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Information card for entry 7708516
Preview
| Coordinates | 7708516.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C50 H76 N4 Ni2 Si2 |
|---|---|
| Calculated formula | C50 H76 N4 Ni2 Si2 |
| Title of publication | A square planar silylene nickel four-membered ring. |
| Authors of publication | Kaufmann, Sebastian; Köppe, Ralf; Roesky, Peter W. |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2021 |
| a | 10.265 ± 0.002 Å |
| b | 11.626 ± 0.002 Å |
| c | 12.091 ± 0.002 Å |
| α | 83.66 ± 0.03° |
| β | 68.19 ± 0.03° |
| γ | 64.34 ± 0.03° |
| Cell volume | 1205.4 ± 0.6 Å3 |
| Cell temperature | 150 K |
| Ambient diffraction temperature | 150 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0714 |
| Residual factor for significantly intense reflections | 0.0464 |
| Weighted residual factors for significantly intense reflections | 0.1068 |
| Weighted residual factors for all reflections included in the refinement | 0.1133 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.892 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 269804 (current) | 2021-10-07 | cif/ Adding structures of 7708516 via cif-deposit CGI script. |
7708516.cif |
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Users of the data should acknowledge the original authors of the
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