.671715 0.625416 11.00000 -1.20000 AFIX 0 C02K 1 0.370602 0.678537 0.179800 11.00000 0.02557 0.03610 = 0.02699 -0.01934 -0.00299 -0.01308 C02L 1 0.273198 0.903257 0.474967 11.00000 0.02776 0.02560 = 0.02953 -0.00855 -0.01345 -0.00810 AFIX 43 H02L 2 0.277724 0.897154 0.426783 11.00000 -1.20000 AFIX 0 C02M 1 0.465637 0.724301 0.710596 11.00000 0.03998 0.03855 = 0.03529 -0.01051 -0.02554 -0.00304 AFIX 43 H02M 2 0.497967 0.692005 0.738637 11.00000 -1.20000 AFIX 0 C02N 1 0.438822 1.019246 0.251699 11.00000 0.04360 0.02991 = 0.03574 -0.00897 -0.01507 -0.01625 C02O 1 0.433166 0.940785 0.289617 11.00000 0.02775 0.02781 = 0.03507 -0.01029 -0.01452 -0.00966 AFIX 43 H02O 2 0.453154 0.917233 0.330752 11.00000 -1.20000 AFIX 0 C02P 1 0.620972 0.676040 0.475632 11.00000 0.03676 0.01797 = 0.05694 -0.00605 -0.02593 -0.00264 AFIX 43 H02P 2 0.630733 0.729816 0.452682 11.00000 -1.20000 AFIX 0 C02Q 1 -0.016843 0.951021 0.610220 11.00000 0.03209 0.02656 = 0.03079 -0.01200 -0.01083 -0.00016 AFIX 43 H02Q 2 0.034796 0.970743 0.569040 11.00000 -1.20000 AFIX 0 C02R 1 -0.084751 1.001107 0.633895 11.00000 0.03751 0.01828 = 0.04315 -0.01128 -0.01903 0.00032 AFIX 43 H02R 2 -0.080253 1.055374 0.608688 11.00000 -1.20000 AFIX 0 C02S 1 0.415019 0.783159 0.737777 11.00000 0.03528 0.05674 = 0.02711 -0.00832 -0.01380 -0.02388 AFIX 43 H02S 2 0.413712 0.792981 0.783069 11.00000 -1.20000 AFIX 0 C02T 1 0.314933 0.864362 0.586682 11.00000 0.03110 0.02489 = 0.02370 -0.00864 -0.01151 -0.00570 C02U 1 0.300708 0.565027 0.635061 11.00000 0.02586 0.03000 = 0.03628 -0.01264 -0.01395 0.00107 AFIX 43 H02U 2 0.329261 0.525353 0.611295 11.00000 -1.20000 AFIX 0 C02V 1 -0.167644 0.891827 0.733087 11.00000 0.02959 0.03592 = 0.05090 -0.01131 -0.00167 0.00045 AFIX 43 H02V 2 -0.218492 0.872233 0.775940 11.00000 -1.20000 AFIX 0 C02W 1 0.364597 0.829094 0.696658 11.00000 0.04528 0.04116 = 0.03324 -0.01659 -0.01607 -0.00704 AFIX 43 H02W 2 0.328905 0.869204 0.715787 11.00000 -1.20000 AFIX 0 C02X 1 0.325673 0.787708 0.051018 11.00000 0.03192 0.05731 = 0.01831 -0.01159 -0.00786 -0.01272 C02Y 1 0.402277 0.979539 -0.017566 11.00000 0.03179 0.05148 = 0.03182 -0.00655 -0.00998 -0.00703 AFIX 43 H02Y 2 0.452215 0.948204 -0.025193 11.00000 -1.20000 AFIX 0 C02Z 1 0.267425 0.624333 0.736232 11.00000 0.03184 0.03738 = 0.03624 -0.00737 -0.02338 -0.00300 AFIX 43 H02Z 2 0.273739 0.625665 0.781800 11.00000 -1.20000 AFIX 0 C030 1 0.260702 1.003538 0.068190 11.00000 0.03040 0.04862 = 0.04168 0.00119 -0.01472 -0.01190 AFIX 43 H030 2 0.213981 0.988591 0.117864 11.00000 -1.20000 AFIX 0 C031 1 0.634331 0.653625 0.248766 11.00000 0.02057 0.03598 = 0.05235 -0.02652 -0.01615 0.00620 AFIX 43 H031 2 0.683495 0.621339 0.236774 11.00000 -1.20000 AFIX 0 C032 1 0.088240 0.826632 0.134472 11.00000 0.04486 0.04916 = 0.02572 -0.00827 -0.02101 -0.00855 AFIX 43 H032 2 0.081327 0.829807 0.087743 11.00000 -1.20000 AFIX 0 C033 1 0.271551 0.358095 0.346147 11.00000 0.04088 0.03500 = 0.05450 -0.01998 -0.01888 0.00721 AFIX 43 H033 2 0.322602 0.334238 0.348896 11.00000 -1.20000 AFIX 0 C034 1 0.684073 0.622681 0.486767 11.00000 0.03210 0.03206 = 0.07276 -0.01868 -0.03718 0.00387 AFIX 43 H034 2 0.737490 0.639854 0.471769 11.00000 -1.20000 AFIX 0 C035 1 0.216412 0.316091 0.347300 11.00000 0.05967 0.02744 = 0.04108 -0.01314 -0.00768 0.00164 AFIX 43 H035 2 0.229604 0.263188 0.349836 11.00000 -1.20000 AFIX 0 C036 1 0.310154 0.568519 0.701665 11.00000 0.02650 0.03334 = 0.03524 -0.00521 -0.01907 0.00282 AFIX 43 H036 2 0.346195 0.532087 0.722440 11.00000 -1.20000 AFIX 0 C037 1 0.174310 0.551461 0.165509 11.00000 0.03728 0.03766 = 0.03228 -0.01339 -0.01383 -0.00827 AFIX 43 H037 2 0.197761 0.504940 0.190801 11.00000 -1.20000 AFIX 0 C038 1 0.221325 0.960515 0.502902 11.00000 0.03615 0.02461 = 0.03756 -0.01132 -0.01666 0.00599 AFIX 43 H038 2 0.190790 0.994213 0.473625 11.00000 -1.20000 AFIX 0 C039 1 0.112703 0.687914 0.086918 11.00000 0.04439 0.04407 = 0.03229 -0.01101 -0.01965 -0.00839 AFIX 43 H039 2 0.091969 0.734583 0.058899 11.00000 -1.20000 AFIX 0 C03A 1 0.364758 0.654219 0.119841 11.00000 0.03339 0.04663 = 0.03269 -0.01859 -0.00559 -0.01485 C03B 1 0.325717 0.682227 0.004218 11.00000 0.04754 0.07957 = 0.03588 -0.02911 -0.00373 -0.03281 AFIX 43 H03B 2 0.333648 0.628798 0.008318 11.00000 -1.20000 AFIX 0 C03C 1 0.259078 0.923086 0.613961 11.00000 0.04568 0.03285 = 0.03135 -0.01796 -0.01425 -0.00011 AFIX 43 H03C 2 0.253475 0.930287 0.662022 11.00000 -1.20000 AFIX 0 C03D 1 0.173916 0.742846 0.815086 11.00000 0.04061 0.04833 = 0.02813 -0.01556 -0.01596 0.00442 AFIX 43 H03D 2 0.212688 0.708612 0.833687 11.00000 -1.20000 AFIX 0 C03E 1 0.062688 0.845420 0.761774 11.00000 0.03847 0.03556 = 0.03636 -0.01643 -0.01752 0.00020 AFIX 43 H03E 2 0.024322 0.881012 0.743716 11.00000 -1.20000 AFIX 0 C03F 1 0.072788 0.891764 0.157755 11.00000 0.04306 0.03690 = 0.03731 -0.00446 -0.02416 -0.00086 AFIX 43 H03F 2 0.054779 0.939030 0.127956 11.00000 -1.20000 AFIX 0 C03G 1 0.338202 0.707645 0.058782 11.00000 0.03122 0.05161 = 0.02246 -0.01635 -0.00207 -0.01549 C03H 1 0.161263 0.555860 0.099796 11.00000 0.05181 0.04270 = 0.03519 -0.01993 -0.01698 -0.00966 AFIX 43 H03H 2 0.175016 0.512550 0.080292 11.00000 -1.20000 AFIX 0 C03I 1 0.417947 0.526822 0.176558 11.00000 0.05623 0.03347 = 0.05637 -0.02807 -0.01720 -0.00467 AFIX 43 H03I 2 0.433511 0.474900 0.175892 11.00000 -1.20000 AFIX 0 C03J 1 0.388480 0.577433 0.121529 11.00000 0.05129 0.04628 = 0.04888 -0.03349 -0.00931 -0.01448 AFIX 43 H03J 2 0.384165 0.559374 0.083354 11.00000 -1.20000 AFIX 0 C03K 1 0.424885 0.551781 0.233040 11.00000 0.04533 0.03535 = 0.03749 -0.01874 -0.01168 0.00017 AFIX 43 H03K 2 0.446324 0.517230 0.270255 11.00000 -1.20000 AFIX 0 C03L 1 0.128075 0.623390 0.061961 11.00000 0.05318 0.06676 = 0.02674 -0.01329 -0.02259 -0.01909 AFIX 43 H03L 2 0.115758 0.625406 0.018469 11.00000 -1.20000 AFIX 0 C03M 1 0.299195 0.837707 -0.008037 11.00000 0.04475 0.05851 = 0.02885 -0.00976 -0.01398 -0.01981 AFIX 43 H03M 2 0.288005 0.891042 -0.011999 11.00000 -1.20000 AFIX 0 C03N 1 0.399241 1.045750 -0.076335 11.00000 0.04090 0.06242 = 0.03183 -0.00234 -0.01238 -0.01387 AFIX 43 H03N 2 0.445920 1.059947 -0.126165 11.00000 -1.20000 AFIX 0 C03P 1 0.257148 1.071677 0.009883 11.00000 0.04036 0.04239 = 0.06441 -0.00250 -0.02915 -0.00145 AFIX 43 H03P 2 0.207903 1.104050 0.018883 11.00000 -1.20000 AFIX 0 C03Q 1 0.302265 0.733435 -0.054812 11.00000 0.06438 0.06999 = 0.03624 -0.01678 -0.02165 -0.03149 AFIX 43 H03Q 2 0.295183 0.715241 -0.091523 11.00000 -1.20000 AFIX 0 C03R 1 0.212912 0.969810 0.573853 11.00000 0.04868 0.02185 = 0.04229 -0.01559 -0.01133 0.00907 AFIX 43 H03R 2 0.175271 1.008433 0.594156 11.00000 -1.20000 AFIX 0 C03S 1 0.128268 0.796167 0.854028 11.00000 0.04921 0.06182 = 0.04019 -0.02566 -0.02339 -0.00646 AFIX 43 H03S 2 0.134657 0.797522 0.899551 11.00000 -1.20000 AFIX 0 C03T 1 0.326298 1.092363 -0.062015 11.00000 0.07321 0.03882 = 0.04278 0.00851 -0.02878 -0.01472 AFIX 43 H03T 2 0.323925 1.139193 -0.102287 11.00000 -1.20000 AFIX 0 C03U 1 0.072286 0.848493 0.826266 11.00000 0.04704 0.05722 = 0.04353 -0.03644 -0.01870 0.00482 AFIX 43 H03U 2 0.041172 0.885960 0.852419 11.00000 -1.20000 AFIX 0 C03W 1 0.289254 0.809551 -0.060797 11.00000 0.04891 0.09571 = 0.02507 -0.01620 -0.01850 -0.02229 AFIX 43 H03W 2 0.273049 0.844279 -0.101789 11.00000 -1.20000 AFIX 0 HKLF 4 REM st242_dc_a.res in P-1 REM wR2 = 0.1405, GooF = S = 1.045, Restrained GooF = 1.045 for all data REM R1 = 0.0485 for 17400 Fo > 4sig(Fo) and 0.0612 for all 21930 data REM 1117 parameters refined using 0 restraints END WGHT 0.0849 1.6817 REM Highest difference peak 3.935, deepest hole -2.828, 1-sigma level 0.167 Q1 1 0.1822 0.6603 0.4576 11.00000 0.05 3.93 Q2 1 0.1070 0.7400 0.4630 11.00000 0.05 3.76 Q3 1 0.1167 0.6949 0.5020 11.00000 0.05 3.55 Q4 1 0.1823 0.7068 0.4015 11.00000 0.05 3.55 Q5 1 0.4075 0.7463 0.3275 11.00000 0.05 3.46 ; _shelx_res_checksum 51551 _shelx_hkl_file ; -2 0 0 84.49 5.60 -2 0 0 83.49 5.50 -2 0 0 89.59 5.80 2 0 0 91.39 5.60 2 0 0 88.89 5.80 2 0 0 88.69 5.50 -3 0 0 36.20 3.20 -3 0 0 35.40 3.00 -3 0 0 34.40 3.70 3 0 0 32.60 3.00 3 0 0 41.30 3.80 -4 0 0 9999.00 566.24 4 0 0 9756.52 566.14 -5 0 0 18.70 3.30 -5 0 0 22.60 2.90 -5 0 0 22.10 2.70 5 0 0 15.20 2.30 5 0 0 14.50 2.40 5 0 0 23.90 3.50 -6 0 0 505.55 31.80 -6 0 0 521.95 31.80 -6 0 0 535.75 32.50 6 0 0 541.15 32.50 6 0 0 552.64 31.90 6 0 0 520.05 32.00 -7 0 0 2.40 2.00 -7 0 0 1.60 2.80 7 0 0 -1.10 1.70 7 0 0 4.10 2.10 7 0 0 -1.30 2.30 -8 0 0 517.15 32.00 8 0 0 498.45 31.00 8 0 0 497.05 31.90 -9 0 0 60.09 8.50 9 0 0 73.79 8.50 9 0 0 79.09 7.30 9 0 0 72.59 6.90 -10 0 0 400.36 27.40 10 0 0 427.26 27.60 10 0 0 409.86 26.30 -11 0 0 4.30 3.70 11 0 0 7.40 2.90 11 0 0 5.00 3.80 11 0 0 8.30 3.50 -12 0 0 94.09 10.20 12 0 0 105.39 9.80 12 0 0 77.49 10.20 -13 0 0 224.28 18.40 13 0 0 223.18 17.30 -14 0 0 228.38 19.10 14 0 0 243.28 19.60 -15 0 0 40.50 8.50 15 0 0 35.20 7.10 -16 0 0 14.40 6.60 16 0 0 20.00 6.20 -17 0 0 98.39 13.50 17 0 0 127.19 13.20 -18 0 0 112.69 14.30 18 0 0 117.59 14.80 -19 0 0 222.58 21.50 19 0 0 223.98 20.60 -20 0 0 1.30 6.60 19 -1 0 67.99 11.20 -19 1 0 74.09 11.80 18 -1 0 172.48 16.50 -18 1 0 162.18 16.80 17 -1 0 56.39 9.30 -17 1 0 51.99 9.60 16 -1 0 32.30 7.20 -16 1 0 25.90 7.20 15 -1 0 114.89 12.30 -15 1 0 127.69 13.60 14 -1 0 100.29 11.50 -14 1 0 88.29 11.10 13 -1 0 306.67 21.90 -13 1 0 299.07 22.60 12 -1 0 99.99 9.90 12 -1 0 105.19 10.70 -12 1 0 97.29 10.50 11 -1 0 79.59 7.70 11 -1 0 77.89 8.60 11 -1 0 75.89 8.30 -11 1 0 83.19 8.80 10 -1 0 128.99 11.00 10 -1 0 136.99 10.80 10 -1 0 115.29 9.90 -10 1 0 126.09 11.10 -10 1 0 134.29 10.20 9 -1 0 364.66 23.60 9 -1 0 375.16 24.50 9 -1 0 380.56 24.10 -9 1 0 370.76 23.60 -9 1 0 359.96 25.80 8 -1 0 165.68 12.00 8 -1 0 185.78 13.10 8 -1 0 161.78 12.80 -8 1 0 162.88 12.60 -8 1 0 171.48 12.90 7 -1 0 57.79 6.70 7 -1 0 64.19 5.90 7 -1 0 41.10 5.20 -7 1 0 56.89 5.50 -7 1 0 60.29 6.70 6 -1 0 36.90 4.70 6 -1 0 39.20 4.30 6 -1 0 25.50 3.90 -6 1 0 46.30 4.60 -6 1 0 46.20 5.20 5 -1 0 2639.64 149.79 5 -1 0 2474.65 149.49 5 -1 0 2544.25 149.29 -5 1 0 2613.24 149.79 -5 1 0 2678.23 149.39 4 -1 0 247.58 15.40 4 -1 0 251.47 15.60 4 -1 0 251.17 15.80 -4 1 0 249.97 15.80 -4 1 0 253.77 15.40 3 -1 0 8.70 1.60 3 -1 0 8.90 1.60 3 -1 0 7.60 1.80 -3 1 0 10.70 1.90 -3 1 0 4.70 1.40 2 -1 0 26.40 2.40 2 -1 0 27.80 2.20 -2 1 0 29.30 2.50 -2 1 0 23.70 2.20 1 1 0 25.40 13.90 -2 -1 0 12.10 1.70 -2 -1 0 10.40 1.30 2 1 0 7.50 1.10 2 1 0 8.10 1.60 2 1 0 11.30 1.40 -3 -1 0 1302.47 70.69 -3 -1 0 1223.58 71.09 3 1 0 1249.68 70.59 3 1 0 1180.28 70.49 3 1 0 1146.59 70.99 -4 -1 0 595.24 32.60 -4 -1 0 541.25 33.00 4 1 0 566.74 32.50 4 1 0 505.25 32.90 4 1 0 534.75 32.40 -5 -1 0 1424.46 86.69 -5 -1 0 1588.04 86.19 5 1 0 1458.05 87.59 5 1 0 1514.75 86.19 5 1 0 1426.46 85.99 -6 -1 0 134.09 9.10 -6 -1 0 120.79 9.70 6 1 0 128.39 8.90 6 1 0 120.89 9.70 6 1 0 129.79 9.10 -7 -1 0 570.64 35.90 -7 -1 0 618.04 35.00 7 1 0 581.84 34.90 7 1 0 592.74 35.00 7 1 0 516.95 35.60 -8 -1 0 33.40 4.60 -8 -1 0 25.20 5.50 8 1 0 28.10 5.50 8 1 0 18.80 3.50 8 1 0 23.90 4.40 -9 -1 0 1276.47 76.29 9 1 0 1237.18 76.09 9 1 0 1302.87 75.29 -10 -1 0 38.10 6.30 10 1 0 29.70 5.80 10 1 0 35.40 5.20 10 1 0 24.90 4.70 -11 -1 0 42.70 6.90 11 1 0 48.10 6.20 11 1 0 41.00 7.00 11 1 0 32.80 5.40 -12 -1 0 28.10 6.40 12 1 0 24.50 5.30 12 1 0 41.00 7.20 -13 -1 0 690.23 44.20 13 1 0 667.23 42.90 -14 -1 0 160.48 15.10 -15 -1 0 82.49 16.30 15 1 0 84.29 11.00 -16 -1 0 7.90 5.60 16 1 0 5.30 4.70 -17 -1 0 96.39 13.30 17 1 0 108.79 13.20 -18 -1 0 52.19 10.00 18 1 0 57.79 9.20 -19 -1 0 52.89 10.40 19 1 0 59.29 10.40 -20 -1 0 -6.90 5.90 20 1 0 1.10 8.40 19 -2 0 248.18 21.60 -19 2 0 240.28 22.20 18 -2 0 86.89 12.20 -18 2 0 54.79 10.20 17 -2 0 19.50 6.50 -17 2 0 23.60 7.00 16 -2 0 40.40 8.10 -16 2 0 47.80 8.20 15 -2 0 151.68 14.90 -15 2 0 177.08 16.00 14 -2 0 116.89 12.80 -14 2 0 154.88 14.40 13 -2 0 43.20 6.60 -13 2 0 51.29 8.10 12 -2 0 3.60 3.50 12 -2 0 0.00 3.50 -12 2 0 -1.90 3.10 11 -2 0 134.99 11.20 11 -2 0 108.09 10.00 -11 2 0 128.19 11.40 -11 2 0 133.69 10.40 10 -2 0 367.36 24.00 10 -2 0 343.07 23.30 10 -2 0 373.36 24.40 -10 2 0 373.96 24.50 -10 2 0 354.46 23.30 9 -2 0 33.00 4.60 9 -2 0 21.30 4.80 9 -2 0 25.10 4.50 -9 2 0 24.90 4.00 -9 2 0 18.70 4.60 8 -2 0 0.10 2.80 8 -2 0 6.60 2.60 8 -2 0 3.50 2.20 -8 2 0 8.40 2.60 -8 2 0 5.50 3.40 7 -2 0 120.59 9.50 7 -2 0 111.39 8.70 -7 2 0 112.69 8.70 -7 2 0 115.19 9.60 6 -2 0 3128.99 189.68 6 -2 0 3419.16 190.38 6 -2 0 3456.65 190.18 -6 2 0 3100.69 189.68 -6 2 0 3362.86 190.38 5 -2 0 200.18 12.90 5 -2 0 194.88 12.60 5 -2 0 193.68 13.00 -5 2 0 192.78 13.10 -5 2 0 202.98 12.70 4 -2 0 30.80 3.40 4 -2 0 30.30 3.20 4 -2 0 25.40 2.90 -4 2 0 27.80 2.90 -4 2 0 31.70 3.40 3 -2 0 0.10 1.30 3 -2 0 -0.60 0.90 -3 2 0 -0.20 1.00 -3 2 0 1.60 1.40 2 -2 0 638.94 41.00 2 -2 0 733.93 40.80 2 -2 0 693.23 41.00 -2 2 0 733.33 40.80 -2 2 0 712.63 41.00 1 -2 0 10.30 1.20 1 -2 0 10.50 1.80 -1 2 0 12.30 1.60 -1 -2 0 16.20 1.40 -1 -2 0 16.10 1.90 1 2 0 19.10 2.10 1 2 0 16.40 1.40 -2 -2 0 977.50 55.79 -2 -2 0 963.60 56.29 2 2 0 955.10 55.79 -3 -2 0 121.59 7.60 3 2 0 110.49 7.50 3 2 0 108.69 8.20 -4 -2 0 4210.58 255.77 -4 -2 0 4948.60 255.37 4 2 0 4385.56 255.17 4 2 0 4672.83 255.27 4 2 0 4004.20 255.67 -5 -2 0 272.67 15.60 -5 -2 0 229.28 16.00 5 2 0 254.67 15.40 5 2 0 224.28 16.00 5 2 0 235.68 15.20 -6 -2 0 54.19 6.10 -6 -2 0 59.39 5.30 6 2 0 52.69 6.00 6 2 0 63.99 5.40 6 2 0 53.99 5.00 -7 -2 0 7.20 2.70 -7 -2 0 0.60 3.00 7 2 0 0.90 2.20 7 2 0 1.40 2.10 7 2 0 6.20 3.30 -8 -2 0 1512.65 89.69 -8 -2 0 1619.14 88.69 8 2 0 1479.65 88.69 8 2 0 1467.25 89.49 8 2 0 1470.15 88.39 -9 -2 0 24.80 5.30 -9 -2 0 18.60 3.70 9 2 0 14.90 3.40 9 2 0 7.40 4.50 9 2 0 13.00 3.30 -10 -2 0 69.39 8.00 10 2 0 58.39 6.90 10 2 0 73.39 7.20 -11 -2 0 59.49 8.70 11 2 0 83.09 7.40 11 2 0 50.19 6.80 11 2 0 64.69 8.80 -12 -2 0 650.23 41.60 12 2 0 625.14 40.10 -13 -2 0 177.08 15.90 13 2 0 163.98 14.40 -14 -2 0 305.87 23.40 -15 -2 0 17.70 5.90 15 2 0 18.40 5.70 -16 -2 0 10.00 5.90 16 2 0 13.40 5.50 -17 -2 0 69.59 11.70 17 2 0 80.49 10.30 -18 -2 0 94.19 13.60 18 2 0 92.79 12.60 -19 -2 0 23.00 7.90 19 2 0 28.90 7.80 -20 -2 0 3.80 6.50 20 2 0 13.70 6.90 19 -3 0 49.10 10.30 -19 3 0 50.89 10.20 18 -3 0 64.39 14.50 -18 3 0 68.69 11.30 17 -3 0 15.50 6.30 -17 3 0 2.60 5.90 16 -3 0 181.28 16.90 -16 3 0 189.18 17.20 15 -3 0 169.68 15.40 -15 3 0 153.98 15.30 14 -3 0 12.30 5.20 -14 3 0 9.50 5.20 13 -3 0 1.50 3.80 -13 3 0 -2.50 4.00 12 -3 0 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0 352.76 24.70 -4 6 0 390.86 24.00 3 -6 0 26.10 4.30 3 -6 0 21.90 3.00 3 -6 0 23.70 3.90 -3 6 0 28.70 4.20 -3 6 0 23.10 2.90 2 -6 0 556.74 33.40 2 -6 0 612.34 34.50 -2 6 0 552.64 34.40 -2 6 0 551.24 33.30 1 -6 0 167.78 10.90 1 -6 0 185.98 12.00 -1 6 0 188.28 12.40 -1 6 0 161.98 10.60 0 -6 0 2.60 1.20 0 -6 0 -0.80 1.80 0 6 0 -1.30 2.10 0 6 0 1.10 1.10 -1 -6 0 701.33 38.40 -1 -6 0 620.34 37.20 1 6 0 567.84 37.20 1 6 0 670.23 38.40 -2 -6 0 4697.83 256.97 -2 -6 0 4156.48 255.77 2 6 0 4677.33 256.97 2 6 0 4315.27 255.87 -3 -6 0 83.99 7.30 -3 -6 0 67.59 5.50 3 6 0 73.29 7.50 3 6 0 77.79 5.70 -4 -6 0 135.29 10.90 -4 -6 0 151.08 9.40 4 6 0 130.99 9.40 4 6 0 125.59 11.10 -5 -6 0 48.10 6.40 -5 -6 0 54.89 5.10 5 6 0 61.49 7.50 5 6 0 57.49 5.40 -6 -6 0 2260.67 128.59 6 6 0 2350.66 128.89 6 6 0 2122.99 128.49 6 6 0 2136.49 130.09 -7 -6 0 407.36 26.40 -7 -6 0 405.16 24.80 7 6 0 391.26 24.70 7 6 0 454.95 25.30 7 6 0 312.27 25.90 -8 -6 0 622.74 38.70 -8 -6 0 721.23 41.00 8 6 0 552.24 41.50 8 6 0 681.43 39.30 8 6 0 608.24 38.60 -9 -6 0 13.10 3.40 -9 -6 0 14.90 4.90 9 6 0 10.80 2.90 9 6 0 11.80 3.60 9 6 0 9.20 4.60 -10 -6 0 110.19 9.70 -10 -6 0 120.09 11.70 10 6 0 102.49 9.00 10 6 0 124.59 9.60 10 6 0 79.09 10.80 -11 -6 0 51.69 7.00 -11 -6 0 57.99 9.40 11 6 0 52.59 6.60 11 6 0 56.39 7.00 -12 -6 0 281.97 21.50 12 6 0 247.48 18.80 -13 -6 0 8.90 6.10 13 6 0 11.20 4.40 -14 -6 0 46.40 9.00 14 6 0 54.79 11.80 -15 -6 0 114.89 14.80 15 6 0 93.89 11.40 -16 -6 0 265.07 22.50 16 6 0 254.87 20.10 -17 -6 0 13.20 7.20 17 6 0 19.00 5.60 -18 -6 0 -2.80 5.60 18 6 0 0.00 5.30 -19 -6 0 36.70 9.60 19 6 0 43.40 9.00 18 -7 0 83.29 13.30 18 -7 0 114.69 13.60 -18 7 0 73.39 12.80 17 -7 0 52.99 10.80 17 -7 0 64.59 11.10 -17 7 0 54.59 10.50 16 -7 0 250.07 20.70 16 -7 0 225.88 19.20 -16 7 0 208.58 19.90 15 -7 0 15.10 5.50 15 -7 0 28.90 7.10 -15 7 0 27.00 7.90 14 -7 0 100.99 12.80 14 -7 0 98.09 12.20 -14 7 0 90.09 12.00 -14 7 0 112.79 10.30 13 -7 0 340.97 25.70 13 -7 0 341.77 24.70 -13 7 0 350.76 23.80 -13 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368.56 23.60 2 -7 0 340.47 21.10 2 -7 0 370.76 22.50 -2 7 0 373.26 22.80 -2 7 0 318.97 20.80 1 -7 0 71.99 7.20 1 -7 0 77.19 5.60 -1 7 0 81.49 8.10 -1 7 0 57.39 5.00 0 -7 0 1.00 2.50 0 -7 0 4.80 1.60 0 7 0 3.90 3.50 0 7 0 6.10 1.70 -1 -7 0 1156.08 64.39 -1 -7 0 1069.89 62.99 1 7 0 1112.19 64.49 1 7 0 1020.10 63.09 -2 -7 0 44.80 5.80 -2 -7 0 45.50 4.10 2 7 0 50.29 4.40 2 7 0 49.80 6.60 -3 -7 0 626.34 41.30 -3 -7 0 797.82 43.10 3 7 0 672.93 41.50 3 7 0 737.63 43.10 -4 -7 0 46.70 4.60 -4 -7 0 49.80 6.50 4 7 0 72.19 8.00 4 7 0 47.40 4.90 -5 -7 0 563.54 33.20 -5 -7 0 487.65 30.60 5 7 0 514.45 32.60 5 7 0 484.15 30.80 -6 -7 0 79.99 6.90 -7 -7 0 480.75 28.40 -7 -7 0 412.76 26.20 7 7 0 410.56 26.10 7 7 0 357.76 27.80 7 7 0 448.26 26.70 -8 -7 0 80.19 9.10 -8 -7 0 77.59 7.20 8 7 0 90.49 9.90 8 7 0 97.49 9.00 8 7 0 80.09 7.30 -9 -7 0 64.99 8.90 -9 -7 0 80.89 7.50 9 7 0 88.59 7.90 9 7 0 72.99 7.20 9 7 0 76.59 10.10 -10 -7 0 5.00 4.20 -10 -7 0 16.20 4.20 10 7 0 9.20 3.50 10 7 0 9.20 3.50 -11 -7 0 362.96 27.40 -11 -7 0 365.56 25.20 11 7 0 408.86 25.70 11 7 0 409.86 25.90 -12 -7 0 7.30 5.50 12 7 0 -0.40 3.30 -13 -7 0 -0.80 5.10 13 7 0 0.50 3.40 -14 -7 0 12.40 6.10 -15 -7 0 518.05 36.20 15 7 0 493.65 34.00 -16 -7 0 29.00 8.60 16 7 0 33.30 7.10 -17 -7 0 53.49 10.30 17 7 0 45.60 8.80 -18 -7 0 16.80 7.80 18 7 0 12.40 6.40 -19 -7 0 87.29 13.80 19 7 0 84.09 12.40 18 -8 0 27.00 8.30 18 -8 0 20.00 8.70 -18 8 0 7.20 7.80 17 -8 0 232.48 21.40 -17 8 0 224.78 21.80 16 -8 0 47.70 8.90 16 -8 0 39.90 9.40 -16 8 0 38.10 9.20 15 -8 0 51.59 10.10 15 -8 0 35.50 7.50 -15 8 0 22.50 7.50 14 -8 0 35.60 8.40 14 -8 0 37.40 7.70 -14 8 0 21.60 7.20 -14 8 0 26.90 5.60 13 -8 0 205.88 18.00 13 -8 0 183.28 16.30 -13 8 0 190.58 17.10 -13 8 0 206.88 15.50 12 -8 0 315.77 22.50 12 -8 0 298.37 22.00 12 -8 0 300.67 23.70 -12 8 0 330.17 23.50 -12 8 0 299.67 21.20 11 -8 0 161.08 14.80 11 -8 0 147.59 13.10 11 -8 0 151.08 13.20 -11 8 0 173.88 12.90 -11 8 0 161.38 14.20 10 -8 0 1.70 2.80 10 -8 0 5.00 3.80 10 -8 0 3.70 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29.40 4 -11 0 458.95 29.80 -4 11 0 439.46 27.50 -4 11 0 476.65 30.00 3 -11 0 224.28 15.60 3 -11 0 169.28 12.40 -3 11 0 177.18 12.00 -3 11 0 179.98 14.60 2 -11 0 14.30 4.80 2 -11 0 17.70 3.10 -2 11 0 12.70 5.10 -2 11 0 15.60 2.60 1 -11 0 269.87 17.70 1 -11 0 276.87 19.30 -1 11 0 264.47 16.90 -1 11 0 301.97 20.40 0 -11 0 2.10 1.80 0 -11 0 4.60 3.50 0 11 0 3.90 1.70 0 11 0 -2.00 4.20 -1 -11 0 329.17 21.60 -1 -11 0 305.07 19.30 1 11 0 348.17 22.40 1 11 0 295.77 19.30 -2 -11 0 23.00 5.00 -2 -11 0 27.30 3.30 2 11 0 30.20 3.70 2 11 0 23.70 6.00 -3 -11 0 432.56 26.20 3 11 0 333.07 23.60 3 11 0 427.26 28.50 -4 -11 0 88.59 9.20 -4 -11 0 63.79 5.90 4 11 0 90.59 9.90 4 11 0 69.09 6.50 -5 -11 0 459.75 30.30 5 11 0 531.15 30.90 5 11 0 524.55 33.50 -6 -11 0 66.49 6.40 -6 -11 0 73.89 9.60 6 11 0 79.99 10.60 6 11 0 63.89 6.80 -7 -11 0 7.60 4.70 -7 -11 0 18.90 3.60 7 11 0 19.40 4.10 -8 -11 0 83.79 10.60 -8 -11 0 78.99 7.40 8 11 0 67.09 7.00 8 11 0 69.39 7.70 -9 -11 0 656.13 40.30 -9 -11 0 689.43 43.30 9 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2.50 -5 -12 0 5.00 4.40 5 12 0 3.50 2.50 5 12 0 7.40 6.20 -6 -12 0 214.38 15.40 -6 -12 0 273.37 19.10 6 12 0 236.58 16.10 -7 -12 0 17.80 3.60 -7 -12 0 19.60 5.60 7 12 0 15.20 4.00 -8 -12 0 349.87 22.80 -8 -12 0 394.46 26.30 8 12 0 335.77 22.80 8 12 0 355.26 23.40 -9 -12 0 2.60 3.10 9 12 0 7.10 3.40 9 12 0 9.00 4.00 -10 -12 0 223.08 19.10 -10 -12 0 207.08 15.90 10 12 0 220.78 15.60 10 12 0 218.48 16.10 -11 -12 0 4.90 6.10 -11 -12 0 7.30 4.20 11 12 0 9.80 4.30 11 12 0 8.70 3.80 -12 -12 0 12.60 6.90 12 12 0 10.90 4.70 -13 -12 0 1.70 5.90 13 12 0 1.90 4.10 -14 -12 0 76.79 13.00 14 12 0 85.29 10.50 -15 -12 0 5.50 11.50 15 12 0 3.10 4.50 -16 -12 0 19.10 7.70 16 12 0 3.10 4.80 17 12 0 2.60 6.20 15 -13 0 2.80 7.50 15 -13 0 17.90 5.70 14 -13 0 217.08 21.50 14 -13 0 250.77 19.50 -14 13 0 228.08 17.50 13 -13 0 14.10 7.60 13 -13 0 32.80 6.90 -13 13 0 11.90 4.40 12 -13 0 5.40 6.30 12 -13 0 17.90 5.20 -12 13 0 8.60 4.00 11 -13 0 103.89 13.00 11 -13 0 106.89 12.80 10 -13 0 491.25 32.40 10 -13 0 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3.30 2.10 6 -10 3 1.40 3.50 6 -10 3 5.90 2.20 -7 10 -3 369.26 22.10 -7 10 -3 335.27 24.90 7 -10 3 349.17 22.50 7 -10 3 338.17 24.30 7 -10 3 356.86 25.90 7 -10 3 355.16 22.20 -8 10 -3 -0.20 2.20 8 -10 3 4.40 5.20 8 -10 3 3.10 3.00 8 -10 3 0.20 3.70 8 -10 3 6.50 2.40 -9 10 -3 11.50 2.90 9 -10 3 0.30 2.90 9 -10 3 6.30 6.00 9 -10 3 7.20 3.10 9 -10 3 -2.10 4.10 10 -10 3 138.59 12.50 10 -10 3 179.78 16.50 10 -10 3 165.98 12.40 11 -10 3 280.27 22.20 11 -10 3 245.58 18.70 12 -10 3 57.69 10.60 12 -10 3 59.19 8.10 13 -10 3 6.00 6.20 13 -10 3 6.80 5.10 14 -10 3 106.09 11.30 14 -10 3 69.49 12.10 15 -10 3 179.78 18.30 15 -10 3 154.28 14.70 16 -10 3 32.30 9.40 16 -10 3 28.10 6.90 17 -10 3 -10.20 7.40 17 -10 3 3.80 5.00 16 9 -3 -4.70 4.90 -16 -9 3 0.50 6.30 15 9 -3 7.30 5.30 -15 -9 3 1.40 8.00 14 9 -3 15.70 5.90 -14 -9 3 32.90 8.80 13 9 -3 184.48 16.20 -13 -9 3 158.68 17.80 12 9 -3 164.68 14.00 -12 -9 3 138.69 15.70 11 9 -3 34.50 6.40 -11 -9 3 24.40 7.50 10 9 -3 21.90 5.10 10 9 -3 39.90 5.50 -10 -9 3 22.60 6.90 9 9 -3 9.30 4.00 9 9 -3 9.00 3.60 -9 -9 3 5.50 5.60 8 9 -3 473.45 29.10 8 9 -3 461.85 28.40 -8 -9 3 417.86 31.20 7 9 -3 63.49 6.80 7 9 -3 58.79 5.80 -7 -9 3 57.59 8.70 6 9 -3 13.90 3.00 6 9 -3 10.40 2.40 -6 -9 3 2.30 4.00 5 9 -3 22.70 3.10 5 9 -3 19.80 6.00 5 9 -3 30.20 3.80 -5 -9 3 17.80 5.60 4 9 -3 482.85 28.20 4 9 -3 486.65 31.50 4 9 -3 455.15 27.90 -4 -9 3 448.96 30.90 3 9 -3 49.30 3.90 3 9 -3 54.59 7.90 3 9 -3 47.30 4.30 -3 -9 3 46.80 7.00 2 9 -3 69.49 4.70 2 9 -3 86.99 10.40 -2 -9 3 73.59 8.60 1 9 -3 4.20 3.90 -1 -9 3 0.50 3.70 0 9 -3 1200.68 77.29 0 -9 3 1379.66 77.69 -1 9 -3 6.40 4.60 1 -9 3 5.40 4.10 -2 9 -3 235.98 17.90 -2 9 -3 236.78 13.80 2 -9 3 234.78 17.50 2 -9 3 223.18 13.80 -3 9 -3 29.40 2.80 -3 9 -3 27.60 6.30 3 -9 3 30.20 3.00 3 -9 3 28.60 3.10 3 -9 3 17.60 5.80 -4 9 -3 1005.80 57.29 -4 9 -3 965.70 60.29 4 -9 3 965.90 57.49 4 -9 3 1028.20 60.39 4 -9 3 959.20 57.39 -5 9 -3 0.40 1.50 -5 9 -3 3.00 3.60 5 -9 3 1.50 1.70 5 -9 3 3.40 4.10 5 -9 3 3.50 3.80 5 -9 3 0.70 1.60 -6 9 -3 741.13 44.30 -6 9 -3 706.83 47.00 6 -9 3 750.52 44.70 6 -9 3 747.33 46.90 6 -9 3 804.62 47.60 6 -9 3 740.63 44.30 -7 9 -3 8.40 4.40 -7 9 -3 2.80 2.00 7 -9 3 1.10 2.00 7 -9 3 5.90 5.20 7 -9 3 3.00 3.80 7 -9 3 1.80 2.30 -8 9 -3 4.90 2.30 8 -9 3 1.80 3.50 8 -9 3 4.70 2.60 8 -9 3 1.60 2.10 8 -9 3 6.50 5.30 -9 9 -3 32.90 4.60 9 -9 3 43.90 8.00 9 -9 3 28.40 5.10 9 -9 3 32.90 4.80 9 -9 3 26.70 5.90 10 -9 3 407.06 27.00 10 -9 3 413.46 26.50 10 -9 3 418.16 28.40 10 -9 3 417.06 29.50 11 -9 3 28.30 7.60 11 -9 3 33.30 6.20 11 -9 3 25.90 5.30 12 -9 3 88.79 9.50 12 -9 3 72.59 11.10 13 -9 3 14.50 5.40 13 -9 3 25.10 8.10 14 -9 3 276.17 32.10 14 -9 3 268.27 20.60 -15 9 -3 14.50 6.80 15 -9 3 0.10 7.00 15 -9 3 2.40 3.90 -16 9 -3 29.20 8.20 16 -9 3 33.90 9.10 16 -9 3 35.50 7.10 -17 9 -3 42.10 10.20 17 -9 3 46.00 11.30 17 -9 3 63.09 9.80 -18 9 -3 76.69 13.30 18 -9 3 91.49 12.20 18 -9 3 75.79 13.60 17 8 -3 12.30 6.40 -17 -8 3 21.60 8.90 16 8 -3 5.00 5.30 -16 -8 3 5.60 6.20 15 8 -3 7.80 5.20 -15 -8 3 -1.00 6.40 14 8 -3 87.79 10.70 -14 -8 3 80.19 12.50 13 8 -3 220.68 18.20 -13 -8 3 201.58 19.20 12 8 -3 108.39 11.20 -12 -8 3 105.39 13.90 11 8 -3 -1.20 3.20 -11 -8 3 5.00 6.00 10 8 -3 9.40 3.90 10 8 -3 10.00 3.30 9 8 -3 507.75 30.80 -9 -8 3 444.16 32.70 8 8 -3 112.79 9.00 8 8 -3 118.09 9.80 -8 -8 3 90.69 11.90 7 8 -3 234.48 15.60 7 8 -3 224.28 15.10 -7 -8 3 218.48 17.90 6 8 -3 5.20 1.90 6 8 -3 13.50 5.80 6 8 -3 4.70 2.40 -6 -8 3 -3.20 3.70 5 8 -3 419.56 24.80 5 8 -3 381.76 27.70 5 8 -3 412.96 25.10 4 8 -3 29.30 6.50 4 8 -3 24.60 3.30 4 8 -3 22.00 2.80 -4 -8 3 29.00 5.80 3 8 -3 449.36 28.00 3 8 -3 458.75 31.00 3 8 -3 501.05 28.40 -3 -8 3 498.65 31.20 2 8 -3 377.76 21.90 2 8 -3 378.76 25.20 2 8 -3 354.46 21.60 -2 -8 3 371.16 24.90 1 8 -3 219.48 17.20 -1 -8 3 240.68 17.10 0 8 -3 88.39 10.30 0 -8 3 87.09 9.50 -1 8 -3 374.36 25.00 1 -8 3 348.57 24.30 -2 8 -3 332.57 18.70 -2 8 -3 313.37 22.40 2 -8 3 299.47 23.00 2 -8 3 325.47 18.70 2 -8 3 301.67 18.60 -3 8 -3 10.70 1.70 -3 8 -3 10.70 4.40 3 -8 3 10.10 2.00 3 -8 3 8.70 1.80 3 -8 3 6.20 4.80 -4 8 -3 32.70 6.40 -4 8 -3 46.40 3.90 4 -8 3 41.40 4.10 4 -8 3 49.60 7.50 4 -8 3 50.29 7.00 4 -8 3 48.40 4.20 -5 8 -3 1027.60 62.49 -5 8 -3 1024.40 59.69 5 -8 3 987.50 59.69 5 -8 3 1017.90 62.29 5 -8 3 1110.49 62.89 5 -8 3 988.50 59.99 -6 8 -3 1.90 3.40 -6 8 -3 5.30 2.00 6 -8 3 2.30 2.10 6 -8 3 5.90 2.30 6 -8 3 3.30 3.90 6 -8 3 2.60 3.30 -7 8 -3 230.88 14.90 7 -8 3 226.28 14.90 7 -8 3 206.88 17.60 7 -8 3 229.48 15.40 7 -8 3 235.48 17.00 8 -8 3 77.99 8.20 8 -8 3 96.19 10.90 8 -8 3 71.49 6.60 9 -8 3 314.77 24.20 9 -8 3 354.96 22.20 9 -8 3 331.87 21.50 9 -8 3 327.17 23.30 10 -8 3 -6.70 2.70 10 -8 3 2.60 4.60 10 -8 3 2.30 3.90 10 -8 3 -2.30 2.40 11 -8 3 72.09 10.50 11 -8 3 70.69 7.60 11 -8 3 67.79 8.20 11 -8 3 78.99 10.80 -12 8 -3 14.40 5.90 12 -8 3 11.10 4.50 12 -8 3 8.60 5.40 -13 8 -3 74.09 11.10 13 -8 3 88.19 10.30 13 -8 3 63.79 11.00 -14 8 -3 98.89 12.90 14 -8 3 98.29 10.90 14 -8 3 121.69 13.40 -15 8 -3 154.08 16.30 15 -8 3 127.09 16.60 15 -8 3 152.88 14.10 -16 8 -3 -5.20 4.80 16 -8 3 -1.40 6.40 16 -8 3 7.20 5.00 -17 8 -3 25.10 8.40 17 -8 3 43.80 8.20 17 -8 3 13.40 7.50 -18 8 -3 99.89 14.10 18 -8 3 82.79 13.90 17 7 -3 19.40 7.30 -17 -7 3 8.10 6.70 16 7 -3 3.60 5.00 -16 -7 3 -1.70 5.60 15 7 -3 39.10 7.40 -15 -7 3 40.80 10.10 14 7 -3 166.88 15.50 -14 -7 3 187.98 17.90 13 7 -3 300.97 21.70 -13 -7 3 259.17 22.90 12 7 -3 34.30 6.30 -12 -7 3 30.30 8.10 11 7 -3 17.20 4.30 -11 -7 3 17.80 7.00 10 7 -3 108.49 9.40 10 7 -3 119.19 9.90 -10 -7 3 72.29 11.00 9 7 -3 176.18 13.00 -9 -7 3 152.98 15.00 8 7 -3 402.96 25.00 8 7 -3 396.06 25.50 -8 -7 3 388.26 27.60 7 7 -3 6.00 4.50 7 7 -3 9.70 2.60 7 7 -3 12.50 3.20 -7 -7 3 10.00 4.80 6 7 -3 48.50 7.90 6 7 -3 67.29 5.60 6 7 -3 53.39 5.80 -6 -7 3 57.69 8.20 5 7 -3 15.60 5.40 5 7 -3 7.90 2.40 5 7 -3 6.70 2.10 -5 -7 3 12.50 4.60 4 7 -3 670.93 42.80 4 7 -3 667.33 40.30 4 7 -3 665.23 39.90 -4 -7 3 717.23 42.70 3 7 -3 315.17 18.20 3 7 -3 277.27 20.80 3 7 -3 292.27 17.90 2 7 -3 315.97 18.00 2 7 -3 309.67 21.10 2 7 -3 274.97 17.70 -2 -7 3 310.87 20.80 1 7 -3 573.44 36.60 -1 -7 3 587.24 37.80 0 7 -3 1197.18 74.29 0 -7 3 1287.87 74.29 -1 7 -3 19.50 6.00 1 -7 3 30.00 6.20 -2 7 -3 23.60 6.10 2 -7 3 15.10 5.20 2 -7 3 15.40 2.00 -3 7 -3 3.60 1.30 -3 7 -3 9.50 4.80 3 -7 3 0.80 1.50 3 -7 3 3.90 1.40 3 -7 3 6.20 4.90 -4 7 -3 1276.97 71.39 -4 7 -3 1129.09 73.69 4 -7 3 1202.08 71.29 4 -7 3 1196.88 73.89 4 -7 3 1208.58 71.49 4 -7 3 1381.06 74.29 -5 7 -3 2.50 1.70 -5 7 -3 0.90 3.50 5 -7 3 -0.40 3.10 5 -7 3 10.10 4.20 5 -7 3 6.40 4.40 5 -7 3 4.10 1.70 -6 7 -3 130.89 11.70 -6 7 -3 141.39 9.30 6 -7 3 137.29 9.40 6 -7 3 116.09 12.50 6 -7 3 144.69 11.80 6 -7 3 118.09 9.60 -7 7 -3 30.20 3.80 7 -7 3 37.70 4.70 7 -7 3 27.60 6.60 7 -7 3 26.60 5.10 7 -7 3 30.00 3.90 -8 7 -3 245.48 15.20 8 -7 3 229.28 16.40 8 -7 3 222.28 17.50 8 -7 3 216.58 14.90 8 -7 3 214.78 16.80 9 -7 3 1.80 2.20 9 -7 3 10.50 4.80 9 -7 3 5.00 2.70 -10 7 -3 166.08 15.20 10 -7 3 186.88 14.50 10 -7 3 170.68 12.50 10 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20.90 9 -17 4 -0.30 6.20 9 -17 4 11.70 3.80 10 -17 4 183.68 14.60 10 -17 4 224.18 21.00 11 -17 4 5.20 4.10 11 -17 4 20.20 8.00 10 16 -4 109.69 11.30 -10 -16 4 129.79 16.80 9 16 -4 89.09 9.90 -9 -16 4 104.79 14.30 8 16 -4 60.59 6.20 -8 -16 4 48.60 11.90 -7 -16 4 -2.50 5.60 -6 -16 4 22.10 8.20 -5 -16 4 195.38 19.60 -4 -16 4 79.29 13.10 -3 -16 4 16.30 7.30 -2 -16 4 0.30 5.50 -1 -16 4 261.87 22.20 0 -16 4 57.99 10.40 1 -16 4 15.80 6.60 2 -16 4 23.30 7.00 3 -16 4 149.59 15.70 4 -16 4 143.89 15.60 5 -16 4 174.08 17.40 6 -16 4 6.70 2.40 6 -16 4 14.20 6.60 6 -16 4 3.10 2.30 7 -16 4 15.60 3.50 7 -16 4 24.40 3.70 7 -16 4 16.80 6.90 8 -16 4 5.30 2.90 8 -16 4 -3.20 3.20 8 -16 4 6.30 6.30 9 -16 4 290.77 19.20 9 -16 4 271.97 24.20 10 -16 4 19.20 7.00 10 -16 4 2.30 3.40 11 -16 4 2.30 7.00 11 -16 4 -5.10 3.40 12 -16 4 2.90 8.00 12 -16 4 9.80 4.70 11 15 -4 106.09 11.20 -11 -15 4 98.79 15.00 10 15 -4 95.59 10.10 -10 -15 4 92.29 14.60 9 15 -4 142.49 11.10 9 15 -4 154.58 13.70 8 15 -4 0.10 3.20 8 15 -4 7.70 2.70 -8 -15 4 0.50 5.80 7 15 -4 76.69 7.20 7 15 -4 95.19 6.90 -7 -15 4 95.69 13.50 -6 -15 4 53.19 10.40 -5 -15 4 154.88 17.50 -4 -15 4 108.49 14.00 -3 -15 4 19.40 7.20 -2 -15 4 116.19 14.20 -1 -15 4 135.29 14.80 0 -15 4 95.39 12.60 1 -15 4 16.60 6.20 2 -15 4 34.50 8.20 3 -15 4 134.89 15.50 4 -15 4 191.48 18.00 5 -15 4 7.20 6.30 5 -15 4 4.40 1.90 6 -15 4 10.40 2.60 6 -15 4 10.10 6.30 6 -15 4 6.20 2.50 7 -15 4 -2.30 2.10 7 -15 4 -3.50 2.80 7 -15 4 -8.90 5.10 8 -15 4 178.48 12.70 8 -15 4 185.18 18.30 8 -15 4 166.78 13.10 9 -15 4 -1.00 3.00 9 -15 4 8.00 7.00 10 -15 4 45.10 9.70 10 -15 4 50.49 7.10 10 -15 4 48.90 6.60 11 -15 4 15.80 7.90 12 -15 4 209.28 15.20 12 -15 4 151.78 19.80 13 -15 4 -6.80 7.50 13 -15 4 8.40 4.80 12 14 -4 18.90 5.90 -12 -14 4 3.60 7.40 11 14 -4 55.89 7.80 -11 -14 4 43.10 10.80 10 14 -4 157.48 12.20 10 14 -4 164.68 13.20 -10 -14 4 131.29 21.20 9 14 -4 39.80 5.00 9 14 -4 27.20 5.70 -9 -14 4 53.39 9.90 8 14 -4 3.70 2.50 8 14 -4 4.70 3.50 -8 -14 4 4.00 6.40 7 14 -4 11.90 2.50 7 14 -4 4.10 3.00 -7 -14 4 9.60 6.40 6 14 -4 47.30 5.00 -6 -14 4 46.00 9.40 -5 -14 4 86.39 12.30 -4 -14 4 -4.10 4.90 -3 -14 4 146.79 15.50 -2 -14 4 84.79 11.70 -1 -14 4 175.28 16.70 1 -14 4 0.90 5.00 2 -14 4 37.30 9.10 3 -14 4 272.47 22.00 4 -14 4 55.19 9.50 5 -14 4 193.28 12.50 5 -14 4 211.78 18.30 5 -14 4 193.58 12.50 6 -14 4 0.90 2.10 6 -14 4 -2.70 4.80 6 -14 4 -4.50 2.20 7 -14 4 131.69 10.50 7 -14 4 147.19 10.30 8 -14 4 2.80 2.60 8 -14 4 6.00 6.20 8 -14 4 -0.30 3.10 9 -14 4 148.19 13.00 9 -14 4 123.89 15.70 9 -14 4 142.69 11.10 10 -14 4 1.40 6.50 10 -14 4 10.00 4.20 10 -14 4 2.80 3.00 11 -14 4 38.70 10.00 11 -14 4 53.49 6.90 12 -14 4 2.20 6.90 12 -14 4 2.90 4.10 13 -14 4 195.38 22.10 13 -14 4 220.88 16.90 14 -14 4 4.10 4.30 14 -14 4 -0.10 7.80 -13 -13 4 4.10 6.70 12 13 -4 -3.60 4.50 -12 -13 4 -16.80 5.10 11 13 -4 95.89 10.60 -11 -13 4 91.69 16.20 10 13 -4 173.08 13.10 10 13 -4 149.79 12.10 -10 -13 4 145.39 18.30 9 13 -4 45.00 5.50 9 13 -4 60.29 7.30 -9 -13 4 88.99 12.50 8 13 -4 10.80 2.70 8 13 -4 10.20 4.00 -8 -13 4 4.90 5.90 7 13 -4 94.79 7.40 7 13 -4 96.49 8.40 -7 -13 4 95.99 12.90 6 13 -4 110.89 8.10 6 13 -4 114.99 8.80 -6 -13 4 125.49 15.20 5 13 -4 50.79 5.10 5 13 -4 60.79 4.70 -5 -13 4 65.09 10.30 -4 -13 4 1.00 5.20 -3 -13 4 207.98 19.70 -2 -13 4 162.08 16.50 -1 -13 4 111.59 13.10 0 -13 4 234.88 19.60 1 -13 4 6.90 5.60 2 -13 4 215.58 18.40 3 -13 4 175.68 16.60 4 -13 4 307.77 24.50 4 -13 4 320.97 19.00 5 -13 4 20.30 3.20 5 -13 4 28.10 3.40 5 -13 4 25.50 7.80 6 -13 4 15.30 3.30 6 -13 4 21.00 3.30 6 -13 4 7.40 5.80 7 -13 4 11.30 3.40 7 -13 4 9.40 6.50 7 -13 4 15.40 3.20 8 -13 4 146.59 11.20 8 -13 4 155.38 11.30 8 -13 4 139.99 15.70 9 -13 4 14.60 8.30 9 -13 4 13.30 3.60 9 -13 4 10.80 3.30 10 -13 4 69.49 11.80 10 -13 4 68.59 7.60 10 -13 4 84.19 8.00 11 -13 4 8.10 3.50 11 -13 4 -6.00 6.70 12 -13 4 272.37 19.40 12 -13 4 258.77 24.20 13 -13 4 4.80 4.20 13 -13 4 11.60 7.30 14 -13 4 3.00 4.20 14 -13 4 4.60 7.90 15 -13 4 11.10 4.80 15 -13 4 -0.60 9.10 14 12 -4 131.69 13.70 -14 -12 4 95.29 14.90 -13 -12 4 6.80 7.00 12 12 -4 40.80 7.20 -12 -12 4 35.60 15.10 11 12 -4 92.79 10.10 -11 -12 4 93.49 13.70 10 12 -4 98.09 8.90 10 12 -4 90.89 9.70 -10 -12 4 91.69 13.00 9 12 -4 5.60 3.70 9 12 -4 4.90 3.00 -9 -12 4 5.80 5.90 8 12 -4 31.30 4.40 -8 -12 4 47.40 9.60 7 12 -4 176.08 12.10 7 12 -4 178.18 13.10 -7 -12 4 183.18 17.70 6 12 -4 263.87 16.50 6 12 -4 235.18 15.60 -6 -12 4 245.18 20.70 5 12 -4 39.90 5.10 5 12 -4 38.50 4.60 -5 -12 4 55.59 9.30 4 12 -4 8.40 1.90 4 12 -4 7.10 1.50 -4 -12 4 2.00 5.20 -3 -12 4 308.87 23.50 -2 -12 4 235.78 19.80 -1 -12 4 423.46 29.80 0 -12 4 45.00 8.40 1 -12 4 54.09 9.00 2 -12 4 89.69 11.70 3 -12 4 281.27 21.70 4 -12 4 155.48 15.90 4 -12 4 152.88 9.90 4 -12 4 159.78 10.00 5 -12 4 113.69 8.30 5 -12 4 103.59 7.80 5 -12 4 132.59 14.40 6 -12 4 181.08 12.10 6 -12 4 184.88 12.30 6 -12 4 160.48 16.50 7 -12 4 96.79 7.90 7 -12 4 98.79 8.10 7 -12 4 87.99 12.20 8 -12 4 36.40 8.30 8 -12 4 28.30 4.40 8 -12 4 27.60 4.50 9 -12 4 31.10 8.60 9 -12 4 36.10 5.40 9 -12 4 42.50 5.20 10 -12 4 21.20 8.30 10 -12 4 30.60 4.90 10 -12 4 25.00 4.50 11 -12 4 280.97 19.80 11 -12 4 286.97 26.70 12 -12 4 3.50 3.60 12 -12 4 -1.40 6.80 13 -12 4 298.67 25.70 14 -12 4 -7.90 6.20 14 -12 4 3.10 4.00 15 -12 4 53.49 13.00 15 -12 4 68.09 9.40 16 -12 4 -1.30 8.90 16 -12 4 4.00 5.40 15 11 -4 195.38 17.30 -15 -11 4 131.69 21.70 14 11 -4 -0.60 5.50 -14 -11 4 17.00 8.20 13 11 -4 22.30 7.40 12 11 -4 23.70 6.00 -12 -11 4 26.60 8.30 11 11 -4 139.49 13.40 -11 -11 4 179.28 17.20 10 11 -4 4.40 3.20 10 11 -4 4.60 3.70 -10 -11 4 -2.50 5.00 9 11 -4 22.30 4.70 -9 -11 4 16.70 6.70 8 11 -4 33.40 5.40 8 11 -4 36.30 4.80 -8 -11 4 29.00 8.00 7 11 -4 339.87 21.60 7 11 -4 335.57 20.90 -7 -11 4 308.97 25.20 6 11 -4 69.59 6.80 6 11 -4 62.49 5.70 5 11 -4 6.00 2.20 5 11 -4 2.60 2.40 -5 -11 4 -0.10 4.50 4 11 -4 140.69 9.40 4 11 -4 137.19 9.00 -4 -11 4 147.09 14.20 -3 -11 4 343.97 25.30 -2 -11 4 301.07 22.50 -1 -11 4 356.56 25.50 0 -11 4 2.60 4.50 -1 11 -4 34.00 7.70 1 -11 4 22.80 6.10 -2 11 -4 207.98 17.60 2 -11 4 190.48 16.60 -3 11 -4 230.68 18.90 3 -11 4 225.28 18.40 -4 11 -4 37.70 7.60 4 -11 4 34.80 3.50 4 -11 4 38.10 3.60 4 -11 4 37.90 8.20 -5 11 -4 -8.90 3.70 5 -11 4 0.50 5.40 5 -11 4 -0.30 1.50 5 -11 4 -0.20 1.90 5 -11 4 -3.10 3.60 6 -11 4 314.77 25.70 6 -11 4 362.26 21.70 6 -11 4 348.77 21.60 7 -11 4 168.78 17.10 7 -11 4 174.08 12.10 7 -11 4 177.98 12.30 8 -11 4 136.39 9.80 8 -11 4 118.09 11.90 8 -11 4 118.09 14.20 9 -11 4 46.20 9.30 9 -11 4 42.50 5.50 9 -11 4 39.10 5.70 10 -11 4 144.69 11.80 10 -11 4 155.68 11.40 10 -11 4 130.19 16.20 11 -11 4 54.09 6.40 11 -11 4 50.49 7.30 11 -11 4 50.99 10.40 12 -11 4 426.26 28.90 12 -11 4 460.25 38.00 13 -11 4 -3.10 3.80 13 -11 4 5.90 7.10 14 -11 4 12.10 8.40 14 -11 4 28.20 6.60 15 -11 4 -5.00 3.80 15 -11 4 -7.00 7.00 16 -11 4 283.27 21.70 16 -11 4 270.87 25.80 17 -11 4 1.40 8.50 17 -11 4 9.10 5.50 15 10 -4 7.40 6.30 -15 -10 4 -3.00 6.80 14 10 -4 6.30 6.00 -14 -10 4 3.20 6.90 13 10 -4 22.00 7.40 -13 -10 4 10.90 7.40 12 10 -4 329.67 22.50 -12 -10 4 267.47 24.60 11 10 -4 6.00 4.20 -11 -10 4 1.30 5.50 10 10 -4 2.20 3.30 10 10 -4 7.10 3.40 -10 -10 4 10.50 5.30 9 10 -4 39.80 6.20 -9 -10 4 40.50 9.20 8 10 -4 150.08 11.80 8 10 -4 185.08 13.00 -8 -10 4 164.68 15.90 7 10 -4 214.78 14.20 7 10 -4 185.28 13.30 -7 -10 4 191.88 19.40 6 10 -4 327.77 19.50 6 10 -4 281.67 18.80 -6 -10 4 292.57 22.90 5 10 -4 38.60 4.00 5 10 -4 44.50 4.80 -5 -10 4 29.40 7.00 4 10 -4 70.99 5.80 4 10 -4 66.89 5.20 -4 -10 4 68.39 9.50 3 10 -4 344.57 22.10 -3 -10 4 433.16 27.00 -2 -10 4 530.55 35.10 1 10 -4 95.99 11.40 -1 -10 4 101.79 10.80 0 10 -4 28.40 6.40 0 -10 4 28.00 6.30 -1 10 -4 449.16 31.00 1 -10 4 464.65 30.90 -2 10 -4 90.39 11.10 2 -10 4 71.79 9.60 -3 10 -4 24.00 6.10 3 -10 4 12.90 5.30 -4 10 -4 42.30 7.70 4 -10 4 47.00 3.90 4 -10 4 48.80 8.10 4 -10 4 46.20 4.20 -5 10 -4 147.59 15.00 5 -10 4 170.18 15.50 5 -10 4 186.88 11.70 5 -10 4 193.98 15.80 5 -10 4 178.68 11.60 -6 10 -4 288.57 23.10 6 -10 4 303.47 23.10 6 -10 4 308.07 23.60 6 -10 4 337.47 19.90 6 -10 4 317.47 19.60 -7 10 -4 466.95 33.70 7 -10 4 526.55 34.40 7 -10 4 519.95 30.70 7 -10 4 492.25 33.60 7 -10 4 500.45 30.90 8 -10 4 44.00 8.60 8 -10 4 46.80 8.50 8 -10 4 49.20 5.60 9 -10 4 5.90 2.80 9 -10 4 -4.30 5.60 9 -10 4 8.70 3.60 10 -10 4 25.60 5.20 10 -10 4 28.40 4.60 10 -10 4 15.80 7.30 11 -10 4 429.36 27.10 11 -10 4 420.76 30.30 11 -10 4 379.46 26.20 12 -10 4 4.40 3.60 12 -10 4 2.70 6.80 13 -10 4 22.80 8.40 13 -10 4 17.40 4.90 14 -10 4 11.20 4.80 14 -10 4 11.00 7.60 15 -10 4 114.19 15.60 15 -10 4 155.08 13.40 16 -10 4 2.70 7.40 16 -10 4 4.70 5.00 17 -10 4 48.20 8.70 17 -10 4 30.90 10.10 16 9 -4 -5.40 5.70 -16 -9 4 11.00 7.10 15 9 -4 3.30 5.30 -15 -9 4 -6.20 6.40 14 9 -4 6.00 5.00 -14 -9 4 11.70 7.10 13 9 -4 197.88 18.10 12 9 -4 -2.60 4.20 -12 -9 4 8.10 6.40 11 9 -4 120.69 10.70 -11 -9 4 80.79 11.80 10 9 -4 18.60 4.00 10 9 -4 28.40 5.60 -10 -9 4 12.20 6.20 9 9 -4 421.16 27.40 9 9 -4 452.55 27.60 -9 -9 4 374.86 29.80 8 9 -4 28.80 4.30 8 9 -4 37.50 5.80 -8 -9 4 23.50 6.90 7 9 -4 386.76 25.40 7 9 -4 393.16 24.70 -7 -9 4 418.76 28.70 6 9 -4 19.40 3.50 6 9 -4 18.60 3.30 -6 -9 4 18.50 5.70 5 9 -4 33.40 3.90 5 9 -4 24.30 3.10 -5 -9 4 18.40 5.90 4 9 -4 149.19 10.40 4 9 -4 149.88 16.00 4 9 -4 175.58 11.00 -4 -9 4 181.28 14.60 3 9 -4 612.54 37.10 3 9 -4 695.23 37.60 3 9 -4 560.14 40.60 -3 -9 4 673.83 41.20 2 9 -4 12.20 5.20 -2 -9 4 24.40 5.60 1 9 -4 3.40 4.20 -1 -9 4 2.50 4.10 0 9 -4 215.88 17.00 0 -9 4 209.48 16.70 -1 9 -4 251.77 21.70 1 -9 4 313.87 21.00 2 -9 4 360.26 25.00 3 -9 4 74.99 9.70 4 -9 4 77.19 5.80 4 -9 4 75.89 9.70 4 -9 4 83.19 5.70 -5 9 -4 139.39 12.80 5 -9 4 134.19 9.20 5 -9 4 129.89 12.50 5 -9 4 122.59 13.00 5 -9 4 141.09 9.10 -6 9 -4 820.92 51.29 6 -9 4 815.12 48.10 6 -9 4 807.72 50.89 6 -9 4 808.52 51.19 6 -9 4 801.42 47.80 -7 9 -4 48.20 8.00 7 -9 4 30.30 7.80 7 -9 4 44.10 7.30 7 -9 4 45.10 4.90 7 -9 4 54.39 5.80 8 -9 4 13.70 6.10 8 -9 4 10.00 3.00 8 -9 4 2.80 3.00 8 -9 4 6.90 4.00 9 -9 4 20.10 7.00 9 -9 4 25.40 4.10 9 -9 4 18.80 5.50 9 -9 4 19.60 4.30 10 -9 4 459.15 29.90 10 -9 4 473.15 33.00 10 -9 4 466.45 29.30 11 -9 4 45.40 6.40 11 -9 4 32.30 5.30 11 -9 4 40.70 9.30 12 -9 4 81.09 8.80 12 -9 4 74.19 12.00 13 -9 4 7.30 3.80 13 -9 4 15.80 6.80 14 -9 4 197.98 16.60 14 -9 4 219.38 20.40 15 -9 4 7.60 5.00 15 -9 4 -1.30 6.00 -16 9 -4 73.99 12.80 16 -9 4 95.69 14.20 16 -9 4 70.79 10.20 -17 9 -4 -6.20 6.80 17 -9 4 10.50 8.20 17 -9 4 3.80 5.20 -18 9 -4 105.09 15.80 18 -9 4 92.59 15.30 18 -9 4 131.09 16.60 16 8 -4 12.90 6.30 -16 -8 4 22.80 8.30 15 8 -4 -3.90 4.00 -15 -8 4 7.30 9.20 14 8 -4 99.79 12.00 -14 -8 4 97.39 13.80 13 8 -4 -0.70 4.70 -13 -8 4 -3.00 5.00 12 8 -4 339.97 24.10 -12 -8 4 338.57 26.50 11 8 -4 8.20 4.10 -11 -8 4 14.60 6.30 10 8 -4 33.10 5.20 10 8 -4 38.60 6.00 -10 -8 4 17.70 7.10 9 8 -4 16.60 4.30 9 8 -4 24.20 4.30 -9 -8 4 13.80 6.20 8 8 -4 375.06 23.00 8 8 -4 331.07 22.10 -8 -8 4 331.77 25.40 7 8 -4 4.10 2.30 7 8 -4 3.50 2.70 -7 -8 4 -3.10 3.40 6 8 -4 44.50 4.60 6 8 -4 38.70 4.90 -6 -8 4 31.80 6.70 5 8 -4 0.70 2.10 5 8 -4 1.60 1.60 5 8 -4 2.00 4.30 -5 -8 4 -4.60 3.40 4 8 -4 213.28 12.60 4 8 -4 172.48 12.00 4 8 -4 178.98 15.70 -4 -8 4 204.28 15.60 3 8 -4 48.90 4.10 3 8 -4 43.30 3.70 3 8 -4 48.00 7.40 -3 -8 4 46.70 7.20 2 8 -4 3.70 4.50 2 8 -4 3.10 1.30 -2 -8 4 1.90 3.50 1 8 -4 84.99 9.90 0 8 -4 134.99 12.70 0 -8 4 143.79 12.40 -1 8 -4 472.85 31.00 1 -8 4 468.55 30.90 -2 8 -4 57.19 8.70 2 -8 4 71.99 8.90 -3 8 -4 0.20 4.10 3 -8 4 2.40 1.30 3 -8 4 -3.70 3.70 3 -8 4 0.00 0.90 -4 8 -4 44.50 7.20 4 -8 4 28.40 6.50 4 -8 4 33.90 3.30 4 -8 4 38.20 3.40 -5 8 -4 767.62 48.10 5 -8 4 772.12 48.10 5 -8 4 775.32 48.10 5 -8 4 756.02 45.00 5 -8 4 759.72 44.90 -6 8 -4 344.37 25.20 6 -8 4 368.86 22.20 6 -8 4 353.56 24.90 6 -8 4 375.46 22.60 6 -8 4 366.96 25.80 -7 8 -4 180.88 16.80 7 -8 4 185.68 12.70 7 -8 4 185.88 13.20 7 -8 4 226.68 16.90 7 -8 4 181.98 16.30 8 -8 4 9.30 4.60 8 -8 4 0.90 4.90 8 -8 4 8.20 2.30 8 -8 4 2.90 2.40 9 -8 4 218.98 14.60 9 -8 4 224.08 18.40 9 -8 4 209.08 16.70 9 -8 4 205.58 15.10 10 -8 4 55.69 8.30 10 -8 4 58.59 9.90 10 -8 4 71.79 8.00 11 -8 4 198.78 15.10 11 -8 4 242.48 19.30 11 -8 4 214.78 15.90 12 -8 4 11.50 6.90 12 -8 4 11.20 4.10 -13 8 -4 58.89 10.50 13 -8 4 66.69 11.50 13 -8 4 79.89 9.30 14 -8 4 17.20 12.10 -15 8 -4 220.98 20.60 15 -8 4 241.18 21.00 15 -8 4 216.78 18.10 -16 8 -4 -0.40 6.00 16 -8 4 0.50 6.00 16 -8 4 -1.20 4.30 -17 8 -4 46.60 10.80 17 -8 4 50.39 8.90 17 -8 4 70.99 12.40 -18 8 -4 -12.40 6.80 18 -8 4 2.20 7.00 18 -8 4 5.00 5.70 19 -8 4 246.58 21.40 16 7 -4 2.50 5.70 -16 -7 4 9.40 6.90 15 7 -4 29.30 7.10 -15 -7 4 19.40 7.70 14 7 -4 2.10 4.80 -14 -7 4 -7.50 6.10 13 7 -4 354.06 26.00 -13 -7 4 389.26 28.60 12 7 -4 -3.20 4.00 -12 -7 4 4.00 5.80 11 7 -4 17.60 5.00 -11 -7 4 15.30 6.70 10 7 -4 3.80 3.20 10 7 -4 0.70 2.90 9 7 -4 799.02 46.30 9 7 -4 753.72 45.80 -9 -7 4 697.43 48.20 8 7 -4 55.59 6.80 8 7 -4 57.69 6.40 -8 -7 4 46.90 8.50 7 7 -4 99.29 8.40 7 7 -4 120.99 9.20 -7 -7 4 110.19 11.80 6 7 -4 8.50 2.50 6 7 -4 7.80 2.30 6 7 -4 11.10 5.10 -6 -7 4 -0.90 3.70 5 7 -4 296.37 22.50 5 7 -4 309.27 19.60 5 7 -4 338.27 20.10 -5 -7 4 323.77 22.40 4 7 -4 162.88 12.00 4 7 -4 199.28 12.20 4 7 -4 194.28 15.30 -4 -7 4 179.58 14.70 3 7 -4 591.14 35.20 3 7 -4 543.15 37.90 3 7 -4 647.44 35.60 -3 -7 4 608.94 38.20 2 7 -4 2.80 1.20 2 7 -4 3.10 1.30 2 7 -4 8.80 4.10 -2 -7 4 -4.50 3.30 1 7 -4 43.70 6.80 -1 -7 4 51.79 7.00 0 7 -4 234.58 17.80 0 -7 4 239.18 17.70 -1 7 -4 1219.48 73.39 1 -7 4 1221.88 73.39 -2 7 -4 367.76 24.60 2 -7 4 340.67 25.30 -3 7 -4 29.90 6.10 3 -7 4 20.00 2.20 3 -7 4 22.50 2.20 3 -7 4 24.20 6.20 -4 7 -4 408.86 28.00 4 -7 4 420.76 24.90 4 -7 4 455.15 28.40 4 -7 4 409.56 25.00 -5 7 -4 582.14 39.20 5 -7 4 596.04 39.10 5 -7 4 621.24 36.60 5 -7 4 673.53 39.80 5 -7 4 616.74 36.40 -6 7 -4 357.26 24.00 6 -7 4 335.07 23.40 6 -7 4 322.67 21.10 6 -7 4 343.17 20.90 6 -7 4 346.47 23.90 -7 7 -4 130.89 12.20 7 -7 4 143.79 9.80 7 -7 4 143.79 10.20 7 -7 4 131.39 12.10 7 -7 4 140.49 13.60 8 -7 4 86.59 7.30 8 -7 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4 397.66 23.30 5 -6 4 368.16 23.40 5 -6 4 412.36 26.10 -6 6 -4 222.98 16.30 6 -6 4 204.88 13.80 6 -6 4 208.08 15.90 6 -6 4 231.68 17.00 6 -6 4 207.38 13.60 7 -6 4 123.59 11.50 7 -6 4 104.99 8.30 7 -6 4 118.19 8.20 7 -6 4 97.29 10.00 8 -6 4 72.69 9.30 8 -6 4 84.59 7.20 8 -6 4 84.89 6.80 8 -6 4 79.09 8.60 -9 6 -4 245.58 18.70 9 -6 4 231.68 18.40 9 -6 4 238.58 15.90 9 -6 4 237.48 16.30 -10 6 -4 84.49 10.40 10 -6 4 73.49 10.00 10 -6 4 70.19 7.70 10 -6 4 89.49 7.30 10 -6 4 74.89 9.30 -11 6 -4 79.09 10.20 11 -6 4 92.29 9.80 11 -6 4 93.79 11.40 11 -6 4 82.49 7.80 11 -6 4 77.99 8.10 -12 6 -4 107.89 12.30 12 -6 4 121.79 13.90 12 -6 4 109.29 10.50 -13 6 -4 140.59 14.90 13 -6 4 134.89 12.40 13 -6 4 145.09 16.30 -14 6 -4 78.09 11.10 14 -6 4 59.29 10.80 14 -6 4 56.79 8.50 -15 6 -4 246.98 22.30 15 -6 4 233.38 21.20 15 -6 4 229.98 18.60 -16 6 -4 -3.90 5.60 16 -6 4 -0.10 4.00 16 -6 4 4.60 5.50 -17 6 -4 154.08 16.90 17 -6 4 158.08 17.00 17 -6 4 146.09 14.80 -18 6 -4 15.10 7.20 18 -6 4 31.90 8.60 18 -6 4 14.30 6.00 -19 6 -4 193.48 21.40 19 -6 4 245.98 20.80 19 -6 4 217.78 21.90 17 5 -4 131.29 23.90 -17 -5 4 128.79 16.50 16 5 -4 7.00 5.90 -16 -5 4 10.00 6.50 15 5 -4 144.69 14.60 -15 -5 4 153.38 16.00 14 5 -4 9.20 5.40 -14 -5 4 -9.10 5.10 13 5 -4 386.96 25.90 -13 -5 4 337.37 27.20 12 5 -4 0.40 4.10 -12 -5 4 1.50 5.30 11 5 -4 45.20 6.90 -11 -5 4 36.10 7.90 10 5 -4 23.50 4.80 10 5 -4 21.80 4.90 -10 -5 4 21.30 6.30 9 5 -4 875.01 50.99 9 5 -4 886.71 51.29 -9 -5 4 756.32 52.59 8 5 -4 120.59 12.60 8 5 -4 130.59 10.00 8 5 -4 129.29 9.80 -8 -5 4 114.99 11.90 7 5 -4 4.50 2.50 7 5 -4 3.80 4.30 7 5 -4 0.50 1.80 -7 -5 4 -0.20 3.50 6 5 -4 34.80 4.30 6 5 -4 34.60 7.10 6 5 -4 31.40 4.40 -6 -5 4 43.80 6.90 5 5 -4 1187.68 68.69 5 5 -4 1170.98 68.89 5 5 -4 1165.58 70.89 -5 -5 4 1173.38 70.79 4 5 -4 210.28 13.70 4 5 -4 201.08 16.10 4 5 -4 221.68 13.60 -4 -5 4 208.08 15.80 3 5 -4 30.30 3.10 3 5 -4 30.40 6.00 3 5 -4 28.10 3.30 2 5 -4 120.09 7.70 2 5 -4 133.39 11.10 2 5 -4 112.79 7.40 -2 -5 4 96.49 10.30 1 5 -4 982.10 57.89 1 5 -4 935.31 55.29 -1 -5 4 972.90 57.99 0 5 -4 38.20 6.60 0 -5 4 43.30 6.60 -1 5 -4 427.16 27.60 1 -5 4 423.26 27.60 -2 5 -4 84.19 8.90 2 -5 4 79.29 8.90 -3 5 -4 31.60 5.60 3 -5 4 41.00 6.70 3 -5 4 37.10 3.00 3 -5 4 34.10 2.90 -4 5 -4 274.67 19.10 4 -5 4 317.97 19.90 4 -5 4 275.87 19.20 4 -5 4 251.47 16.40 4 -5 4 260.07 16.30 -5 5 -4 244.98 18.90 5 -5 4 260.27 16.30 5 -5 4 268.27 16.60 5 -5 4 293.57 19.60 5 -5 4 265.97 18.90 -6 5 -4 4.10 3.90 6 -5 4 6.20 2.30 6 -5 4 4.10 1.90 6 -5 4 5.60 4.50 6 -5 4 0.60 3.50 7 -5 4 49.00 6.50 7 -5 4 49.90 4.90 7 -5 4 66.19 9.20 7 -5 4 51.09 5.20 -8 5 -4 281.17 21.00 8 -5 4 294.77 18.80 8 -5 4 315.37 21.30 8 -5 4 278.17 19.00 8 -5 4 303.97 20.60 -9 5 -4 34.60 6.50 9 -5 4 44.20 5.00 9 -5 4 38.50 6.10 9 -5 4 34.60 5.00 9 -5 4 38.70 7.10 -10 5 -4 43.90 7.40 10 -5 4 38.30 6.30 10 -5 4 41.80 5.20 10 -5 4 54.39 8.20 10 -5 4 43.70 5.90 -11 5 -4 6.20 4.70 11 -5 4 5.00 3.40 11 -5 4 2.10 4.60 11 -5 4 4.60 2.40 11 -5 4 1.40 3.40 -12 5 -4 278.17 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9.20 19 -4 4 34.90 9.40 19 -4 4 33.10 9.10 -20 4 -4 -5.90 6.20 20 -4 4 -6.60 5.00 20 -4 4 -4.00 6.10 -17 -3 4 22.60 7.50 16 3 -4 11.40 6.00 -16 -3 4 14.60 6.20 15 3 -4 181.38 16.20 -15 -3 4 172.38 17.10 14 3 -4 10.70 5.10 -14 -3 4 0.50 5.50 13 3 -4 28.50 6.40 -13 -3 4 39.70 8.00 12 3 -4 83.59 9.60 -12 -3 4 76.09 10.80 11 3 -4 212.98 16.60 -11 -3 4 225.58 18.20 10 3 -4 -0.80 2.60 10 3 -4 4.80 3.50 -10 -3 4 -4.50 3.90 9 3 -4 492.85 32.50 9 3 -4 534.05 32.50 9 3 -4 516.65 34.30 -9 -3 4 521.55 32.30 -9 -3 4 523.85 34.20 8 3 -4 16.10 3.30 8 3 -4 22.40 5.30 8 3 -4 17.10 3.90 -8 -3 4 15.20 4.30 -8 -3 4 12.30 3.00 7 3 -4 707.33 40.70 7 3 -4 610.54 40.70 7 3 -4 707.03 42.60 -7 -3 4 664.43 42.20 -7 -3 4 674.83 40.60 6 3 -4 24.60 3.80 6 3 -4 23.20 5.60 6 3 -4 21.90 3.70 -6 -3 4 29.80 3.90 -6 -3 4 25.40 5.10 5 3 -4 1017.70 58.49 5 3 -4 1007.40 58.59 5 3 -4 995.00 60.09 -5 -3 4 1003.60 58.39 -5 -3 4 940.71 59.79 4 3 -4 58.69 5.30 4 3 -4 59.09 5.30 4 3 -4 67.49 7.60 -4 -3 4 52.89 5.00 -4 -3 4 62.49 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7.60 -3 -15 5 29.90 8.20 -2 -15 5 -5.50 5.00 -1 -15 5 179.48 17.20 0 -15 5 93.79 13.20 1 -15 5 130.69 15.20 2 -15 5 -1.00 5.60 3 -15 5 227.98 20.50 4 -15 5 62.49 10.40 5 -15 5 306.87 25.10 6 -15 5 42.70 9.10 7 -15 5 31.30 3.70 7 -15 5 27.60 4.00 7 -15 5 43.80 9.10 8 -15 5 34.10 5.20 8 -15 5 33.90 9.60 8 -15 5 52.19 5.30 9 -15 5 74.69 8.20 9 -15 5 91.19 7.90 9 -15 5 99.09 13.50 10 -15 5 91.89 8.40 10 -15 5 81.99 8.90 10 -15 5 87.49 14.00 11 -15 5 7.60 3.90 11 -15 5 17.00 8.30 12 -15 5 12.70 8.70 12 -15 5 17.20 4.90 13 -15 5 19.00 9.60 11 14 -5 1.40 4.60 -11 -14 5 -4.40 6.90 10 14 -5 256.77 18.50 -10 -14 5 244.18 23.20 9 14 -5 -1.90 3.80 9 14 -5 2.70 3.10 8 14 -5 122.49 10.00 8 14 -5 117.99 9.00 -8 -14 5 107.29 15.80 7 14 -5 5.00 2.30 7 14 -5 -3.50 2.30 -7 -14 5 0.50 5.00 -6 -14 5 114.59 15.50 -5 -14 5 15.90 7.30 -4 -14 5 65.09 10.80 -3 -14 5 8.10 6.30 -2 -14 5 54.49 10.00 -1 -14 5 8.80 5.90 0 -14 5 256.37 21.60 1 -14 5 16.20 6.60 2 -14 5 42.50 9.10 3 -14 5 43.80 9.50 4 -14 5 245.28 21.20 5 -14 5 97.49 13.10 6 -14 5 3.40 1.90 6 -14 5 1.30 1.90 6 -14 5 9.50 6.50 7 -14 5 16.00 3.40 7 -14 5 19.70 3.10 7 -14 5 14.00 7.40 8 -14 5 35.00 4.90 8 -14 5 29.00 8.80 8 -14 5 29.40 4.30 9 -14 5 151.38 17.50 9 -14 5 145.09 11.70 9 -14 5 162.58 11.50 10 -14 5 10.90 7.40 10 -14 5 12.40 4.20 10 -14 5 12.40 3.50 11 -14 5 6.00 3.90 11 -14 5 1.90 3.40 11 -14 5 2.60 7.50 12 -14 5 69.19 8.50 12 -14 5 53.39 11.40 13 -14 5 178.28 16.00 13 -14 5 186.68 21.20 14 -14 5 4.30 4.20 14 -14 5 11.70 9.10 12 13 -5 -1.60 4.90 -12 -13 5 -7.20 7.10 11 13 -5 116.69 10.90 -11 -13 5 83.59 13.50 10 13 -5 19.00 5.20 10 13 -5 16.50 4.30 -10 -13 5 18.60 8.70 9 13 -5 219.18 15.30 9 13 -5 198.78 14.00 -9 -13 5 191.78 20.00 8 13 -5 13.10 2.90 8 13 -5 7.30 3.80 -8 -13 5 -0.40 6.20 7 13 -5 71.49 6.80 7 13 -5 68.29 5.90 -7 -13 5 55.19 10.50 6 13 -5 10.80 3.30 6 13 -5 11.40 2.90 -6 -13 5 8.20 5.90 -5 -13 5 232.28 20.30 -4 -13 5 2.80 5.30 -3 -13 5 1.30 5.40 -2 -13 5 23.00 7.20 -1 -13 5 497.05 35.10 1 -13 5 81.69 11.40 2 -13 5 1.70 5.30 3 -13 5 361.96 26.90 4 -13 5 75.69 11.60 5 -13 5 278.77 23.10 6 -13 5 63.79 10.60 6 -13 5 47.70 5.50 6 -13 5 51.49 4.70 7 -13 5 210.48 14.10 7 -13 5 212.28 13.90 8 -13 5 186.18 19.30 8 -13 5 188.48 13.70 8 -13 5 216.98 13.90 9 -13 5 186.58 18.60 9 -13 5 173.88 13.00 9 -13 5 189.78 13.30 10 -13 5 4.30 3.40 10 -13 5 7.00 6.80 10 -13 5 -3.10 2.80 11 -13 5 58.69 7.20 11 -13 5 56.29 11.40 11 -13 5 54.79 6.70 12 -13 5 195.08 14.80 12 -13 5 169.88 20.10 13 -13 5 126.09 11.70 13 -13 5 128.09 16.40 14 -13 5 57.79 8.10 14 -13 5 40.10 11.50 15 -13 5 -6.60 7.50 15 -13 5 6.70 4.70 13 12 -5 13.30 5.80 -13 -12 5 9.60 7.30 12 12 -5 61.09 8.40 -12 -12 5 37.80 10.40 11 12 -5 1.10 4.90 -11 -12 5 -2.50 6.40 10 12 -5 143.49 11.80 10 12 -5 144.09 12.60 -10 -12 5 163.68 16.80 9 12 -5 2.60 4.00 9 12 -5 -1.80 3.40 -9 -12 5 -1.30 5.60 8 12 -5 3.80 2.40 -8 -12 5 6.80 5.90 7 12 -5 27.00 4.30 7 12 -5 18.10 3.20 -7 -12 5 17.30 6.90 6 12 -5 319.07 20.40 6 12 -5 341.67 21.10 -6 -12 5 351.46 26.20 5 12 -5 28.70 3.70 5 12 -5 25.00 3.00 -5 -12 5 28.10 8.00 -4 -12 5 20.70 7.30 -3 -12 5 23.70 10.40 -2 -12 5 456.25 32.10 -1 -12 5 11.60 6.00 0 -12 5 133.19 14.20 1 -12 5 -4.40 5.10 2 -12 5 2.30 5.00 3 -12 5 133.29 14.60 4 -12 5 258.47 21.20 5 -12 5 11.60 2.00 5 -12 5 14.10 2.20 5 -12 5 10.20 6.50 6 -12 5 2.30 1.70 6 -12 5 3.60 5.90 7 -12 5 56.19 9.90 7 -12 5 55.19 5.60 7 -12 5 60.39 5.90 8 -12 5 48.30 5.60 8 -12 5 51.09 5.60 8 -12 5 55.69 10.30 9 -12 5 10.00 2.80 9 -12 5 5.30 6.40 9 -12 5 -3.00 2.30 10 -12 5 5.10 3.20 10 -12 5 4.50 3.20 10 -12 5 -5.70 6.10 11 -12 5 34.50 5.10 11 -12 5 37.40 9.70 11 -12 5 28.80 5.20 12 -12 5 142.09 12.00 12 -12 5 126.59 16.70 13 -12 5 206.98 15.60 13 -12 5 158.88 19.50 14 -12 5 22.60 5.50 14 -12 5 21.30 8.90 15 -12 5 -3.10 7.70 15 -12 5 5.00 4.60 16 -12 5 35.20 11.20 16 -12 5 48.30 7.70 14 11 -5 15.40 6.50 -14 -11 5 16.70 9.30 13 11 -5 0.40 4.90 -13 -11 5 -0.90 5.20 12 11 -5 25.60 6.20 -12 -11 5 17.70 13.00 11 11 -5 117.29 12.00 -11 -11 5 128.39 16.20 10 11 -5 37.80 4.90 10 11 -5 41.60 7.00 -10 -11 5 30.90 8.00 9 11 -5 23.00 5.20 9 11 -5 25.60 5.80 -9 -11 5 22.90 7.10 8 11 -5 -2.00 2.60 8 11 -5 3.20 2.40 -8 -11 5 -2.60 4.30 7 11 -5 329.87 20.80 7 11 -5 317.77 20.00 -7 -11 5 291.57 24.50 6 11 -5 36.50 4.90 6 11 -5 38.60 4.20 -6 -11 5 29.00 7.80 5 11 -5 219.28 14.40 -5 -11 5 224.28 19.30 4 11 -5 3.20 1.80 4 11 -5 2.10 1.30 -4 -11 5 7.40 5.80 -3 -11 5 289.07 22.60 -2 -11 5 51.59 8.70 -1 -11 5 385.36 27.70 0 -11 5 -5.00 3.80 1 -11 5 4.30 5.20 2 -11 5 114.59 13.40 3 -11 5 480.55 33.00 4 -11 5 -2.50 5.10 5 -11 5 54.19 4.60 5 -11 5 50.89 9.40 5 -11 5 47.60 4.10 6 -11 5 116.19 13.90 6 -11 5 130.19 8.80 7 -11 5 302.97 19.40 7 -11 5 319.27 19.50 7 -11 5 289.47 24.60 8 -11 5 83.69 11.80 8 -11 5 73.59 6.70 8 -11 5 73.19 6.70 9 -11 5 -0.30 2.60 9 -11 5 6.40 7.10 9 -11 5 -0.90 2.80 10 -11 5 20.60 4.40 10 -11 5 21.20 7.80 11 -11 5 198.08 14.70 11 -11 5 195.28 27.60 11 -11 5 218.28 15.40 12 -11 5 333.57 27.60 12 -11 5 339.67 23.20 13 -11 5 179.48 14.30 13 -11 5 151.88 18.80 14 -11 5 4.90 7.60 14 -11 5 6.50 4.20 15 -11 5 24.70 6.00 15 -11 5 19.00 9.10 16 -11 5 229.88 18.00 16 -11 5 188.28 22.00 17 -11 5 24.90 10.80 17 -11 5 45.60 8.20 14 10 -5 31.10 7.50 -14 -10 5 28.20 9.80 13 10 -5 13.10 5.70 12 10 -5 130.69 12.90 -12 -10 5 152.88 17.50 11 10 -5 42.70 7.10 -11 -10 5 24.20 7.50 10 10 -5 16.20 3.50 10 10 -5 7.10 4.00 -10 -10 5 -3.40 4.90 9 10 -5 -0.30 3.10 9 10 -5 -2.00 2.40 -9 -10 5 -3.00 4.70 8 10 -5 388.46 24.20 8 10 -5 352.96 23.10 -8 -10 5 357.26 27.60 7 10 -5 35.50 5.30 7 10 -5 33.00 4.40 -7 -10 5 36.60 8.10 6 10 -5 269.87 17.00 6 10 -5 240.38 16.10 5 10 -5 14.80 2.60 5 10 -5 23.50 3.40 -5 -10 5 25.00 6.70 4 10 -5 75.99 5.60 4 10 -5 79.79 6.10 -4 -10 5 68.79 10.00 -3 -10 5 -2.10 4.50 -2 -10 5 769.32 49.20 -1 -10 5 11.90 5.20 0 -10 5 38.60 7.30 -1 10 -5 19.50 6.50 1 -10 5 23.30 6.50 -2 10 -5 349.17 25.50 2 -10 5 357.06 25.40 -3 10 -5 32.50 7.40 3 -10 5 34.30 7.10 -4 10 -5 80.89 10.70 4 -10 5 94.99 11.50 -5 10 -5 4.30 5.00 5 -10 5 8.00 2.00 5 -10 5 9.70 4.30 5 -10 5 4.70 1.70 5 -10 5 6.60 5.70 6 -10 5 219.68 14.10 6 -10 5 212.08 18.80 6 -10 5 225.68 14.40 7 -10 5 165.88 11.70 7 -10 5 171.28 11.60 7 -10 5 167.78 16.10 8 -10 5 437.46 26.30 8 -10 5 410.16 25.90 8 -10 5 398.96 30.40 9 -10 5 8.60 2.80 9 -10 5 12.80 3.20 9 -10 5 2.40 5.80 10 -10 5 150.58 11.60 10 -10 5 137.79 16.60 10 -10 5 135.89 11.10 11 -10 5 145.59 16.90 11 -10 5 135.49 11.60 11 -10 5 147.99 11.40 12 -10 5 193.38 28.80 12 -10 5 161.28 13.30 13 -10 5 69.19 8.70 13 -10 5 59.99 11.70 14 -10 5 10.20 5.20 14 -10 5 5.10 6.70 15 -10 5 73.39 9.60 15 -10 5 68.09 12.80 16 -10 5 56.69 8.90 16 -10 5 42.10 11.00 17 -10 5 72.99 14.20 17 -10 5 84.59 11.10 15 9 -5 20.20 7.60 -15 -9 5 22.30 8.80 14 9 -5 0.90 4.70 -14 -9 5 0.40 6.10 13 9 -5 60.29 9.00 -13 -9 5 63.09 11.90 12 9 -5 133.39 12.50 -12 -9 5 90.89 14.10 11 9 -5 106.99 10.70 -11 -9 5 92.29 13.50 10 9 -5 6.40 3.20 10 9 -5 2.00 3.20 -10 -9 5 -3.60 4.60 9 9 -5 59.89 6.20 9 9 -5 53.59 7.10 -9 -9 5 46.90 9.90 8 9 -5 60.09 7.30 8 9 -5 62.99 6.40 -8 -9 5 57.79 9.90 7 9 -5 213.28 14.20 7 9 -5 212.38 15.10 -7 -9 5 202.88 18.40 6 9 -5 14.10 3.50 6 9 -5 11.00 2.70 -6 -9 5 8.90 5.80 5 9 -5 184.68 12.40 5 9 -5 198.78 13.10 -5 -9 5 200.68 16.80 4 9 -5 94.79 7.00 4 9 -5 109.99 7.60 -4 -9 5 102.09 12.30 3 9 -5 619.94 40.00 3 9 -5 725.03 40.40 -3 -9 5 748.33 44.70 2 9 -5 27.90 6.50 -2 -9 5 27.10 6.30 1 9 -5 101.59 11.10 -1 -9 5 75.69 9.90 0 9 -5 46.40 7.60 0 -9 5 45.40 7.60 -1 9 -5 208.78 16.80 1 -9 5 205.38 16.80 -2 9 -5 -1.60 4.40 2 -9 5 2.10 4.00 -3 9 -5 212.98 17.60 3 -9 5 222.98 17.80 -4 9 -5 17.80 6.20 4 -9 5 19.30 2.30 4 -9 5 20.00 2.10 4 -9 5 24.20 6.50 -5 9 -5 425.16 30.50 5 -9 5 465.75 26.80 5 -9 5 444.36 30.90 5 -9 5 447.46 26.70 5 -9 5 448.36 30.80 -6 9 -5 88.49 11.60 6 -9 5 120.69 8.00 6 -9 5 115.09 8.00 6 -9 5 101.99 12.20 6 -9 5 100.29 11.60 -7 9 -5 915.11 59.59 7 -9 5 957.30 55.99 7 -9 5 955.90 59.99 7 -9 5 962.40 56.29 7 -9 5 962.60 59.39 -8 9 -5 210.18 18.80 8 -9 5 171.18 12.80 8 -9 5 186.18 12.50 8 -9 5 178.78 16.90 8 -9 5 183.48 16.90 9 -9 5 246.58 21.60 9 -9 5 265.97 17.00 9 -9 5 253.27 17.30 10 -9 5 139.79 10.70 10 -9 5 121.49 14.90 10 -9 5 123.89 9.90 11 -9 5 467.35 35.10 11 -9 5 493.15 31.50 11 -9 5 508.85 31.10 12 -9 5 180.98 14.40 12 -9 5 187.38 18.00 13 -9 5 22.80 8.50 13 -9 5 16.20 5.00 14 -9 5 51.09 10.60 15 -9 5 124.59 11.80 15 -9 5 84.19 13.60 16 -9 5 168.88 14.90 16 -9 5 141.29 17.90 17 -9 5 33.60 7.60 17 -9 5 24.40 10.10 18 -9 5 7.70 9.20 18 -9 5 24.90 7.70 15 8 -5 14.70 6.30 -15 -8 5 11.10 7.30 14 8 -5 20.00 5.50 -14 -8 5 16.50 7.90 13 8 -5 66.29 9.60 -13 -8 5 72.89 12.30 12 8 -5 130.59 12.90 -12 -8 5 139.09 15.60 11 8 -5 4.70 3.90 -11 -8 5 0.70 5.00 10 8 -5 0.50 2.60 10 8 -5 -1.20 3.40 -10 -8 5 -4.00 4.90 9 8 -5 36.40 5.80 9 8 -5 39.20 5.30 -9 -8 5 25.20 7.80 8 8 -5 354.86 22.30 8 8 -5 372.36 23.10 -8 -8 5 300.37 25.50 7 8 -5 53.19 5.80 7 8 -5 67.99 7.00 -7 -8 5 53.59 9.50 6 8 -5 164.38 11.50 6 8 -5 144.69 10.70 -6 -8 5 159.28 14.30 5 8 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92.99 9.50 12 -8 5 97.39 13.10 13 -8 5 6.50 6.10 13 -8 5 4.60 3.50 14 -8 5 107.69 14.70 14 -8 5 119.29 11.40 -15 8 -5 125.69 15.80 15 -8 5 120.39 12.30 15 -8 5 129.39 16.00 -16 8 -5 39.70 10.10 16 -8 5 65.99 9.30 16 -8 5 59.19 11.30 -17 8 -5 -0.60 6.10 17 -8 5 -6.50 5.50 17 -8 5 -0.30 4.60 -18 8 -5 45.60 11.00 18 -8 5 55.59 9.50 18 -8 5 28.10 10.00 -19 8 -5 77.09 13.80 19 -8 5 72.89 14.90 19 -8 5 99.79 12.90 16 7 -5 12.00 6.40 -16 -7 5 14.80 7.60 15 7 -5 5.70 5.50 14 7 -5 36.20 7.70 -14 -7 5 36.00 9.10 13 7 -5 113.79 12.50 -13 -7 5 116.99 14.70 12 7 -5 54.49 8.20 -12 -7 5 49.80 10.00 11 7 -5 141.19 12.70 -11 -7 5 139.09 15.70 10 7 -5 7.70 4.40 10 7 -5 12.20 4.20 -10 -7 5 1.30 5.70 9 7 -5 188.88 14.70 9 7 -5 209.78 14.20 -9 -7 5 174.28 16.90 8 7 -5 107.09 9.10 8 7 -5 92.59 8.10 -8 -7 5 66.39 10.60 7 7 -5 225.48 14.70 -7 -7 5 204.68 17.90 6 7 -5 42.00 5.20 6 7 -5 31.10 4.20 -6 -7 5 36.60 6.90 5 7 -5 16.00 5.00 5 7 -5 7.90 2.10 5 7 -5 9.40 2.50 -5 -7 5 4.10 4.30 4 7 -5 13.20 4.90 4 7 -5 5.30 2.00 4 7 -5 7.90 2.10 -4 -7 5 10.60 4.50 3 7 -5 487.85 27.10 3 7 -5 423.16 29.80 3 7 -5 439.66 26.70 -3 -7 5 445.26 30.00 2 7 -5 -3.00 3.90 2 7 -5 3.40 1.30 2 7 -5 0.70 1.00 -2 -7 5 -6.30 2.90 1 7 -5 8.00 4.40 -1 -7 5 8.10 4.20 0 7 -5 33.00 6.10 0 -7 5 21.90 5.50 -1 7 -5 947.41 59.19 1 -7 5 991.40 59.49 -2 7 -5 91.99 10.50 2 -7 5 99.99 10.90 -3 7 -5 24.20 5.60 3 -7 5 24.60 6.50 -4 7 -5 17.10 5.40 4 -7 5 18.00 6.10 4 -7 5 17.20 2.00 4 -7 5 17.20 2.10 -5 7 -5 453.05 32.20 5 -7 5 489.45 32.70 5 -7 5 494.55 29.20 5 -7 5 508.95 32.60 5 -7 5 501.85 29.10 -6 7 -5 114.39 11.50 6 -7 5 139.99 8.90 6 -7 5 119.19 8.80 6 -7 5 135.09 13.20 6 -7 5 129.59 11.80 -7 7 -5 657.83 46.00 7 -7 5 745.33 43.20 7 -7 5 792.92 46.60 7 -7 5 713.33 46.60 7 -7 5 724.13 43.40 8 -7 5 33.00 4.50 8 -7 5 27.70 5.70 8 -7 5 31.40 4.10 8 -7 5 36.70 7.50 9 -7 5 136.49 10.60 9 -7 5 131.29 12.70 9 -7 5 147.69 10.30 9 -7 5 127.89 13.80 10 -7 5 432.26 30.00 10 -7 5 414.46 26.50 10 -7 5 413.26 28.70 10 -7 5 425.36 27.00 11 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6.90 3 -12 7 184.38 17.90 4 -12 7 118.29 14.70 5 -12 7 440.56 32.40 6 -12 7 106.49 13.50 7 -12 7 -0.50 6.30 7 -12 7 8.10 2.40 7 -12 7 8.50 1.80 8 -12 7 252.57 23.80 8 -12 7 274.67 17.30 8 -12 7 277.67 17.10 9 -12 7 166.78 11.40 9 -12 7 156.08 11.40 9 -12 7 157.08 18.20 10 -12 7 11.60 3.40 10 -12 7 17.20 3.60 10 -12 7 8.90 7.40 11 -12 7 5.60 7.40 11 -12 7 2.80 2.90 12 -12 7 134.29 11.40 12 -12 7 148.39 11.30 12 -12 7 134.89 17.50 13 -12 7 108.99 10.30 13 -12 7 100.49 15.60 14 -12 7 122.79 11.10 14 -12 7 108.69 16.30 15 -12 7 17.00 10.60 15 -12 7 13.40 4.70 16 -12 7 13.00 5.40 12 11 -7 -5.30 5.70 -12 -11 7 -4.20 6.20 11 11 -7 -3.50 4.20 -11 -11 7 -3.60 5.80 10 11 -7 222.18 16.80 -10 -11 7 194.38 21.50 9 11 -7 -1.00 3.40 9 11 -7 6.90 3.30 -9 -11 7 6.60 6.10 8 11 -7 4.40 3.80 8 11 -7 6.30 2.70 -8 -11 7 9.10 7.10 7 11 -7 3.20 2.60 7 11 -7 -3.90 2.80 -7 -11 7 6.50 6.20 6 11 -7 69.09 6.00 6 11 -7 67.59 6.60 -6 -11 7 57.39 10.30 5 11 -7 72.19 6.40 5 11 -7 77.39 6.20 -5 -11 7 70.09 11.90 -4 -11 7 216.78 19.50 -3 -11 7 1.90 5.30 -2 -11 7 372.36 28.00 -1 -11 7 21.50 7.90 0 -11 7 570.34 41.60 1 -11 7 10.30 6.60 2 -11 7 1.40 4.80 3 -11 7 50.79 9.60 4 -11 7 187.68 18.50 5 -11 7 98.09 13.60 6 -11 7 62.49 11.00 7 -11 7 57.29 13.40 7 -11 7 80.19 5.80 7 -11 7 73.49 6.10 8 -11 7 128.79 9.40 8 -11 7 133.09 9.50 8 -11 7 152.98 18.20 9 -11 7 137.29 9.70 9 -11 7 124.69 9.70 9 -11 7 114.89 15.00 10 -11 7 75.39 13.10 10 -11 7 105.49 8.50 10 -11 7 113.79 8.80 11 -11 7 20.90 4.40 11 -11 7 10.10 7.60 12 -11 7 51.09 6.30 12 -11 7 53.79 6.80 12 -11 7 32.30 10.30 13 -11 7 218.28 23.20 13 -11 7 251.87 17.80 14 -11 7 112.09 11.00 14 -11 7 114.49 16.30 15 -11 7 12.00 9.10 15 -11 7 35.50 6.30 16 -11 7 15.30 5.20 16 -11 7 4.30 9.20 17 -11 7 201.68 17.00 13 10 -7 21.80 6.90 -13 -10 7 35.40 9.10 -12 -10 7 5.50 7.80 11 10 -7 121.99 12.60 -11 -10 7 79.69 15.50 10 10 -7 12.80 4.90 -10 -10 7 10.80 7.70 9 10 -7 93.79 8.60 9 10 -7 91.49 10.00 -9 -10 7 103.19 14.30 8 10 -7 14.60 3.30 8 10 -7 11.80 4.00 -8 -10 7 9.50 6.30 7 10 -7 159.48 12.80 7 10 -7 173.88 12.00 -7 -10 7 189.18 17.80 6 10 -7 5.30 3.00 6 10 -7 4.90 2.40 -6 -10 7 6.20 6.30 5 10 -7 298.47 19.60 5 10 -7 348.77 20.30 -5 -10 7 309.87 25.10 4 10 -7 0.00 1.80 4 10 -7 -0.40 1.80 -4 -10 7 2.90 5.20 -2 -10 7 -0.10 4.70 -1 -10 7 551.14 37.70 0 -10 7 61.89 10.20 1 -10 7 3.20 5.00 2 -10 7 -4.10 4.20 3 -10 7 339.27 25.60 4 -10 7 199.18 18.30 5 -10 7 73.99 11.50 6 -10 7 18.50 7.70 6 -10 7 12.60 2.00 6 -10 7 14.40 2.20 7 -10 7 434.66 35.10 7 -10 7 547.95 30.40 8 -10 7 237.48 14.50 8 -10 7 222.68 14.40 8 -10 7 175.58 19.70 9 -10 7 237.38 14.90 9 -10 7 221.68 14.90 9 -10 7 180.98 20.00 10 -10 7 75.09 6.50 10 -10 7 61.69 12.30 10 -10 7 69.79 6.90 11 -10 7 201.48 21.80 11 -10 7 273.67 17.40 12 -10 7 270.47 25.20 12 -10 7 278.67 19.40 12 -10 7 321.77 20.40 13 -10 7 245.68 17.60 13 -10 7 225.28 22.60 14 -10 7 69.89 12.50 14 -10 7 54.39 8.00 15 -10 7 0.40 3.80 15 -10 7 -5.90 7.10 16 -10 7 116.29 12.30 16 -10 7 143.99 19.00 17 -10 7 93.29 16.00 17 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365.86 24.40 12 -9 7 370.46 30.10 12 -9 7 392.96 25.20 13 -9 7 306.17 26.10 13 -9 7 325.57 22.30 14 -9 7 33.60 9.60 14 -9 7 30.70 6.00 15 -9 7 0.10 3.70 15 -9 7 9.80 7.90 16 -9 7 103.09 15.40 16 -9 7 98.99 10.90 17 -9 7 189.68 21.50 17 -9 7 183.78 16.50 18 -9 7 18.90 6.40 14 8 -7 4.60 5.80 -14 -8 7 9.90 7.40 13 8 -7 -0.20 4.90 -13 -8 7 -5.40 7.20 12 8 -7 -6.90 4.10 -12 -8 7 -5.00 6.80 11 8 -7 256.87 19.90 -11 -8 7 265.57 22.90 10 8 -7 47.50 7.20 -10 -8 7 34.30 8.60 9 8 -7 0.80 3.80 9 8 -7 5.40 3.10 -9 -8 7 -7.50 4.50 8 8 -7 8.50 3.90 8 8 -7 9.00 3.50 -8 -8 7 9.10 6.30 7 8 -7 507.35 31.10 7 8 -7 477.45 30.20 -7 -8 7 490.55 34.50 6 8 -7 12.70 2.90 6 8 -7 10.90 3.50 5 8 -7 340.97 20.60 5 8 -7 318.07 19.90 -5 -8 7 292.27 24.20 4 8 -7 68.79 5.70 4 8 -7 70.79 6.10 -4 -8 7 67.09 10.30 3 8 -7 232.38 14.20 3 8 -7 230.68 14.50 -3 -8 7 220.18 18.60 -2 -8 7 48.10 8.50 -1 -8 7 585.24 38.70 0 -8 7 7.10 4.90 -1 8 -7 125.29 12.80 1 -8 7 129.99 13.00 -2 8 -7 -0.90 4.50 2 -8 7 -5.10 4.30 -3 8 -7 491.35 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50.19 10.70 5 -17 8 19.70 9.20 6 -17 8 97.29 14.70 7 -17 8 2.80 6.80 -4 -16 8 52.89 12.30 -3 -16 8 150.78 19.10 -2 -16 8 13.00 7.70 -1 -16 8 108.79 15.50 1 -16 8 72.49 15.10 2 -16 8 -5.50 5.30 3 -16 8 102.69 14.70 4 -16 8 1.70 7.00 5 -16 8 111.99 15.30 6 -16 8 8.10 7.60 7 -16 8 191.98 19.90 9 -16 8 53.79 11.50 10 -16 8 27.20 9.60 -6 -15 8 26.20 9.50 -5 -15 8 7.60 6.90 -4 -15 8 101.29 14.60 -2 -15 8 141.99 18.10 -1 -15 8 10.50 7.90 0 -15 8 5.30 6.60 1 -15 8 7.90 6.70 2 -15 8 167.88 18.50 3 -15 8 -0.10 6.60 4 -15 8 9.30 7.00 5 -15 8 -3.40 5.60 6 -15 8 374.76 29.70 7 -15 8 24.00 7.60 8 -15 8 47.00 10.00 9 -15 8 -1.50 6.90 10 -15 8 133.59 17.60 12 -15 8 90.09 14.90 -8 -14 8 42.70 12.00 -7 -14 8 240.38 23.00 -6 -14 8 13.80 7.60 -4 -14 8 39.70 9.80 -3 -14 8 360.46 29.00 -2 -14 8 21.00 8.20 -1 -14 8 20.10 8.50 0 -14 8 -4.70 5.30 1 -14 8 194.88 19.20 2 -14 8 15.50 7.50 3 -14 8 1.80 6.10 4 -14 8 -5.50 5.40 5 -14 8 397.36 30.70 6 -14 8 2.30 7.10 7 -14 8 126.29 16.20 8 -14 8 14.40 7.90 9 -14 8 107.09 15.10 10 -14 8 12.00 8.30 10 -14 8 2.90 2.50 11 -14 8 165.18 18.60 11 -14 8 159.28 11.80 12 -14 8 -3.40 8.40 12 -14 8 -3.80 3.10 13 -14 8 -0.80 12.00 13 -14 8 16.30 4.40 9 13 -8 89.19 10.00 -9 -13 8 99.69 14.90 8 13 -8 264.17 17.80 -8 -13 8 251.47 24.30 7 13 -8 1.50 3.20 -7 -13 8 14.80 6.20 -6 -13 8 7.10 7.40 -5 -13 8 17.30 8.00 -4 -13 8 401.06 31.40 -3 -13 8 56.29 11.10 -2 -13 8 8.50 6.50 -1 -13 8 21.20 6.90 0 -13 8 242.48 21.50 1 -13 8 -3.30 5.20 2 -13 8 154.88 17.90 3 -13 8 -3.10 6.00 4 -13 8 215.08 19.90 5 -13 8 1.10 5.20 6 -13 8 398.76 30.80 7 -13 8 0.50 6.40 8 -13 8 17.70 8.30 9 -13 8 9.30 7.60 9 -13 8 -0.60 1.90 9 -13 8 0.00 2.30 10 -13 8 181.08 12.00 10 -13 8 135.49 18.00 10 -13 8 163.48 11.60 11 -13 8 10.20 3.40 11 -13 8 23.20 4.00 11 -13 8 6.10 7.30 12 -13 8 0.30 3.10 12 -13 8 6.10 8.30 13 -13 8 6.80 8.80 13 -13 8 19.00 4.50 14 -13 8 119.69 11.00 14 -13 8 108.39 26.00 10 12 -8 43.80 7.30 -10 -12 8 46.70 11.20 9 12 -8 157.78 13.40 -9 -12 8 176.58 18.50 8 12 -8 57.69 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6.30 8 -11 9 3.30 1.50 8 -11 9 5.20 1.90 9 -11 9 6.00 2.00 9 -11 9 8.00 2.30 9 -11 9 13.00 6.60 10 -11 9 154.38 10.70 10 -11 9 148.19 17.90 10 -11 9 143.59 10.70 11 -11 9 36.90 9.90 11 -11 9 40.00 4.70 11 -11 9 30.20 4.20 12 -11 9 6.70 3.10 12 -11 9 0.30 8.00 12 -11 9 5.70 3.30 13 -11 9 4.10 8.60 13 -11 9 16.20 3.60 13 -11 9 9.20 3.90 14 -11 9 213.98 22.70 14 -11 9 211.18 16.00 15 -11 9 45.20 13.00 16 -11 9 -14.00 8.80 16 -11 9 6.40 4.20 11 10 -9 -11.10 5.50 -11 -10 9 5.60 7.40 10 10 -9 41.60 7.80 -10 -10 9 45.80 10.30 9 10 -9 7.50 4.40 9 10 -9 9.80 4.60 8 10 -9 198.18 16.60 8 10 -9 155.88 13.70 -8 -10 9 185.38 19.50 7 10 -9 -0.80 5.10 7 10 -9 2.90 3.20 -7 -10 9 -6.80 5.30 6 10 -9 39.40 5.20 6 10 -9 48.40 5.30 -6 -10 9 39.70 10.20 5 10 -9 8.30 3.00 5 10 -9 11.10 2.80 -5 -10 9 4.90 6.30 4 10 -9 186.68 12.00 -4 -10 9 189.98 18.70 -3 -10 9 5.70 5.90 -2 -10 9 -2.60 5.30 -1 -10 9 107.39 14.30 0 -10 9 484.35 34.60 1 -10 9 92.39 12.80 2 -10 9 14.20 7.30 3 -10 9 6.50 6.60 4 -10 9 172.48 17.40 5 -10 9 78.79 12.50 6 -10 9 67.49 11.70 7 -10 9 -6.60 5.90 8 -10 9 4.90 1.80 8 -10 9 -10.10 5.80 8 -10 9 8.80 2.10 9 -10 9 80.69 6.70 9 -10 9 81.09 6.50 9 -10 9 80.49 12.40 10 -10 9 24.20 8.90 10 -10 9 29.00 3.90 10 -10 9 28.70 4.20 11 -10 9 9.20 7.80 11 -10 9 20.30 3.40 11 -10 9 12.90 3.40 12 -10 9 6.40 3.20 12 -10 9 0.40 7.60 12 -10 9 12.20 3.30 13 -10 9 182.08 14.10 13 -10 9 205.38 22.20 13 -10 9 184.58 13.70 14 -10 9 57.09 7.30 14 -10 9 56.59 12.00 15 -10 9 132.19 17.50 15 -10 9 129.89 13.20 16 -10 9 4.50 9.40 16 -10 9 7.20 4.40 17 -10 9 43.60 7.20 17 -10 9 20.30 10.70 11 9 -9 35.20 8.10 10 9 -9 -0.20 4.30 9 9 -9 197.68 15.80 -9 -9 9 208.38 21.00 8 9 -9 1.90 3.50 8 9 -9 2.60 3.10 -8 -9 9 0.00 5.70 7 9 -9 13.20 3.30 7 9 -9 9.30 4.20 -7 -9 9 11.70 7.60 6 9 -9 8.90 3.30 6 9 -9 6.00 3.20 -6 -9 9 1.50 5.70 5 9 -9 396.66 24.20 5 9 -9 389.36 23.90 -5 -9 9 352.66 28.90 4 9 -9 22.00 4.10 4 9 -9 23.40 3.50 -4 -9 9 23.30 7.80 3 9 -9 39.10 3.80 -3 -9 9 35.30 9.30 -2 -9 9 -3.60 5.00 -1 -9 9 423.36 31.60 0 -9 9 102.49 15.10 1 -9 9 47.60 9.10 2 -9 9 21.40 7.20 3 -9 9 80.39 12.10 4 -9 9 21.20 7.30 5 -9 9 132.69 15.50 6 -9 9 44.80 9.90 7 -9 9 35.90 3.50 7 -9 9 31.50 3.30 7 -9 9 35.90 10.20 8 -9 9 101.89 7.50 8 -9 9 104.99 15.30 8 -9 9 106.69 7.60 9 -9 9 133.39 9.20 9 -9 9 116.39 15.30 9 -9 9 118.59 9.00 10 -9 9 92.59 7.50 10 -9 9 99.89 8.10 10 -9 9 68.99 12.10 11 -9 9 -0.10 2.60 11 -9 9 3.90 7.50 11 -9 9 1.10 2.20 12 -9 9 64.39 12.70 12 -9 9 91.99 8.20 12 -9 9 104.59 8.80 13 -9 9 110.49 15.50 13 -9 9 115.49 10.00 13 -9 9 132.59 10.60 14 -9 9 200.08 15.90 14 -9 9 235.08 22.70 15 -9 9 32.00 6.30 15 -9 9 37.70 10.40 16 -9 9 3.70 4.50 16 -9 9 -11.10 6.70 17 -9 9 22.90 6.30 18 -9 9 85.59 14.70 18 -9 9 92.09 11.30 12 8 -9 -5.40 5.20 -12 -8 9 11.90 7.40 11 8 -9 -8.80 5.30 10 8 -9 132.09 13.60 -10 -8 9 143.59 17.80 9 8 -9 1.70 4.40 -9 -8 9 2.10 5.80 8 8 -9 4.90 3.10 8 8 -9 3.20 4.10 -8 -8 9 5.00 5.80 7 8 -9 26.00 5.10 7 8 -9 30.40 5.00 -7 -8 9 13.20 7.60 6 8 -9 259.67 17.30 -6 -8 9 270.07 22.50 5 8 -9 13.70 3.40 5 8 -9 5.10 3.10 -5 -8 9 13.00 6.50 4 8 -9 215.68 14.50 4 8 -9 223.28 14.30 -4 -8 9 203.78 19.20 3 8 -9 42.30 4.60 3 8 -9 40.70 4.40 -2 -8 9 243.88 20.60 -1 -8 9 9.80 5.80 0 -8 9 430.16 30.70 1 -8 9 89.49 11.90 2 -8 9 9.50 5.70 3 -8 9 45.10 8.80 4 -8 9 494.65 34.50 5 -8 9 248.48 21.10 6 -8 9 18.10 7.60 6 -8 9 22.40 2.40 7 -8 9 34.10 8.80 7 -8 9 41.70 4.10 7 -8 9 47.20 4.10 8 -8 9 489.85 37.70 8 -8 9 553.64 32.90 8 -8 9 582.34 33.00 9 -8 9 471.35 28.40 9 -8 9 461.35 28.20 9 -8 9 445.86 33.40 10 -8 9 80.19 13.20 10 -8 9 78.09 7.00 11 -8 9 -2.70 6.30 11 -8 9 6.40 2.80 11 -8 9 4.80 2.70 12 -8 9 11.30 3.50 12 -8 9 8.40 8.20 12 -8 9 17.20 3.70 13 -8 9 242.98 17.20 13 -8 9 248.28 17.60 13 -8 9 253.67 23.00 14 -8 9 91.99 9.50 14 -8 9 96.69 14.60 15 -8 9 106.99 16.20 15 -8 9 144.49 12.30 16 -8 9 -1.50 7.00 16 -8 9 4.90 4.50 17 -8 9 87.29 15.20 17 -8 9 128.29 12.40 18 -8 9 11.50 8.40 18 -8 9 19.50 6.20 -13 -7 9 4.00 7.40 12 7 -9 5.40 6.10 -12 -7 9 0.60 11.50 11 7 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163.78 18.10 12 -7 9 175.48 12.90 12 -7 9 181.88 13.40 13 -7 9 110.59 9.90 13 -7 9 112.79 14.80 13 -7 9 134.99 10.80 14 -7 9 189.18 14.40 14 -7 9 165.18 18.40 15 -7 9 -0.10 3.80 15 -7 9 -4.70 6.10 16 -7 9 73.69 13.60 16 -7 9 85.19 10.20 17 -7 9 81.39 14.40 17 -7 9 118.89 12.10 18 -7 9 40.60 11.90 18 -7 9 53.49 9.00 19 -7 9 -17.90 7.10 19 -7 9 3.50 5.20 13 6 -9 -3.80 5.80 -13 -6 9 8.60 7.60 12 6 -9 57.99 10.50 -12 -6 9 80.49 13.00 11 6 -9 13.40 6.20 -11 -6 9 13.20 8.20 10 6 -9 196.98 16.00 -10 -6 9 180.08 18.20 9 6 -9 13.60 4.90 -9 -6 9 21.80 7.40 8 6 -9 42.70 6.00 8 6 -9 51.29 7.20 -8 -6 9 55.29 10.20 7 6 -9 9.90 3.80 7 6 -9 8.60 3.10 -7 -6 9 3.20 5.50 6 6 -9 509.25 31.10 6 6 -9 473.25 30.30 5 6 -9 33.50 4.60 5 6 -9 22.90 4.50 -5 -6 9 33.20 8.20 4 6 -9 75.49 7.00 4 6 -9 84.89 7.00 -4 -6 9 65.39 6.30 -4 -6 9 85.29 11.30 3 6 -9 16.20 3.10 3 6 -9 10.30 3.00 -3 -6 9 18.70 2.90 -3 -6 9 17.80 6.40 2 6 -9 232.88 15.60 2 6 -9 260.87 17.10 -2 -6 9 254.07 15.40 -2 -6 9 235.78 19.80 1 6 -9 37.50 4.00 1 6 -9 45.20 4.20 -1 -6 9 37.00 7.70 -1 -6 9 39.10 3.60 0 6 -9 220.58 12.80 0 6 -9 195.68 12.70 0 -6 9 206.38 12.50 0 -6 9 195.08 17.50 -1 6 -9 -2.10 4.30 1 -6 9 -5.50 4.00 -2 6 -9 291.17 21.80 2 -6 9 294.17 22.20 -3 6 -9 168.68 15.10 3 -6 9 187.78 16.50 -4 6 -9 239.48 19.20 4 -6 9 259.17 20.20 -5 6 -9 3.80 4.30 -5 6 -9 1.90 1.40 5 -6 9 13.90 5.50 5 -6 9 2.70 1.50 5 -6 9 4.80 4.50 5 -6 9 0.80 1.10 -6 6 -9 265.97 17.30 6 -6 9 290.27 17.20 6 -6 9 266.07 21.80 6 -6 9 288.57 17.10 -7 6 -9 146.89 10.60 7 -6 9 159.38 10.50 7 -6 9 157.18 15.80 7 -6 9 160.38 10.30 -8 6 -9 447.96 28.70 8 -6 9 426.76 32.40 8 -6 9 484.95 28.50 8 -6 9 505.85 28.70 -9 6 -9 136.29 11.10 9 -6 9 148.89 15.80 9 -6 9 169.78 11.20 9 -6 9 158.28 10.90 -10 6 -9 7.80 3.10 10 -6 9 23.80 3.90 10 -6 9 13.70 7.10 10 -6 9 8.10 2.80 11 -6 9 144.49 16.10 11 -6 9 153.08 11.20 11 -6 9 144.79 11.40 12 -6 9 32.00 5.50 12 -6 9 30.00 4.70 13 -6 9 110.49 9.70 13 -6 9 120.19 14.70 13 -6 9 110.19 10.10 14 -6 9 53.99 7.20 14 -6 9 48.10 10.00 15 -6 9 9.50 4.60 15 -6 9 -4.80 5.30 -16 6 -9 10.90 7.50 16 -6 9 28.70 6.30 16 -6 9 22.70 8.90 -17 6 -9 173.18 19.30 17 -6 9 173.78 15.50 17 -6 9 185.48 20.20 -18 6 -9 32.40 9.90 18 -6 9 33.70 10.30 18 -6 9 47.50 8.50 -19 6 -9 3.30 9.10 19 -6 9 3.40 5.20 19 -6 9 1.50 7.50 13 5 -9 16.60 7.00 -13 -5 9 30.80 9.70 12 5 -9 15.40 5.50 -12 -5 9 5.00 6.40 11 5 -9 383.86 27.00 -11 -5 9 363.26 29.40 10 5 -9 3.30 4.90 -10 -5 9 10.70 6.30 9 5 -9 25.40 5.70 -9 -5 9 37.50 8.10 8 5 -9 17.30 4.40 -8 -5 9 9.60 5.80 7 5 -9 419.26 26.20 7 5 -9 401.66 26.90 -7 -5 9 407.86 26.30 6 5 -9 13.20 3.80 6 5 -9 5.80 2.90 -6 -5 9 -0.70 4.50 -6 -5 9 6.00 2.80 5 5 -9 273.17 18.40 5 5 -9 279.17 17.90 -5 -5 9 277.07 21.50 -5 -5 9 262.27 17.80 4 5 -9 42.30 4.90 4 5 -9 38.70 5.00 -4 -5 9 42.20 8.30 -4 -5 9 37.20 4.60 3 5 -9 233.38 16.00 3 5 -9 266.57 16.20 -3 -5 9 246.48 15.90 -3 -5 9 241.78 19.70 2 5 -9 2.40 4.90 2 5 -9 9.10 2.60 2 5 -9 7.20 2.20 -2 -5 9 9.10 2.30 -2 -5 9 4.70 4.50 1 5 -9 922.71 51.09 1 5 -9 722.93 53.29 -1 -5 9 912.41 54.59 -1 -5 9 891.51 50.69 0 5 -9 4.50 1.90 0 5 -9 -1.30 3.90 0 -5 9 5.20 1.60 0 -5 9 4.70 4.70 -1 5 -9 595.44 32.10 -1 5 -9 478.95 34.90 1 -5 9 495.95 35.40 1 -5 9 556.54 31.70 -2 5 -9 48.70 3.90 -2 5 -9 32.50 7.10 2 -5 9 38.00 7.60 2 -5 9 41.10 3.40 -3 5 -9 573.94 30.80 -3 5 -9 471.55 34.10 3 -5 9 492.85 30.50 3 -5 9 539.45 35.00 -4 5 -9 71.39 9.80 -4 5 -9 82.59 6.00 4 -5 9 83.09 6.00 4 -5 9 82.59 10.20 -5 5 -9 42.20 4.10 -5 5 -9 41.20 6.80 5 -5 9 43.10 8.10 5 -5 9 43.00 3.90 5 -5 9 37.20 7.50 -6 5 -9 152.78 14.10 -6 5 -9 141.19 10.70 6 -5 9 164.08 14.40 6 -5 9 153.38 14.90 6 -5 9 164.78 10.30 -7 5 -9 380.46 27.80 -7 5 -9 380.86 24.30 7 -5 9 404.26 27.90 7 -5 9 380.16 23.90 7 -5 9 394.76 27.90 7 -5 9 424.96 24.30 -8 5 -9 415.26 26.90 8 -5 9 457.05 30.90 8 -5 9 412.46 26.50 8 -5 9 470.15 26.90 -9 5 -9 55.69 6.40 9 -5 9 71.19 11.10 9 -5 9 64.59 5.80 9 -5 9 61.69 6.30 -10 5 -9 65.89 7.00 10 -5 9 63.79 6.50 10 -5 9 71.29 6.50 10 -5 9 83.29 11.20 -11 5 -9 172.98 12.60 11 -5 9 165.98 12.30 11 -5 9 156.08 16.10 11 -5 9 155.68 12.00 -12 5 -9 164.38 13.40 12 -5 9 178.28 13.00 12 -5 9 186.18 17.90 12 -5 9 194.08 13.60 -13 5 -9 3.50 3.70 13 -5 9 5.50 6.50 13 -5 9 8.50 3.20 13 -5 9 5.90 3.30 -14 5 -9 3.80 6.60 14 -5 9 -0.90 6.60 14 -5 9 14.90 3.80 -15 5 -9 102.59 14.50 15 -5 9 108.29 15.00 15 -5 9 110.69 10.80 -16 5 -9 256.17 21.70 16 -5 9 225.18 17.70 16 -5 9 189.18 20.10 -17 5 -9 54.89 11.50 17 -5 9 83.09 13.60 17 -5 9 64.39 9.40 -18 5 -9 8.30 7.30 18 -5 9 7.30 5.10 18 -5 9 18.10 8.70 -19 5 -9 12.80 9.40 19 -5 9 -0.30 13.40 19 -5 9 13.60 6.30 -20 5 -9 88.59 15.00 20 -5 9 92.89 15.40 14 4 -9 3.10 6.40 13 4 -9 17.20 6.50 -13 -4 9 -2.30 6.20 12 4 -9 178.98 16.40 -12 -4 9 156.28 17.30 11 4 -9 11.50 5.70 -11 -4 9 9.60 6.80 10 4 -9 212.68 17.10 -10 -4 9 201.48 18.90 9 4 -9 17.40 4.80 -9 -4 9 14.70 4.00 -9 -4 9 9.40 6.00 8 4 -9 51.29 7.00 -8 -4 9 42.00 14.50 -8 -4 9 59.79 7.00 7 4 -9 5.00 3.00 7 4 -9 1.20 3.30 -7 -4 9 8.20 3.30 -7 -4 9 7.90 4.80 6 4 -9 528.75 33.10 -6 -4 9 514.55 35.70 -6 -4 9 524.45 32.50 5 4 -9 14.80 3.80 5 4 -9 10.60 3.20 -5 -4 9 11.20 5.70 -5 -4 9 14.20 3.20 4 4 -9 1.80 2.70 4 4 -9 -0.50 2.50 -4 -4 9 5.60 4.40 -4 -4 9 0.80 1.90 3 4 -9 6.50 2.30 3 4 -9 14.20 4.90 3 4 -9 3.70 2.40 -3 -4 9 10.50 2.50 -3 -4 9 5.90 5.10 2 4 -9 382.46 28.80 2 4 -9 457.15 26.70 -2 -4 9 438.06 26.50 -2 -4 9 462.65 30.20 1 4 -9 2.80 4.30 1 4 -9 2.70 2.00 -1 -4 9 1.40 4.20 -1 -4 9 4.20 1.70 0 4 -9 21.10 3.00 0 4 -9 7.20 5.10 0 -4 9 7.00 4.80 0 -4 9 23.10 2.80 -1 4 -9 3.10 1.70 -1 4 -9 5.60 4.30 1 -4 9 1.00 4.20 1 -4 9 2.30 1.50 -2 4 -9 620.54 44.10 -2 4 -9 776.02 41.10 2 -4 9 692.03 44.30 2 -4 9 672.03 40.60 -3 4 -9 112.99 7.50 -3 4 -9 101.79 12.30 3 -4 9 94.79 7.20 3 -4 9 101.49 11.90 -4 4 -9 306.97 18.00 -4 4 -9 275.27 20.90 4 -4 9 276.27 21.60 4 -4 9 288.67 17.80 -5 4 -9 6.60 1.90 -5 4 -9 -2.20 3.50 5 -4 9 1.90 1.60 5 -4 9 1.30 3.70 5 -4 9 0.50 4.50 -6 4 -9 283.47 22.50 -6 4 -9 310.17 19.70 6 -4 9 301.07 23.00 6 -4 9 351.26 19.60 6 -4 9 307.07 22.80 -7 4 -9 296.87 19.10 -7 4 -9 267.77 21.90 7 -4 9 313.87 22.30 7 -4 9 308.87 18.90 7 -4 9 301.07 22.00 -8 4 -9 528.65 38.70 -8 4 -9 583.74 36.10 8 -4 9 588.04 38.90 8 -4 9 634.34 36.00 8 -4 9 629.44 39.10 -9 4 -9 33.70 4.60 9 -4 9 32.60 4.50 9 -4 9 36.20 7.70 9 -4 9 15.80 6.00 9 -4 9 29.10 4.00 -10 4 -9 100.69 8.80 10 -4 9 112.69 13.30 10 -4 9 104.09 8.60 10 -4 9 101.59 8.20 -11 4 -9 27.80 5.10 11 -4 9 24.60 4.30 11 -4 9 29.10 4.30 11 -4 9 28.10 7.80 -12 4 -9 96.49 9.50 -12 4 -9 87.19 12.60 12 -4 9 103.29 13.00 12 -4 9 105.19 9.40 12 -4 9 106.59 8.80 -13 4 -9 43.70 9.20 -13 4 -9 36.80 6.60 13 -4 9 44.10 6.40 13 -4 9 49.20 6.20 13 -4 9 45.80 9.40 -14 4 -9 -2.40 5.10 14 -4 9 1.70 6.30 14 -4 9 4.00 3.60 -15 4 -9 81.19 12.80 15 -4 9 93.59 9.70 15 -4 9 96.29 13.90 -16 4 -9 52.19 10.90 16 -4 9 97.29 10.90 16 -4 9 76.29 12.50 -17 4 -9 139.99 17.40 17 -4 9 129.39 17.10 17 -4 9 149.49 14.00 -18 4 -9 3.30 7.20 18 -4 9 4.30 6.40 18 -4 9 1.90 4.70 -19 4 -9 52.89 11.40 19 -4 9 57.49 12.50 19 -4 9 65.79 9.90 -20 4 -9 36.50 9.70 20 -4 9 39.90 10.90 14 3 -9 -7.50 5.80 -14 -3 9 -5.40 6.00 13 3 -9 78.29 11.10 -13 -3 9 80.29 12.40 12 3 -9 6.30 5.50 -12 -3 9 10.00 7.20 11 3 -9 191.88 17.10 -11 -3 9 200.08 18.40 -11 -3 9 208.08 15.90 -10 -3 9 3.40 6.10 -10 -3 9 1.60 4.90 9 3 -9 31.30 5.90 -9 -3 9 21.50 4.90 8 3 -9 24.50 5.40 -8 -3 9 24.80 7.20 -8 -3 9 28.10 4.90 7 3 -9 447.06 28.30 7 3 -9 449.95 29.00 -7 -3 9 435.26 30.90 -7 -3 9 439.76 28.30 6 3 -9 6.40 3.30 6 3 -9 11.20 3.80 -6 -3 9 13.70 3.20 -6 -3 9 10.10 5.50 5 3 -9 0.20 2.20 5 3 -9 -1.40 2.40 5 3 -9 1.40 3.90 -5 -3 9 -3.00 1.90 -5 -3 9 -5.20 3.80 4 3 -9 4.80 4.20 4 3 -9 0.30 2.40 -4 -3 9 4.50 4.40 -4 -3 9 4.10 2.50 3 3 -9 554.24 32.70 3 3 -9 505.15 34.50 -3 -3 9 529.55 35.20 -3 -3 9 551.44 32.70 2 3 -9 23.30 3.40 2 3 -9 7.90 4.40 -2 -3 9 16.80 2.90 -2 -3 9 16.50 5.30 1 3 -9 43.20 7.90 1 3 -9 52.89 5.20 -1 -3 9 65.99 8.30 -1 -3 9 49.40 4.60 0 3 -9 -0.90 1.70 0 3 -9 2.80 4.00 0 -3 9 -2.30 3.80 0 -3 9 1.70 1.60 -1 3 -9 736.03 49.60 -1 3 -9 897.21 47.70 1 -3 9 817.92 47.40 1 -3 9 757.22 50.19 -2 3 -9 81.39 6.20 -2 3 -9 66.29 8.50 2 -3 9 74.39 9.40 2 -3 9 68.89 5.70 -3 3 -9 547.85 39.10 -3 3 -9 662.03 37.20 3 -3 9 653.53 40.10 3 -3 9 621.44 36.90 -4 3 -9 20.70 3.20 -4 3 -9 18.40 5.10 4 -3 9 16.40 6.10 4 -3 9 21.80 3.00 -5 3 -9 139.99 13.00 5 -3 9 154.88 10.20 5 -3 9 154.48 13.30 5 -3 9 157.18 14.20 -6 3 -9 96.29 8.00 6 -3 9 107.99 11.50 6 -3 9 111.99 7.80 -7 3 -9 226.58 17.70 -7 3 -9 227.28 15.10 7 -3 9 217.38 14.70 7 -3 9 231.48 17.90 7 -3 9 227.28 17.60 -8 3 -9 17.80 3.40 8 -3 9 15.30 5.20 8 -3 9 9.00 2.50 8 -3 9 12.10 4.20 -9 3 -9 21.50 3.70 9 -3 9 14.30 4.70 9 -3 9 15.30 5.30 9 -3 9 28.60 4.20 -10 3 -9 48.00 6.20 -10 3 -9 53.89 9.00 10 -3 9 50.39 5.90 10 -3 9 50.89 5.30 10 -3 9 39.50 7.70 -11 3 -9 512.95 32.20 -11 3 -9 467.55 34.50 11 -3 9 507.85 31.70 11 -3 9 496.75 31.30 11 -3 9 535.25 34.60 -12 3 -9 77.49 8.50 -12 3 -9 73.89 10.90 12 -3 9 84.09 11.70 12 -3 9 93.99 8.50 12 -3 9 81.49 7.50 -13 3 -9 8.30 3.80 -13 3 -9 16.40 7.20 13 -3 9 6.40 3.60 13 -3 9 13.70 3.70 13 -3 9 22.20 7.00 14 -3 9 93.59 15.40 14 -3 9 131.19 11.10 -15 3 -9 169.08 18.10 15 -3 9 204.68 18.50 15 -3 9 179.28 14.90 -16 3 -9 172.08 17.80 16 -3 9 137.99 13.60 16 -3 9 167.38 18.00 -17 3 -9 13.70 7.80 17 -3 9 35.50 6.90 17 -3 9 38.90 10.20 -18 3 -9 0.90 7.10 18 -3 9 2.30 6.90 18 -3 9 0.30 4.40 -19 3 -9 43.90 11.40 19 -3 9 52.79 9.10 19 -3 9 63.89 12.50 -20 3 -9 145.99 20.40 20 -3 9 144.19 15.30 20 -3 9 167.38 19.20 -21 3 -9 41.40 11.00 21 -3 9 25.00 9.00 21 -3 9 41.60 8.90 14 2 -9 -2.20 4.70 -14 -2 9 20.00 6.90 13 2 -9 16.10 6.60 -13 -2 9 16.70 7.70 12 2 -9 174.58 17.40 -12 -2 9 204.28 15.80 -12 -2 9 200.28 18.40 11 2 -9 26.40 6.60 -11 -2 9 39.00 8.30 -11 -2 9 30.40 5.70 10 2 -9 83.09 11.30 -10 -2 9 82.79 8.40 -10 -2 9 64.79 11.60 9 2 -9 0.80 3.70 -9 -2 9 -0.60 4.60 -9 -2 9 0.60 2.90 8 2 -9 253.77 18.00 -8 -2 9 231.28 19.30 -8 -2 9 228.68 16.90 7 2 -9 9.80 3.90 7 2 -9 9.60 3.60 -7 -2 9 10.90 5.20 -7 -2 9 5.40 3.10 6 2 -9 52.49 7.80 6 2 -9 53.49 6.80 6 2 -9 60.69 6.80 -6 -2 9 49.00 6.10 -6 -2 9 55.29 8.00 5 2 -9 8.40 3.80 5 2 -9 -1.70 2.20 -5 -2 9 5.50 4.00 -5 -2 9 2.50 2.30 4 2 -9 222.38 14.00 4 2 -9 200.88 15.50 -4 -2 9 194.78 15.90 -4 -2 9 181.58 13.70 3 2 -9 0.90 2.30 3 2 -9 4.50 4.00 -3 -2 9 1.20 3.50 -3 -2 9 0.50 1.80 2 2 -9 171.18 11.60 2 2 -9 166.28 13.50 -2 -2 9 161.38 11.30 -2 -2 9 158.38 13.70 1 2 -9 6.10 2.50 1 2 -9 14.90 4.30 -1 -2 9 10.00 2.50 -1 -2 9 7.30 4.50 0 2 -9 114.09 7.80 0 2 -9 92.79 10.20 0 -2 9 92.59 7.30 0 -2 9 91.49 10.30 -1 2 -9 27.80 5.40 -1 2 -9 25.50 3.50 1 -2 9 17.60 5.50 1 -2 9 18.20 3.00 -2 2 -9 811.42 51.49 2 -2 9 848.82 52.09 2 -2 9 862.11 49.60 -3 2 -9 7.50 2.70 -3 2 -9 1.80 3.80 3 -2 9 -2.40 4.80 3 -2 9 6.10 2.50 -4 2 -9 13.00 4.30 4 -2 9 2.40 4.80 4 -2 9 5.80 3.80 4 -2 9 7.40 2.20 -5 2 -9 129.39 12.50 -5 2 -9 166.38 10.90 5 -2 9 152.78 10.30 5 -2 9 146.89 13.20 5 -2 9 153.78 13.70 -6 2 -9 277.37 22.10 -6 2 -9 315.47 20.10 6 -2 9 334.17 22.50 6 -2 9 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10 87.09 12.70 4 8 -10 311.87 19.80 4 8 -10 319.87 19.80 -4 -8 10 283.27 24.40 3 8 -10 33.60 4.20 -3 -8 10 43.70 8.70 2 8 -10 7.20 1.90 2 8 -10 4.90 1.90 -2 -8 10 13.60 6.40 -1 -8 10 82.59 11.90 0 -8 10 238.78 23.10 1 -8 10 30.40 8.10 2 -8 10 29.60 8.40 3 -8 10 3.30 5.70 4 -8 10 12.10 6.30 5 -8 10 9.00 6.50 6 -8 10 254.27 21.90 7 -8 10 0.90 1.40 7 -8 10 2.20 1.50 7 -8 10 6.70 8.00 8 -8 10 163.08 10.70 8 -8 10 154.78 18.50 8 -8 10 159.88 10.70 9 -8 10 8.10 2.40 9 -8 10 4.80 2.40 9 -8 10 9.70 7.50 10 -8 10 264.67 17.50 10 -8 10 288.07 17.80 10 -8 10 255.97 23.80 11 -8 10 9.80 3.00 11 -8 10 24.30 8.90 11 -8 10 13.90 3.10 12 -8 10 50.29 6.20 12 -8 10 53.49 6.00 12 -8 10 37.20 10.10 13 -8 10 28.70 9.20 13 -8 10 16.00 4.20 13 -8 10 23.70 4.50 14 -8 10 318.57 27.30 14 -8 10 315.27 22.00 15 -8 10 38.90 11.30 15 -8 10 28.00 6.10 16 -8 10 16.20 5.10 16 -8 10 2.00 8.10 17 -8 10 -7.30 14.70 17 -8 10 -1.90 4.40 18 -8 10 104.69 16.30 12 7 -10 1.40 6.20 -12 -7 10 6.30 6.80 11 7 -10 5.50 5.30 10 7 -10 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73.29 10.40 -1 5 -10 43.00 4.00 -1 5 -10 24.00 9.40 1 -5 10 22.10 6.70 1 -5 10 29.30 3.20 -2 5 -10 37.20 3.80 -2 5 -10 43.60 7.80 2 -5 10 28.90 3.20 2 -5 10 37.40 7.90 -3 5 -10 705.53 49.20 -3 5 -10 880.51 46.10 3 -5 10 777.42 50.19 3 -5 10 754.22 45.70 -4 5 -10 31.00 3.30 -4 5 -10 15.90 5.30 4 -5 10 26.60 3.00 4 -5 10 31.00 7.60 -5 5 -10 8.60 5.10 -5 5 -10 10.80 2.30 5 -5 10 8.50 7.10 5 -5 10 11.10 5.90 5 -5 10 15.30 2.50 6 -5 10 10.70 6.00 6 -5 10 8.10 2.20 -7 5 -10 510.15 30.60 7 -5 10 451.55 34.10 7 -5 10 530.35 30.40 -8 5 -10 -3.60 1.90 8 -5 10 0.80 2.20 8 -5 10 -0.10 1.90 8 -5 10 -1.50 4.80 -9 5 -10 323.77 21.60 9 -5 10 352.76 21.40 9 -5 10 348.07 25.80 9 -5 10 322.87 21.00 -10 5 -10 4.50 2.80 10 -5 10 4.50 2.50 10 -5 10 19.60 7.40 10 -5 10 2.40 2.40 -11 5 -10 125.69 11.20 11 -5 10 168.98 11.50 11 -5 10 132.49 15.40 11 -5 10 145.79 10.90 -12 5 -10 -2.80 3.00 12 -5 10 5.50 2.90 12 -5 10 4.90 11.20 12 -5 10 -2.80 2.20 -13 5 -10 215.78 16.40 13 -5 10 240.98 16.10 13 -5 10 203.48 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10 -7 11 153.58 10.60 11 -7 11 13.50 2.80 11 -7 11 12.60 3.10 11 -7 11 6.40 7.40 12 -7 11 6.20 2.70 12 -7 11 -0.20 2.70 12 -7 11 2.00 6.70 13 -7 11 294.47 20.80 13 -7 11 344.37 21.50 13 -7 11 311.97 26.80 14 -7 11 65.89 8.20 14 -7 11 74.29 13.10 15 -7 11 121.69 17.50 15 -7 11 165.18 13.20 16 -7 11 13.10 4.90 16 -7 11 16.60 8.90 17 -7 11 48.30 7.50 17 -7 11 33.20 13.90 18 -7 11 16.70 9.80 18 -7 11 11.80 5.30 11 6 -11 16.60 6.50 -11 -6 11 5.40 8.00 10 6 -11 2.10 5.30 -10 -6 11 -0.40 6.10 9 6 -11 164.48 15.20 -9 -6 11 165.48 18.00 8 6 -11 3.70 4.50 -8 -6 11 -1.30 5.20 7 6 -11 -3.60 3.60 7 6 -11 4.60 3.70 -7 -6 11 -11.10 4.80 6 6 -11 -3.30 3.00 6 6 -11 -4.10 3.10 -6 -6 11 -6.90 5.50 5 6 -11 338.27 21.80 5 6 -11 328.47 22.10 -5 -6 11 328.67 21.50 -5 -6 11 335.37 26.00 4 6 -11 34.50 5.20 4 6 -11 41.80 6.50 -4 -6 11 38.70 8.90 3 6 -11 49.90 5.70 3 6 -11 45.00 5.50 -3 -6 11 51.09 9.90 -3 -6 11 48.20 5.10 2 6 -11 -0.30 2.30 2 6 -11 0.40 2.30 -2 -6 11 0.20 5.50 -2 -6 11 5.50 1.90 1 6 -11 132.99 9.40 1 6 -11 128.09 9.30 -1 -6 11 118.59 14.20 -1 -6 11 140.39 9.10 0 6 -11 46.60 4.60 0 6 -11 51.99 4.80 0 -6 11 49.60 4.20 0 -6 11 31.40 8.40 -1 6 -11 194.78 12.00 1 -6 11 184.28 11.50 1 -6 11 163.98 17.20 2 -6 11 42.10 3.40 2 -6 11 38.70 8.80 3 -6 11 75.39 11.10 4 -6 11 167.48 16.20 4 -6 11 154.38 9.80 -5 6 -11 26.80 3.20 5 -6 11 31.40 3.20 5 -6 11 31.10 8.40 -6 6 -11 9.90 2.40 6 -6 11 14.10 2.20 6 -6 11 1.50 5.90 6 -6 11 8.90 2.20 -7 6 -11 24.30 3.60 7 -6 11 29.70 3.40 7 -6 11 27.10 3.40 7 -6 11 13.70 7.20 -8 6 -11 246.88 15.80 8 -6 11 223.88 21.10 8 -6 11 235.18 15.30 8 -6 11 246.68 15.50 -9 6 -11 300.87 20.30 9 -6 11 310.77 25.50 9 -6 11 323.97 20.00 9 -6 11 326.97 20.10 -10 6 -11 53.79 6.40 10 -6 11 46.90 9.80 10 -6 11 54.79 5.60 -11 6 -11 10.20 3.10 11 -6 11 9.10 2.80 11 -6 11 9.00 3.20 11 -6 11 2.00 5.70 -12 6 -11 3.40 2.70 12 -6 11 12.80 3.10 12 -6 11 13.00 7.80 12 -6 11 4.20 2.80 -13 6 -11 107.89 9.40 13 -6 11 79.19 8.50 13 -6 11 107.99 15.00 13 -6 11 91.89 9.00 14 -6 11 233.48 16.60 14 -6 11 207.28 21.50 15 -6 11 7.90 7.10 15 -6 11 2.20 3.60 16 -6 11 16.00 4.70 16 -6 11 3.00 7.50 17 -6 11 1.80 3.90 17 -6 11 2.10 7.20 18 -6 11 132.99 20.00 18 -6 11 192.78 15.70 19 -6 11 5.30 8.90 19 -6 11 4.80 4.80 11 5 -11 -4.50 5.50 -11 -5 11 5.00 7.10 10 5 -11 156.18 15.60 -10 -5 11 195.38 18.50 9 5 -11 3.50 4.60 -9 -5 11 -0.90 6.00 8 5 -11 63.99 8.50 -8 -5 11 76.89 8.20 -8 -5 11 62.29 11.00 7 5 -11 3.90 3.80 -7 -5 11 -5.10 5.20 -7 -5 11 3.40 3.10 6 5 -11 295.67 21.00 6 5 -11 322.77 21.90 -6 -5 11 315.57 25.10 -6 -5 11 331.37 21.10 5 5 -11 4.50 3.60 5 5 -11 2.10 4.60 -5 -5 11 3.40 2.90 -5 -5 11 10.00 6.60 4 5 -11 336.27 22.40 4 5 -11 340.57 22.10 -4 -5 11 332.17 26.40 -4 -5 11 350.26 21.90 3 5 -11 0.20 3.00 3 5 -11 -0.90 2.40 -3 -5 11 0.90 2.20 -3 -5 11 3.60 5.60 2 5 -11 287.57 17.70 2 5 -11 249.97 17.40 -2 -5 11 279.57 17.30 -2 -5 11 251.77 21.80 1 5 -11 60.99 5.70 -1 -5 11 53.49 5.10 -1 -5 11 41.40 8.50 0 5 -11 372.16 21.50 0 -5 11 328.67 21.10 0 -5 11 336.47 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110.39 14.80 7 -9 13 53.59 10.20 8 -9 13 91.89 13.90 9 -9 13 2.30 5.70 10 -9 13 48.60 5.00 10 -9 13 67.09 5.30 10 -9 13 56.59 11.60 11 -9 13 4.30 8.20 11 -9 13 17.30 3.10 11 -9 13 10.90 3.00 12 -9 13 175.18 12.40 12 -9 13 171.18 20.10 12 -9 13 179.38 12.40 13 -9 13 7.80 3.10 13 -9 13 12.90 9.70 14 -9 13 46.20 11.60 14 -9 13 46.40 6.10 15 -9 13 8.20 3.80 15 -9 13 14.70 8.90 16 -9 13 177.78 21.70 7 8 -13 72.89 8.80 -7 -8 13 29.90 10.50 6 8 -13 88.49 9.60 5 8 -13 -1.20 3.80 -5 -8 13 1.20 7.20 4 8 -13 54.59 6.20 4 8 -13 45.00 6.20 -4 -8 13 62.29 11.70 3 8 -13 110.39 9.20 3 8 -13 125.99 9.00 -3 -8 13 102.39 15.20 2 8 -13 93.69 7.40 -2 -8 13 80.89 13.20 -1 -8 13 9.20 7.10 0 -8 13 50.79 10.20 1 -8 13 112.39 14.80 2 -8 13 86.69 12.40 3 -8 13 27.90 7.90 4 -8 13 7.80 6.00 5 -8 13 87.29 13.30 6 -8 13 17.10 6.90 7 -8 13 174.78 18.30 8 -8 13 10.90 7.00 9 -8 13 62.69 12.10 9 -8 13 74.89 6.00 9 -8 13 79.49 6.00 10 -8 13 40.80 4.50 10 -8 13 52.99 11.50 10 -8 13 38.00 4.30 11 -8 13 147.49 10.50 11 -8 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8.10 -9 7 -13 1.80 2.50 9 -7 13 -0.60 2.00 9 -7 13 0.90 1.80 9 -7 13 -0.10 6.70 -10 7 -13 162.28 12.40 10 -7 13 156.28 18.60 10 -7 13 178.58 12.00 10 -7 13 188.38 12.00 11 -7 13 54.39 5.70 11 -7 13 46.20 10.80 11 -7 13 47.70 5.50 12 -7 13 150.48 11.60 12 -7 13 148.39 18.00 12 -7 13 143.09 11.10 13 -7 13 5.70 3.30 13 -7 13 -0.60 7.20 13 -7 13 0.30 2.90 14 -7 13 233.68 24.20 14 -7 13 256.07 17.70 15 -7 13 21.90 9.50 15 -7 13 18.00 4.50 16 -7 13 223.88 24.60 16 -7 13 226.08 17.20 17 -7 13 1.00 8.60 17 -7 13 1.30 4.10 18 -7 13 21.40 10.80 18 -7 13 24.30 5.90 9 6 -13 -4.50 5.60 -9 -6 13 2.00 6.70 8 6 -13 170.28 15.20 -8 -6 13 151.48 18.20 7 6 -13 33.70 6.80 -7 -6 13 22.90 8.90 6 6 -13 3.30 4.10 -6 -6 13 -3.70 6.50 5 6 -13 45.70 6.40 5 6 -13 23.10 5.50 -5 -6 13 22.50 8.60 -5 -6 13 38.60 5.00 4 6 -13 205.28 15.10 4 6 -13 213.98 15.40 -4 -6 13 205.68 14.30 -4 -6 13 188.58 19.70 3 6 -13 110.29 9.90 -3 -6 13 132.79 9.90 -3 -6 13 131.39 16.10 2 6 -13 74.69 7.40 2 6 -13 82.59 7.40 -2 -6 13 76.39 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160.68 11.20 2 -5 13 160.08 17.20 -3 5 -13 -2.50 3.60 3 -5 13 -4.30 5.70 3 -5 13 1.10 1.70 4 -5 13 80.39 11.80 4 -5 13 65.69 5.50 -5 5 -13 401.26 23.90 5 -5 13 360.06 28.60 5 -5 13 381.56 23.40 -6 5 -13 129.29 9.30 6 -5 13 117.09 14.90 6 -5 13 120.49 9.00 -7 5 -13 35.50 4.40 7 -5 13 31.00 4.20 -8 5 -13 82.39 7.20 8 -5 13 81.29 12.00 8 -5 13 71.09 6.50 -9 5 -13 34.30 5.30 9 -5 13 48.30 5.40 9 -5 13 48.60 10.50 -10 5 -13 458.55 28.50 10 -5 13 470.55 28.00 10 -5 13 435.16 27.80 10 -5 13 423.96 32.70 -11 5 -13 199.68 14.30 11 -5 13 210.08 13.80 11 -5 13 177.98 13.30 11 -5 13 177.98 19.00 -12 5 -13 -3.00 2.70 12 -5 13 0.00 2.20 12 -5 13 -3.20 5.60 12 -5 13 1.70 2.70 -13 5 -13 28.10 5.80 13 -5 13 30.80 8.80 13 -5 13 34.00 5.60 13 -5 13 32.30 4.90 14 -5 13 271.67 25.90 14 -5 13 335.27 21.50 15 -5 13 11.00 8.50 15 -5 13 9.30 4.40 16 -5 13 51.49 7.40 16 -5 13 60.69 11.80 17 -5 13 8.20 9.90 17 -5 13 8.20 4.90 18 -5 13 92.79 16.30 18 -5 13 139.09 12.60 19 -5 13 5.70 5.10 19 -5 13 2.50 7.70 10 4 -13 211.88 18.20 -10 -4 13 182.78 19.40 9 4 -13 -5.30 5.50 -9 -4 13 -4.80 3.60 -9 -4 13 2.00 6.40 8 4 -13 169.38 14.10 -8 -4 13 118.19 15.70 -8 -4 13 134.69 12.10 7 4 -13 1.50 4.00 -7 -4 13 -4.90 5.30 -7 -4 13 7.40 3.60 6 4 -13 33.80 6.20 -6 -4 13 33.10 8.50 -6 -4 13 43.50 6.30 5 4 -13 11.30 4.60 5 4 -13 3.50 4.50 -5 -4 13 11.30 3.60 -5 -4 13 -0.50 5.50 4 4 -13 539.25 32.60 4 4 -13 500.35 32.60 -4 -4 13 470.15 36.30 -4 -4 13 522.15 32.10 3 4 -13 92.19 9.50 3 4 -13 93.99 9.20 -3 -4 13 95.09 8.40 -3 -4 13 123.69 13.60 2 4 -13 3.80 3.40 -2 -4 13 6.70 2.80 -2 -4 13 -4.20 9.80 1 4 -13 159.18 11.70 -1 -4 13 145.79 15.70 -1 -4 13 166.78 11.90 0 4 -13 421.86 24.90 0 -4 13 387.96 24.50 0 -4 13 366.76 28.80 -1 4 -13 57.19 6.10 1 -4 13 61.99 10.70 1 -4 13 58.89 5.60 -2 4 -13 69.19 6.60 2 -4 13 58.39 5.60 2 -4 13 74.99 11.40 -3 4 -13 202.28 13.00 3 -4 13 161.68 17.10 3 -4 13 179.28 12.30 -4 4 -13 395.26 24.20 4 -4 13 379.76 23.60 4 -4 13 366.96 28.20 -5 4 -13 371.66 22.30 5 -4 13 315.37 26.30 5 -4 13 343.57 21.70 -6 4 -13 380.46 22.80 6 -4 13 315.57 26.70 6 -4 13 355.46 22.30 -7 4 -13 234.38 16.10 7 -4 13 234.58 15.60 7 -4 13 250.87 21.00 -8 4 -13 228.48 14.70 8 -4 13 198.88 13.90 8 -4 13 174.88 19.10 -9 4 -13 719.93 42.20 9 -4 13 616.34 53.69 -10 4 -13 303.27 20.20 10 -4 13 304.87 19.50 10 -4 13 272.07 24.00 -11 4 -13 4.60 3.90 11 -4 13 4.50 2.60 11 -4 13 -0.80 5.60 -12 4 -13 13.70 4.30 12 -4 13 15.90 3.50 12 -4 13 9.40 7.10 12 -4 13 16.40 3.90 -13 4 -13 96.79 10.40 13 -4 13 128.09 10.10 13 -4 13 106.09 9.40 13 -4 13 101.79 14.00 14 -4 13 36.80 6.20 14 -4 13 37.10 9.50 15 -4 13 147.49 12.50 15 -4 13 136.99 16.80 16 -4 13 0.60 3.80 16 -4 13 -0.90 6.70 17 -4 13 126.99 17.00 17 -4 13 136.89 12.60 18 -4 13 9.90 8.80 18 -4 13 10.70 5.10 19 -4 13 121.29 17.90 19 -4 13 154.28 14.20 20 -4 13 23.50 6.40 10 3 -13 -0.50 5.50 -10 -3 13 11.50 4.60 -10 -3 13 0.70 6.30 9 3 -13 172.78 17.90 -9 -3 13 215.78 16.30 -9 -3 13 223.18 19.70 8 3 -13 11.40 5.60 -8 -3 13 15.30 6.30 -8 -3 13 10.00 4.10 7 3 -13 12.60 5.40 -7 -3 13 2.80 3.70 -7 -3 13 7.50 6.90 6 3 -13 5.80 4.00 -6 -3 13 -5.70 5.40 -6 -3 13 7.80 3.40 5 3 -13 322.77 22.40 -5 -3 13 332.37 21.70 -5 -3 13 304.67 25.60 4 3 -13 66.69 7.80 -4 -3 13 60.59 7.10 3 3 -13 41.10 6.10 -3 -3 13 37.20 8.90 -3 -3 13 65.49 6.80 2 3 -13 -2.60 2.80 -2 -3 13 0.60 2.30 -2 -3 13 9.00 5.90 1 3 -13 250.37 16.50 -1 -3 13 203.08 19.40 -1 -3 13 254.57 16.30 0 3 -13 61.69 6.30 0 -3 13 55.89 6.10 0 -3 13 47.10 9.00 -1 3 -13 169.98 11.50 1 -3 13 145.69 10.70 1 -3 13 137.19 15.50 -2 3 -13 64.29 6.40 2 -3 13 47.00 5.40 2 -3 13 49.00 9.50 -3 3 -13 258.97 16.90 3 -3 13 235.78 16.20 3 -3 13 275.07 21.30 -4 3 -13 504.55 30.30 4 -3 13 483.15 29.70 4 -3 13 464.95 33.70 -5 3 -13 731.93 41.60 5 -3 13 639.64 44.50 5 -3 13 662.83 40.80 -6 3 -13 93.19 8.00 6 -3 13 71.89 11.60 6 -3 13 78.59 7.40 -7 3 -13 27.20 4.80 7 -3 13 23.80 3.90 7 -3 13 14.80 7.20 -8 3 -13 455.95 28.80 8 -3 13 446.76 32.20 8 -3 13 455.55 28.10 -9 3 -13 582.04 36.30 9 -3 13 610.24 35.80 9 -3 13 544.35 39.50 -10 3 -13 209.18 15.80 10 -3 13 200.68 19.80 10 -3 13 239.18 15.50 -11 3 -13 60.19 8.60 11 -3 13 87.89 12.10 11 -3 13 66.59 7.30 -12 3 -13 27.80 5.60 12 -3 13 34.00 5.20 12 -3 13 39.10 9.40 13 -3 13 115.09 15.00 13 -3 13 144.99 11.50 14 -3 13 120.79 10.60 14 -3 13 111.69 15.30 15 -3 13 28.40 5.60 15 -3 13 33.50 9.70 16 -3 13 54.69 7.80 16 -3 13 58.19 12.30 -17 3 -13 6.70 8.00 17 -3 13 12.00 8.10 17 -3 13 14.40 5.10 -18 3 -13 225.68 22.80 18 -3 13 210.48 22.50 18 -3 13 238.08 18.40 -19 3 -13 -6.50 6.20 19 -3 13 5.90 8.30 19 -3 13 5.10 4.70 -20 3 -13 -9.20 7.40 20 -3 13 -9.60 7.30 20 -3 13 -0.10 4.80 10 2 -13 272.67 23.20 -10 -2 13 286.37 21.80 -10 -2 13 326.07 25.60 9 2 -13 8.50 5.50 -9 -2 13 2.40 4.00 -9 -2 13 -3.20 4.90 8 2 -13 80.49 10.60 -8 -2 13 90.19 12.70 -8 -2 13 87.49 9.20 7 2 -13 5.50 4.30 -7 -2 13 -2.30 5.00 6 2 -13 266.07 19.60 -6 -2 13 273.07 18.90 -6 -2 13 245.68 21.40 -5 -2 13 11.00 3.60 -5 -2 13 4.40 4.90 4 2 -13 168.78 12.80 -4 -2 13 153.88 15.70 -4 -2 13 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4.80 -5 -8 14 8.20 6.90 4 8 -14 32.60 5.50 -4 -8 14 34.90 11.80 3 8 -14 6.90 3.60 3 8 -14 -2.10 3.10 -3 -8 14 0.90 7.10 2 8 -14 265.67 17.40 -2 -8 14 295.97 25.00 -1 -8 14 19.20 8.00 0 -8 14 1.30 6.00 1 -8 14 4.50 6.50 2 -8 14 719.53 49.40 3 -8 14 0.80 5.60 4 -8 14 49.60 10.60 5 -8 14 19.70 8.00 6 -8 14 57.19 11.50 7 -8 14 0.50 6.70 8 -8 14 247.88 22.80 9 -8 14 5.80 7.50 9 -8 14 0.60 2.10 10 -8 14 46.40 4.90 10 -8 14 53.59 11.00 10 -8 14 52.89 5.10 11 -8 14 15.70 3.00 11 -8 14 16.30 3.00 11 -8 14 16.20 8.00 12 -8 14 53.69 5.80 12 -8 14 49.99 5.50 12 -8 14 58.39 12.00 13 -8 14 11.10 3.90 13 -8 14 11.20 3.40 13 -8 14 18.20 10.00 14 -8 14 23.40 9.50 14 -8 14 25.60 4.70 15 -8 14 88.29 9.00 15 -8 14 75.09 14.30 16 -8 14 30.50 11.30 7 7 -14 109.19 11.60 -7 -7 14 85.99 14.50 6 7 -14 -2.60 4.60 -6 -7 14 -8.30 7.90 5 7 -14 5.00 4.40 -5 -7 14 -1.90 6.60 4 7 -14 0.50 4.00 4 7 -14 -2.60 3.80 -4 -7 14 5.80 6.70 3 7 -14 383.16 24.40 3 7 -14 395.56 24.10 -3 -7 14 337.67 29.70 2 7 -14 7.50 3.00 2 7 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333.97 23.30 4 6 -14 394.46 24.90 -4 -6 14 352.36 22.60 -4 -6 14 308.67 27.90 3 6 -14 18.50 4.80 3 6 -14 13.30 4.20 -3 -6 14 27.30 8.40 -3 -6 14 16.90 3.30 2 6 -14 137.49 10.80 2 6 -14 132.49 10.40 -2 -6 14 135.79 11.10 -2 -6 14 140.19 16.40 1 6 -14 18.40 3.80 1 6 -14 21.10 4.00 -1 -6 14 22.40 3.40 -1 -6 14 17.40 7.20 0 6 -14 158.38 11.40 0 6 -14 164.78 11.40 0 -6 14 163.28 11.00 0 -6 14 167.18 17.50 -1 6 -14 4.50 2.80 1 -6 14 6.60 1.90 1 -6 14 16.20 6.60 -2 6 -14 649.64 40.80 2 -6 14 648.04 45.60 2 -6 14 709.23 39.80 -3 6 -14 0.50 2.40 3 -6 14 2.10 6.30 3 -6 14 3.30 1.60 -4 6 -14 -0.80 2.20 4 -6 14 4.50 6.10 4 -6 14 5.90 1.80 -5 6 -14 42.20 4.80 5 -6 14 48.30 4.20 5 -6 14 57.79 10.60 6 -6 14 434.86 25.90 6 -6 14 422.96 32.20 -7 6 -14 0.90 2.40 7 -6 14 0.00 2.00 7 -6 14 -1.10 6.80 -8 6 -14 61.49 6.50 8 -6 14 72.19 6.30 8 -6 14 78.29 5.90 8 -6 14 63.89 11.70 -9 6 -14 27.00 4.50 9 -6 14 43.10 10.10 9 -6 14 24.80 3.80 9 -6 14 26.70 3.60 -10 6 -14 533.15 32.80 10 -6 14 511.75 37.90 10 -6 14 530.65 32.10 -11 6 -14 42.00 6.00 11 -6 14 43.10 10.00 11 -6 14 44.50 5.20 11 -6 14 39.60 5.10 -12 6 -14 112.39 10.40 12 -6 14 122.09 9.80 12 -6 14 135.49 17.00 12 -6 14 111.59 10.40 -13 6 -14 11.10 4.30 13 -6 14 5.40 3.00 13 -6 14 12.60 3.70 13 -6 14 -3.30 7.50 14 -6 14 90.79 14.50 14 -6 14 94.49 9.00 15 -6 14 230.58 16.30 15 -6 14 181.38 21.90 16 -6 14 119.49 17.00 16 -6 14 122.69 11.60 17 -6 14 8.10 4.00 17 -6 14 -0.20 8.80 18 -6 14 1.40 9.20 18 -6 14 7.10 4.50 8 5 -14 28.30 7.50 -8 -5 14 51.49 11.50 7 5 -14 112.29 12.00 -7 -5 14 93.59 9.70 -7 -5 14 93.89 14.10 6 5 -14 6.20 4.70 -6 -5 14 9.00 6.60 -6 -5 14 13.00 4.00 5 5 -14 140.89 12.50 -5 -5 14 131.59 16.80 -5 -5 14 148.09 11.50 4 5 -14 4.90 4.00 4 5 -14 1.50 4.80 -4 -5 14 16.80 7.50 -4 -5 14 11.00 3.30 3 5 -14 219.48 16.40 3 5 -14 224.98 17.20 -3 -5 14 228.88 15.50 -3 -5 14 219.98 21.40 2 5 -14 59.49 6.70 2 5 -14 57.39 6.70 -2 -5 14 61.79 6.30 -2 -5 14 56.19 10.20 1 5 -14 4.20 2.80 -1 -5 14 -1.30 2.10 -1 -5 14 11.20 5.90 0 5 -14 -0.20 2.60 0 -5 14 1.60 5.70 0 -5 14 0.40 2.20 -1 5 -14 435.46 25.20 1 -5 14 389.86 24.60 1 -5 14 360.56 29.70 -2 5 -14 7.30 3.10 2 -5 14 0.80 6.70 2 -5 14 10.10 2.50 -3 5 -14 2.10 2.60 3 -5 14 3.00 5.70 3 -5 14 8.20 2.30 -4 5 -14 5.60 2.70 4 -5 14 3.00 2.10 4 -5 14 9.70 6.90 -5 5 -14 437.16 25.50 5 -5 14 397.46 24.90 5 -5 14 386.86 30.20 -6 5 -14 2.80 2.70 6 -5 14 0.70 6.40 6 -5 14 -0.60 2.10 -7 5 -14 60.89 6.20 7 -5 14 51.19 5.70 7 -5 14 47.70 10.50 -8 5 -14 15.90 3.70 8 -5 14 12.70 3.10 8 -5 14 8.50 7.20 -9 5 -14 121.49 9.90 9 -5 14 130.99 15.70 9 -5 14 121.89 9.30 -10 5 -14 53.19 6.30 10 -5 14 44.90 5.50 10 -5 14 62.49 11.20 -11 5 -14 324.87 20.80 11 -5 14 318.87 20.10 11 -5 14 259.97 24.80 11 -5 14 299.87 19.80 -12 5 -14 -5.50 3.30 12 -5 14 7.30 3.20 12 -5 14 -3.20 6.10 12 -5 14 8.00 3.40 -13 5 -14 13.70 4.40 13 -5 14 -1.40 7.30 13 -5 14 14.20 3.60 13 -5 14 12.00 3.20 14 -5 14 24.80 4.80 14 -5 14 26.80 9.70 15 -5 14 287.07 19.80 15 -5 14 263.17 24.70 16 -5 14 72.29 13.90 16 -5 14 63.39 8.40 17 -5 14 -2.00 3.70 17 -5 14 -0.20 8.00 18 -5 14 9.20 9.40 18 -5 14 17.80 5.10 19 -5 14 128.49 13.20 9 4 -14 31.20 8.20 -9 -4 14 24.10 9.60 -9 -4 14 33.40 6.50 8 4 -14 95.49 11.20 -8 -4 14 88.89 9.70 -8 -4 14 72.89 12.20 7 4 -14 55.29 10.70 -7 -4 14 42.20 10.40 -7 -4 14 57.09 8.40 6 4 -14 7.10 4.90 -6 -4 14 4.80 5.90 -6 -4 14 3.00 3.50 5 4 -14 24.50 6.10 -5 -4 14 25.90 9.00 -5 -4 14 28.00 5.10 4 4 -14 274.07 19.40 4 4 -14 266.67 19.60 -4 -4 14 253.57 22.70 -4 -4 14 300.17 19.10 3 4 -14 49.20 6.80 3 4 -14 43.10 6.40 -3 -4 14 40.20 5.50 -3 -4 14 61.19 10.60 2 4 -14 63.29 7.40 -2 -4 14 68.19 11.00 -2 -4 14 68.39 6.80 1 4 -14 0.30 2.80 -1 -4 14 0.80 6.00 -1 -4 14 -1.60 2.20 0 4 -14 312.97 20.20 0 -4 14 315.17 25.10 0 -4 14 307.97 20.20 -1 4 -14 49.20 5.60 1 -4 14 29.90 4.20 -2 4 -14 49.20 6.00 2 -4 14 50.49 5.30 2 -4 14 54.59 11.10 -3 4 -14 0.00 3.00 3 -4 14 -0.70 2.00 3 -4 14 8.20 6.20 -4 4 -14 536.15 31.60 4 -4 14 474.45 35.50 4 -4 14 508.95 30.90 -5 4 -14 1.90 2.70 5 -4 14 2.40 2.50 5 -4 14 5.10 7.00 -6 4 -14 345.37 21.90 6 -4 14 344.77 21.40 6 -4 14 296.57 34.20 -7 4 -14 14.50 3.50 7 -4 14 8.00 8.10 7 -4 14 10.30 3.10 -8 4 -14 34.70 5.20 8 -4 14 28.40 4.30 8 -4 14 37.40 9.20 -9 4 -14 52.69 6.60 9 -4 14 57.69 6.30 9 -4 14 51.69 10.30 -10 4 -14 549.65 34.50 10 -4 14 555.54 33.80 10 -4 14 537.65 38.50 11 -4 14 4.30 2.90 11 -4 14 -2.60 6.50 -12 4 -14 15.00 4.30 12 -4 14 17.20 3.90 12 -4 14 8.10 3.10 12 -4 14 6.20 6.10 13 -4 14 6.20 3.60 13 -4 14 7.00 7.10 13 -4 14 5.40 3.50 14 -4 14 298.47 26.60 14 -4 14 340.37 22.20 15 -4 14 74.59 12.70 15 -4 14 84.69 9.10 16 -4 14 48.30 7.10 16 -4 14 32.70 10.10 17 -4 14 15.40 14.40 17 -4 14 9.70 4.60 18 -4 14 56.89 8.50 18 -4 14 61.19 12.70 19 -4 14 65.89 12.60 19 -4 14 87.39 10.90 9 3 -14 182.18 17.00 -9 -3 14 145.89 17.80 -9 -3 14 190.28 14.90 8 3 -14 48.80 9.10 -8 -3 14 54.49 10.50 -8 -3 14 65.49 8.30 7 3 -14 27.60 6.50 -7 -3 14 20.20 5.20 -7 -3 14 21.50 7.80 6 3 -14 38.80 7.50 -6 -3 14 27.60 8.00 -6 -3 14 38.80 5.90 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25.50 8.70 7 -1 21 26.40 4.70 8 -1 21 136.59 11.20 8 -1 21 121.29 15.90 9 -1 21 3.30 3.70 9 -1 21 -3.40 6.90 10 -1 21 5.40 4.00 10 -1 21 12.30 8.10 11 -1 21 8.60 8.90 11 -1 21 -1.20 4.20 12 -1 21 154.48 14.10 12 -1 21 136.09 18.10 13 -1 21 5.10 4.70 13 -1 21 2.30 7.50 14 -1 21 75.79 8.90 14 -1 21 90.49 14.80 1 0 21 25.30 4.90 1 0 21 32.30 8.10 2 0 21 17.40 6.90 2 0 21 10.30 4.20 3 0 21 186.38 14.50 3 0 21 187.88 19.00 4 0 21 13.20 4.70 4 0 21 18.60 8.20 5 0 21 6.30 3.40 5 0 21 2.30 6.30 6 0 21 5.40 6.60 6 0 21 7.60 3.60 7 0 21 127.99 15.70 7 0 21 128.59 11.30 8 0 21 -3.50 3.50 8 0 21 5.70 7.40 9 0 21 110.29 14.90 9 0 21 108.79 10.70 10 0 21 2.40 6.70 10 0 21 -2.10 4.00 11 0 21 58.09 8.80 11 0 21 43.50 11.00 12 0 21 -3.80 4.30 12 0 21 6.80 8.00 13 0 21 249.78 18.60 14 0 21 -5.20 4.00 14 0 21 -3.90 6.40 15 0 21 -21.90 6.60 15 0 21 -1.40 3.90 0 1 21 62.99 10.70 0 1 21 44.50 7.20 1 1 21 12.40 6.80 1 1 21 3.20 3.70 2 1 21 38.30 8.80 2 1 21 33.70 6.40 3 1 21 36.80 6.00 3 1 21 43.30 8.90 4 1 21 65.69 8.00 4 1 21 68.29 11.00 5 1 21 0.90 3.80 5 1 21 13.90 6.80 6 1 21 68.89 11.30 7 1 21 17.00 7.60 8 1 21 207.98 20.00 9 1 21 -3.70 6.70 10 1 21 8.60 5.00 10 1 21 14.00 8.10 11 1 21 4.10 6.70 11 1 21 -7.50 4.20 12 1 21 207.28 16.30 12 1 21 193.18 21.10 13 1 21 -0.70 4.40 13 1 21 5.10 7.50 14 1 21 -0.20 4.00 15 1 21 -2.60 4.10 15 1 21 2.40 7.10 16 1 21 46.90 11.80 16 1 21 64.09 8.60 0 2 21 -0.40 3.90 0 2 21 9.20 6.10 1 2 21 33.10 7.80 2 2 21 17.10 5.20 2 2 21 23.50 6.70 3 2 21 308.17 24.30 3 2 21 290.77 21.40 4 2 21 0.20 3.50 4 2 21 12.30 6.80 5 2 21 13.20 4.40 5 2 21 15.20 7.20 6 2 21 18.40 6.90 6 2 21 1.30 3.90 7 2 21 408.36 26.70 7 2 21 369.06 29.10 8 2 21 1.90 6.80 8 2 21 -3.50 4.00 9 2 21 11.50 7.20 9 2 21 12.50 5.10 10 2 21 -5.90 4.30 10 2 21 -1.60 6.60 11 2 21 168.68 18.30 11 2 21 130.09 13.20 12 2 21 -0.90 4.40 12 2 21 2.50 6.80 13 2 21 48.40 10.90 13 2 21 50.69 8.00 14 2 21 8.10 9.10 14 2 21 -5.00 3.90 15 2 21 35.40 7.20 16 2 21 -2.70 4.50 16 2 21 -6.20 7.30 17 2 21 43.80 10.90 17 2 21 56.79 8.50 -1 3 21 10.50 4.60 -1 3 21 14.20 6.30 0 3 21 -1.70 4.10 0 3 21 4.00 6.40 1 3 21 65.59 9.50 1 3 21 57.89 8.20 2 3 21 188.18 17.50 2 3 21 152.58 14.00 3 3 21 43.20 7.30 3 3 21 59.89 10.00 4 3 21 21.30 7.70 4 3 21 29.90 5.60 5 3 21 5.70 4.20 5 3 21 2.20 5.10 6 3 21 100.99 12.60 6 3 21 109.19 11.10 7 3 21 54.09 8.00 7 3 21 58.59 10.30 8 3 21 60.19 10.90 8 3 21 74.69 8.90 9 3 21 -0.50 6.60 9 3 21 -6.90 4.00 10 3 21 15.80 5.70 10 3 21 30.40 8.30 11 3 21 1.40 7.50 11 3 21 -4.60 4.20 12 3 21 140.19 13.40 12 3 21 143.89 16.80 13 3 21 3.80 4.50 13 3 21 -10.40 5.90 14 3 21 18.60 8.50 14 3 21 13.20 5.40 15 3 21 2.40 7.90 15 3 21 -4.30 4.30 16 3 21 197.08 16.10 16 3 21 162.48 20.80 17 3 21 4.50 8.00 17 3 21 -0.20 4.50 -1 4 21 6.20 4.90 -1 4 21 11.30 6.90 0 4 21 19.90 5.90 1 4 21 165.78 14.40 1 4 21 159.38 17.60 2 4 21 67.19 8.80 2 4 21 77.09 11.40 3 4 21 133.09 12.70 3 4 21 161.68 15.60 4 4 21 3.10 5.80 4 4 21 11.80 4.90 5 4 21 81.29 9.80 6 4 21 58.99 9.70 6 4 21 41.70 6.80 7 4 21 268.47 20.20 7 4 21 274.67 22.10 8 4 21 11.80 5.50 8 4 21 1.50 6.20 9 4 21 0.10 6.40 9 4 21 0.10 4.90 10 4 21 -7.60 4.50 10 4 21 -11.00 6.10 11 4 21 233.08 21.20 11 4 21 250.17 19.20 12 4 21 20.50 6.10 12 4 21 17.40 7.80 13 4 21 -0.40 4.60 13 4 21 3.20 7.30 14 4 21 -6.70 6.10 14 4 21 12.20 5.50 15 4 21 174.48 15.00 15 4 21 163.28 19.10 16 4 21 -2.30 8.10 16 4 21 4.40 4.80 17 4 21 29.70 10.00 17 4 21 18.10 6.20 18 4 21 4.60 5.80 -1 5 21 11.70 5.80 -1 5 21 1.00 4.60 0 5 21 59.39 8.90 0 5 21 55.29 9.00 1 5 21 202.68 17.30 1 5 21 172.98 15.70 2 5 21 73.29 9.90 2 5 21 95.09 11.50 3 5 21 31.40 7.50 3 5 21 26.90 5.80 4 5 21 -3.30 5.40 4 5 21 6.90 4.20 5 5 21 20.10 5.80 5 5 21 23.00 6.40 6 5 21 195.78 15.70 6 5 21 174.78 17.50 7 5 21 25.80 7.90 7 5 21 21.00 6.00 8 5 21 0.50 4.90 8 5 21 8.20 9.40 9 5 21 1.40 5.20 9 5 21 -1.50 6.10 10 5 21 148.69 16.70 10 5 21 163.58 14.90 11 5 21 47.70 8.10 11 5 21 52.49 10.40 12 5 21 -0.30 5.00 12 5 21 -13.10 5.40 13 5 21 -9.90 6.50 13 5 21 5.50 4.90 14 5 21 239.68 18.40 14 5 21 198.58 20.90 15 5 21 1.10 7.90 15 5 21 -10.00 3.90 16 5 21 134.79 17.50 16 5 21 152.28 14.40 17 5 21 3.90 5.40 17 5 21 -4.10 8.10 18 5 21 50.69 12.20 18 5 21 54.79 9.30 -1 6 21 5.00 5.00 -1 6 21 -0.30 5.50 0 6 21 111.79 12.20 0 6 21 110.09 12.30 1 6 21 141.89 13.60 1 6 21 137.59 13.70 2 6 21 31.00 6.40 2 6 21 35.40 8.00 3 6 21 42.80 8.80 3 6 21 45.00 7.60 4 6 21 10.00 4.70 4 6 21 -1.00 5.30 5 6 21 218.68 18.90 5 6 21 227.48 17.90 6 6 21 33.10 6.90 6 6 21 34.70 8.00 7 6 21 17.80 7.50 7 6 21 9.70 5.50 8 6 21 11.70 5.50 8 6 21 29.50 8.60 9 6 21 170.08 21.20 9 6 21 132.99 13.60 10 6 21 21.70 6.70 10 6 21 13.10 7.40 11 6 21 115.69 12.70 11 6 21 126.99 15.20 12 6 21 -3.00 4.30 12 6 21 1.30 6.50 13 6 21 64.99 9.30 13 6 21 70.89 12.00 14 6 21 -1.10 4.10 14 6 21 -6.00 6.70 15 6 21 167.48 18.00 15 6 21 160.48 15.10 16 6 21 9.50 7.10 16 6 21 -0.50 5.20 17 6 21 1.90 9.90 17 6 21 -10.10 7.10 18 6 21 9.40 5.90 18 6 21 -13.00 7.10 -1 7 21 20.80 7.00 -1 7 21 27.10 5.90 0 7 21 85.29 11.20 0 7 21 95.29 10.90 1 7 21 139.09 13.40 1 7 21 128.29 13.70 2 7 21 55.29 8.40 2 7 21 42.80 8.20 2 7 21 77.19 9.00 3 7 21 -0.20 5.40 3 7 21 -0.30 3.80 3 7 21 1.10 4.90 4 7 21 83.29 10.80 4 7 21 116.39 12.30 4 7 21 81.09 10.60 5 7 21 90.09 10.90 5 7 21 67.49 9.50 6 7 21 42.50 8.70 6 7 21 36.60 7.80 7 7 21 9.20 6.00 7 7 21 20.90 7.70 8 7 21 51.79 9.00 8 7 21 44.90 8.40 9 7 21 36.60 8.30 9 7 21 54.49 9.70 10 7 21 171.08 15.70 10 7 21 166.08 17.60 11 7 21 24.30 7.90 11 7 21 29.10 7.50 12 7 21 0.00 6.10 12 7 21 -4.70 5.20 13 7 21 0.40 4.90 13 7 21 -0.50 6.70 14 7 21 317.37 25.60 14 7 21 310.87 23.50 15 7 21 16.00 8.10 15 7 21 5.30 5.50 16 7 21 17.20 5.60 16 7 21 13.40 8.00 -17 -7 -21 -5.30 7.40 17 7 21 -5.80 7.90 17 7 21 0.60 5.80 -18 -7 -21 141.99 19.00 18 7 21 133.29 14.20 18 7 21 123.49 17.00 -1 8 21 11.20 5.20 -1 8 21 9.70 5.20 0 8 21 82.99 15.50 0 8 21 50.79 7.80 1 8 21 51.69 8.00 1 8 21 43.00 7.10 2 8 21 23.20 6.40 2 8 21 33.00 6.80 3 8 21 19.80 5.50 3 8 21 9.00 4.90 3 8 21 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9 21 -2.70 4.90 7 9 21 10.50 5.80 7 9 21 -7.20 4.80 8 9 21 171.08 16.50 8 9 21 186.08 16.70 9 9 21 98.59 12.80 9 9 21 109.09 12.70 10 9 21 173.48 16.00 10 9 21 150.48 16.00 11 9 21 -3.70 5.90 11 9 21 -8.20 5.20 12 9 21 78.69 11.40 12 9 21 87.89 11.50 13 9 21 7.70 6.50 13 9 21 14.80 7.00 14 9 21 241.28 19.80 14 9 21 211.28 20.40 15 9 21 21.80 7.80 15 9 21 25.30 7.00 -16 -9 -21 34.40 9.70 16 9 21 44.10 9.80 16 9 21 35.50 10.20 -17 -9 -21 -4.90 7.20 17 9 21 0.40 5.20 -18 -9 -21 111.79 26.70 18 9 21 190.78 16.70 -1 10 21 15.50 5.70 0 10 21 59.39 9.20 1 10 21 18.70 6.60 2 10 21 15.90 6.10 2 10 21 4.40 3.80 3 10 21 64.79 7.60 3 10 21 82.89 9.30 3 10 21 67.09 10.00 4 10 21 146.39 14.50 4 10 21 149.99 13.30 4 10 21 136.99 12.40 5 10 21 198.18 15.20 5 10 21 182.48 17.00 5 10 21 161.48 14.50 6 10 21 4.10 4.90 6 10 21 -11.90 4.70 6 10 21 0.30 4.30 7 10 21 63.29 10.00 7 10 21 61.19 8.70 7 10 21 83.79 10.00 8 10 21 81.89 10.60 8 10 21 81.19 11.30 8 10 21 64.89 9.50 9 10 21 271.17 20.80 9 10 21 239.08 21.30 10 10 21 -6.20 5.90 10 10 21 0.20 6.60 11 10 21 -4.10 5.40 11 10 21 -1.40 5.30 12 10 21 9.80 6.90 12 10 21 6.30 8.30 13 10 21 115.59 13.40 13 10 21 91.19 12.40 14 10 21 8.40 7.10 14 10 21 6.00 5.90 -15 -10 -21 2.60 7.00 15 10 21 2.40 6.70 -16 -10 -21 -9.70 6.30 16 10 21 -5.90 5.20 16 10 21 -7.10 6.70 -17 -10 -21 139.69 17.80 17 10 21 132.69 17.70 17 10 21 150.98 14.80 18 10 21 -0.80 10.20 18 10 21 4.10 6.20 0 11 21 31.60 7.70 1 11 21 5.80 5.30 2 11 21 16.90 7.50 3 11 21 158.78 16.20 4 11 21 153.08 12.60 4 11 21 161.28 16.20 4 11 21 161.48 12.80 5 11 21 42.50 6.60 5 11 21 41.00 8.60 5 11 21 57.69 7.30 6 11 21 8.30 5.70 6 11 21 2.40 4.40 6 11 21 15.80 8.20 7 11 21 71.19 8.80 7 11 21 87.89 9.90 7 11 21 59.69 10.40 8 11 21 152.48 14.80 8 11 21 164.28 14.90 8 11 21 188.88 17.50 9 11 21 71.79 10.50 9 11 21 76.59 11.70 9 11 21 71.79 10.20 10 11 21 5.50 7.00 10 11 21 22.90 7.40 11 11 21 -1.50 6.40 11 11 21 2.30 6.10 12 11 21 151.98 16.40 12 11 21 132.99 14.50 13 11 21 32.00 8.90 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0.5614 20 10 4 9.3147 -0.6012 20 10 5 -2.6308 -1.8431 20 10 6 -0.5851 -0.4201 20 10 7 0.3341 -0.2288 20 10 8 9.2580 0.3043 20 10 9 1.5670 -0.4940 20 10 10 2.6267 -1.1790 20 10 11 -7.4840 2.7203 20 10 12 -3.6050 -2.1762 20 10 13 -9.6510 -0.0788 20 10 14 1.9230 0.9590 20 10 15 -0.1758 -0.4948 20 10 16 1.0168 0.5167 20 10 17 0.2978 -0.8732 20 10 18 2.0865 -3.7754 20 11 5 -7.4174 -2.3255 20 11 6 -2.4597 -1.2155 20 11 7 4.4520 -0.2829 20 11 8 0.3686 0.2839 20 11 9 -7.2223 0.4321 20 11 10 -5.8765 -1.6556 20 11 11 -1.2712 1.6631 20 11 12 6.5090 -1.1195 20 11 13 2.2711 -0.1183 20 11 14 -1.4931 1.5135 20 11 15 -6.6190 -1.1962 20 11 16 -0.3976 0.6844 20 11 17 -0.4385 2.9580 20 11 18 3.0572 -1.0384 20 12 7 1.8110 0.7141 20 12 8 0.2506 1.1454 20 12 9 11.3825 0.9067 20 12 10 10.6604 -1.9061 20 12 11 10.3426 1.6146 20 12 12 2.5948 1.1863 20 12 13 5.1866 -1.7789 20 12 14 2.1009 1.7738 20 12 15 4.9885 -0.6403 20 12 16 6.9892 -1.8116 20 12 17 1.9661 -0.7688 20 13 9 5.7391 1.8667 20 13 10 -3.1498 -1.7515 20 13 11 -1.9544 -0.8993 20 13 12 -8.3171 1.6141 20 13 13 0.7741 -2.9973 20 13 14 -0.8896 0.4820 20 13 15 1.4307 1.5973 20 14 12 -1.2624 3.4955 21 -3 5 -0.1421 -2.1628 21 -3 6 -1.5012 2.0591 21 -3 7 4.2569 -0.1095 21 -3 8 -1.4784 0.1474 21 -3 9 3.2068 -0.9007 21 -3 10 -0.1865 4.2189 21 -2 5 5.1217 -0.5236 21 -2 6 5.7873 -0.6595 21 -2 7 5.0346 1.2240 21 -2 8 -1.5975 0.3409 21 -2 9 4.0766 -1.2993 21 -2 10 -1.9126 0.4435 21 -2 11 -0.0414 0.4488 21 -2 12 -1.7372 -3.8153 21 -1 4 8.2227 0.6545 21 -1 5 2.6495 1.1939 21 -1 6 2.0931 -2.5564 21 -1 7 -1.1969 1.4649 21 -1 8 2.8965 0.3370 21 -1 9 4.3423 -1.0360 21 -1 10 -2.4913 -1.1725 21 -1 11 -2.5469 2.4411 21 -1 12 -1.7185 -0.4538 21 -1 13 -1.7561 -1.5042 21 0 3 -4.6579 0.9434 21 0 4 -4.9607 -1.6705 21 0 5 -6.1612 1.7244 21 0 6 2.3597 0.0710 21 0 7 -5.8545 -0.6239 21 0 8 -1.0520 -0.3929 21 0 9 -5.1056 1.1898 21 0 10 2.0174 -1.2479 21 0 11 -0.4435 0.8270 21 0 12 3.9486 0.8806 21 0 13 0.6315 -2.1308 21 0 14 2.7511 -0.0828 21 1 3 -0.8984 1.4547 21 1 4 0.8351 -1.3058 21 1 5 -1.8707 -1.6834 21 1 6 -1.7731 2.4271 21 1 7 -2.2746 1.3864 21 1 8 8.1058 -0.7895 21 1 9 2.6743 -0.3373 21 1 10 10.7635 0.3784 21 1 11 -3.6280 -0.7923 21 1 12 -0.2177 1.5849 21 1 13 -2.9699 -0.6214 21 1 14 1.7672 -0.8805 21 1 15 0.7016 2.3169 21 2 3 5.2301 0.2598 21 2 4 -1.2120 1.2689 21 2 5 0.7004 -0.9532 21 2 6 -4.4226 -0.7843 21 2 7 6.1083 0.6295 21 2 8 6.6995 2.2062 21 2 9 -3.0318 -1.3425 21 2 10 0.6476 0.9681 21 2 11 -0.5361 0.0551 21 2 12 5.4059 -0.0767 21 2 13 1.8262 1.3725 21 2 14 3.1215 -1.0294 21 2 15 1.4887 -0.2773 21 2 16 1.7989 2.7426 21 3 3 2.8674 0.6782 21 3 4 1.6330 1.0742 21 3 5 12.5237 0.4861 21 3 6 0.0821 -1.2945 21 3 7 -0.3239 -2.1973 21 3 8 -8.7358 0.8701 21 3 9 1.2251 -0.4236 21 3 10 2.1526 -1.1496 21 3 11 2.6746 1.0312 21 3 12 0.4881 -0.0400 21 3 13 -0.5529 1.1125 21 3 14 -3.6065 0.3053 21 3 15 -0.6292 -1.5031 21 3 16 -3.7584 0.7237 21 4 3 1.8131 -1.1776 21 4 4 -0.6399 -0.5543 21 4 5 2.9150 0.2491 21 4 6 -3.0487 0.5333 21 4 7 -1.9954 0.1715 21 4 8 -1.9139 -0.1406 21 4 9 11.2059 1.0926 21 4 10 3.9341 -1.0553 21 4 11 -7.7016 0.0694 21 4 12 -14.9360 0.2919 21 4 13 -7.7378 0.6031 21 4 14 -7.0685 2.0283 21 4 15 1.9758 -0.0709 21 4 16 0.0204 -1.8771 21 4 17 5.2026 3.1505 21 5 4 -5.5367 -0.2938 21 5 5 -11.8475 0.9399 21 5 6 0.3280 0.7633 21 5 7 3.5735 0.4331 21 5 8 0.3832 -0.9938 21 5 9 -7.7985 1.2014 21 5 10 -3.4079 0.8538 21 5 11 2.0113 -0.9363 21 5 12 12.3024 0.2091 21 5 13 6.8573 -0.2051 21 5 14 -2.4863 0.5498 21 5 15 -1.9487 1.8645 21 5 16 -3.0564 -0.9974 21 5 17 3.8625 -0.5499 21 6 4 0.8472 -2.6066 21 6 5 -3.0745 -0.1497 21 6 6 6.5094 0.9054 21 6 7 2.1930 0.9735 21 6 8 4.6856 -0.0832 21 6 9 -2.7395 -0.9612 21 6 10 10.1266 0.4355 21 6 11 3.2097 -0.3959 21 6 12 5.9913 -0.2570 21 6 13 -5.7133 1.3541 21 6 14 -4.5090 -1.2799 21 6 15 -2.9759 0.3578 21 6 16 4.5296 0.6270 21 6 17 5.2931 -3.2267 21 7 5 -1.0595 -1.3078 21 7 6 0.7473 0.5024 21 7 7 -6.2243 0.6960 21 7 8 1.2522 0.7791 21 7 9 -1.5590 -1.3407 21 7 10 3.7548 -1.0256 21 7 11 -5.7105 1.9875 21 7 12 -0.1565 -1.5416 21 7 13 -0.8448 1.0567 21 7 14 6.2922 -1.1401 21 7 15 -1.5554 -1.2987 21 7 16 1.5503 0.7708 21 7 17 -3.7839 1.1551 21 8 5 -1.5816 -1.7618 21 8 6 -4.4513 -0.8319 21 8 7 -4.4570 0.6786 21 8 8 -1.9437 1.2498 21 8 9 -6.2568 -0.1146 21 8 10 -2.5762 -1.5155 21 8 11 -1.7261 2.4895 21 8 12 -2.3040 -1.8260 21 8 13 -1.5520 1.0114 21 8 14 2.5198 0.1779 21 8 15 -5.7057 -0.8480 21 8 16 -2.1430 0.8115 21 8 17 -2.0644 3.2566 21 9 6 -0.2625 -2.1754 21 9 7 5.7879 -0.4478 21 9 8 4.9630 1.7682 21 9 9 -0.7551 0.9422 21 9 10 -3.8550 -2.2858 21 9 11 2.6329 2.0358 21 9 12 -1.9303 -0.0466 21 9 13 0.3343 -1.0319 21 9 14 4.6691 2.2052 21 9 15 0.4054 -0.2563 21 9 16 -1.5539 -2.0772 21 10 8 -1.4479 0.4951 21 10 9 2.7627 1.4343 21 10 10 0.8896 -1.3311 21 10 11 6.0715 -1.2593 21 10 12 2.0143 3.1031 21 10 13 2.5602 -2.3682 21 10 14 -4.9631 -0.0199 21 10 15 -1.8524 1.4641 21 10 16 1.8554 0.3535 21 11 9 4.6785 1.0795 21 11 10 2.3107 0.7443 21 11 11 4.5601 -3.6159 21 11 12 -0.0890 2.7431 21 11 13 5.0165 -0.2820 21 11 14 -2.1709 -1.0170 22 1 9 2.6838 -1.1580 22 1 10 -0.2224 -0.3968 22 1 11 2.7004 0.0376 22 2 8 -0.8739 0.0962 22 2 9 5.5973 0.5367 22 2 10 -1.9500 -1.6339 22 2 11 6.0642 1.2114 22 2 12 1.4563 -0.4280 22 3 7 -3.6877 0.9341 22 3 8 -4.0348 -0.5306 22 3 9 -0.0753 3.1511 22 3 10 -3.6140 -0.4615 22 3 11 -4.5730 -1.5435 22 3 12 -6.4608 1.0252 22 3 13 0.0956 0.4247 22 4 8 4.1204 -1.9134 22 4 9 -1.6298 -0.4721 22 4 10 2.0682 1.6917 22 4 11 1.9109 -1.1621 22 4 12 1.9592 -0.3116 22 4 13 -2.7714 1.0659 22 4 14 -3.0180 1.8197 22 5 8 3.0611 0.4956 22 5 9 -5.7046 -2.1298 22 5 10 -1.9666 0.8913 22 5 11 2.9920 0.7571 22 5 12 5.1689 -1.3172 22 5 13 -1.5904 0.8373 22 5 14 -0.9383 0.2463 22 6 9 2.7545 -0.7832 22 6 10 -0.2829 -1.5257 22 6 11 0.5501 2.2603 22 6 12 -7.4044 -0.1764 22 6 13 -3.7845 -0.7677 22 7 11 -0.1810 -0.3100 0 0 0 0.0 0.0 ; _shelx_fab_checksum 81720 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ir01 Ir 0.14736(2) 0.69910(2) 0.45417(2) 0.01707(7) Uani 1 1 d . . . . . Ir02 Ir 0.36732(2) 0.78599(2) 0.32407(2) 0.01767(7) Uani 1 1 d . . . . . Cl03 Cl 0.21459(8) 0.82739(7) 0.37331(8) 0.0208(3) Uani 1 1 d . . . . . Cl04 Cl 0.29993(8) 0.65827(7) 0.40804(8) 0.0209(3) Uani 1 1 d . . . . . Cl05 Cl 0.05121(11) 0.44685(9) 0.74448(9) 0.0379(4) Uani 1 1 d . . . . . Cl06 Cl -0.14997(10) 0.77324(10) 0.39685(11) 0.0406(4) Uani 1 1 d . . . . . Cl07 Cl 0.67460(10) 0.70465(11) 0.08984(10) 0.0454(4) Uani 1 1 d . . . . . Cl08 Cl 0.48216(16) 1.07507(11) 0.27915(14) 0.0665(6) Uani 1 1 d . . . . . N00I N 0.3564(3) 0.8026(3) 0.2182(3) 0.0221(10) Uani 1 1 d . . . . . N00J N 0.1489(3) 0.6551(2) 0.3677(3) 0.0189(9) Uani 1 1 d . . . . . N00L N 0.3991(3) 0.7715(2) 0.4206(3) 0.0196(9) Uani 1 1 d . . . . . N00N N 0.1603(3) 0.5495(3) 0.3336(3) 0.0242(10) Uani 1 1 d . . . . . N00P N 0.1219(3) 0.7384(2) 0.5515(3) 0.0196(9) Uani 1 1 d . . . . . N00Q N 0.0441(3) 0.8201(3) 0.6189(3) 0.0238(10) Uani 1 1 d . . . . . N00R N 0.4788(3) 0.7027(3) 0.4842(3) 0.0245(10) Uani 1 1 d . . . . . N00S N 0.3370(3) 0.8851(3) 0.1126(3) 0.0273(11) Uani 1 1 d . . . . . C00T C 0.0333(3) 0.7437(3) 0.4726(3) 0.0210(11) Uani 1 1 d . . . . . C00U C 0.1144(3) 0.4596(3) 0.5177(3) 0.0244(12) Uani 1 1 d . . . . . H00U H 0.120287 0.425719 0.488415 0.029 Uiso 1 1 calc R U . . . C00V C 0.4624(3) 0.7197(3) 0.4181(3) 0.0214(11) Uani 1 1 d . . . . . C00W C 0.1479(3) 0.6786(3) 0.2919(3) 0.0188(11) Uani 1 1 d . . . . . C00X C 0.0059(3) 0.7971(3) 0.5171(3) 0.0195(11) Uani 1 1 d . . . . . C00Y C 0.1568(3) 0.6121(3) 0.2694(3) 0.0244(12) Uani 1 1 d . . . . . C00Z C 0.5130(3) 0.7002(3) 0.3441(3) 0.0228(11) Uani 1 1 d . . . . . C010 C 0.1272(3) 0.7531(3) 0.2458(3) 0.0228(12) Uani 1 1 d . . . . . C011 C 0.1794(4) 0.4688(3) 0.3374(3) 0.0263(12) Uani 1 1 d . . . . . C012 C 0.1159(3) 0.5915(3) 0.5209(3) 0.0213(11) Uani 1 1 d . . . . . C013 C 0.1540(4) 0.6137(3) 0.1962(3) 0.0267(13) Uani 1 1 d . . . . . C014 C 0.1119(3) 0.8200(3) 0.2684(3) 0.0289(13) Uani 1 1 d . . . . . H014 H 0.120993 0.818470 0.313542 0.035 Uiso 1 1 calc R U . . . C015 C -0.0189(3) 0.7354(3) 0.4384(3) 0.0226(11) Uani 1 1 d . . . . . H015 H -0.004827 0.697784 0.411231 0.027 Uiso 1 1 calc R U . . . C016 C 0.0575(3) 0.7893(3) 0.5600(3) 0.0186(11) Uani 1 1 d . . . . . C017 C 0.1509(3) 0.5778(3) 0.3932(3) 0.0213(11) Uani 1 1 d . . . . . C018 C -0.0669(3) 0.8445(3) 0.5225(3) 0.0247(12) Uani 1 1 d . . . . . H018 H -0.083318 0.880953 0.551305 0.030 Uiso 1 1 calc R U . . . C01A C 0.0907(4) 0.4312(3) 0.6005(4) 0.0290(13) Uani 1 1 d . . . . . H01A H 0.082058 0.377703 0.628068 0.035 Uiso 1 1 calc R U . . . C01B C 0.1296(3) 0.5387(3) 0.4778(3) 0.0223(11) Uani 1 1 d . . . . . C01C C 0.1138(3) 0.7556(3) 0.1771(3) 0.0255(12) Uani 1 1 d . . . . . C01D C 0.3766(3) 0.7928(3) 0.4886(3) 0.0194(11) Uani 1 1 d . . . . . C01E C 0.3514(3) 0.7596(3) 0.1740(3) 0.0244(12) Uani 1 1 d . . . . . C01F C 0.0913(3) 0.5613(3) 0.6038(3) 0.0212(11) Uani 1 1 d . . . . . H01F H 0.082260 0.594819 0.634450 0.025 Uiso 1 1 calc R U . . . C01G C 0.1483(3) 0.7318(3) 0.6113(3) 0.0195(11) Uani 1 1 d . . . . . C01H C 0.4010(4) 0.6257(3) 0.2350(4) 0.0291(13) Uani 1 1 d . . . . . H01H H 0.404908 0.641858 0.274579 0.035 Uiso 1 1 calc R U . . . C01I C 0.3743(3) 0.9319(3) 0.2022(3) 0.0237(12) Uani 1 1 d . . . . . C01J C 0.3505(3) 0.8757(3) 0.1793(3) 0.0240(12) Uani 1 1 d . . . . . C01K C 0.3368(4) 0.8107(4) 0.1092(3) 0.0280(13) Uani 1 1 d . . . . . C01L C 0.1271(4) 0.6860(4) 0.1529(3) 0.0294(13) Uani 1 1 d . . . . . C01M C 0.3321(4) 0.9578(4) 0.0538(4) 0.0309(13) Uani 1 1 d . . . . . C01N C 0.4825(3) 0.7426(3) 0.2831(3) 0.0224(11) Uani 1 1 d . . . . . C01O C 0.2134(3) 0.6811(3) 0.7068(3) 0.0230(12) Uani 1 1 d . . . . . C01P C 0.2063(3) 0.6775(3) 0.6380(3) 0.0217(11) Uani 1 1 d . . . . . C01Q C 0.0840(4) 0.8878(4) 0.2269(4) 0.0335(14) Uani 1 1 d . . . . . H01Q H 0.072142 0.932232 0.244370 0.040 Uiso 1 1 calc R U . . . C01R C 0.2540(4) 0.4360(4) 0.3410(4) 0.0339(14) Uani 1 1 d . . . . . H01R H 0.292593 0.465798 0.339890 0.041 Uiso 1 1 calc R U . . . C01S C 0.1652(4) 0.7372(4) 0.7486(3) 0.0284(13) Uani 1 1 d . . . . . C01T C 0.5437(3) 0.6493(3) 0.4986(3) 0.0247(12) Uani 1 1 d . . . . . C01U C -0.1004(4) 0.8414(4) 0.7078(4) 0.0330(14) Uani 1 1 d . . . . . H01U H -0.105364 0.786951 0.731320 0.040 Uiso 1 1 calc R U . . . C01V C 0.4258(3) 0.7498(3) 0.5295(3) 0.0239(12) Uani 1 1 d . . . . . C01W C -0.0900(3) 0.7820(3) 0.4447(4) 0.0260(12) Uani 1 1 d . . . . . C01X C 0.1082(4) 0.7907(3) 0.7205(3) 0.0270(13) Uani 1 1 d . . . . . C01Y C 0.3660(4) 0.8170(3) 0.6292(3) 0.0294(13) Uani 1 1 d . . . . . C01Z C 0.3792(4) 1.0121(3) 0.1657(4) 0.0321(14) Uani 1 1 d . . . . . H01Z H 0.360178 1.036250 0.123937 0.039 Uiso 1 1 calc R U . . . C020 C 0.3980(3) 0.8958(3) 0.2675(3) 0.0232(12) Uani 1 1 d . . . . . C021 C 0.6094(4) 0.7005(3) 0.1888(4) 0.0299(13) Uani 1 1 d . . . . . C022 C 0.1012(3) 0.7826(3) 0.6527(3) 0.0228(12) Uani 1 1 d . . . . . C023 C 0.3197(3) 0.8535(3) 0.5163(3) 0.0233(12) Uani 1 1 d . . . . . C024 C 0.5342(3) 0.7428(3) 0.2048(3) 0.0250(12) Uani 1 1 d . . . . . H024 H 0.517837 0.772046 0.162107 0.030 Uiso 1 1 calc R U . . . C025 C 0.1221(4) 0.4259(3) 0.3414(4) 0.0319(14) Uani 1 1 d . . . . . H025 H 0.069655 0.448656 0.341836 0.038 Uiso 1 1 calc R U . . . C027 C 0.4214(3) 0.7572(3) 0.6019(3) 0.0228(12) Uani 1 1 d . . . . . C028 C -0.1601(4) 0.9707(4) 0.6954(4) 0.0411(17) Uani 1 1 d . . . . . H028 H -0.206690 1.004794 0.711584 0.049 Uiso 1 1 calc R U . . . C029 C 0.5865(4) 0.6546(3) 0.3263(4) 0.0298(13) Uani 1 1 d . . . . . H029 H 0.603761 0.624032 0.368015 0.036 Uiso 1 1 calc R U . . . C02A C -0.1150(4) 0.8368(3) 0.4844(4) 0.0292(13) Uani 1 1 d . . . . . H02A H -0.163734 0.868775 0.486005 0.035 Uiso 1 1 calc R U . . . C02B C 0.0800(3) 0.4826(3) 0.6415(3) 0.0236(12) Uani 1 1 d . . . . . C02C C 0.5287(3) 0.5710(3) 0.5330(3) 0.0254(12) Uani 1 1 d . . . . . H02C H 0.474984 0.553584 0.549546 0.030 Uiso 1 1 calc R U . . . C02D C 0.5918(4) 0.5187(3) 0.5430(4) 0.0312(14) Uani 1 1 d . . . . . H02D H 0.582106 0.464904 0.565870 0.037 Uiso 1 1 calc R U . . . C02E C 0.1416(5) 0.3490(4) 0.3448(4) 0.0424(17) Uani 1 1 d . . . . . H02E H 0.103413 0.319037 0.345506 0.051 Uiso 1 1 calc R U . . . C02F C -0.0250(4) 0.8726(3) 0.6469(3) 0.0242(12) Uani 1 1 d . . . . . C02G C 0.2502(3) 0.6190(3) 0.6043(3) 0.0230(12) Uani 1 1 d . . . . . H02G H 0.244890 0.616449 0.558706 0.028 Uiso 1 1 calc R U . . . C02H C 0.4119(4) 1.0570(4) 0.1905(4) 0.0399(16) Uani 1 1 d . . . . . H02H H 0.415419 1.111444 0.166144 0.048 Uiso 1 1 calc R U . . . C02I C 0.6690(4) 0.5447(4) 0.5196(4) 0.0373(15) Uani 1 1 d . . . . . H02I H 0.712692 0.508463 0.526249 0.045 Uiso 1 1 calc R U . . . C02J C 0.4699(4) 0.7118(4) 0.6439(4) 0.0333(14) Uani 1 1 d . . . . . H02J H 0.506333 0.671715 0.625416 0.040 Uiso 1 1 calc R U . . . C02K C 0.3706(4) 0.6785(3) 0.1798(3) 0.0278(13) Uani 1 1 d . . . . . C02L C 0.2732(4) 0.9033(3) 0.4750(3) 0.0258(12) Uani 1 1 d . . . . . H02L H 0.277724 0.897154 0.426783 0.031 Uiso 1 1 calc R U . . . C02M C 0.4656(4) 0.7243(4) 0.7106(4) 0.0340(14) Uani 1 1 d . . . . . H02M H 0.497967 0.692005 0.738637 0.041 Uiso 1 1 calc R U . . . C02N C 0.4388(4) 1.0192(4) 0.2517(4) 0.0348(14) Uani 1 1 d . . . . . C02O C 0.4332(4) 0.9408(3) 0.2896(4) 0.0280(13) Uani 1 1 d . . . . . H02O H 0.453154 0.917233 0.330752 0.034 Uiso 1 1 calc R U . . . C02P C 0.6210(4) 0.6760(3) 0.4756(4) 0.0359(15) Uani 1 1 d . . . . . H02P H 0.630733 0.729816 0.452682 0.043 Uiso 1 1 calc R U . . . C02Q C -0.0168(4) 0.9510(3) 0.6102(4) 0.0297(13) Uani 1 1 d . . . . . H02Q H 0.034796 0.970743 0.569040 0.036 Uiso 1 1 calc R U . . . C02R C -0.0848(4) 1.0011(3) 0.6339(4) 0.0316(14) Uani 1 1 d . . . . . H02R H -0.080253 1.055374 0.608688 0.038 Uiso 1 1 calc R U . . . C02S C 0.4150(4) 0.7832(4) 0.7378(4) 0.0373(16) Uani 1 1 d . . . . . H02S H 0.413712 0.792981 0.783069 0.045 Uiso 1 1 calc R U . . . C02T C 0.3149(4) 0.8644(3) 0.5867(3) 0.0253(12) Uani 1 1 d . . . . . C02U C 0.3007(4) 0.5650(3) 0.6351(4) 0.0298(13) Uani 1 1 d . . . . . H02U H 0.329261 0.525353 0.611295 0.036 Uiso 1 1 calc R U . . . C02V C -0.1676(4) 0.8918(4) 0.7331(4) 0.0451(18) Uani 1 1 d . . . . . H02V H -0.218492 0.872233 0.775940 0.054 Uiso 1 1 calc R U . . . C02W C 0.3646(4) 0.8291(4) 0.6967(4) 0.0375(15) Uani 1 1 d . . . . . H02W H 0.328905 0.869204 0.715787 0.045 Uiso 1 1 calc R U . . . C02X C 0.3257(4) 0.7877(4) 0.0510(3) 0.0350(15) Uani 1 1 d . . . . . C02Y C 0.4023(4) 0.9795(4) -0.0176(4) 0.0404(16) Uani 1 1 d . . . . . H02Y H 0.452215 0.948204 -0.025193 0.049 Uiso 1 1 calc R U . . . C02Z C 0.2674(4) 0.6243(4) 0.7362(4) 0.0324(14) Uani 1 1 d . . . . . H02Z H 0.273739 0.625665 0.781800 0.039 Uiso 1 1 calc R U . . . C030 C 0.2607(4) 1.0035(4) 0.0682(4) 0.0430(17) Uani 1 1 d . . . . . H030 H 0.213981 0.988591 0.117864 0.052 Uiso 1 1 calc R U . . . C031 C 0.6343(4) 0.6536(4) 0.2488(4) 0.0330(14) Uani 1 1 d . . . . . H031 H 0.683495 0.621339 0.236774 0.040 Uiso 1 1 calc R U . . . C032 C 0.0882(4) 0.8266(4) 0.1345(4) 0.0373(15) Uani 1 1 d . . . . . H032 H 0.081327 0.829807 0.087743 0.045 Uiso 1 1 calc R U . . . C033 C 0.2716(4) 0.3581(4) 0.3461(4) 0.0430(17) Uani 1 1 d . . . . . H033 H 0.322602 0.334238 0.348896 0.052 Uiso 1 1 calc R U . . . C034 C 0.6841(4) 0.6227(4) 0.4868(5) 0.0396(16) Uani 1 1 d . . . . . H034 H 0.737490 0.639854 0.471769 0.047 Uiso 1 1 calc R U . . . C035 C 0.2164(5) 0.3161(4) 0.3473(4) 0.0472(19) Uani 1 1 d . . . . . H035 H 0.229604 0.263188 0.349836 0.057 Uiso 1 1 calc R U . . . C036 C 0.3102(4) 0.5685(4) 0.7017(4) 0.0313(14) Uani 1 1 d . . . . . H036 H 0.346195 0.532087 0.722440 0.038 Uiso 1 1 calc R U . . . C037 C 0.1743(4) 0.5515(4) 0.1655(4) 0.0340(14) Uani 1 1 d . . . . . H037 H 0.197761 0.504940 0.190801 0.041 Uiso 1 1 calc R U . . . C038 C 0.2213(4) 0.9605(3) 0.5029(4) 0.0326(14) Uani 1 1 d . . . . . H038 H 0.190790 0.994213 0.473625 0.039 Uiso 1 1 calc R U . . . C039 C 0.1127(4) 0.6879(4) 0.0869(4) 0.0379(15) Uani 1 1 d . . . . . H039 H 0.091969 0.734583 0.058899 0.045 Uiso 1 1 calc R U . . . C03A C 0.3648(4) 0.6542(4) 0.1198(4) 0.0366(15) Uani 1 1 d . . . . . C03B C 0.3257(5) 0.6822(5) 0.0042(4) 0.051(2) Uani 1 1 d . . . . . H03B H 0.333648 0.628798 0.008318 0.062 Uiso 1 1 calc R U . . . C03C C 0.2591(4) 0.9231(4) 0.6140(4) 0.0349(15) Uani 1 1 d . . . . . H03C H 0.253475 0.930287 0.662022 0.042 Uiso 1 1 calc R U . . . C03D C 0.1739(4) 0.7428(4) 0.8151(4) 0.0380(16) Uani 1 1 d . . . . . H03D H 0.212688 0.708612 0.833687 0.046 Uiso 1 1 calc R U . . . C03E C 0.0627(4) 0.8454(4) 0.7618(4) 0.0345(14) Uani 1 1 d . . . . . H03E H 0.024322 0.881012 0.743716 0.041 Uiso 1 1 calc R U . . . C03F C 0.0728(4) 0.8918(4) 0.1578(4) 0.0382(15) Uani 1 1 d . . . . . H03F H 0.054779 0.939030 0.127956 0.046 Uiso 1 1 calc R U . . . C03G C 0.3382(4) 0.7076(4) 0.0588(3) 0.0348(15) Uani 1 1 d . . . . . C03H C 0.1613(4) 0.5559(4) 0.0998(4) 0.0399(16) Uani 1 1 d . . . . . H03H H 0.175016 0.512550 0.080292 0.048 Uiso 1 1 calc R U . . . C03I C 0.4179(5) 0.5268(4) 0.1766(4) 0.0461(18) Uani 1 1 d . . . . . H03I H 0.433511 0.474900 0.175892 0.055 Uiso 1 1 calc R U . . . C03J C 0.3885(4) 0.5774(4) 0.1215(4) 0.0455(18) Uani 1 1 d . . . . . H03J H 0.384165 0.559374 0.083354 0.055 Uiso 1 1 calc R U . . . C03K C 0.4249(4) 0.5518(4) 0.2330(4) 0.0393(16) Uani 1 1 d . . . . . H03K H 0.446324 0.517230 0.270255 0.047 Uiso 1 1 calc R U . . . C03L C 0.1281(4) 0.6234(4) 0.0620(4) 0.0442(18) Uani 1 1 d . . . . . H03L H 0.115758 0.625406 0.018469 0.053 Uiso 1 1 calc R U . . . C03M C 0.2992(4) 0.8377(4) -0.0080(4) 0.0427(17) Uani 1 1 d . . . . . H03M H 0.288005 0.891042 -0.011999 0.051 Uiso 1 1 calc R U . . . C03N C 0.3992(5) 1.0458(5) -0.0763(4) 0.0477(18) Uani 1 1 d . . . . . H03N H 0.445920 1.059947 -0.126165 0.057 Uiso 1 1 calc R U . . . C03P C 0.2571(5) 1.0717(4) 0.0099(5) 0.0501(19) Uani 1 1 d . . . . . H03P H 0.207903 1.104050 0.018883 0.060 Uiso 1 1 calc R U . . . C03Q C 0.3023(5) 0.7334(5) -0.0548(4) 0.052(2) Uani 1 1 d . . . . . H03Q H 0.295183 0.715241 -0.091523 0.062 Uiso 1 1 calc R U . . . C03R C 0.2129(4) 0.9698(3) 0.5739(4) 0.0401(17) Uani 1 1 d . . . . . H03R H 0.175271 1.008433 0.594156 0.048 Uiso 1 1 calc R U . . . C03S C 0.1283(4) 0.7962(4) 0.8540(4) 0.0448(17) Uani 1 1 d . . . . . H03S H 0.134657 0.797522 0.899551 0.054 Uiso 1 1 calc R U . . . C03T C 0.3263(5) 1.0924(4) -0.0620(5) 0.054(2) Uani 1 1 d . . . . . H03T H 0.323925 1.139193 -0.102287 0.065 Uiso 1 1 calc R U . . . C03U C 0.0723(4) 0.8485(4) 0.8263(4) 0.0440(17) Uani 1 1 d . . . . . H03U H 0.041172 0.885960 0.852419 0.053 Uiso 1 1 calc R U . . . C03W C 0.2893(5) 0.8096(5) -0.0608(4) 0.053(2) Uani 1 1 d . . . . . H03W H 0.273049 0.844279 -0.101789 0.064 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ir01 0.01701(11) 0.01613(11) 0.02118(11) -0.00709(9) -0.00935(8) -0.00067(8) Ir02 0.01742(11) 0.01831(11) 0.02106(11) -0.00782(9) -0.00931(8) -0.00165(8) Cl03 0.0179(6) 0.0181(6) 0.0284(7) -0.0077(5) -0.0108(5) -0.0004(5) Cl04 0.0192(6) 0.0174(6) 0.0262(6) -0.0069(5) -0.0096(5) 0.0005(5) Cl05 0.0530(10) 0.0316(8) 0.0272(7) -0.0007(7) -0.0167(7) -0.0121(7) Cl06 0.0339(8) 0.0443(9) 0.0656(11) -0.0269(9) -0.0346(8) 0.0062(7) Cl07 0.0312(9) 0.0631(11) 0.0401(9) -0.0297(9) -0.0023(7) -0.0008(8) Cl08 0.1094(18) 0.0398(10) 0.0769(14) -0.0096(10) -0.0559(13) -0.0320(11) N00I 0.021(2) 0.021(2) 0.021(2) -0.008(2) -0.0051(18) -0.0001(18) N00J 0.018(2) 0.018(2) 0.023(2) -0.0065(19) -0.0096(18) -0.0018(17) N00L 0.019(2) 0.023(2) 0.024(2) -0.010(2) -0.0137(18) 0.0028(18) N00N 0.026(3) 0.020(2) 0.033(3) -0.011(2) -0.015(2) 0.0018(19) N00P 0.019(2) 0.016(2) 0.023(2) -0.0057(19) -0.0086(18) 0.0001(17) N00Q 0.025(2) 0.021(2) 0.026(2) -0.008(2) -0.012(2) 0.0010(19) N00R 0.025(2) 0.028(3) 0.030(3) -0.016(2) -0.017(2) 0.006(2) N00S 0.023(3) 0.036(3) 0.023(2) -0.004(2) -0.011(2) -0.007(2) C00T 0.014(3) 0.024(3) 0.023(3) -0.006(2) -0.006(2) -0.001(2) C00U 0.028(3) 0.021(3) 0.028(3) -0.008(2) -0.012(2) -0.005(2) C00V 0.019(3) 0.021(3) 0.032(3) -0.011(2) -0.015(2) -0.001(2) C00W 0.015(3) 0.027(3) 0.019(3) -0.011(2) -0.007(2) -0.002(2) C00X 0.018(3) 0.019(3) 0.026(3) -0.009(2) -0.012(2) 0.003(2) C00Y 0.021(3) 0.031(3) 0.026(3) -0.012(3) -0.010(2) -0.004(2) C00Z 0.024(3) 0.022(3) 0.028(3) -0.011(2) -0.014(2) -0.002(2) C010 0.019(3) 0.026(3) 0.021(3) -0.004(2) -0.007(2) -0.005(2) C011 0.028(3) 0.028(3) 0.029(3) -0.013(3) -0.011(2) -0.003(2) C012 0.016(3) 0.026(3) 0.030(3) -0.017(2) -0.012(2) 0.004(2) C013 0.028(3) 0.033(3) 0.024(3) -0.012(3) -0.012(2) -0.005(2) C014 0.022(3) 0.037(3) 0.027(3) -0.009(3) -0.009(2) -0.004(2) C015 0.020(3) 0.023(3) 0.028(3) -0.008(2) -0.011(2) -0.004(2) C016 0.022(3) 0.019(3) 0.018(2) -0.010(2) -0.007(2) -0.003(2) C017 0.016(3) 0.023(3) 0.030(3) -0.011(2) -0.011(2) -0.002(2) C018 0.023(3) 0.021(3) 0.032(3) -0.012(2) -0.009(2) -0.001(2) C01A 0.028(3) 0.022(3) 0.039(3) -0.008(3) -0.015(3) -0.003(2) C01B 0.014(3) 0.026(3) 0.029(3) -0.010(2) -0.010(2) -0.002(2) C01C 0.024(3) 0.032(3) 0.025(3) -0.006(3) -0.012(2) -0.010(2) C01D 0.018(3) 0.021(3) 0.027(3) -0.011(2) -0.013(2) -0.002(2) C01E 0.018(3) 0.035(3) 0.025(3) -0.015(3) -0.007(2) -0.006(2) C01F 0.020(3) 0.021(3) 0.027(3) -0.009(2) -0.011(2) -0.003(2) C01G 0.019(3) 0.023(3) 0.020(3) -0.005(2) -0.009(2) -0.007(2) C01H 0.031(3) 0.032(3) 0.031(3) -0.018(3) -0.011(3) -0.005(2) C01I 0.016(3) 0.024(3) 0.028(3) -0.008(2) -0.004(2) -0.004(2) C01J 0.020(3) 0.030(3) 0.021(3) -0.004(2) -0.008(2) -0.005(2) C01K 0.024(3) 0.036(3) 0.027(3) -0.009(3) -0.012(2) -0.006(2) C01L 0.029(3) 0.039(3) 0.024(3) -0.009(3) -0.011(2) -0.011(3) C01M 0.029(3) 0.037(3) 0.027(3) -0.003(3) -0.014(3) -0.007(3) C01N 0.018(3) 0.023(3) 0.031(3) -0.015(2) -0.009(2) -0.002(2) C01O 0.023(3) 0.021(3) 0.031(3) -0.008(2) -0.014(2) -0.007(2) C01P 0.023(3) 0.021(3) 0.024(3) -0.006(2) -0.011(2) -0.006(2) C01Q 0.038(4) 0.031(3) 0.042(4) -0.016(3) -0.021(3) -0.001(3) C01R 0.030(3) 0.034(3) 0.040(4) -0.017(3) -0.013(3) 0.000(3) C01S 0.025(3) 0.034(3) 0.029(3) -0.006(3) -0.012(2) -0.010(2) C01T 0.027(3) 0.028(3) 0.030(3) -0.014(3) -0.021(2) 0.009(2) C01U 0.034(3) 0.028(3) 0.028(3) -0.009(3) -0.004(3) -0.002(3) C01V 0.025(3) 0.022(3) 0.028(3) -0.009(2) -0.011(2) -0.004(2) C01W 0.026(3) 0.023(3) 0.036(3) -0.006(3) -0.019(3) -0.008(2) C01X 0.028(3) 0.028(3) 0.024(3) -0.008(3) -0.010(2) -0.002(2) C01Y 0.036(3) 0.026(3) 0.027(3) -0.005(3) -0.012(3) -0.011(3) C01Z 0.038(4) 0.024(3) 0.032(3) -0.001(3) -0.016(3) -0.005(3) C020 0.020(3) 0.027(3) 0.023(3) -0.010(2) -0.007(2) -0.001(2) C021 0.028(3) 0.028(3) 0.033(3) -0.014(3) -0.006(2) -0.004(2) C022 0.026(3) 0.017(3) 0.025(3) -0.004(2) -0.011(2) -0.005(2) C023 0.025(3) 0.022(3) 0.027(3) -0.011(2) -0.010(2) -0.003(2) C024 0.025(3) 0.032(3) 0.026(3) -0.016(3) -0.011(2) -0.006(2) C025 0.033(3) 0.032(3) 0.035(3) -0.007(3) -0.013(3) -0.016(3) C027 0.023(3) 0.023(3) 0.030(3) -0.009(2) -0.015(2) -0.006(2) C028 0.042(4) 0.034(4) 0.040(4) -0.017(3) -0.010(3) 0.011(3) C029 0.029(3) 0.032(3) 0.040(3) -0.019(3) -0.019(3) 0.004(2) C02A 0.027(3) 0.025(3) 0.040(3) -0.008(3) -0.021(3) 0.004(2) C02B 0.023(3) 0.026(3) 0.025(3) -0.004(2) -0.013(2) -0.005(2) C02C 0.019(3) 0.030(3) 0.034(3) -0.011(3) -0.015(2) -0.003(2) C02D 0.036(3) 0.021(3) 0.041(3) -0.005(3) -0.023(3) 0.001(2) C02E 0.056(5) 0.031(3) 0.039(4) -0.013(3) -0.010(3) -0.019(3) C02F 0.031(3) 0.022(3) 0.022(3) -0.010(2) -0.011(2) 0.001(2) C02G 0.018(3) 0.027(3) 0.027(3) -0.008(2) -0.011(2) -0.005(2) C02H 0.055(4) 0.023(3) 0.039(4) -0.004(3) -0.017(3) -0.010(3) C02I 0.031(3) 0.031(3) 0.061(4) -0.017(3) -0.030(3) 0.007(3) C02J 0.035(3) 0.031(3) 0.043(4) -0.010(3) -0.024(3) -0.003(3) C02K 0.026(3) 0.036(3) 0.027(3) -0.019(3) -0.003(2) -0.013(2) C02L 0.028(3) 0.026(3) 0.030(3) -0.009(3) -0.013(2) -0.008(2) C02M 0.040(4) 0.039(4) 0.035(3) -0.011(3) -0.026(3) -0.003(3) C02N 0.044(4) 0.030(3) 0.036(3) -0.009(3) -0.015(3) -0.016(3) C02O 0.028(3) 0.028(3) 0.035(3) -0.010(3) -0.015(3) -0.010(2) C02P 0.037(4) 0.018(3) 0.057(4) -0.006(3) -0.026(3) -0.003(2) C02Q 0.032(3) 0.027(3) 0.031(3) -0.012(3) -0.011(3) 0.000(2) C02R 0.038(4) 0.018(3) 0.043(4) -0.011(3) -0.019(3) 0.000(2) C02S 0.035(4) 0.057(4) 0.027(3) -0.008(3) -0.014(3) -0.024(3) C02T 0.031(3) 0.025(3) 0.024(3) -0.009(2) -0.012(2) -0.006(2) C02U 0.026(3) 0.030(3) 0.036(3) -0.013(3) -0.014(3) 0.001(2) C02V 0.030(4) 0.036(4) 0.051(4) -0.011(3) -0.002(3) 0.000(3) C02W 0.045(4) 0.041(4) 0.033(3) -0.017(3) -0.016(3) -0.007(3) C02X 0.032(3) 0.057(4) 0.018(3) -0.012(3) -0.008(2) -0.013(3) C02Y 0.032(4) 0.051(4) 0.032(3) -0.007(3) -0.010(3) -0.007(3) C02Z 0.032(3) 0.037(3) 0.036(3) -0.007(3) -0.023(3) -0.003(3) C030 0.030(4) 0.049(4) 0.042(4) 0.001(3) -0.015(3) -0.012(3) C031 0.021(3) 0.036(3) 0.052(4) -0.027(3) -0.016(3) 0.006(2) C032 0.045(4) 0.049(4) 0.026(3) -0.008(3) -0.021(3) -0.009(3) C033 0.041(4) 0.035(4) 0.055(4) -0.020(3) -0.019(3) 0.007(3) C034 0.032(3) 0.032(3) 0.073(5) -0.019(3) -0.037(3) 0.004(3) C035 0.060(5) 0.027(3) 0.041(4) -0.013(3) -0.008(3) 0.002(3) C036 0.026(3) 0.033(3) 0.035(3) -0.005(3) -0.019(3) 0.003(3) C037 0.037(4) 0.038(4) 0.032(3) -0.013(3) -0.014(3) -0.008(3) C038 0.036(4) 0.025(3) 0.038(3) -0.011(3) -0.017(3) 0.006(3) C039 0.044(4) 0.044(4) 0.032(3) -0.011(3) -0.020(3) -0.008(3) C03A 0.033(4) 0.047(4) 0.033(3) -0.019(3) -0.006(3) -0.015(3) C03B 0.048(4) 0.080(6) 0.036(4) -0.029(4) -0.004(3) -0.033(4) C03C 0.046(4) 0.033(3) 0.031(3) -0.018(3) -0.014(3) 0.000(3) C03D 0.041(4) 0.048(4) 0.028(3) -0.016(3) -0.016(3) 0.004(3) C03E 0.038(4) 0.036(3) 0.036(3) -0.016(3) -0.018(3) 0.000(3) C03F 0.043(4) 0.037(4) 0.037(4) -0.004(3) -0.024(3) -0.001(3) C03G 0.031(3) 0.052(4) 0.022(3) -0.016(3) -0.002(3) -0.015(3) C03H 0.052(4) 0.043(4) 0.035(4) -0.020(3) -0.017(3) -0.010(3) C03I 0.056(5) 0.033(4) 0.056(5) -0.028(4) -0.017(4) -0.005(3) C03J 0.051(4) 0.046(4) 0.049(4) -0.033(4) -0.009(3) -0.014(3) C03K 0.045(4) 0.035(4) 0.037(4) -0.019(3) -0.012(3) 0.000(3) C03L 0.053(4) 0.067(5) 0.027(3) -0.013(3) -0.023(3) -0.019(4) C03M 0.045(4) 0.059(5) 0.029(3) -0.010(3) -0.014(3) -0.020(3) C03N 0.041(4) 0.062(5) 0.032(4) -0.002(4) -0.012(3) -0.014(4) C03P 0.040(4) 0.042(4) 0.064(5) -0.003(4) -0.029(4) -0.001(3) C03Q 0.064(5) 0.070(5) 0.036(4) -0.017(4) -0.022(4) -0.031(4) C03R 0.049(4) 0.022(3) 0.042(4) -0.016(3) -0.011(3) 0.009(3) C03S 0.049(4) 0.062(5) 0.040(4) -0.026(4) -0.023(3) -0.006(4) C03T 0.073(6) 0.039(4) 0.043(4) 0.009(4) -0.029(4) -0.015(4) C03U 0.047(4) 0.057(4) 0.044(4) -0.036(4) -0.019(3) 0.005(3) C03W 0.049(5) 0.096(7) 0.025(3) -0.016(4) -0.018(3) -0.022(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ir Ir -1.4442 7.9887 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cl03 Ir01 Cl04 78.42(4) . . ? N00J Ir01 Cl03 103.94(12) . . ? N00J Ir01 Cl04 84.94(12) . . ? N00J Ir01 N00P 169.17(16) . . ? N00P Ir01 Cl03 83.07(12) . . ? N00P Ir01 Cl04 104.75(12) . . ? C00T Ir01 Cl03 94.08(16) . . ? C00T Ir01 Cl04 170.58(16) . . ? C00T Ir01 N00J 91.4(2) . . ? C00T Ir01 N00P 79.7(2) . . ? C00T Ir01 C012 96.9(2) . . ? C012 Ir01 Cl03 168.32(15) . . ? C012 Ir01 Cl04 91.07(15) . . ? C012 Ir01 N00J 79.92(19) . . ? C012 Ir01 N00P 94.85(19) . . ? Cl04 Ir02 Cl03 78.36(4) . . ? N00I Ir02 Cl03 84.24(12) . . ? N00I Ir02 Cl04 101.21(13) . . ? N00I Ir02 N00L 170.74(17) . . ? N00L Ir02 Cl03 104.29(12) . . ? N00L Ir02 Cl04 84.27(12) . . ? C01N Ir02 Cl03 172.55(16) . . ? C01N Ir02 Cl04 96.18(16) . . ? C01N Ir02 N00I 92.0(2) . . ? C01N Ir02 N00L 80.0(2) . . ? C01N Ir02 C020 95.2(2) . . ? C020 Ir02 Cl03 90.42(16) . . ? C020 Ir02 Cl04 168.59(15) . . ? C020 Ir02 N00I 79.4(2) . . ? C020 Ir02 N00L 96.7(2) . . ? Ir01 Cl03 Ir02 101.50(4) . . ? Ir02 Cl04 Ir01 101.69(4) . . ? C01E N00I Ir02 140.0(4) . . ? C01J N00I Ir02 112.7(4) . . ? C01J N00I C01E 107.3(5) . . ? C00W N00J Ir01 141.8(4) . . ? C017 N00J Ir01 110.8(3) . . ? C017 N00J C00W 107.4(4) . . ? C00V N00L Ir02 109.4(3) . . ? C00V N00L C01D 106.8(4) . . ? C01D N00L Ir02 143.8(3) . . ? C00Y N00N C011 128.4(5) . . ? C017 N00N C00Y 107.6(4) . . ? C017 N00N C011 123.6(4) . . ? C016 N00P Ir01 110.2(3) . . ? C016 N00P C01G 106.5(4) . . ? C01G N00P Ir01 143.4(4) . . ? C016 N00Q C022 106.8(4) . . ? C016 N00Q C02F 124.5(5) . . ? C022 N00Q C02F 128.1(5) . . ? C00V N00R C01T 124.2(5) . . ? C00V N00R C01V 107.4(4) . . ? C01V N00R C01T 128.3(5) . . ? C01J N00S C01K 106.5(5) . . ? C01J N00S C01M 126.1(5) . . ? C01K N00S C01M 127.1(5) . . ? C00X C00T Ir01 115.3(4) . . ? C015 C00T Ir01 126.9(4) . . ? C015 C00T C00X 117.3(5) . . ? C01A C00U H00U 120.2 . . ? C01A C00U C01B 119.7(5) . . ? C01B C00U H00U 120.2 . . ? N00L C00V N00R 111.0(5) . . ? N00L C00V C00Z 119.7(5) . . ? N00R C00V C00Z 128.2(5) . . ? N00J C00W C00Y 107.9(5) . . ? N00J C00W C010 130.0(5) . . ? C00Y C00W C010 121.2(5) . . ? C00T C00X C016 110.8(4) . . ? C018 C00X C00T 122.0(5) . . ? C018 C00X C016 127.0(5) . . ? N00N C00Y C00W 106.4(5) . . ? N00N C00Y C013 129.9(5) . . ? C00W C00Y C013 123.5(5) . . ? C01N C00Z C00V 110.4(4) . . ? C029 C00Z C00V 128.5(5) . . ? C029 C00Z C01N 120.8(5) . . ? C00W C010 C01C 116.9(5) . . ? C014 C010 C00W 123.5(5) . . ? C014 C010 C01C 119.3(5) . . ? C01R C011 N00N 118.5(5) . . ? C025 C011 N00N 120.0(5) . . ? C025 C011 C01R 121.4(6) . . ? C01B C012 Ir01 115.5(4) . . ? C01F C012 Ir01 126.5(4) . . ? C01F C012 C01B 117.6(5) . . ? C01L C013 C00Y 115.6(5) . . ? C037 C013 C00Y 125.6(6) . . ? C037 C013 C01L 118.8(5) . . ? C010 C014 H014 119.4 . . ? C01Q C014 C010 121.2(6) . . ? C01Q C014 H014 119.4 . . ? C00T C015 H015 120.1 . . ? C01W C015 C00T 119.8(5) . . ? C01W C015 H015 120.1 . . ? N00P C016 N00Q 111.0(5) . . ? N00P C016 C00X 119.4(4) . . ? N00Q C016 C00X 128.9(5) . . ? N00J C017 N00N 110.4(5) . . ? N00J C017 C01B 118.5(5) . . ? N00N C017 C01B 130.1(5) . . ? C00X C018 H018 120.6 . . ? C02A C018 C00X 118.8(5) . . ? C02A C018 H018 120.6 . . ? C00U C01A H01A 120.7 . . ? C02B C01A C00U 118.6(5) . . ? C02B C01A H01A 120.7 . . ? C00U C01B C012 121.2(5) . . ? C00U C01B C017 126.6(5) . . ? C012 C01B C017 111.9(5) . . ? C010 C01C C01L 120.7(5) . . ? C032 C01C C010 117.8(5) . . ? C032 C01C C01L 121.5(5) . . ? N00L C01D C01V 108.8(4) . . ? N00L C01D C023 131.1(5) . . ? C01V C01D C023 119.8(5) . . ? N00I C01E C02K 130.8(5) . . ? C01K C01E N00I 108.0(5) . . ? C01K C01E C02K 120.4(5) . . ? C012 C01F H01F 119.9 . . ? C02B C01F C012 120.2(5) . . ? C02B C01F H01F 119.9 . . ? N00P C01G C01P 130.4(5) . . ? C022 C01G N00P 108.9(5) . . ? C022 C01G C01P 120.3(5) . . ? C02K C01H H01H 119.3 . . ? C03K C01H H01H 119.3 . . ? C03K C01H C02K 121.3(6) . . ? C01Z C01I C01J 127.9(6) . . ? C01Z C01I C020 120.4(5) . . ? C020 C01I C01J 111.6(5) . . ? N00I C01J N00S 111.5(5) . . ? N00I C01J C01I 117.6(5) . . ? N00S C01J C01I 129.6(5) . . ? N00S C01K C02X 129.4(6) . . ? C01E C01K N00S 106.4(5) . . ? C01E C01K C02X 124.2(6) . . ? C013 C01L C01C 121.3(5) . . ? C039 C01L C013 117.8(6) . . ? C039 C01L C01C 120.9(6) . . ? C02Y C01M N00S 117.9(6) . . ? C030 C01M N00S 120.7(5) . . ? C030 C01M C02Y 121.4(6) . . ? C00Z C01N Ir02 114.5(4) . . ? C024 C01N Ir02 128.5(4) . . ? C024 C01N C00Z 116.8(5) . . ? C01P C01O C01S 122.5(5) . . ? C01P C01O C02Z 116.9(5) . . ? C02Z C01O C01S 120.6(5) . . ? C01O C01P C01G 116.7(5) . . ? C02G C01P C01G 123.8(5) . . ? C02G C01P C01O 119.3(5) . . ? C014 C01Q H01Q 120.0 . . ? C014 C01Q C03F 120.1(6) . . ? C03F C01Q H01Q 120.0 . . ? C011 C01R H01R 120.8 . . ? C011 C01R C033 118.4(6) . . ? C033 C01R H01R 120.8 . . ? C01X C01S C01O 119.5(5) . . ? C03D C01S C01O 122.8(6) . . ? C03D C01S C01X 117.7(6) . . ? C02C C01T N00R 119.1(5) . . ? C02P C01T N00R 119.8(5) . . ? C02P C01T C02C 121.0(5) . . ? C02F C01U H01U 120.7 . . ? C02V C01U H01U 120.7 . . ? C02V C01U C02F 118.6(6) . . ? N00R C01V C01D 105.9(5) . . ? N00R C01V C027 129.3(5) . . ? C01D C01V C027 124.7(5) . . ? C015 C01W Cl06 118.3(4) . . ? C015 C01W C02A 123.3(5) . . ? C02A C01W Cl06 118.4(4) . . ? C01S C01X C022 115.7(5) . . ? C03E C01X C01S 118.4(5) . . ? C03E C01X C022 125.9(5) . . ? C027 C01Y C02T 120.9(5) . . ? C02W C01Y C027 117.0(6) . . ? C02W C01Y C02T 122.1(6) . . ? C01I C01Z H01Z 119.8 . . ? C01I C01Z C02H 120.4(6) . . ? C02H C01Z H01Z 119.8 . . ? C01I C020 Ir02 114.4(4) . . ? C02O C020 Ir02 127.0(4) . . ? C02O C020 C01I 118.4(5) . . ? C024 C021 Cl07 119.4(5) . . ? C031 C021 Cl07 118.3(4) . . ? C031 C021 C024 122.3(5) . . ? N00Q C022 C01X 128.0(5) . . ? C01G C022 N00Q 106.7(5) . . ? C01G C022 C01X 125.2(5) . . ? C02L C023 C01D 123.2(5) . . ? C02L C023 C02T 119.4(5) . . ? C02T C023 C01D 117.4(5) . . ? C01N C024 H024 119.8 . . ? C021 C024 C01N 120.4(5) . . ? C021 C024 H024 119.8 . . ? C011 C025 H025 120.4 . . ? C011 C025 C02E 119.1(6) . . ? C02E C025 H025 120.4 . . ? C01Y C027 C01V 115.7(5) . . ? C02J C027 C01V 124.1(5) . . ? C02J C027 C01Y 120.1(5) . . ? C02R C028 H028 119.4 . . ? C02V C028 H028 119.4 . . ? C02V C028 C02R 121.2(6) . . ? C00Z C029 H029 119.7 . . ? C031 C029 C00Z 120.5(6) . . ? C031 C029 H029 119.7 . . ? C018 C02A H02A 120.6 . . ? C01W C02A C018 118.8(5) . . ? C01W C02A H02A 120.6 . . ? C01A C02B Cl05 118.4(4) . . ? C01A C02B C01F 122.6(5) . . ? C01F C02B Cl05 119.0(4) . . ? C01T C02C H02C 120.1 . . ? C02D C02C C01T 119.8(5) . . ? C02D C02C H02C 120.1 . . ? C02C C02D H02D 120.2 . . ? C02C C02D C02I 119.6(6) . . ? C02I C02D H02D 120.2 . . ? C025 C02E H02E 120.1 . . ? C035 C02E C025 119.8(7) . . ? C035 C02E H02E 120.1 . . ? C01U C02F N00Q 118.6(5) . . ? C02Q C02F N00Q 119.4(5) . . ? C02Q C02F C01U 121.9(5) . . ? C01P C02G H02G 119.0 . . ? C02U C02G C01P 122.0(5) . . ? C02U C02G H02G 119.0 . . ? C01Z C02H H02H 121.1 . . ? C02N C02H C01Z 117.8(6) . . ? C02N C02H H02H 121.1 . . ? C02D C02I H02I 119.5 . . ? C02D C02I C034 121.0(6) . . ? C034 C02I H02I 119.5 . . ? C027 C02J H02J 119.4 . . ? C02M C02J C027 121.2(6) . . ? C02M C02J H02J 119.4 . . ? C01H C02K C01E 124.0(5) . . ? C01H C02K C03A 119.4(5) . . ? C03A C02K C01E 116.3(6) . . ? C023 C02L H02L 119.5 . . ? C038 C02L C023 120.9(5) . . ? C038 C02L H02L 119.5 . . ? C02J C02M H02M 119.6 . . ? C02J C02M C02S 120.8(6) . . ? C02S C02M H02M 119.6 . . ? C02H C02N Cl08 117.1(5) . . ? C02O C02N Cl08 120.0(5) . . ? C02O C02N C02H 122.9(6) . . ? C020 C02O H02O 120.0 . . ? C02N C02O C020 119.9(6) . . ? C02N C02O H02O 120.0 . . ? C01T C02P H02P 120.6 . . ? C01T C02P C034 118.7(6) . . ? C034 C02P H02P 120.6 . . ? C02F C02Q H02Q 120.3 . . ? C02F C02Q C02R 119.4(6) . . ? C02R C02Q H02Q 120.3 . . ? C028 C02R H02R 120.4 . . ? C02Q C02R C028 119.2(6) . . ? C02Q C02R H02R 120.4 . . ? C02M C02S H02S 120.6 . . ? C02M C02S C02W 118.7(6) . . ? C02W C02S H02S 120.6 . . ? C023 C02T C01Y 121.4(5) . . ? C03C C02T C01Y 121.2(5) . . ? C03C C02T C023 117.4(5) . . ? C02G C02U H02U 120.1 . . ? C02G C02U C036 119.8(6) . . ? C036 C02U H02U 120.1 . . ? C01U C02V H02V 120.2 . . ? C028 C02V C01U 119.7(6) . . ? C028 C02V H02V 120.2 . . ? C01Y C02W C02S 122.1(6) . . ? C01Y C02W H02W 119.0 . . ? C02S C02W H02W 119.0 . . ? C03G C02X C01K 116.0(6) . . ? C03M C02X C01K 124.6(6) . . ? C03M C02X C03G 119.3(6) . . ? C01M C02Y H02Y 120.0 . . ? C03N C02Y C01M 119.9(6) . . ? C03N C02Y H02Y 120.0 . . ? C01O C02Z H02Z 118.7 . . ? C036 C02Z C01O 122.6(6) . . ? C036 C02Z H02Z 118.7 . . ? C01M C030 H030 120.3 . . ? C01M C030 C03P 119.3(6) . . ? C03P C030 H030 120.3 . . ? C021 C031 H031 120.7 . . ? C029 C031 C021 118.7(5) . . ? C029 C031 H031 120.7 . . ? C01C C032 H032 118.9 . . ? C03F C032 C01C 122.3(6) . . ? C03F C032 H032 118.9 . . ? C01R C033 H033 119.8 . . ? C035 C033 C01R 120.4(7) . . ? C035 C033 H033 119.8 . . ? C02I C034 C02P 119.9(6) . . ? C02I C034 H034 120.0 . . ? C02P C034 H034 120.0 . . ? C02E C035 H035 119.6 . . ? C033 C035 C02E 120.8(6) . . ? C033 C035 H035 119.6 . . ? C02U C036 H036 120.3 . . ? C02Z C036 C02U 119.5(5) . . ? C02Z C036 H036 120.3 . . ? C013 C037 H037 119.2 . . ? C03H C037 C013 121.5(6) . . ? C03H C037 H037 119.2 . . ? C02L C038 H038 119.8 . . ? C02L C038 C03R 120.5(6) . . ? C03R C038 H038 119.8 . . ? C01L C039 H039 119.4 . . ? C03L C039 C01L 121.2(7) . . ? C03L C039 H039 119.4 . . ? C02K C03A C03G 121.6(6) . . ? C03J C03A C02K 116.9(6) . . ? C03J C03A C03G 121.5(6) . . ? C03G C03B H03B 119.4 . . ? C03Q C03B H03B 119.4 . . ? C03Q C03B C03G 121.2(7) . . ? C02T C03C H03C 118.8 . . ? C03R C03C C02T 122.3(6) . . ? C03R C03C H03C 118.8 . . ? C01S C03D H03D 118.8 . . ? C03S C03D C01S 122.3(6) . . ? C03S C03D H03D 118.8 . . ? C01X C03E H03E 118.9 . . ? C03U C03E C01X 122.1(6) . . ? C03U C03E H03E 118.9 . . ? C01Q C03F H03F 120.4 . . ? C032 C03F C01Q 119.2(6) . . ? C032 C03F H03F 120.4 . . ? C02X C03G C03A 120.7(6) . . ? C03B C03G C02X 117.9(6) . . ? C03B C03G C03A 121.4(7) . . ? C037 C03H H03H 120.1 . . ? C037 C03H C03L 119.8(6) . . ? C03L C03H H03H 120.1 . . ? C03J C03I H03I 120.0 . . ? C03J C03I C03K 120.0(6) . . ? C03K C03I H03I 120.0 . . ? C03A C03J H03J 118.8 . . ? C03I C03J C03A 122.4(6) . . ? C03I C03J H03J 118.8 . . ? C01H C03K C03I 120.0(7) . . ? C01H C03K H03K 120.0 . . ? C03I C03K H03K 120.0 . . ? C039 C03L C03H 120.4(6) . . ? C039 C03L H03L 119.8 . . ? C03H C03L H03L 119.8 . . ? C02X C03M H03M 119.9 . . ? C03W C03M C02X 120.1(7) . . ? C03W C03M H03M 119.9 . . ? C02Y C03N H03N 120.6 . . ? C02Y C03N C03T 118.7(7) . . ? C03T C03N H03N 120.6 . . ? C030 C03P H03P 120.4 . . ? C030 C03P C03T 119.2(7) . . ? C03T C03P H03P 120.4 . . ? C03B C03Q H03Q 119.8 . . ? C03W C03Q C03B 120.3(7) . . ? C03W C03Q H03Q 119.8 . . ? C038 C03R H03R 120.3 . . ? C03C C03R C038 119.4(6) . . ? C03C C03R H03R 120.3 . . ? C03D C03S H03S 120.1 . . ? C03D C03S C03U 119.7(6) . . ? C03U C03S H03S 120.1 . . ? C03N C03T H03T 119.4 . . ? C03P C03T C03N 121.3(7) . . ? C03P C03T H03T 119.4 . . ? C03E C03U C03S 119.7(6) . . ? C03E C03U H03U 120.1 . . ? C03S C03U H03U 120.1 . . ? C03M C03W H03W 119.5 . . ? C03Q C03W C03M 121.1(7) . . ? C03Q C03W H03W 119.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ir01 Cl03 2.5181(13) . ? Ir01 Cl04 2.5230(12) . ? Ir01 N00J 2.098(4) . ? Ir01 N00P 2.100(4) . ? Ir01 C00T 1.974(5) . ? Ir01 C012 1.981(6) . ? Ir02 Cl03 2.5280(12) . ? Ir02 Cl04 2.5165(13) . ? Ir02 N00I 2.062(5) . ? Ir02 N00L 2.107(4) . ? Ir02 C01N 1.976(5) . ? Ir02 C020 1.987(6) . ? Cl05 C02B 1.735(6) . ? Cl06 C01W 1.754(6) . ? Cl07 C021 1.744(6) . ? Cl08 C02N 1.731(6) . ? N00I C01E 1.397(7) . ? N00I C01J 1.307(7) . ? N00J C00W 1.391(7) . ? N00J C017 1.336(7) . ? N00L C00V 1.331(6) . ? N00L C01D 1.382(7) . ? N00N C00Y 1.388(7) . ? N00N C011 1.449(7) . ? N00N C017 1.368(7) . ? N00P C016 1.332(6) . ? N00P C01G 1.395(7) . ? N00Q C016 1.366(7) . ? N00Q C022 1.397(7) . ? N00Q C02F 1.446(7) . ? N00R C00V 1.361(7) . ? N00R C01T 1.433(7) . ? N00R C01V 1.389(7) . ? N00S C01J 1.366(7) . ? N00S C01K 1.401(8) . ? N00S C01M 1.443(8) . ? C00T C00X 1.417(7) . ? C00T C015 1.414(7) . ? C00U H00U 0.9500 . ? C00U C01A 1.393(8) . ? C00U C01B 1.407(7) . ? C00V C00Z 1.458(8) . ? C00W C00Y 1.402(8) . ? C00W C010 1.437(8) . ? C00X C016 1.450(7) . ? C00X C018 1.408(7) . ? C00Y C013 1.436(8) . ? C00Z C01N 1.439(8) . ? C00Z C029 1.393(8) . ? C010 C014 1.397(8) . ? C010 C01C 1.438(8) . ? C011 C01R 1.375(8) . ? C011 C025 1.369(8) . ? C012 C01B 1.420(7) . ? C012 C01F 1.395(8) . ? C013 C01L 1.428(8) . ? C013 C037 1.396(8) . ? C014 H014 0.9500 . ? C014 C01Q 1.368(8) . ? C015 H015 0.9500 . ? C015 C01W 1.377(8) . ? C017 C01B 1.447(8) . ? C018 H018 0.9500 . ? C018 C02A 1.407(8) . ? C01A H01A 0.9500 . ? C01A C02B 1.380(8) . ? C01C C01L 1.466(9) . ? C01C C032 1.399(9) . ? C01D C01V 1.391(8) . ? C01D C023 1.449(7) . ? C01E C01K 1.380(8) . ? C01E C02K 1.448(8) . ? C01F H01F 0.9500 . ? C01F C02B 1.388(7) . ? C01G C01P 1.436(7) . ? C01G C022 1.370(8) . ? C01H H01H 0.9500 . ? C01H C02K 1.405(8) . ? C01H C03K 1.360(8) . ? C01I C01J 1.456(8) . ? C01I C01Z 1.400(8) . ? C01I C020 1.416(8) . ? C01K C02X 1.437(8) . ? C01L C039 1.403(8) . ? C01M C02Y 1.392(8) . ? C01M C030 1.367(9) . ? C01N C024 1.395(7) . ? C01O C01P 1.424(8) . ? C01O C01S 1.456(8) . ? C01O C02Z 1.427(8) . ? C01P C02G 1.393(8) . ? C01Q H01Q 0.9500 . ? C01Q C03F 1.419(9) . ? C01R H01R 0.9500 . ? C01R C033 1.390(9) . ? C01S C01X 1.428(8) . ? C01S C03D 1.408(8) . ? C01T C02C 1.386(8) . ? C01T C02P 1.382(8) . ? C01U H01U 0.9500 . ? C01U C02F 1.404(8) . ? C01U C02V 1.392(8) . ? C01V C027 1.431(8) . ? C01W C02A 1.378(8) . ? C01X C022 1.437(8) . ? C01X C03E 1.420(8) . ? C01Y C027 1.421(8) . ? C01Y C02T 1.459(8) . ? C01Y C02W 1.396(8) . ? C01Z H01Z 0.9500 . ? C01Z C02H 1.404(9) . ? C020 C02O 1.399(8) . ? C021 C024 1.386(8) . ? C021 C031 1.381(9) . ? C023 C02L 1.398(8) . ? C023 C02T 1.416(8) . ? C024 H024 0.9500 . ? C025 H025 0.9500 . ? C025 C02E 1.382(9) . ? C027 C02J 1.408(8) . ? C028 H028 0.9500 . ? C028 C02R 1.402(9) . ? C028 C02V 1.384(9) . ? C029 H029 0.9500 . ? C029 C031 1.376(8) . ? C02A H02A 0.9500 . ? C02C H02C 0.9500 . ? C02C C02D 1.375(8) . ? C02D H02D 0.9500 . ? C02D C02I 1.375(9) . ? C02E H02E 0.9500 . ? C02E C035 1.373(10) . ? C02F C02Q 1.376(8) . ? C02G H02G 0.9500 . ? C02G C02U 1.370(8) . ? C02H H02H 0.9500 . ? C02H C02N 1.387(9) . ? C02I H02I 0.9500 . ? C02I C034 1.380(9) . ? C02J H02J 0.9500 . ? C02J C02M 1.363(9) . ? C02K C03A 1.437(8) . ? C02L H02L 0.9500 . ? C02L C038 1.367(8) . ? C02M H02M 0.9500 . ? C02M C02S 1.377(9) . ? C02N C02O 1.376(8) . ? C02O H02O 0.9500 . ? C02P H02P 0.9500 . ? C02P C034 1.390(8) . ? C02Q H02Q 0.9500 . ? C02Q C02R 1.388(8) . ? C02R H02R 0.9500 . ? C02S H02S 0.9500 . ? C02S C02W 1.426(9) . ? C02T C03C 1.410(8) . ? C02U H02U 0.9500 . ? C02U C036 1.402(8) . ? C02V H02V 0.9500 . ? C02W H02W 0.9500 . ? C02X C03G 1.417(9) . ? C02X C03M 1.400(9) . ? C02Y H02Y 0.9500 . ? C02Y C03N 1.361(10) . ? C02Z H02Z 0.9500 . ? C02Z C036 1.357(9) . ? C030 H030 0.9500 . ? C030 C03P 1.380(10) . ? C031 H031 0.9500 . ? C032 H032 0.9500 . ? C032 C03F 1.370(9) . ? C033 H033 0.9500 . ? C033 C035 1.353(10) . ? C034 H034 0.9500 . ? C035 H035 0.9500 . ? C036 H036 0.9500 . ? C037 H037 0.9500 . ? C037 C03H 1.369(9) . ? C038 H038 0.9500 . ? C038 C03R 1.390(9) . ? C039 H039 0.9500 . ? C039 C03L 1.378(10) . ? C03A C03G 1.449(9) . ? C03A C03J 1.395(9) . ? C03B H03B 0.9500 . ? C03B C03G 1.412(9) . ? C03B C03Q 1.376(11) . ? C03C H03C 0.9500 . ? C03C C03R 1.361(9) . ? C03D H03D 0.9500 . ? C03D C03S 1.375(9) . ? C03E H03E 0.9500 . ? C03E C03U 1.359(9) . ? C03F H03F 0.9500 . ? C03H H03H 0.9500 . ? C03H C03L 1.380(10) . ? C03I H03I 0.9500 . ? C03I C03J 1.378(10) . ? C03I C03K 1.390(9) . ? C03J H03J 0.9500 . ? C03K H03K 0.9500 . ? C03L H03L 0.9500 . ? C03M H03M 0.9500 . ? C03M C03W 1.387(9) . ? C03N H03N 0.9500 . ? C03N C03T 1.395(10) . ? C03P H03P 0.9500 . ? C03P C03T 1.387(10) . ? C03Q H03Q 0.9500 . ? C03Q C03W 1.353(11) . ? C03R H03R 0.9500 . ? C03S H03S 0.9500 . ? C03S C03U 1.402(10) . ? C03T H03T 0.9500 . ? C03U H03U 0.9500 . ? C03W H03W 0.9500 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Ir01 N00J C00W C00Y 175.5(4) . . . . ? Ir01 N00J C00W C010 -15.2(9) . . . . ? Ir01 N00J C017 N00N -173.9(3) . . . . ? Ir01 N00J C017 C01B 16.2(6) . . . . ? Ir01 N00P C016 N00Q -175.2(3) . . . . ? Ir01 N00P C016 C00X 13.1(6) . . . . ? Ir01 N00P C01G C01P -11.7(10) . . . . ? Ir01 N00P C01G C022 175.8(4) . . . . ? Ir01 C00T C00X C016 -17.7(6) . . . . ? Ir01 C00T C00X C018 167.9(4) . . . . ? Ir01 C00T C015 C01W -167.3(4) . . . . ? Ir01 C012 C01B C00U 176.3(4) . . . . ? Ir01 C012 C01B C017 -9.9(6) . . . . ? Ir01 C012 C01F C02B -172.7(4) . . . . ? Ir02 N00I C01E C01K 174.4(4) . . . . ? Ir02 N00I C01E C02K -15.9(9) . . . . ? Ir02 N00I C01J N00S -175.4(3) . . . . ? Ir02 N00I C01J C01I 16.1(6) . . . . ? Ir02 N00L C00V N00R -173.5(4) . . . . ? Ir02 N00L C00V C00Z 17.7(6) . . . . ? Ir02 N00L C01D C01V 173.0(5) . . . . ? Ir02 N00L C01D C023 -13.4(10) . . . . ? Ir02 C01N C024 C021 -171.4(4) . . . . ? Ir02 C020 C02O C02N -169.8(5) . . . . ? Cl06 C01W C02A C018 -179.6(4) . . . . ? Cl07 C021 C024 C01N -177.7(4) . . . . ? Cl07 C021 C031 C029 175.0(5) . . . . ? Cl08 C02N C02O C020 179.8(5) . . . . ? N00I C01E C01K N00S 2.8(6) . . . . ? N00I C01E C01K C02X -178.4(5) . . . . ? N00I C01E C02K C01H -0.8(9) . . . . ? N00I C01E C02K C03A -175.0(5) . . . . ? N00J C00W C00Y N00N 1.9(6) . . . . ? N00J C00W C00Y C013 176.4(5) . . . . ? N00J C00W C010 C014 7.4(9) . . . . ? N00J C00W C010 C01C -166.4(5) . . . . ? N00J C017 C01B C00U 168.4(5) . . . . ? N00J C017 C01B C012 -5.0(7) . . . . ? N00L C00V C00Z C01N -1.1(7) . . . . ? N00L C00V C00Z C029 172.2(6) . . . . ? N00L C01D C01V N00R 0.5(6) . . . . ? N00L C01D C01V C027 178.7(5) . . . . ? N00L C01D C023 C02L 1.7(9) . . . . ? N00L C01D C023 C02T -175.2(5) . . . . ? N00N C00Y C013 C01L 162.8(6) . . . . ? N00N C00Y C013 C037 -16.7(10) . . . . ? N00N C011 C01R C033 178.8(5) . . . . ? N00N C011 C025 C02E 179.9(5) . . . . ? N00N C017 C01B C00U 0.8(9) . . . . ? N00N C017 C01B C012 -172.6(5) . . . . ? N00P C01G C01P C01O -173.5(5) . . . . ? N00P C01G C01P C02G 1.4(9) . . . . ? N00P C01G C022 N00Q 0.9(6) . . . . ? N00P C01G C022 C01X 177.8(5) . . . . ? N00Q C02F C02Q C02R 176.2(5) . . . . ? N00R C00V C00Z C01N -167.7(5) . . . . ? N00R C00V C00Z C029 5.6(10) . . . . ? N00R C01T C02C C02D 176.3(5) . . . . ? N00R C01T C02P C034 -177.0(6) . . . . ? N00R C01V C027 C01Y 173.3(6) . . . . ? N00R C01V C027 C02J -4.1(10) . . . . ? N00S C01K C02X C03G 172.9(6) . . . . ? N00S C01K C02X C03M -11.0(10) . . . . ? N00S C01M C02Y C03N 176.9(6) . . . . ? N00S C01M C030 C03P -178.3(6) . . . . ? C00T C00X C016 N00P 2.0(7) . . . . ? C00T C00X C016 N00Q -168.1(5) . . . . ? C00T C00X C018 C02A 1.9(8) . . . . ? C00T C015 C01W Cl06 176.7(4) . . . . ? C00T C015 C01W C02A -1.2(9) . . . . ? C00U C01A C02B Cl05 -179.6(4) . . . . ? C00U C01A C02B C01F 0.6(9) . . . . ? C00V N00L C01D C01V -2.6(6) . . . . ? C00V N00L C01D C023 171.1(6) . . . . ? C00V N00R C01T C02C -84.2(7) . . . . ? C00V N00R C01T C02P 93.6(7) . . . . ? C00V N00R C01V C01D 1.7(6) . . . . ? C00V N00R C01V C027 -176.3(6) . . . . ? C00V C00Z C01N Ir02 -18.0(6) . . . . ? C00V C00Z C01N C024 166.8(5) . . . . ? C00V C00Z C029 C031 -168.1(6) . . . . ? C00W N00J C017 N00N 6.5(6) . . . . ? C00W N00J C017 C01B -163.4(4) . . . . ? C00W C00Y C013 C01L -10.4(8) . . . . ? C00W C00Y C013 C037 170.1(6) . . . . ? C00W C010 C014 C01Q -173.2(5) . . . . ? C00W C010 C01C C01L -4.3(8) . . . . ? C00W C010 C01C C032 175.9(5) . . . . ? C00X C00T C015 C01W 4.3(8) . . . . ? C00X C018 C02A C01W 1.4(8) . . . . ? C00Y N00N C011 C01R 109.4(7) . . . . ? C00Y N00N C011 C025 -73.7(8) . . . . ? C00Y N00N C017 N00J -5.3(6) . . . . ? C00Y N00N C017 C01B 163.0(5) . . . . ? C00Y C00W C010 C014 175.4(5) . . . . ? C00Y C00W C010 C01C 1.6(8) . . . . ? C00Y C013 C01L C01C 7.4(8) . . . . ? C00Y C013 C01L C039 -171.8(6) . . . . ? C00Y C013 C037 C03H 172.9(6) . . . . ? C00Z C01N C024 C021 3.1(8) . . . . ? C00Z C029 C031 C021 2.1(9) . . . . ? C010 C00W C00Y N00N -168.5(5) . . . . ? C010 C00W C00Y C013 6.0(8) . . . . ? C010 C014 C01Q C03F -2.2(9) . . . . ? C010 C01C C01L C013 -0.3(9) . . . . ? C010 C01C C01L C039 178.8(6) . . . . ? C010 C01C C032 C03F -2.5(9) . . . . ? C011 N00N C00Y C00W -171.6(5) . . . . ? C011 N00N C00Y C013 14.3(10) . . . . ? C011 N00N C017 N00J 168.6(5) . . . . ? C011 N00N C017 C01B -23.0(9) . . . . ? C011 C01R C033 C035 0.3(10) . . . . ? C011 C025 C02E C035 2.5(10) . . . . ? C012 C01F C02B Cl05 178.9(4) . . . . ? C012 C01F C02B C01A -1.3(8) . . . . ? C013 C01L C039 C03L -3.3(10) . . . . ? C013 C037 C03H C03L 0.7(10) . . . . ? C014 C010 C01C C01L -178.3(5) . . . . ? C014 C010 C01C C032 1.9(8) . . . . ? C014 C01Q C03F C032 1.6(10) . . . . ? C015 C00T C00X C016 169.8(5) . . . . ? C015 C00T C00X C018 -4.7(8) . . . . ? C015 C01W C02A C018 -1.8(9) . . . . ? C016 N00P C01G C01P 169.4(5) . . . . ? C016 N00P C01G C022 -3.1(6) . . . . ? C016 N00Q C022 C01G 1.5(6) . . . . ? C016 N00Q C022 C01X -175.3(5) . . . . ? C016 N00Q C02F C01U 86.7(7) . . . . ? C016 N00Q C02F C02Q -89.5(7) . . . . ? C016 C00X C018 C02A -171.7(5) . . . . ? C017 N00J C00W C00Y -5.1(6) . . . . ? C017 N00J C00W C010 164.2(5) . . . . ? C017 N00N C00Y C00W 2.0(6) . . . . ? C017 N00N C00Y C013 -172.1(6) . . . . ? C017 N00N C011 C01R -63.2(8) . . . . ? C017 N00N C011 C025 113.6(6) . . . . ? C018 C00X C016 N00P 176.1(5) . . . . ? C018 C00X C016 N00Q 6.1(9) . . . . ? C01A C00U C01B C012 -4.2(8) . . . . ? C01A C00U C01B C017 -177.0(5) . . . . ? C01B C00U C01A C02B 2.1(8) . . . . ? C01B C012 C01F C02B -0.8(8) . . . . ? C01C C010 C014 C01Q 0.4(9) . . . . ? C01C C01L C039 C03L 177.5(6) . . . . ? C01C C032 C03F C01Q 0.8(10) . . . . ? C01D N00L C00V N00R 3.7(6) . . . . ? C01D N00L C00V C00Z -165.1(5) . . . . ? C01D C01V C027 C01Y -4.4(8) . . . . ? C01D C01V C027 C02J 178.2(6) . . . . ? C01D C023 C02L C038 -178.9(6) . . . . ? C01D C023 C02T C01Y 0.8(8) . . . . ? C01D C023 C02T C03C -179.5(5) . . . . ? C01E N00I C01J N00S 3.3(6) . . . . ? C01E N00I C01J C01I -165.2(5) . . . . ? C01E C01K C02X C03G -5.7(9) . . . . ? C01E C01K C02X C03M 170.4(6) . . . . ? C01E C02K C03A C03G -2.1(8) . . . . ? C01E C02K C03A C03J 175.8(5) . . . . ? C01F C012 C01B C00U 3.5(8) . . . . ? C01F C012 C01B C017 177.2(5) . . . . ? C01G N00P C016 N00Q 4.1(6) . . . . ? C01G N00P C016 C00X -167.6(5) . . . . ? C01G C01P C02G C02U -175.4(5) . . . . ? C01H C02K C03A C03G -176.5(6) . . . . ? C01H C02K C03A C03J 1.4(9) . . . . ? C01I C01Z C02H C02N 0.0(10) . . . . ? C01I C020 C02O C02N 4.4(8) . . . . ? C01J N00I C01E C01K -3.8(6) . . . . ? C01J N00I C01E C02K 166.0(6) . . . . ? C01J N00S C01K C01E -0.8(6) . . . . ? C01J N00S C01K C02X -179.6(6) . . . . ? C01J N00S C01M C02Y 99.9(7) . . . . ? C01J N00S C01M C030 -79.8(8) . . . . ? C01J C01I C01Z C02H -173.2(6) . . . . ? C01J C01I C020 Ir02 -13.6(6) . . . . ? C01J C01I C020 C02O 171.5(5) . . . . ? C01K N00S C01J N00I -1.6(6) . . . . ? C01K N00S C01J C01I 165.2(5) . . . . ? C01K N00S C01M C02Y -73.7(8) . . . . ? C01K N00S C01M C030 106.5(7) . . . . ? C01K C01E C02K C01H 167.9(6) . . . . ? C01K C01E C02K C03A -6.3(8) . . . . ? C01K C02X C03G C03A -3.0(9) . . . . ? C01K C02X C03G C03B 178.3(6) . . . . ? C01K C02X C03M C03W -179.1(6) . . . . ? C01L C013 C037 C03H -6.6(9) . . . . ? C01L C01C C032 C03F 177.7(6) . . . . ? C01L C039 C03L C03H -2.5(11) . . . . ? C01M N00S C01J N00I -176.3(5) . . . . ? C01M N00S C01J C01I -9.5(9) . . . . ? C01M N00S C01K C01E 173.8(5) . . . . ? C01M N00S C01K C02X -5.0(10) . . . . ? C01M C02Y C03N C03T 2.9(11) . . . . ? C01M C030 C03P C03T -0.2(12) . . . . ? C01N C00Z C029 C031 4.6(9) . . . . ? C01O C01P C02G C02U -0.6(8) . . . . ? C01O C01S C01X C022 1.9(8) . . . . ? C01O C01S C01X C03E -179.3(5) . . . . ? C01O C01S C03D C03S 179.8(6) . . . . ? C01O C02Z C036 C02U -0.9(10) . . . . ? C01P C01G C022 N00Q -172.5(5) . . . . ? C01P C01G C022 C01X 4.4(9) . . . . ? C01P C01O C01S C01X 0.3(8) . . . . ? C01P C01O C01S C03D -177.8(6) . . . . ? C01P C01O C02Z C036 -0.6(9) . . . . ? C01P C02G C02U C036 -0.9(9) . . . . ? C01R C011 C025 C02E -3.4(9) . . . . ? C01R C033 C035 C02E -1.2(11) . . . . ? C01S C01O C01P C01G -0.5(8) . . . . ? C01S C01O C01P C02G -175.7(5) . . . . ? C01S C01O C02Z C036 176.5(6) . . . . ? C01S C01X C022 N00Q 171.8(5) . . . . ? C01S C01X C022 C01G -4.5(9) . . . . ? C01S C01X C03E C03U 0.4(10) . . . . ? C01S C03D C03S C03U -1.6(11) . . . . ? C01T N00R C00V N00L -179.5(5) . . . . ? C01T N00R C00V C00Z -12.0(9) . . . . ? C01T N00R C01V C01D 177.6(5) . . . . ? C01T N00R C01V C027 -0.5(10) . . . . ? C01T C02C C02D C02I 0.8(9) . . . . ? C01T C02P C034 C02I 0.5(11) . . . . ? C01U C02F C02Q C02R 0.2(9) . . . . ? C01V N00R C00V N00L -3.4(6) . . . . ? C01V N00R C00V C00Z 164.1(5) . . . . ? C01V N00R C01T C02C 100.6(7) . . . . ? C01V N00R C01T C02P -81.7(8) . . . . ? C01V C01D C023 C02L 174.7(5) . . . . ? C01V C01D C023 C02T -2.2(8) . . . . ? C01V C027 C02J C02M 176.8(6) . . . . ? C01X C01S C03D C03S 1.7(10) . . . . ? C01X C03E C03U C03S -0.3(11) . . . . ? C01Y C027 C02J C02M -0.6(9) . . . . ? C01Y C02T C03C C03R 177.7(6) . . . . ? C01Z C01I C01J N00I 174.8(5) . . . . ? C01Z C01I C01J N00S 8.8(10) . . . . ? C01Z C01I C020 Ir02 169.2(4) . . . . ? C01Z C01I C020 C02O -5.8(8) . . . . ? C01Z C02H C02N Cl08 177.9(5) . . . . ? C01Z C02H C02N C02O -1.4(10) . . . . ? C020 C01I C01J N00I -2.2(7) . . . . ? C020 C01I C01J N00S -168.3(5) . . . . ? C020 C01I C01Z C02H 3.6(9) . . . . ? C022 N00Q C016 N00P -3.6(6) . . . . ? C022 N00Q C016 C00X 167.2(5) . . . . ? C022 N00Q C02F C01U -82.8(8) . . . . ? C022 N00Q C02F C02Q 101.0(7) . . . . ? C022 C01G C01P C01O -1.7(8) . . . . ? C022 C01G C01P C02G 173.2(5) . . . . ? C022 C01X C03E C03U 179.1(6) . . . . ? C023 C01D C01V N00R -174.0(5) . . . . ? C023 C01D C01V C027 4.2(9) . . . . ? C023 C02L C038 C03R -0.9(9) . . . . ? C023 C02T C03C C03R -2.0(9) . . . . ? C024 C021 C031 C029 -6.2(9) . . . . ? C025 C011 C01R C033 2.1(10) . . . . ? C025 C02E C035 C033 -0.2(11) . . . . ? C027 C01Y C02T C023 -1.2(9) . . . . ? C027 C01Y C02T C03C 179.2(6) . . . . ? C027 C01Y C02W C02S -1.0(9) . . . . ? C027 C02J C02M C02S -1.6(10) . . . . ? C029 C00Z C01N Ir02 168.1(4) . . . . ? C029 C00Z C01N C024 -7.1(8) . . . . ? C02C C01T C02P C034 0.7(10) . . . . ? C02C C02D C02I C034 0.4(10) . . . . ? C02D C02I C034 C02P -1.1(11) . . . . ? C02F N00Q C016 N00P -175.0(5) . . . . ? C02F N00Q C016 C00X -4.2(9) . . . . ? C02F N00Q C022 C01G 172.5(5) . . . . ? C02F N00Q C022 C01X -4.3(9) . . . . ? C02F C01U C02V C028 3.0(11) . . . . ? C02F C02Q C02R C028 0.7(9) . . . . ? C02G C02U C036 C02Z 1.6(9) . . . . ? C02H C02N C02O C020 -0.9(10) . . . . ? C02J C02M C02S C02W 2.4(10) . . . . ? C02K C01E C01K N00S -168.3(5) . . . . ? C02K C01E C01K C02X 10.6(9) . . . . ? C02K C01H C03K C03I -1.3(10) . . . . ? C02K C03A C03G C02X 6.8(9) . . . . ? C02K C03A C03G C03B -174.5(6) . . . . ? C02K C03A C03J C03I -1.3(10) . . . . ? C02L C023 C02T C01Y -176.3(5) . . . . ? C02L C023 C02T C03C 3.4(8) . . . . ? C02L C038 C03R C03C 2.3(10) . . . . ? C02M C02S C02W C01Y -1.0(10) . . . . ? C02P C01T C02C C02D -1.4(9) . . . . ? C02R C028 C02V C01U -2.2(12) . . . . ? C02T C01Y C027 C01V 2.7(8) . . . . ? C02T C01Y C027 C02J -179.7(5) . . . . ? C02T C01Y C02W C02S -179.5(6) . . . . ? C02T C023 C02L C038 -2.1(9) . . . . ? C02T C03C C03R C038 -0.8(10) . . . . ? C02V C01U C02F N00Q -178.1(6) . . . . ? C02V C01U C02F C02Q -2.0(10) . . . . ? C02V C028 C02R C02Q 0.3(11) . . . . ? C02W C01Y C027 C01V -175.8(5) . . . . ? C02W C01Y C027 C02J 1.8(9) . . . . ? C02W C01Y C02T C023 177.3(6) . . . . ? C02W C01Y C02T C03C -2.4(9) . . . . ? C02X C03M C03W C03Q 2.1(11) . . . . ? C02Y C01M C030 C03P 2.0(11) . . . . ? C02Y C03N C03T C03P -1.2(12) . . . . ? C02Z C01O C01P C01G 176.5(5) . . . . ? C02Z C01O C01P C02G 1.3(8) . . . . ? C02Z C01O C01S C01X -176.6(5) . . . . ? C02Z C01O C01S C03D 5.3(9) . . . . ? C030 C01M C02Y C03N -3.4(11) . . . . ? C030 C03P C03T C03N -0.2(13) . . . . ? C031 C021 C024 C01N 3.6(9) . . . . ? C032 C01C C01L C013 179.4(6) . . . . ? C032 C01C C01L C039 -1.4(9) . . . . ? C037 C013 C01L C01C -173.1(6) . . . . ? C037 C013 C01L C039 7.7(9) . . . . ? C037 C03H C03L C039 4.0(11) . . . . ? C03B C03Q C03W C03M 0.0(12) . . . . ? C03D C01S C01X C022 -179.8(5) . . . . ? C03D C01S C01X C03E -1.0(9) . . . . ? C03D C03S C03U C03E 0.9(11) . . . . ? C03E C01X C022 N00Q -6.9(10) . . . . ? C03E C01X C022 C01G 176.9(6) . . . . ? C03G C02X C03M C03W -3.1(10) . . . . ? C03G C03A C03J C03I 176.6(6) . . . . ? C03G C03B C03Q C03W -1.1(11) . . . . ? C03J C03A C03G C02X -171.0(6) . . . . ? C03J C03A C03G C03B 7.6(10) . . . . ? C03J C03I C03K C01H 1.4(11) . . . . ? C03K C01H C02K C01E -174.1(6) . . . . ? C03K C01H C02K C03A -0.1(9) . . . . ? C03K C03I C03J C03A 0.0(11) . . . . ? C03M C02X C03G C03A -179.4(6) . . . . ? C03M C02X C03G C03B 2.0(9) . . . . ? C03Q C03B C03G C02X 0.1(10) . . . . ? C03Q C03B C03G C03A -178.6(6) . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 -0.152 -0.533 0.058 1851.9 648.5 '16 CH2Cl2'