#------------------------------------------------------------------------------ #$Date: 2021-10-13 01:56:35 +0300 (Wed, 13 Oct 2021) $ #$Revision: 269905 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/85/7708549.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708549 loop_ _publ_author_name 'Karmakar, Gourab' 'Halankar, Kruti' 'Tyagi, Adish' 'Mandal, Balaji P.' 'Wadawale, Amey' 'Gotluru, Kedarnath' 'Srivastava, A. P.' 'Singh, Vishal' _publ_section_title ; Dimethyltin(IV)-4,6-dimethyl-2-pyridylselenolate: An Efficient Single Source Precursor for the Preparation of SnSe Nanosheets as Anode Material for Lithium Ion Batteries ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT01312B _journal_year 2021 _chemical_formula_sum 'C16 H22 N2 Se2 Sn' _chemical_formula_weight 518.96 _space_group_crystal_system orthorhombic _space_group_IT_number 62 _space_group_name_Hall '-P 2c 2n' _space_group_name_H-M_alt 'P n a m' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2017/1 _audit_update_record ; 2020-02-24 deposited with the CCDC. 2021-10-11 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.4320(5) _cell_length_b 7.5736(2) _cell_length_c 21.0055(8) _cell_measurement_reflns_used 3653 _cell_measurement_temperature 298(2) _cell_measurement_theta_max 25.8840 _cell_measurement_theta_min 2.8510 _cell_volume 1977.77(12) _computing_cell_refinement 'CrysAlisPro 1.171.40.57a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.57a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.57a (Rigaku OD, 2019)' _computing_structure_refinement 'SHELXL-2017/1 (Sheldrick, 2017)' _computing_structure_solution OLEX1.2 _diffrn_ambient_temperature 298(2) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.859 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, HyPix' _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0288 _diffrn_reflns_av_unetI/netI 0.0280 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.859 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -28 _diffrn_reflns_number 8392 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.859 _diffrn_reflns_theta_full 26.000 _diffrn_reflns_theta_max 29.485 _diffrn_reflns_theta_min 2.859 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 4.969 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.27212 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.57a (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.743 _exptl_crystal_description needle _exptl_crystal_F_000 1000 _exptl_crystal_size_max 0.400 _exptl_crystal_size_mid 0.150 _exptl_crystal_size_min 0.100 _refine_diff_density_max 0.767 _refine_diff_density_min -0.265 _refine_diff_density_rms 0.078 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.057 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 104 _refine_ls_number_reflns 2428 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.057 _refine_ls_R_factor_all 0.0610 _refine_ls_R_factor_gt 0.0384 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0442P)^2^+0.5500P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0848 _refine_ls_wR_factor_ref 0.0921 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1775 _reflns_number_total 2428 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt01312b2.cif _cod_data_source_block shelx _cod_depositor_comments ; The following automatic conversions were performed: data item '_space_group_crystal_system' value 'Orthorhombic' was changed to 'orthorhombic' in accordance with the /home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 last updated on 2011-04-26. data item '_atom_sites_solution_secondary' value 'diffmap' was changed to 'difmap'. Automatic conversion script Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas ; _cod_database_code 7708549 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.241 _shelx_estimated_absorpt_t_max 0.636 _oxdiff_exptl_absorpt_empirical_full_min 0.647 _oxdiff_exptl_absorpt_empirical_full_max 2.707 _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _shelx_res_file ; TITL shelx.res created by SHELXL-2017/1 at 12:03:15 on 08-Jan-2020 CELL 0.71073 12.4320 7.5736 21.0055 90.000 90.000 90.000 ZERR 4.00 0.0005 0.0002 0.0008 0.000 0.000 0.000 LATT 1 SYMM - X, - Y, 1/2 + Z SYMM 1/2 + X, 1/2 - Y, 1/2 - Z SYMM 1/2 - X, 1/2 + Y, - Z SFAC C H N SE SN UNIT 64 88 8 8 4 MERG 2 MORE -1 FMAP 2 PLAN 20 SIZE 0.100 0.150 0.400 ACTA 52.00 BOND $H CONF L.S. 4 TEMP 25.00 WGHT 0.044200 0.550000 FVAR 0.55686 SN1 5 0.706435 0.485274 0.750000 10.50000 0.06606 0.05032 = 0.07028 0.00000 0.00000 0.00693 SE1 4 0.564594 0.424100 0.660797 11.00000 0.06487 0.08773 = 0.08342 0.00617 -0.00534 -0.00204 N1 3 0.770774 0.517516 0.629217 11.00000 0.06732 0.05393 = 0.06806 -0.00095 -0.00938 0.00037 C1 1 0.675049 0.484059 0.602245 11.00000 0.07252 0.05208 = 0.08032 -0.00022 -0.01045 0.00059 C2 1 0.659815 0.488803 0.536779 11.00000 0.07172 0.06827 = 0.07607 0.00228 -0.01944 -0.00197 AFIX 43 H2 2 0.592149 0.466255 0.519740 11.00000 -1.20000 AFIX 0 C3 1 0.744871 0.526888 0.497062 11.00000 0.08884 0.05756 = 0.06958 0.00290 -0.00952 -0.00070 C4 1 0.843195 0.559859 0.525549 11.00000 0.07955 0.06445 = 0.07308 0.00015 -0.00050 -0.00583 AFIX 43 H4 2 0.902510 0.585384 0.500190 11.00000 -1.20000 AFIX 0 C5 1 0.854959 0.555603 0.590889 11.00000 0.07422 0.05298 = 0.07816 -0.00306 -0.01062 -0.00253 C6 1 0.732152 0.529637 0.425974 11.00000 0.11530 0.09972 = 0.07028 0.00801 -0.01455 -0.01819 AFIX 137 H6A 2 0.759026 0.421232 0.408424 11.00000 -1.50000 H6B 2 0.771875 0.627145 0.408654 11.00000 -1.50000 H6C 2 0.657424 0.542293 0.415400 11.00000 -1.50000 AFIX 0 C7 1 0.959518 0.591269 0.622433 11.00000 0.08058 0.09222 = 0.09678 0.00169 -0.01859 -0.01136 AFIX 137 H7A 2 0.947056 0.646644 0.662877 11.00000 -1.50000 H7B 2 1.001845 0.668132 0.596106 11.00000 -1.50000 H7C 2 0.997300 0.482108 0.628726 11.00000 -1.50000 AFIX 0 C8 1 0.732695 0.761991 0.750000 10.50000 0.12979 0.05541 = 0.08057 0.00000 0.00000 0.00364 AFIX 137 H8A 2 0.803640 0.786611 0.765713 10.50000 -1.50000 H8B 2 0.680448 0.818112 0.776890 10.50000 -1.50000 H8C 2 0.725884 0.806494 0.707397 10.50000 -1.50000 AFIX 0 C9 1 0.815250 0.270489 0.750000 10.50000 0.09179 0.06169 = 0.07120 0.00000 0.00000 0.02111 AFIX 137 H9A 2 0.826134 0.230392 0.707126 10.50000 -1.50000 H9B 2 0.786260 0.175961 0.775154 10.50000 -1.50000 H9C 2 0.882732 0.307655 0.767721 10.50000 -1.50000 AFIX 0 HKLF 4 REM REM R1 = 0.0384 for 1775 Fo > 4sig(Fo) and 0.0610 for all 2428 data REM 104 parameters refined using 0 restraints END WGHT 0.0442 0.5500 REM Highest difference peak 0.767, deepest hole -0.265, 1-sigma level 0.078 Q1 1 0.7713 0.5199 0.7500 10.50000 0.05 0.77 Q2 1 0.6704 0.5328 0.7791 11.00000 0.05 0.50 Q3 1 0.5613 0.5256 0.6877 11.00000 0.05 0.43 Q4 1 0.6190 0.4784 0.6406 11.00000 0.05 0.42 Q5 1 0.7004 0.6233 0.7500 10.50000 0.05 0.39 Q6 1 0.5214 0.4303 0.6282 11.00000 0.05 0.38 Q7 1 0.7140 0.3435 0.7500 10.50000 0.05 0.29 Q8 1 0.9506 0.5721 0.6577 11.00000 0.05 0.28 Q9 1 0.6227 0.2508 0.7500 10.50000 0.05 0.28 Q10 1 0.9063 0.5600 0.6696 11.00000 0.05 0.26 Q11 1 0.9419 0.7249 0.6356 11.00000 0.05 0.23 Q12 1 0.5636 0.2796 0.6720 11.00000 0.05 0.22 Q13 1 0.6233 0.7307 0.7500 10.50000 0.05 0.22 Q14 1 0.7059 0.4955 0.6083 11.00000 0.05 0.22 Q15 1 0.7947 0.7160 0.7500 10.50000 0.05 0.22 Q16 1 0.6790 0.4419 0.6021 11.00000 0.05 0.21 Q17 1 0.8044 0.5818 0.6232 11.00000 0.05 0.21 Q18 1 0.8229 0.5083 0.6119 11.00000 0.05 0.20 Q19 1 0.6555 0.7042 0.7785 11.00000 0.05 0.20 Q20 1 0.8095 0.4802 0.5139 11.00000 0.05 0.19 ; _shelx_res_checksum 48521 _shelx_hkl_file ; 0 0 -26 1.65508 14.1377 1 0 0 -25-16.7093 13.5921 1 0 0 -24 274.187 18.0647 1 0 0 -23 1.95728 11.9287 1 0 0 -22 585.004 21.9408 1 0 0 -21 15.3502 10.0544 1 0 0 -20 376.828 16.7665 1 0 0 -19-3.18197 8.19374 1 0 0 -18 89.7328 9.62921 1 0 0 -17 2.79998 7.25076 1 0 0 -16 8.85698 6.81267 1 0 0 -15 0.30981 5.70351 1 0 0 -14 2124.03 45.8043 1 0 0 -13 0.52254 4.78252 1 0 0 -12 13075.1 241.041 1 0 0 -11 8.24601 4.08707 1 0 0 -10 12112.2 222.547 1 0 0 -9-0.17598 3.00639 1 0 0 3 0.44300 0.84584 1 0 0 3 0.52828 0.85284 2 0 0 4 19.3707 1.87469 2 0 0 4 16.0008 1.62799 1 0 0 5 1.12907 1.52544 2 0 0 5-0.82454 1.56774 1 0 0 6 102.308 4.62170 2 0 0 6 120.261 4.53636 1 0 0 7-0.76154 2.09961 1 0 0 7-1.53035 2.09437 2 0 0 8 11578.4 211.099 1 0 0 8 11511.1 212.806 2 0 0 9 1.90103 3.14178 2 0 0 9 5.13545 3.16907 1 0 0 10 11192.2 209.426 2 0 0 10 11334.4 207.138 1 0 0 11 5.60399 4.40307 2 0 0 12 11998.9 224.229 2 0 0 13 8.20629 5.46294 2 0 0 14 1928.18 44.5103 2 0 0 15 0.83347 5.98732 2 0 0 16 5.81404 6.85997 2 0 0 17 2.42229 7.60998 2 0 0 18 60.8383 9.90037 2 0 0 19-5.52697 9.28624 2 0 0 20 350.533 18.5109 2 0 0 21 3.68576 10.2149 2 0 -1 -26 8.80100 13.8788 1 0 -1 -25 1.06891 13.2378 1 0 -1 -24-7.19040 12.3686 1 0 -1 -23 43.0590 12.5810 1 0 -1 -22 13.9377 10.9849 1 0 -1 -21 63.0943 11.4008 1 0 -1 -20 7.19411 9.64539 1 0 -1 -19 16.0020 8.95578 1 0 1 -19-14.7825 9.80205 1 0 -1 -18 9.10264 8.15921 1 0 1 -18-14.4295 8.95608 1 0 1 -17 147.567 10.9013 1 0 -1 -17 127.102 10.1093 1 0 -1 -16-1.99620 6.80733 1 0 1 -16-6.39341 7.02161 1 0 -1 -15 61.1284 7.69818 1 0 1 -15 47.0337 7.25549 1 0 1 -14-3.97903 5.98319 1 0 -1 -14 7.22523 5.55792 1 0 1 -13 243.372 10.7390 1 0 1 -12 1.02703 4.61844 1 0 1 -11 1812.36 38.6401 1 0 1 -10 2.28978 3.62030 1 0 1 -10 2.89606 4.23853 3 0 1 -9 180.127 7.34596 1 0 1 -9 177.718 7.84093 3 0 1 -8 0.15870 2.52175 1 0 1 -8 0.17577 3.19887 3 0 1 -7 976.302 21.6146 3 0 -1 -7 981.766 21.5718 1 0 1 -6 7.59532 2.49461 3 0 -1 -6 7.30179 2.41834 1 0 1 -5 1176.06 24.3654 3 0 -1 -5 1215.12 25.0973 2 0 -1 -5 1215.92 24.7956 1 0 1 -4 0.64782 1.35837 3 0 -1 -4 0.97475 1.43972 1 0 -1 -4 3.11519 1.75458 2 0 1 -3 296.002 6.81555 3 0 -1 -3 291.263 7.55341 1 0 -1 -3 305.489 7.54834 2 0 -1 -2 3.80757 1.14637 2 0 -1 -2 1.86721 1.17963 1 0 -1 -1 1252.72 28.8160 1 0 -1 -1 1106.22 29.2470 5 0 -1 0 1.55213 0.94126 5 0 1 2 3.06946 1.13915 1 0 -1 3 291.783 6.73154 2 0 -1 4 0.25698 1.21920 2 0 -1 5 1167.62 22.9602 1 0 -1 5 1154.65 23.7562 2 0 -1 6 8.07751 2.07036 1 0 -1 6 2.97272 1.93469 2 0 -1 7 866.167 17.3553 2 0 -1 7 908.981 16.3944 1 0 1 8 0.72456 3.09469 1 0 -1 8 0.61678 2.48899 1 0 -1 8 1.30271 2.41926 2 0 1 8 3.45997 3.09080 2 0 -1 9 165.937 6.45478 1 0 1 9 154.939 7.78716 2 0 -1 9 149.980 7.24185 2 0 -1 10 3.89018 3.52294 1 0 -1 10-0.74682 3.65890 2 0 1 10 0.86679 4.16085 2 0 -1 11 1698.50 37.5011 2 0 1 11 1683.26 38.3682 2 0 1 12-4.54032 5.31298 2 0 -1 12-2.77155 4.92168 2 0 -1 13 208.685 10.5934 2 0 1 13 221.842 11.3941 2 0 -1 14 4.44131 5.43983 2 0 1 14-0.40822 5.57138 2 0 -1 15 53.9430 7.62517 2 0 1 15 36.8349 7.55993 2 0 -1 16 2.56875 6.90607 2 0 1 16-10.4592 7.66884 2 0 -1 17 119.164 10.4343 2 0 1 17 109.924 11.0834 2 0 1 18 0.54281 8.78813 2 0 -1 18-6.00771 8.52501 2 0 1 19-3.45037 10.0483 2 0 -1 19-4.26577 8.71159 2 0 -1 20-3.39707 9.26638 2 0 1 20 3.03422 9.86046 2 0 -1 21 59.4192 11.7651 2 0 1 22 3.82106 6.26377 5 0 -2 -26 16.6755 15.0159 1 0 -2 -25 9.52202 13.9287 1 0 -2 -24 142.411 15.7574 1 0 -2 -23 8.18201 12.4370 1 0 -2 -22 191.438 15.4788 1 0 -2 -21 8.86832 10.7366 1 0 -2 -20 156.118 13.2419 1 0 -2 -19 9.38888 9.58279 1 0 -2 -18 103.703 10.8219 1 0 2 -11-0.23473 4.79155 3 0 -2 -11 0.53736 4.40521 1 0 2 -10 3695.38 72.7088 3 0 -2 -10 3772.71 73.6641 1 0 -2 -9 2.32823 3.38381 1 0 2 -9 0.55974 3.80871 3 0 2 -8 4660.44 87.5084 3 0 -2 -8 4586.62 88.7611 1 0 2 -7-0.69122 2.71254 3 0 -2 -7 2.40250 2.96865 1 0 -2 -6 142.839 6.30439 1 0 2 -6 136.014 5.12750 3 0 2 -5 0.61822 1.70676 3 0 -2 -5-0.34247 2.33094 1 0 -2 -4 42.5431 3.24507 2 0 2 -4 47.5147 2.38807 3 0 -2 -3 5.20420 2.12032 1 0 -2 -3 0.40994 1.61031 2 0 -2 -2 531.485 13.5289 5 0 -2 -2 493.185 12.0570 1 0 -2 -2 475.587 10.8413 2 0 -2 -1 1.07184 2.28222 5 0 -2 -1-1.21802 1.17360 2 0 -2 -1 1.10805 1.89977 1 0 -2 0 70615.4 1268.98 1 0 2 0 70587.6 1270.75 5 0 -2 2 486.390 12.7589 5 0 2 3-1.19633 1.78161 2 0 -2 3 0.36316 0.86593 2 0 2 4 38.1819 3.12345 2 0 -2 4 39.9226 2.20756 2 0 -2 5-0.56775 1.56799 2 0 2 5 2.23917 2.73643 5 0 2 5-0.34563 2.31555 2 0 2 6 137.917 6.28436 2 0 2 6 146.437 7.02862 5 0 -2 6 118.573 4.67534 2 0 -2 7-0.91897 2.37701 1 0 2 7-0.25963 3.08437 5 0 2 7-2.06110 3.16546 2 0 -2 7 2.32326 2.38074 2 0 -2 8 4286.68 80.8439 1 0 2 8 4326.00 84.3936 2 0 -2 8 4307.71 82.2785 2 0 2 8 4377.22 84.7428 5 0 2 9-1.14549 4.04686 2 0 -2 9 2.26313 2.98330 2 0 2 9 2.57307 3.86138 5 0 -2 9-1.26249 3.06423 1 0 2 10 3388.47 69.4066 5 0 -2 10 3496.97 67.9014 2 0 -2 10 3445.66 65.7114 1 0 2 10 3308.35 69.7391 2 0 -2 11 0.26372 4.37001 2 0 2 11-0.34377 5.21833 2 0 -2 12 4194.64 83.2148 2 0 2 13 1.67614 4.49187 5 0 -2 13 1.94829 5.16972 2 0 -2 14 1006.13 26.7033 2 0 -2 15 5.73094 6.23143 2 0 -2 16 70.6815 8.48384 2 0 2 17-1.87758 5.98995 5 0 -2 17-4.97603 7.62609 2 0 2 18 95.5946 8.76347 5 0 -2 18 95.4004 10.7265 2 0 2 19 3.56371 6.66389 5 0 -2 19-2.58417 9.26892 2 0 2 20 129.540 10.2575 5 0 -2 20 126.848 12.6644 2 0 2 21-0.39407 6.92878 5 0 2 22 147.151 11.0697 5 0 -3 -25 11.7437 14.6814 1 0 -3 -24 19.7531 14.2434 1 0 -3 -23 93.7482 14.7723 1 0 -3 -22 11.5057 12.3111 1 0 -3 -21 147.642 14.9407 1 0 -3 -16 9.00448 8.05249 1 0 -3 -15 66.9296 8.76820 1 0 -3 -14-1.46574 6.98074 1 0 -3 -13 697.362 20.8896 1 0 -3 -12 5.26930 5.95088 1 0 -3 -11 4795.92 95.8252 1 0 3 -11 4942.53 93.6499 3 0 3 -10 10.9459 4.56063 3 0 -3 -10 2.64537 5.20963 1 0 3 -9 740.192 17.7329 3 0 -3 -9 727.110 19.8397 1 0 -3 -8 8.87966 4.63871 1 0 3 -8 1.73863 3.07852 3 0 3 -7 1560.26 31.1468 3 0 -3 -7 1539.86 34.3759 1 0 3 -6 5.92080 2.29606 3 0 -3 -6 7.58563 3.76138 1 0 -3 -5 2316.70 47.6648 1 0 -3 -4-0.42332 3.07611 1 0 -3 -3 736.029 19.4593 5 0 -3 -3 703.488 17.7399 1 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4.86001 3.83585 2 1 2 -8 2.01376 3.33053 3 1 -2 -8 3.54525 3.87800 3 1 -2 -8 7.76089 3.51849 1 -1 -2 -8 5.64144 3.50543 1 1 -2 -7 1251.65 27.6301 3 -1 -2 -7 1336.37 27.8466 1 1 -2 -7 1335.53 28.4380 1 1 2 -7 1282.20 26.5642 3 1 2 -6 169.593 5.84334 3 1 -2 -6 161.479 6.63119 3 1 -2 -6 165.711 6.98075 1 -1 2 -6 163.071 5.82661 2 -1 -2 -6 170.694 7.10698 2 -1 -2 -6 172.249 6.85827 1 1 -2 -5 4826.02 92.3683 3 1 -2 -5 4975.13 93.5728 1 -1 -2 -5 4875.38 93.0956 2 -1 2 -5 4955.85 91.2004 2 -1 -2 -5 4963.18 92.8046 1 -1 -2 -5 5053.30 94.2873 5 -1 -2 -4 9.59457 2.41384 1 1 -2 -4 4.91214 2.35611 3 -1 -2 -4 4.39324 2.35578 2 -1 2 -4 5.74193 1.50651 2 1 -2 -4 5.71380 2.24682 1 -1 -2 -4 5.42245 2.96672 5 -1 -2 -3 1152.89 23.7144 1 -1 2 -3 1132.77 21.7096 2 1 -2 -3 1103.25 22.8503 3 -1 -2 -3 1154.76 25.2966 5 1 -2 -3 1150.74 24.6102 1 -1 -2 -3 1118.46 23.6263 2 1 -2 -2 3216.18 61.3213 3 -1 -2 -2 3348.07 62.4812 1 -1 2 -2 3373.68 63.9991 5 -1 -2 -2 3297.72 64.3413 5 1 -2 -2 3373.60 63.3880 1 -1 2 -1 10291.3 188.066 5 -1 -2 -1 10166.0 185.803 1 1 -2 -1 10102.4 187.040 1 -1 -2 -1 10340.6 188.203 5 -1 2 0 370.348 7.62452 3 -1 -2 0 378.330 9.01755 1 -1 2 0 395.972 11.1964 5 1 2 0 363.638 7.85353 4 1 -2 0 364.530 7.83475 4 -1 2 1 10062.6 181.918 3 1 2 1 10081.3 183.198 1 -1 2 1 9970.28 181.866 4 -1 -2 1 10154.1 182.726 1 -1 -2 1 10063.2 181.775 4 1 -2 2 3390.03 64.7356 5 1 2 2 3358.69 63.8049 1 1 -2 3 1119.90 23.7513 5 1 2 3 1087.24 23.1888 1 -1 2 3 1101.10 23.9427 1 -1 -2 3 1110.17 21.6049 3 1 2 4 9.14414 2.70307 5 1 2 4 6.50278 2.61325 1 1 -2 4 7.59806 2.35737 5 -1 2 4 6.56099 2.17490 2 -1 -2 4 4.40190 1.59541 3 -1 2 5 4884.15 90.7315 2 -1 -2 5 4834.85 89.1005 3 1 -2 5 4727.10 89.9797 5 1 2 5 4794.22 92.1987 5 1 -2 6 162.593 5.96871 5 -1 -2 6 159.700 5.78655 3 -1 -2 6 159.977 5.09874 1 -1 2 6 154.202 6.63954 2 1 2 6 167.403 7.39732 5 -1 2 7 1297.64 28.3060 2 1 -2 7 1263.93 26.2091 5 -1 -2 7 1256.63 25.2618 1 1 2 7 1213.92 28.3948 5 -1 -2 8 5.71640 2.72769 1 -1 2 8 4.92089 3.57728 2 1 2 8 8.40268 3.26841 5 1 -2 8 3.60791 3.08678 1 -1 2 9 617.027 17.2127 2 -1 -2 9 626.138 14.4282 1 1 2 9 595.949 17.0074 5 1 -2 9 606.358 15.1586 1 -1 -2 10 998.565 21.4621 1 1 2 10 982.362 24.2863 5 -1 -2 10 1016.45 23.7002 2 1 2 11 1392.48 32.2121 5 -1 -2 11 1428.23 29.6296 1 -1 2 11 1361.46 33.5626 2 -1 -2 11 1391.06 31.9544 2 1 2 12 389.744 13.4523 5 -1 -2 12 377.589 13.5784 2 -1 -2 13 405.236 14.1018 2 1 2 13 450.860 14.6449 5 -1 -2 14 81.1936 7.71010 2 1 2 14 82.8421 6.95712 5 1 2 15 161.692 9.01326 5 -1 -2 15 163.193 10.4065 2 -1 -2 16 9.36751 6.65597 2 -1 -2 17 271.140 13.9421 2 -1 -2 18 5.20930 8.35297 2 -1 -2 19 13.1134 8.85728 2 1 2 20 36.5483 6.74143 5 -1 -2 20 22.4009 9.62490 2 1 2 21 40.7292 7.30126 5 -1 -2 21 41.7124 10.6929 2 -1 2 21 42.0572 8.62041 5 -1 -2 22 32.7760 11.9212 2 -1 2 22 27.9436 8.62110 5 -1 -2 23 51.1289 12.8111 2 -1 2 23 36.1940 13.5728 2 -1 2 23 41.8476 9.28044 5 -1 -2 24-6.65010 12.7193 2 1 -3 -25 75.8404 16.4451 1 1 -3 -24 3.92903 13.3136 1 1 -3 -23 68.8232 14.2540 1 1 -3 -22 37.8243 13.0082 1 1 -3 -21 98.4893 13.6279 1 1 -3 -20 29.5228 11.3965 1 1 -3 -19 268.747 15.9156 1 -1 -3 -19 286.005 16.0656 1 -1 -3 -18 21.3291 10.3540 1 1 -3 -18 3.60714 8.95895 1 -1 -3 -17 207.574 13.3531 1 -1 -3 -16 26.4860 8.87652 1 -1 -3 -15 803.087 23.9108 1 -1 -3 -14 148.261 10.1801 1 -1 -3 -13 1220.83 30.6127 1 -1 -3 -12 192.575 10.5844 1 1 -3 -12 199.223 10.6314 1 1 3 -11 753.075 19.0197 3 -1 3 -11 713.245 18.7763 3 -1 -3 -11 680.800 20.0534 1 1 -3 -11 717.972 20.7311 1 -1 3 -10 300.926 10.2935 3 1 3 -10 289.701 10.3132 3 1 -3 -10 283.926 11.8011 1 -1 -3 -10 281.472 11.5012 1 1 -3 -9 3745.56 75.0257 1 -1 3 -9 3811.03 71.8232 3 -1 -3 -9 3622.77 74.0928 1 1 -3 -8 102.578 6.80599 3 1 -3 -8 112.595 7.32652 1 -1 -3 -8 103.826 7.07094 1 -1 3 -8 110.252 5.53074 3 1 -3 -7 3495.77 69.1197 1 -1 -3 -7 3466.60 68.4150 1 1 -3 -7 3386.82 67.4242 3 -1 -3 -7 3410.77 68.1348 2 -1 3 -7 3514.22 65.4569 3 -1 -3 -6 85.2169 5.30644 2 -1 -3 -6 80.6645 5.61548 1 -1 3 -6 75.8114 3.78106 3 1 -3 -6 69.9263 5.69169 1 1 -3 -6 68.1850 5.24917 3 -1 -3 -5 2870.89 57.4573 1 -1 -3 -5 2976.52 59.6951 5 1 -3 -5 2834.64 56.0538 3 -1 -3 -5 2841.92 56.7384 2 1 -3 -5 2841.46 58.1790 1 -1 3 -5 2940.96 53.8088 3 1 -3 -4 198.782 8.21111 1 -1 3 -4 199.694 4.83352 3 -1 -3 -4 212.853 7.51993 2 1 -3 -4 206.305 6.95387 3 -1 -3 -4 206.253 7.84689 1 -1 -3 -4 211.006 9.48540 5 -1 -3 -3 2013.47 41.2010 1 1 -3 -3 2024.88 39.2822 3 -1 -3 -3 2028.80 43.5605 5 -1 -3 -3 2001.83 40.1414 2 1 -3 -3 2104.06 42.5021 1 1 -3 -2 478.248 10.6479 3 -1 -3 -2 461.346 11.4709 2 -1 -3 -2 471.704 14.4688 5 -1 -3 -2 460.892 12.4229 1 1 -3 -2 458.994 13.3391 1 -1 3 -2 461.058 14.2489 5 1 -3 -1 9540.55 177.134 1 -1 3 -1 9627.55 179.135 5 -1 -3 -1 9563.53 175.722 1 -1 -3 -1 9503.06 178.775 5 -1 -3 0 1879.39 40.6625 5 -1 3 0 1867.31 34.8856 2 -1 3 0 1911.46 41.2256 5 -1 -3 0 1904.60 37.8885 1 1 -3 1 9543.43 177.826 5 -1 3 1 9495.74 173.013 2 1 3 1 9518.68 172.277 4 -1 -3 1 9585.04 175.083 1 -1 3 1 9514.74 179.126 5 1 -3 1 9568.99 172.203 4 1 3 2 466.899 12.5538 1 -1 3 2 474.178 10.9263 2 1 -3 2 489.236 14.0202 5 -1 3 2 450.691 10.0450 4 -1 -3 2 444.980 9.94783 4 -1 -3 3 1951.05 37.1430 3 1 3 3 1980.92 40.5562 1 1 -3 3 2001.23 41.7429 5 -1 3 3 2036.12 39.1065 2 -1 -3 4 194.923 5.50778 3 -1 3 4 210.347 7.27884 2 1 3 4 209.716 8.06746 1 1 -3 4 207.214 8.32823 5 1 3 5 2771.64 55.2946 1 -1 3 5 2816.36 54.8405 2 1 -3 5 2768.68 55.7402 5 1 3 5 2857.11 58.2119 5 -1 -3 5 2731.74 52.2567 3 1 3 6 69.9468 6.13176 5 1 -3 6 73.5935 5.45013 5 -1 -3 6 70.1752 3.84922 3 -1 3 6 69.7717 5.15339 2 1 3 6 58.8391 5.31497 1 -1 3 7 3303.19 65.5657 2 1 3 7 3324.04 67.9466 5 1 -3 7 3245.09 64.6391 5 1 -3 8 100.987 5.84360 5 -1 3 8 89.6609 6.58786 2 -1 -3 9 3609.98 67.4585 1 1 -3 9 3484.47 69.3505 5 -1 3 9 3615.31 71.8791 2 -1 -3 9 3484.97 68.7958 2 -1 3 10 289.637 13.2338 5 -1 -3 10 272.086 8.75983 1 -1 -3 10 250.997 9.55220 2 -1 3 10 281.367 11.8366 2 1 -3 10 267.411 9.70549 5 1 -3 11 640.379 16.9163 5 -1 -3 11 685.185 16.1880 1 -1 3 11 641.756 20.1565 2 -1 -3 11 645.362 17.6812 2 -1 3 11 633.289 21.2396 5 1 -3 12 194.103 8.32179 5 -1 -3 12 188.082 8.88225 2 -1 3 12 201.642 11.2879 2 -1 3 12 207.430 11.9814 5 -1 3 13 1177.85 31.0691 2 -1 -3 13 1154.70 28.2106 2 1 3 13 1107.85 29.6834 5 -1 3 13 1168.92 31.8704 5 1 -3 13 1115.46 25.7531 5 -1 3 14 127.187 10.3970 5 -1 -3 14 159.099 9.72069 2 1 -3 14 167.929 7.48520 5 -1 3 14 147.426 11.0280 2 1 3 14 145.816 9.64351 5 1 -3 15 711.508 17.9223 5 -1 3 15 696.726 23.5954 5 -1 3 15 723.155 24.0775 2 -1 -3 15 704.409 21.5359 2 1 3 15 747.591 22.4851 5 1 3 16 19.7582 6.93579 5 -1 3 16 14.5068 8.95908 2 1 -3 16 24.4987 4.64931 5 -1 -3 16 13.9043 7.65525 2 -1 3 16 11.5000 7.59744 5 1 3 17 176.273 11.3861 5 -1 3 17 196.998 14.0263 2 -1 3 17 190.275 12.8453 5 -1 -3 17 218.225 12.7642 2 -1 3 18 11.2585 9.85317 2 -1 3 18 5.70639 8.10103 5 1 3 18-5.50723 7.10523 5 -1 -3 18-3.64197 8.51044 2 -1 -3 19 274.885 14.7979 2 -1 3 19 251.863 14.8518 5 1 3 19 228.474 13.0323 5 -1 3 19 271.888 17.3869 2 1 3 20 10.7365 7.63469 5 -1 3 20-7.22787 11.4825 2 -1 -3 20 17.7889 10.2161 2 -1 3 20 15.2716 9.28891 5 1 3 21 63.6205 9.25588 5 -1 -3 21 66.1173 11.9413 2 -1 3 21 50.4932 10.5908 5 -1 3 21 70.2220 13.4524 2 1 3 22 9.02695 8.19003 5 -1 -3 22 8.20874 10.5477 2 -1 3 22 5.83599 9.41588 5 -1 3 23 35.6683 10.1048 5 -1 -4 -23 24.1904 14.6921 1 1 -4 -23 58.5630 14.4008 1 1 -4 -22 57.0898 14.3631 1 -1 -4 -22 47.7274 14.0904 1 -1 -4 -21 31.4335 12.6155 1 -1 -4 -20 74.4136 13.6432 1 -1 -4 -19 31.2393 11.6133 1 -1 -4 -18 14.0628 11.3429 1 -1 -4 -17 140.899 12.5780 1 -1 -4 -16 0.44142 8.63974 1 1 -4 -16-4.98764 9.61132 1 1 -4 -15 57.7956 9.96694 1 -1 -4 -15 56.7482 9.84400 1 -1 -4 -14 133.670 10.7704 1 1 -4 -14 129.953 11.3822 1 1 -4 -13 415.702 17.1178 1 -1 -4 -13 445.117 16.6735 1 -1 -4 -12 310.867 13.7991 1 -1 4 -12 301.981 11.2728 3 1 -4 -12 305.949 13.8929 1 -1 4 -11 1035.42 23.4529 3 1 -4 -11 1016.71 27.4337 1 1 -4 -10 763.315 22.6067 1 -1 -4 -10 721.241 21.5846 1 -1 4 -9 431.350 11.5207 3 -1 -4 -9 389.817 14.4208 1 1 -4 -9 406.205 15.1914 1 -1 -4 -8 17.5668 5.34262 1 -1 4 -8 17.3147 3.48246 3 1 -4 -8 16.9957 5.58836 1 -1 4 -7 606.018 13.0789 3 -1 -4 -7 573.292 17.2448 1 1 -4 -7 568.302 16.0029 3 -1 -4 -7 579.108 16.5274 2 1 -4 -7 596.066 18.1560 1 -1 -4 -6 16.4197 4.59257 2 1 -4 -6 17.8100 4.57100 3 1 -4 -6 18.0251 5.26697 1 -1 -4 -6 21.5983 5.03670 1 -1 -4 -5 1503.44 32.1392 2 1 -4 -5 1475.44 34.4276 1 1 -4 -5 1507.13 31.3624 3 -1 -4 -5 1511.50 33.6312 1 1 -4 -4-2.02225 4.50250 1 1 -4 -4-1.65819 3.22975 3 -1 -4 -4 0.49764 3.17261 2 -1 -4 -4-0.99018 3.86569 1 -1 -4 -3 176.388 6.74156 2 1 -4 -3 186.575 6.23863 3 1 -4 -3 181.161 9.23169 1 -1 -4 -3 170.212 7.99419 1 -1 -4 -2 1735.31 37.2038 1 1 -4 -2 1745.12 33.6799 3 1 -4 -2 1721.04 38.4982 1 -1 -4 -2 1758.49 34.8312 2 -1 -4 -1 4450.91 81.8902 2 -1 -4 -1 4347.60 84.8630 1 1 -4 -1 4298.71 86.0864 1 -1 4 -1 4452.25 89.0509 5 1 -4 0 248.052 10.1352 1 -1 -4 0 242.660 8.96088 1 -1 -4 0 232.607 6.59958 2 -1 4 0 251.819 11.6700 5 -1 -4 1 4317.31 82.9642 1 1 4 2 1627.20 30.7284 4 -1 -4 2 1683.54 35.0378 1 -1 -4 3 165.210 4.41298 3 -1 4 3 174.060 6.55108 2 1 4 3 176.331 8.29545 1 -1 4 3 171.044 5.11829 4 -1 -4 3 168.104 4.92511 4 -1 -4 4 0.70630 1.68839 3 -1 4 4 0.54498 3.11371 2 -1 -4 4 1.34795 2.10537 4 -1 4 5 1491.26 32.3475 2 -1 4 6 15.7267 4.28315 2 1 -4 7 561.552 17.0294 5 1 4 7 550.857 19.1749 5 -1 4 7 556.623 16.5804 2 -1 4 7 575.727 20.3309 5 -1 -4 7 554.677 13.2739 2 1 4 8 25.7131 6.54647 5 -1 -4 8 15.4445 3.52986 2 1 -4 8 11.1824 5.03429 5 -1 4 8 11.3988 6.16726 5 -1 4 8 12.0771 5.24890 2 1 -4 9 373.300 13.2857 5 -1 4 9 371.653 14.0527 2 -1 -4 9 367.594 10.9243 2 -1 4 9 387.732 16.8669 5 1 4 9 364.331 15.8081 5 -1 4 10 691.569 23.9453 5 1 -4 10 704.250 19.4464 5 -1 -4 10 686.985 17.2864 2 1 4 10 692.354 22.7421 5 -1 4 10 679.930 20.9324 2 -1 4 11 879.981 28.3867 5 1 4 11 920.975 27.4373 5 -1 -4 11 963.621 22.7072 2 -1 4 11 901.652 26.0010 2 1 -4 11 886.762 23.2434 5 1 -4 12 284.167 11.4097 5 -1 4 12 273.721 15.1229 5 -1 -4 12 274.534 10.9257 2 1 4 12 269.259 14.1168 5 -1 4 12 285.606 14.1086 2 1 4 13 394.584 17.0695 5 1 -4 13 379.708 13.4142 5 -1 4 13 394.606 18.3073 5 -1 4 13 410.208 17.2495 2 -1 -4 13 412.498 14.0812 2 -1 4 14 124.538 11.8316 5 -1 4 14 131.788 11.5755 2 1 -4 14 133.731 8.14817 5 1 4 14 129.141 10.8815 5 -1 -4 14 132.934 9.09216 2 1 4 15 61.3059 9.20949 5 -1 4 15 44.1287 9.67702 5 1 -4 15 61.0244 6.45664 5 -1 4 15 62.4517 10.0043 2 -1 -4 15 62.2603 8.05613 2 -1 4 16 9.53659 9.32840 2 1 4 16 1.54943 8.03380 5 -1 4 16 4.84150 8.89506 5 -1 -4 16 1.88317 7.27894 2 -1 4 17 153.980 13.2788 5 -1 4 17 136.122 13.3393 2 -1 -4 17 131.204 10.8048 2 -1 4 18 5.50262 9.89907 5 -1 -4 18 6.20291 8.62904 2 1 4 18 9.47721 8.41487 5 -1 4 18 4.35257 10.8139 2 -1 4 19 9.24721 9.85396 5 -1 -4 19 10.3945 9.38777 2 1 4 19 14.8391 9.40692 5 1 4 20 38.9205 9.64132 5 -1 -4 20 16.4942 10.0142 2 -1 4 20 30.3273 10.8268 5 1 4 21 20.3261 9.88741 5 -1 4 21 34.5516 11.2229 5 -1 4 22 35.5339 11.4707 5 -1 4 23 30.3750 11.3072 5 -1 -5 -22 21.8668 14.1648 1 -1 -5 -21 61.0341 15.0567 1 1 -5 -20 11.5346 12.4996 1 -1 -5 -20 21.6558 13.6107 1 1 -5 -19 117.802 14.0934 1 -1 -5 -19 149.068 15.4092 1 -1 -5 -18 69.8232 12.7186 1 1 -5 -18 64.3964 12.7312 1 -1 -5 -17 201.714 14.9445 1 1 -5 -17 183.395 14.9229 1 -1 -5 -16 150.284 13.4524 1 1 -5 -16 149.480 13.7702 1 -1 -5 -15 533.049 20.4914 1 1 -5 -15 502.752 20.6082 1 -1 -5 -14 67.0763 10.5388 1 1 -5 -14 60.5105 11.3883 1 1 -5 -13 291.126 15.3781 1 -1 -5 -13 283.747 14.8698 1 -1 5 -13 299.933 11.5593 3 -1 -5 -12 102.133 10.6353 1 1 -5 -12 114.210 11.0573 1 -1 -5 -11 147.775 11.0414 1 1 -5 -11 151.046 11.5192 1 1 -5 -10 145.370 10.8392 1 -1 -5 -10 122.923 10.0012 1 1 -5 -9 838.374 25.2174 1 -1 -5 -9 922.358 25.1505 1 1 -5 -8 192.018 11.4161 1 -1 -5 -8 183.331 10.8321 1 1 -5 -7 1962.70 40.8817 3 1 -5 -7 1862.47 44.2903 1 -1 -5 -7 1949.25 43.6835 1 1 -5 -6 1193.82 31.1668 1 -1 -5 -6 1219.06 30.2153 1 1 -5 -6 1243.15 27.3331 3 1 -5 -5 1991.02 39.4770 3 1 -5 -5 1900.35 43.9670 1 -1 -5 -5 1869.09 42.6525 1 1 -5 -4 686.873 16.0774 3 -1 -5 -4 650.668 19.2448 1 1 -5 -4 671.748 20.3937 1 1 -5 -3 1126.35 23.3237 3 -1 -5 -3 1126.48 24.4086 2 1 -5 -3 1133.73 29.1621 1 -1 -5 -3 1119.94 27.7253 1 -1 -5 -2 56.7625 6.34988 1 -1 -5 -2 55.6851 4.25413 2 1 -5 -2 72.5868 7.39919 1 -1 -5 -1 1225.85 25.0292 2 1 -5 -1 1233.76 30.5403 1 -1 -5 -1 1264.12 29.3669 1 1 -5 0 95.7212 7.75439 1 -1 -5 0 102.742 7.38574 1 -1 -5 0 88.9976 3.81802 2 -1 5 1 1225.42 33.7230 5 -1 -5 1 1245.28 29.3394 1 1 -5 1 1248.47 30.6236 1 -1 5 2 66.9253 8.70164 5 -1 -5 2 57.5769 6.02046 1 -1 5 3 1118.45 31.8303 5 -1 -5 3 1064.81 26.0201 1 -1 -5 4 626.847 13.3218 4 -1 5 4 662.533 23.1287 5 -1 5 4 658.137 13.9341 4 -1 5 5 1852.36 35.6322 4 -1 5 5 1767.18 45.7921 5 -1 -5 5 1772.80 35.0554 4 -1 -5 6 1102.96 21.5702 2 -1 -5 7 1815.54 35.1687 2 -1 -5 8 166.966 6.35680 2 -1 5 8 178.442 12.8762 5 -1 5 9 818.923 28.1850 5 -1 -5 9 851.922 19.2849 2 -1 -5 10 115.468 6.39823 2 -1 5 10 120.377 11.7890 5 -1 5 11 144.127 13.0054 5 -1 -5 11 150.347 7.66557 2 -1 -5 12 88.5296 7.04521 2 1 5 12 91.6843 10.8185 5 -1 5 12 113.572 12.3904 5 -1 -5 13 242.548 10.7439 2 -1 5 13 255.793 16.4789 5 1 5 13 218.619 14.8044 5 -1 -5 14 62.8133 7.78375 2 -1 5 14 89.6349 12.0960 5 1 5 14 68.4237 11.2491 5 -1 5 15 482.067 22.4080 5 1 5 15 505.003 21.6481 5 -1 -5 15 494.803 16.9299 2 1 5 16 129.966 12.9882 5 -1 5 16 122.676 13.6323 5 -1 5 17 172.827 15.2548 5 -1 5 18 59.3625 12.5286 5 -1 5 19 100.283 13.6144 5 -1 5 20-11.3815 11.7685 5 -1 5 21 14.8838 11.9307 5 -1 5 22 10.6461 12.3245 5 -1 5 23 16.2762 12.4266 5 -1 -6 -20 26.6327 14.4805 1 1 -6 -20 44.6688 15.5110 1 1 -6 -19 4.19493 13.3519 1 -1 -6 -19 8.15721 13.4865 1 -1 -6 -18 16.2307 12.6992 1 1 -6 -18 13.9150 13.1920 1 1 -6 -17-7.94826 12.6976 1 -1 -6 -17 0.54206 11.6123 1 1 -6 -16 21.5344 12.8191 1 -1 -6 -16 16.6800 11.7852 1 -1 -6 -15 14.1033 11.2652 1 1 -6 -15-12.2513 11.6939 1 1 -6 -14 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17.7733 2.54145 4 -2 -2 2 34.9292 1.93256 1 -2 2 2 21.6956 2.54284 4 -2 2 2 24.6852 2.53123 3 -2 2 3 2141.49 40.8829 3 -2 -2 3 2086.09 41.0219 4 -2 2 3 2086.88 41.0435 4 2 2 3 2093.97 41.0058 1 -2 2 4 5079.04 93.3377 3 2 2 4 4899.35 93.2774 1 -2 2 5 87.3056 4.82142 3 -2 -2 5 90.2903 3.09878 1 2 2 5 91.8703 4.96326 1 -2 2 5 94.3900 5.46942 1 -2 -2 5 90.7910 4.31519 3 -2 2 6 7761.32 143.922 3 -2 -2 6 7850.71 142.706 3 2 2 6 7671.05 143.626 1 -2 -2 6 7702.76 140.650 1 -2 -2 7 35.8703 3.70514 3 -2 -2 7 39.3872 2.83101 1 2 2 7 42.9075 4.61833 1 -2 -2 8 4249.14 77.2788 1 2 2 8 3937.52 80.2739 1 2 -2 8 4149.61 77.3958 5 -2 -2 8 4175.27 79.5679 3 -2 -2 9 1838.91 35.3427 1 2 -2 9 1748.53 34.6615 5 -2 -2 9 1763.44 37.5151 3 2 2 10 120.367 6.73648 5 -2 -2 10 127.521 7.05847 3 -2 -2 10 133.999 5.85171 1 -2 2 10 116.942 7.59963 2 2 -2 10 131.196 4.64368 5 2 2 11 1831.08 41.3863 5 -2 -2 11 2004.98 39.1290 1 2 -2 11 1963.16 37.4188 5 -2 2 11 1923.04 43.5985 2 2 -2 12 266.966 6.95394 5 2 2 12 256.613 10.1921 5 -2 2 12 267.790 12.2829 2 -2 -2 12 268.639 9.12511 1 -2 -2 13 867.121 23.4122 2 2 2 13 826.480 21.9979 5 2 -2 13 875.673 17.6378 5 -2 -2 14 348.528 13.7446 2 2 -2 14 325.898 7.58363 5 2 2 14 321.562 11.9004 5 2 2 15 159.787 8.57471 5 -2 -2 15 172.236 10.3986 2 2 2 16 873.544 23.0183 5 -2 -2 16 943.252 26.3680 2 2 2 17 17.4146 5.32020 5 -2 -2 17 26.7643 7.58974 2 -2 -2 18 470.082 18.8580 2 2 2 18 436.814 14.5576 5 -2 -2 19 67.5441 10.1788 2 -2 -2 20 99.5883 11.8730 2 -2 -2 21 108.738 12.8515 2 -2 -2 22 8.36775 11.2051 2 -2 -2 23 50.6060 12.7853 2 -2 2 24 21.2508 13.2070 2 -2 -2 24 31.1990 13.1785 2 -2 -2 25 8.38107 13.5679 2 -2 2 25 13.4433 14.4765 2 -2 -2 26 7.28805 14.1393 2 2 -3 -25 24.3777 15.4666 1 2 -3 -24 21.6794 14.6678 1 2 -3 -23 28.7720 13.5163 1 2 -3 -22 80.0040 13.9647 1 -2 -3 -22 83.5244 13.8316 1 2 -3 -21 16.2140 12.2052 1 -2 -3 -21 9.08534 11.6638 1 2 -3 -20 27.7138 11.2184 1 -2 -3 -20 3.83227 10.2654 1 -2 -3 -19 31.4795 10.8108 1 2 -3 -19 54.2244 11.4747 1 2 -3 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652.895 16.0470 1 -2 3 -4 646.066 17.5426 5 2 -3 -4 647.709 17.6205 1 -2 3 -4 633.473 13.5872 2 -2 -3 -4 623.166 18.0724 5 -2 -3 -3 307.116 9.40177 1 -2 3 -3 301.113 11.0475 5 -2 -3 -3 330.206 11.9619 5 2 -3 -3 311.159 10.8795 1 2 -3 -2 694.023 17.9733 1 -2 -3 -2 665.581 15.9665 1 -2 -3 -2 704.581 19.1917 5 -2 3 -2 690.795 18.6812 5 2 -3 -1 761.010 18.6444 1 -2 3 -1 667.510 13.8107 3 -2 -3 -1 715.385 16.0856 1 -2 3 -1 736.461 19.3795 5 2 3 0 12890.9 236.188 4 2 -3 0 13032.1 236.169 4 -2 3 0 13501.2 242.374 5 -2 -3 0 13161.3 237.078 1 -2 3 0 12960.2 235.411 3 -2 3 1 699.892 19.9036 5 2 -3 1 721.078 15.6107 4 -2 3 1 695.714 15.2417 3 -2 -3 1 764.771 16.3917 1 2 3 1 717.676 16.7246 1 2 3 1 736.988 15.6707 4 2 3 2 698.340 16.1903 1 -2 -3 2 668.159 14.9094 1 -2 -3 2 673.589 14.8067 4 -2 3 2 667.635 14.8809 3 -2 3 2 646.828 14.8256 4 -2 3 3 299.543 8.50629 3 -2 3 3 292.569 8.26764 4 -2 -3 3 270.236 7.96186 4 2 3 3 287.659 9.35556 1 -2 -3 4 604.867 14.2853 4 -2 3 4 592.545 14.3195 4 2 3 4 599.708 15.3108 1 -2 -3 5 3953.25 74.6576 3 2 3 5 4026.76 76.8656 1 2 3 6 1193.67 27.1771 1 -2 -3 6 1206.99 25.1816 3 -2 -3 7 2518.85 48.9299 3 2 -3 7 2449.64 49.8814 5 -2 3 7 2497.00 51.1007 2 -2 -3 8 94.8321 4.45218 1 2 -3 8 86.7594 5.29878 5 -2 3 8 87.9555 6.70766 2 -2 -3 8 86.3505 5.37479 3 -2 -3 9 12.9084 3.89631 3 -2 -3 9 15.2410 3.26867 1 2 -3 9 14.5021 3.49834 5 -2 3 9 19.7669 4.97891 2 -2 -3 10 1027.14 21.6582 1 2 -3 10 977.965 22.6143 5 -2 3 10 1016.48 26.1450 2 -2 -3 11 383.923 10.6010 1 2 -3 11 363.733 10.8727 5 -2 3 11 347.600 14.0012 2 2 -3 12 1032.13 23.0811 5 -2 -3 12 1064.94 23.1875 1 -2 3 12 1005.07 27.2674 2 2 -3 13 38.7976 4.07992 5 -2 -3 13 42.9768 5.82423 2 -2 3 13 51.3023 7.80251 2 2 -3 14 92.7923 5.11928 5 -2 3 14 91.4160 9.58596 2 -2 -3 14 97.9294 8.37230 2 2 -3 15 280.102 8.63287 5 -2 -3 15 312.694 13.6031 2 -2 3 15 301.202 15.0687 2 -2 3 16 236.894 14.3761 2 2 -3 16 215.542 7.05273 5 -2 -3 16 213.147 11.6205 2 -2 -3 17 367.556 15.8533 2 -2 3 17 337.835 17.4356 2 -2 -3 18 19.0331 8.81815 2 -2 3 18 11.0079 9.77065 2 -2 -3 19 28.9079 8.95667 2 -2 3 19 21.3988 10.6424 2 -2 -3 20 22.7170 10.1090 2 -2 3 20 7.67715 10.9872 2 -2 3 21-1.73849 9.20885 5 -2 3 21 20.9886 12.0150 2 -2 -3 21 2.18528 10.3804 2 -2 3 22 64.7737 11.6267 5 -2 3 22 55.3064 13.8194 2 -2 -3 22 66.9460 12.5496 2 -2 3 23-4.08162 9.86276 5 -2 3 23 2.25249 13.6649 2 -2 -3 23 0.60916 11.7269 2 -2 3 24 14.1922 10.4955 5 -2 3 24 2.35150 14.1214 2 -2 -3 24 13.4786 12.9359 2 -2 -3 25-6.03901 13.7760 2 2 -4 -23 19.9489 15.1526 1 -2 -4 -23 20.6963 14.3330 1 -2 -4 -22 77.3609 14.4029 1 2 -4 -22 90.1655 15.2635 1 -2 -4 -21 2.65261 12.0140 1 2 -4 -21 21.3904 13.2962 1 -2 -4 -20 109.225 14.0752 1 2 -4 -20 104.117 14.4244 1 2 -4 -19 38.7051 11.8199 1 -2 -4 -19 60.2821 12.5483 1 -2 -4 -18 125.289 13.1609 1 -2 -4 -17 69.9034 11.3864 1 -2 -4 -16 283.034 15.7654 1 -2 -4 -15 257.525 13.9430 1 -2 -4 -14 371.317 16.0744 1 -2 -4 -13 157.733 10.9597 1 2 -4 -13 174.388 11.8768 1 -2 4 -12 1101.51 25.4778 3 2 -4 -12 1066.18 29.3966 1 -2 -4 -12 1008.08 27.7271 1 -2 -4 -11 7.99248 6.46979 1 2 -4 -11 11.4945 6.84999 1 -2 4 -11 3.08139 4.85312 3 -2 -4 -10 1340.88 32.9152 1 2 -4 -10 1358.80 34.1473 1 -2 4 -10 1429.04 29.9559 3 -2 4 -9 258.090 8.94091 3 -2 -4 -9 270.644 11.4928 1 2 -4 -9 275.252 12.6492 1 -2 -4 -8 2516.08 54.1313 1 2 -4 -8 2548.26 55.8945 1 -2 4 -8 2663.56 50.3183 3 2 -4 -7 735.176 18.9849 3 2 -4 -7 719.160 21.3394 1 -2 -4 -7 727.830 19.9443 1 -2 4 -7 751.780 16.1819 3 -2 -4 -6 1138.78 27.1854 1 2 -4 -6 1118.74 28.6788 1 2 -4 -6 1184.79 25.9445 3 -2 -4 -6 1136.40 27.0201 2 -2 4 -6 1158.63 22.8670 3 2 -4 -5 1590.22 37.2195 1 -2 4 -5 1597.29 30.6954 3 2 -4 -5 1693.51 34.0327 3 -2 -4 -5 1679.88 35.4426 2 -2 -4 -5 1719.08 35.9784 1 -2 -4 -4 1042.82 24.3839 2 -2 -4 -4 1049.57 24.8246 1 2 -4 -4 1111.00 27.4885 1 -2 -4 -3 385.773 11.9213 1 -2 -4 -3 377.053 11.4879 2 -2 4 -3 392.092 14.5451 5 2 -4 -3 420.578 14.2197 1 -2 -4 -2 1976.17 41.5280 1 -2 4 -2 2071.39 45.7725 5 2 -4 -2 2017.82 43.8925 1 2 -4 -1 293.537 11.8630 1 -2 -4 -1 311.516 10.1681 1 -2 4 -1 304.148 12.9924 5 -2 4 0 9924.56 185.163 5 -2 -4 0 9972.41 179.350 1 -2 4 0 9595.88 175.969 2 -2 -4 1 318.818 10.0027 1 2 -4 1 299.075 7.49126 4 2 4 1 292.692 7.60701 4 -2 4 1 305.398 13.2895 5 -2 4 1 290.511 7.79409 2 2 4 2 1936.85 37.8391 4 -2 4 2 1971.87 38.4352 2 -2 -4 2 1986.49 39.8065 1 2 4 2 2027.67 40.8935 1 2 -4 2 1909.74 37.6810 4 -2 4 3 383.759 9.92856 4 2 4 3 388.338 12.3562 1 -2 4 3 380.550 10.6435 2 -2 -4 3 382.461 11.0642 1 -2 -4 3 372.225 9.66035 4 -2 4 4 1004.18 21.5413 4 2 4 4 948.092 23.6454 1 -2 4 4 1013.41 22.6644 2 -2 -4 4 999.805 21.2405 4 -2 4 5 1581.55 33.5933 2 -2 -4 5 1564.73 32.0156 4 -2 -4 5 1541.84 31.0758 3 -2 4 5 1584.86 32.2948 4 -2 -4 6 1063.63 22.1488 3 -2 4 6 1014.09 24.4472 2 -2 -4 7 668.683 15.5755 3 2 -4 7 683.517 18.4967 5 -2 4 7 614.577 17.4618 2 -2 -4 8 2468.18 48.2413 3 2 -4 8 2398.04 50.7271 5 -2 4 8 2504.99 57.5894 5 -2 4 8 2414.14 51.5109 2 2 -4 9 220.728 9.81205 5 -2 -4 9 261.627 8.30324 1 -2 4 9 242.340 11.3302 2 -2 4 9 244.998 14.3985 5 -2 4 10 1313.52 32.3042 2 2 -4 10 1247.03 29.6763 5 -2 -4 10 1310.89 27.2272 1 -2 4 10 1337.72 37.1294 5 -2 4 11 1.78499 7.90932 5 -2 -4 11 9.33858 4.50027 1 -2 4 11 3.10954 5.90166 2 2 -4 11 5.98754 4.53581 5 -2 -4 11 11.6566 4.87451 2 2 -4 12 898.862 22.7608 5 -2 4 12 978.175 30.8006 5 -2 -4 12 946.232 23.5980 2 -2 4 12 952.630 26.9986 2 -2 4 13 141.467 12.6772 5 2 -4 13 143.305 7.75525 5 -2 4 13 132.818 10.9950 2 -2 -4 13 161.336 9.21844 2 -2 4 14 323.336 17.7175 5 2 -4 14 310.634 10.8795 5 -2 4 14 317.359 15.7471 2 -2 -4 14 299.325 12.6630 2 2 -4 15 231.110 9.27408 5 -2 4 15 238.578 14.8116 2 -2 -4 15 232.900 11.4317 2 -2 4 15 237.718 16.1321 5 -2 4 16 228.143 15.0709 2 -2 -4 16 270.845 13.0817 2 -2 4 16 231.983 16.1264 5 -2 -4 17 67.4846 8.97390 2 -2 4 17 60.4342 11.4509 2 -2 4 17 65.5171 11.4620 5 -2 4 18 120.456 13.5702 2 -2 -4 18 99.7961 10.7525 2 -2 4 18 100.982 13.5633 5 -2 -4 19 41.9602 10.1579 2 -2 4 19 49.9713 12.5058 2 -2 4 19 51.6663 11.6046 5 -2 4 20 84.5907 13.8475 5 -2 4 20 76.4772 13.9657 2 -2 -4 20 102.625 12.3794 2 -2 4 21 4.09462 11.0486 5 -2 4 21-2.85689 12.5386 2 -2 -4 21 9.38543 10.6926 2 -2 -4 22 79.9582 13.2427 2 -2 4 22 44.3976 12.2488 5 -2 4 22 44.6490 14.3794 2 -2 4 23 8.61210 10.6075 5 -2 -4 23 6.39715 11.8446 2 -2 4 24 34.5057 12.5725 5 -2 -5 -22 15.3259 15.1631 1 -2 -5 -21 15.1046 13.9807 1 -2 -5 -20 19.1228 13.5034 1 -2 -5 -19 41.6226 12.6981 1 -2 -5 -18 7.46601 11.9735 1 -2 -5 -17 106.056 12.9809 1 2 -5 -17 96.5162 13.7955 1 -2 -5 -16 41.7687 11.2860 1 2 -5 -16 29.7856 11.0543 1 2 -5 -15 81.2706 11.9721 1 -2 -5 -15 98.3498 11.0289 1 2 -5 -14 90.0963 11.6168 1 -2 -5 -14 89.5007 10.6119 1 -2 -5 -13-2.87830 8.36488 1 2 -5 -13 14.7344 8.86113 1 -2 5 -12 288.733 10.6012 3 2 -5 -12 242.147 14.0848 1 -2 -5 -12 248.103 13.3963 1 -2 -5 -11-0.37559 7.55104 1 -2 5 -11 0.88311 5.00689 3 2 -5 -11 4.53981 7.79405 1 -2 5 -10 193.074 7.48666 3 -2 -5 -10 158.081 10.5975 1 2 -5 -10 154.718 11.6859 1 2 -5 -9 13.2109 7.24859 1 -2 5 -9 15.3263 3.61474 3 -2 -5 -9 7.87755 6.61495 1 2 -5 -8 28.7101 7.26857 1 -2 -5 -8 48.2970 7.36619 1 2 -5 -7 641.567 20.8900 1 -2 -5 -7 616.997 18.9137 1 2 -5 -6 60.7713 7.95798 1 2 -5 -6 64.9098 6.01385 3 -2 -5 -6 62.7148 7.08904 1 2 -5 -5 1161.31 30.8095 1 -2 -5 -5 1202.30 27.6042 2 -2 -5 -5 1199.52 29.0002 1 2 -5 -4 28.8584 6.84896 1 -2 -5 -4 27.7135 5.12778 2 -2 -5 -4 26.8131 5.55311 1 -2 -5 -3 259.337 10.4718 1 2 -5 -3 226.077 11.7716 1 -2 -5 -3 241.778 9.09813 2 -2 -5 -2 92.4542 5.70244 2 2 -5 -2 103.961 8.58886 1 -2 -5 -2 106.325 6.94459 1 -2 5 -1 27.0512 7.53319 5 -2 -5 -1 18.2448 3.96506 2 2 -5 -1 14.9156 6.18051 1 -2 -5 -1 8.40476 4.68020 1 2 -5 0 2352.87 50.9380 1 -2 -5 0 2289.70 47.9469 1 -2 5 0 2333.28 54.2909 5 -2 5 1 9.21013 6.79220 5 -2 -5 1 26.7213 5.04199 1 -2 5 2 94.2444 9.29556 5 2 5 2 98.4228 3.48673 4 -2 -5 2 100.582 6.70612 1 -2 5 3 249.235 8.35498 2 2 -5 3 233.525 6.41556 4 -2 5 3 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2 -3 -2 21 11.8494 10.3160 2 -3 -2 22 64.8212 12.3743 2 -3 -2 23 4.39927 11.7812 2 -3 -2 24 17.8672 12.8581 2 -3 2 25-8.55218 14.2520 2 -3 -2 25 13.8121 13.4318 2 -3 -2 26-0.71574 13.7249 2 3 -3 -25 29.5127 15.7524 1 -3 -3 -24 29.8561 14.5445 1 3 -3 -24 44.5034 14.9876 1 3 -3 -23 43.9113 14.3102 1 -3 -3 -23 14.3649 14.1264 1 -3 -3 -22 35.4327 13.4490 1 3 -3 -22 40.0514 13.4542 1 -3 -3 -21 50.8073 12.6312 1 3 -3 -21 56.9606 12.6426 1 3 -3 -20 141.559 13.6913 1 -3 -3 -20 130.053 13.7822 1 3 -3 -19 141.251 13.1501 1 -3 -3 -19 132.748 12.8940 1 3 -3 -18 130.324 12.1431 1 -3 -3 -18 143.071 12.9098 1 -3 -3 -17 243.863 14.3893 1 3 -3 -17 219.654 13.7850 1 3 -3 -16 183.770 12.6643 1 -3 -3 -16 180.194 12.0775 1 -3 -3 -15 460.063 17.4842 1 3 -3 -15 465.057 18.0497 1 -3 -3 -14 577.023 19.1731 1 3 -3 -14 557.308 19.6667 1 3 -3 -13 156.886 10.3087 1 -3 -3 -13 165.430 10.3325 1 -3 -3 -12 492.327 16.7537 1 3 -3 -12 497.605 17.5671 1 -3 -3 -11 263.261 11.8037 1 -3 3 -11 238.967 9.94714 2 -3 -3 -10 912.630 22.7511 1 -3 3 -10 797.074 20.3033 2 -3 -3 -9 1485.18 34.2967 1 -3 3 -9 1601.42 33.4821 2 -3 -3 -8 1188.02 27.3595 1 -3 3 -8 1169.87 26.0990 2 -3 -3 -7 2837.21 56.4505 1 -3 3 -7 2800.83 55.1537 2 -3 3 -6 2486.98 50.8099 5 -3 -3 -6 2481.84 49.9145 1 -3 -3 -5 1073.20 24.1328 1 -3 3 -5 1068.34 25.5996 5 -3 -3 -5 1098.94 27.1136 5 3 -3 -5 1098.10 26.7864 1 -3 3 -4 2627.99 53.9772 5 -3 -3 -4 2591.94 51.4921 1 -3 -3 -4 2710.59 55.2899 5 3 -3 -4 2602.04 54.3001 1 -3 -3 -3 2144.19 42.8569 1 3 -3 -3 2207.62 45.9708 1 -3 3 -3 2183.71 46.1374 5 -3 -3 -2 1517.85 30.7605 1 3 -3 -2 1515.07 34.0457 1 -3 3 -2 1512.86 34.4125 5 3 3 -1 1943.02 39.0089 4 3 -3 -1 1965.53 39.0294 4 -3 -3 -1 1997.54 38.3526 1 -3 3 -1 1860.33 42.4992 5 3 3 0 2935.35 54.8535 1 -3 -3 0 2884.38 54.4021 1 3 3 0 2830.11 55.5393 4 3 -3 0 2837.35 55.5361 4 3 -3 1 1927.65 38.8702 4 3 3 1 1940.82 38.8251 4 -3 -3 1 1954.11 37.2666 1 -3 3 1 1888.82 37.7351 3 3 3 1 1989.72 38.4764 1 -3 3 2 1473.88 30.1481 4 -3 -3 2 1425.46 28.2120 1 -3 3 2 1452.88 29.5010 3 -3 -3 2 1474.11 30.1264 4 3 3 2 1461.34 29.9808 1 3 -3 2 1430.04 30.2371 4 -3 -3 3 2184.67 42.4399 4 -3 3 3 2090.22 41.9359 3 -3 3 3 2176.03 42.5500 4 -3 -3 3 2100.71 40.1101 1 3 3 3 2062.47 42.1412 1 -3 3 4 2566.66 49.6484 4 3 3 4 2492.04 49.5687 1 -3 3 4 2538.93 49.4885 3 -3 -3 4 2507.27 49.3296 4 -3 -3 4 2435.16 46.9694 1 -3 3 5 1023.17 23.2462 4 3 3 5 986.256 23.3546 1 -3 3 5 1035.00 23.4599 3 -3 -3 5 1036.34 23.2809 4 -3 -3 6 2419.74 44.3391 1 3 3 6 2346.24 48.4060 1 -3 3 6 2333.43 48.3712 3 -3 -3 6 2337.78 47.0553 3 -3 -3 6 2313.87 47.8722 4 -3 3 7 2651.19 54.2751 3 -3 -3 7 2687.06 52.8735 3 -3 -3 7 2667.53 49.8919 1 -3 -3 8 1130.25 22.3783 1 -3 -3 8 1077.02 25.0495 3 -3 -3 9 1465.16 32.1161 3 -3 -3 9 1471.51 29.1465 1 -3 -3 10 836.928 21.2726 3 -3 -3 10 862.804 18.5427 1 -3 -3 11 232.689 10.1420 3 -3 3 11 221.456 11.3006 2 -3 -3 11 240.989 7.95014 1 -3 -3 12 469.765 12.0830 1 -3 -3 12 417.829 14.4701 3 -3 3 12 422.879 16.2930 2 -3 -3 13 144.326 6.89540 1 -3 3 13 144.815 10.4743 2 -3 3 14 485.701 18.4660 2 -3 3 15 393.771 17.1105 2 -3 -3 15 377.494 15.0087 2 -3 3 16 157.791 11.5951 2 -3 -3 16 175.324 11.4623 2 -3 3 17 230.872 14.6512 2 -3 -3 17 221.008 13.0359 2 -3 3 18 118.270 12.5724 2 -3 -3 18 118.203 10.8499 2 -3 3 19 137.648 13.9961 2 -3 -3 19 106.446 10.8793 2 -3 -3 20 114.446 12.4068 2 -3 3 20 115.035 14.1939 2 -3 3 21 33.7441 12.4414 2 -3 -3 21 38.6216 10.9687 2 -3 -3 22 22.3987 11.6662 2 -3 3 22 33.9156 13.1816 2 -3 3 23-2.20361 13.2526 2 -3 -3 23 19.3808 11.7356 2 -3 3 24 34.9404 15.2786 2 -3 -3 24 32.9867 13.2067 2 -3 3 24 10.6645 10.8305 5 -3 -3 25 1.97544 13.3481 2 -3 -3 26 23.6493 13.7393 2 3 -4 -23 9.87885 14.9080 1 -3 -4 -23 23.0238 15.0731 1 -3 -4 -22 23.8165 13.6299 1 3 -4 -22 28.7994 14.4967 1 -3 -4 -21 12.2075 12.6647 1 3 -4 -21-1.13472 12.4436 1 -3 -4 -20 25.4161 12.0512 1 3 -4 -20 10.4318 12.5403 1 -3 -4 -19 71.5019 12.4548 1 3 -4 -19 57.5572 12.6421 1 3 -4 -18 161.480 14.1779 1 -3 -4 -18 191.038 14.6358 1 3 -4 -17 87.6824 12.0975 1 -3 -4 -17 124.751 12.6207 1 3 -4 -16 191.756 14.2773 1 -3 -4 -16 238.396 14.2053 1 -3 -4 -15 54.9363 10.3902 1 -3 -4 -14 66.6949 9.59661 1 -3 -4 -13 97.8015 9.70010 1 -3 -4 -12 376.403 15.1462 1 -3 -4 -11 21.5437 6.83332 1 -3 -4 -10 366.665 13.7884 1 3 -4 -9 64.6113 8.02841 1 -3 -4 -9 70.2767 7.24791 1 -3 4 -9 74.2051 5.36393 2 3 -4 -8 243.124 11.9857 1 -3 -4 -8 232.415 10.1322 1 -3 4 -8 227.527 8.05964 2 -3 -4 -7 611.003 16.9946 1 -3 4 -7 560.379 13.7541 2 3 -4 -7 603.298 19.1457 1 3 -4 -6 3221.67 67.1845 1 -3 -4 -6 3222.92 64.2625 1 -3 4 -6 3227.79 60.9824 2 -3 4 -5 1703.28 39.2422 5 -3 -4 -5 1743.67 36.4919 1 3 -4 -5 1735.71 39.9298 1 -3 4 -5 1678.32 33.2056 2 -3 -4 -4 1369.31 29.8278 1 3 -4 -4 1319.12 32.7981 1 -3 4 -4 1380.44 33.3221 5 3 -4 -3 9.95728 5.09492 1 -3 -4 -3 16.2564 4.08585 1 -3 4 -3 7.63790 4.77276 5 -3 4 -2 70.1124 7.22306 5 -3 -4 -2 89.2508 5.34941 1 3 -4 -2 76.3537 7.11082 1 -3 4 -1 43.0279 6.20845 5 3 -4 -1 46.5682 6.46488 1 -3 4 -1 50.6578 3.06029 3 -3 -4 -1 52.0960 4.46984 1 3 4 0 2090.35 41.8443 4 -3 -4 0 2213.13 42.4731 1 -3 4 0 2125.42 40.7348 3 3 -4 0 2052.30 41.5671 4 -3 4 0 2200.61 48.8257 5 3 -4 1 55.2465 4.01521 4 -3 4 1 46.7149 6.92953 5 -3 4 1 49.1608 3.67792 3 3 4 1 53.2859 3.94913 4 -3 -4 1 48.8072 4.00078 1 3 -4 2 81.8331 4.78098 4 3 4 2 72.3512 4.59948 4 -3 4 2 76.7353 4.68660 3 -3 -4 2 70.4577 4.25077 1 3 4 2 78.5650 5.42998 1 -3 4 2 76.6611 7.99802 5 -3 -4 3 12.0376 3.27942 4 -3 4 3 8.14443 3.30575 4 -3 4 3 9.48796 3.55990 3 3 -4 3 10.8508 3.34918 4 -3 -4 3 9.17439 2.94967 1 3 4 3 11.2032 4.38256 1 -3 4 4 1344.19 28.4760 4 -3 -4 4 1297.57 28.0475 4 -3 -4 4 1308.53 27.1896 1 3 4 4 1328.92 29.7221 1 -3 4 5 1671.55 34.5400 4 -3 -4 5 1641.27 33.0281 1 -3 -4 5 1605.34 34.1305 4 -3 -4 6 3034.42 59.6820 4 -3 -4 6 2974.04 58.5895 3 -3 4 6 3103.29 60.0989 4 -3 -4 7 555.781 15.2113 4 -3 -4 7 551.412 14.4319 3 -3 4 7 571.392 15.8038 4 -3 -4 8 224.593 8.53104 3 -3 -4 8 227.311 6.98633 1 -3 4 8 216.258 10.2218 2 -3 -4 9 77.6064 4.44448 1 -3 -4 9 57.2427 5.61376 3 -3 4 9 71.4329 7.13423 2 -3 -4 10 322.545 9.17281 1 -3 4 10 324.911 13.5282 2 -3 -4 10 327.575 11.4141 3 -3 4 11 24.5031 6.85638 2 -3 -4 11 21.0288 4.12563 1 -3 -4 11 19.8576 5.60703 3 -3 -4 12 340.230 10.2101 1 -3 4 12 332.469 14.7416 2 -3 4 13 72.7123 8.64155 2 -3 -4 14 55.7742 7.58863 2 -3 4 14 70.0491 9.50336 2 -3 4 15 42.6551 9.97412 2 -3 -4 15 34.9316 7.42973 2 -3 4 16 213.275 14.6845 2 -3 -4 16 202.425 12.1224 2 -3 4 17 86.8965 12.2226 2 -3 -4 17 81.0585 9.69609 2 -3 4 18 149.387 14.1002 2 -3 -4 18 139.329 10.7077 2 -3 4 19 47.0572 12.8101 5 -3 4 19 48.6047 12.3677 2 -3 -4 19 37.5151 9.94166 2 -3 4 20-0.66890 11.5954 2 -3 -4 20 0.98161 9.48507 2 -3 4 20 2.19257 10.7179 5 -3 4 21 12.4074 11.1490 5 -3 -4 21 11.9592 10.0886 2 -3 4 21 1.39469 11.9733 2 -3 4 22 9.47942 12.0846 5 -3 4 22 8.10698 13.3951 2 -3 -4 22 14.3154 11.6351 2 -3 4 23 4.43116 12.4503 5 -3 4 23-20.1048 14.1548 2 -3 -4 23-4.00920 11.9448 2 -3 4 24 18.1187 12.7523 5 3 -5 -21 64.2094 15.6328 1 -3 -5 -21 46.7481 14.3989 1 3 -5 -20 44.9023 14.0440 1 -3 -5 -20 58.0149 14.4811 1 3 -5 -19 21.7954 13.2386 1 -3 -5 -19 36.7349 12.4657 1 -3 -5 -18 46.2077 12.3606 1 -3 -5 -17 24.9112 11.3215 1 -3 -5 -16 16.9264 10.9133 1 -3 -5 -15 41.9942 10.2137 1 -3 -5 -14 218.682 13.8650 1 3 -5 -14 204.776 14.5151 1 -3 -5 -13 242.122 13.8918 1 3 -5 -13 289.004 15.6236 1 -3 5 -12 430.283 13.5038 3 -3 -5 -12 394.796 16.4527 1 3 -5 -12 418.696 18.5394 1 3 -5 -11 885.207 27.4702 1 -3 -5 -11 882.151 25.4571 1 -3 5 -11 965.644 21.9690 3 -3 5 -10 454.218 12.3400 3 -3 -5 -10 395.762 15.7704 1 3 -5 -10 417.632 17.8028 1 -3 -5 -9 957.260 25.9643 1 3 -5 -9 941.555 28.1318 1 -3 5 -9 1012.68 21.4938 3 3 -5 -8 237.535 13.1928 1 -3 5 -8 243.028 7.42264 3 -3 -5 -8 234.158 11.3001 1 3 -5 -7 115.898 10.3847 1 -3 -5 -7 133.303 8.77159 1 -3 5 -7 135.046 4.73916 3 3 -5 -6 248.581 12.7505 1 -3 -5 -6 245.407 10.9722 1 3 -5 -5 87.0228 8.94671 1 -3 -5 -5 98.0418 7.26449 1 -3 -5 -4 464.728 14.5976 1 -3 -5 -4 442.359 14.4477 2 3 -5 -4 472.728 17.3556 1 -3 5 -4 489.143 17.9630 5 -3 5 -3 279.581 13.8268 5 -3 -5 -3 263.048 10.0957 1 3 -5 -3 252.688 12.5814 1 -3 5 -2 454.970 18.1734 5 3 -5 -2 477.872 17.5219 1 -3 -5 -2 476.789 14.1486 1 3 -5 -1 2949.04 57.1021 1 -3 5 -1 2887.81 59.1663 5 -3 -5 -1 2833.15 51.7914 1 -3 5 0 1775.86 35.1809 2 3 -5 0 1940.28 43.4915 1 -3 -5 0 1916.43 38.8006 1 -3 5 0 1921.40 45.9271 5 -3 -5 1 2952.79 56.8386 1 -3 5 1 2809.64 64.1116 5 -3 5 1 2812.97 54.3783 2 3 5 2 458.368 11.6343 4 3 -5 2 447.237 11.3451 4 -3 -5 2 468.427 13.1157 1 -3 5 2 452.444 12.0099 2 -3 5 2 478.566 19.4004 5 3 5 3 266.257 8.58927 4 -3 -5 3 259.002 9.30788 1 3 -5 3 247.716 8.15030 4 -3 5 3 281.434 9.26428 2 -3 5 3 301.518 15.6528 5 -3 -5 4 411.739 11.4375 4 -3 5 4 440.629 19.1583 5 3 -5 4 435.188 11.8647 4 -3 5 4 446.775 13.0265 2 -3 -5 4 432.868 12.4791 1 -3 5 4 437.659 11.9836 4 3 5 4 426.858 11.9590 4 -3 5 5 93.8418 5.96968 4 -3 -5 5 84.8703 5.42920 4 -3 -5 5 80.2901 4.72984 3 -3 -5 5 86.5212 5.70344 1 -3 5 5 82.1303 6.51591 2 -3 5 5 87.9037 10.3711 5 -3 -5 6 225.374 8.59268 4 -3 -5 6 230.846 7.89536 3 -3 -5 6 238.807 8.79024 1 -3 5 6 237.850 9.10277 4 -3 5 6 240.587 10.1070 2 -3 5 6 262.840 16.0502 5 -3 5 7 116.438 7.25491 4 -3 -5 7 126.154 6.14699 3 -3 -5 7 117.341 6.73766 4 -3 5 7 111.504 7.69834 2 -3 5 8 217.128 9.49431 4 -3 -5 8 199.211 8.93587 4 -3 -5 8 212.351 8.14967 3 -3 5 8 224.213 10.8065 2 -3 -5 9 862.301 20.9643 3 -3 5 9 945.268 24.9952 2 -3 5 10 400.565 21.4554 5 -3 5 10 452.800 17.0124 2 -3 5 11 849.477 32.2238 5 -3 5 11 904.488 26.3881 2 -3 5 12 362.739 21.4175 5 -3 5 12 386.176 16.9138 2 -3 -5 13 244.172 11.1861 2 -3 5 13 229.232 14.2954 2 -3 5 13 261.348 18.9491 5 -3 5 14 225.360 18.0743 5 -3 5 14 205.295 14.0085 2 -3 -5 14 191.757 10.5828 2 -3 5 15 39.5828 12.9927 5 -3 5 15 23.0702 9.70480 2 -3 -5 15 34.6360 7.41385 2 -3 5 16-6.93762 12.0469 5 -3 5 16 3.47881 10.0670 2 -3 -5 16 4.17412 6.40152 2 -3 5 17-7.92917 12.3300 5 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14.1430 2 -5 -4 22 31.7893 10.9787 2 -5 -4 23 0.56208 10.8205 2 -5 4 25-1.63023 13.1237 5 -5 -5 -21 12.6974 14.4440 1 5 -5 -21-11.2563 14.6290 1 5 -5 -20 40.3509 14.5316 1 -5 -5 -20 63.8717 14.4847 1 5 -5 -19-1.79414 13.2485 1 -5 -5 -19 29.2515 13.2528 1 5 -5 -18 13.6416 13.0744 1 -5 -5 -18 55.6639 13.1836 1 -5 -5 -17 127.931 13.6518 1 5 -5 -17 142.239 14.4663 1 5 -5 -16 48.3955 12.3327 1 -5 -5 -16 25.4095 10.8101 1 -5 -5 -15 61.6455 11.0838 1 5 -5 -15 83.4132 12.6789 1 -5 -5 -14 218.055 13.8215 1 5 -5 -14 199.699 14.8473 1 -5 -5 -13 24.5007 9.36277 1 5 -5 -13 10.6376 9.75518 1 -5 -5 -12 536.588 18.9759 1 -5 -5 -11 81.4609 9.77476 1 -5 -5 -10 570.407 17.9949 1 -5 5 -10 472.648 14.0593 2 -5 -5 -9 4.08691 6.92983 1 -5 5 -9 5.89752 4.63874 2 -5 -5 -8 411.116 14.4316 1 -5 5 -8 372.413 11.5338 2 -5 -5 -7 326.419 12.0628 1 5 -5 -7 267.963 14.5911 1 -5 5 -7 283.986 9.58029 2 -5 5 -7 320.836 14.2635 5 -5 -5 -6 352.151 12.4866 1 5 -5 -6 387.781 17.6220 1 -5 -5 -5 451.666 13.8683 1 5 -5 -5 425.584 17.8162 1 -5 5 -5 444.496 17.2543 5 -5 -5 -4 465.490 13.9142 1 5 -5 -4 490.885 18.7276 1 -5 5 -4 456.441 17.9080 5 5 -5 -3 166.980 11.8613 1 -5 -5 -3 165.674 7.73031 1 -5 5 -3 152.198 11.4608 5 -5 -5 -2 922.048 21.1283 1 5 -5 -2 855.948 27.2809 1 -5 -5 -1 215.222 8.06207 1 -5 5 -1 229.869 8.00560 3 5 -5 -1 228.391 13.2145 1 -5 5 -1 218.934 13.5867 5 5 -5 0 1807.10 38.3125 4 5 5 0 1853.72 38.8257 4 -5 5 0 1797.61 36.9560 3 -5 -5 0 1782.65 36.3820 1 -5 5 0 1919.99 47.2741 5 5 -5 1 213.347 9.18707 4 5 5 1 244.048 10.0663 4 -5 5 1 224.061 8.65495 3 -5 -5 1 219.418 7.48568 1 -5 5 1 239.113 14.8326 5 5 5 2 912.729 22.8874 4 5 -5 2 903.119 22.6541 4 -5 5 2 945.570 21.9776 3 -5 -5 2 882.658 19.5626 1 5 5 2 1007.97 22.5858 1 -5 5 2 909.184 30.4693 5 5 5 3 162.892 8.59782 4 5 -5 3 169.739 8.67743 4 -5 5 3 170.485 8.23563 3 -5 -5 3 163.352 5.68280 1 -5 5 3 167.705 13.6326 5 5 5 4 449.917 14.4977 4 5 -5 4 427.635 14.2311 4 -5 5 4 444.159 14.0281 3 -5 -5 4 452.262 10.6043 1 -5 5 4 496.199 22.5651 5 -5 5 5 438.091 14.0579 4 5 -5 5 425.709 14.1724 4 -5 -5 5 400.674 13.3357 4 5 5 5 423.063 14.2246 4 -5 5 5 447.444 14.2600 3 -5 -5 5 396.912 9.62102 1 -5 5 6 338.518 12.7467 3 -5 -5 6 305.201 7.64583 1 -5 -5 7 287.307 10.7447 3 -5 -5 8 384.539 12.7592 3 -5 -5 9 7.64491 5.52776 3 -5 -5 10 479.628 15.2101 3 -5 -5 11 60.4203 7.53075 3 -5 5 11 75.6719 9.85801 2 -5 -5 12 439.698 15.6382 3 -5 5 12 482.694 19.0132 2 -5 5 13 10.2009 9.09451 2 -5 -5 13 7.50686 7.02398 3 -5 -5 14 183.340 11.2283 3 -5 5 14 172.695 13.6185 2 -5 5 15 47.3262 10.9993 2 -5 5 16 20.6160 10.0817 2 -5 5 17 95.1383 13.1711 2 -5 5 18 22.7506 11.8372 2 -5 5 19 16.3154 15.0542 5 -5 5 19-0.66202 12.4610 2 -5 5 20 50.0493 14.3365 2 -5 5 20 60.3438 16.8964 5 -5 5 21 10.8971 13.2414 2 -5 5 21 3.92146 15.0057 5 -5 5 22 31.8869 16.2441 5 -5 5 23 6.66108 15.2074 5 -5 -6 -19 14.7001 13.8058 1 5 -6 -18-9.03856 15.4567 1 -5 -6 -18 15.1008 13.1144 1 5 -6 -17 46.9898 13.7854 1 -5 -6 -17 20.8796 12.7002 1 -5 -6 -16-6.20689 12.2982 1 -5 -6 -15 83.7392 12.6516 1 -5 -6 -14 35.1430 11.3567 1 -5 -6 -13 50.9281 10.7624 1 -5 -6 -12 32.5248 10.1261 1 -5 -6 -11 64.1139 10.1520 1 5 -6 -11 49.6203 12.3390 1 5 -6 -10 9.66469 10.1833 1 -5 -6 -10 16.2284 8.33575 1 -5 -6 -9 121.856 10.0634 1 5 -6 -9 95.7254 12.3852 1 5 -6 -8 3.88551 10.0459 1 -5 -6 -8 17.4636 7.57483 1 -5 -6 -7 211.072 11.0816 1 5 -6 -7 221.514 14.8774 1 5 -6 -6 13.3461 9.29599 1 -5 6 -6 7.47460 2.81926 3 -5 -6 -6 7.47339 6.75460 1 -5 -6 -5 190.415 9.99694 1 -5 6 -5 168.068 5.21758 3 5 -6 -5 216.377 14.2755 1 -5 6 -5 206.706 13.4238 5 -5 6 -4 16.1991 8.46282 5 -5 -6 -4 6.48692 5.77315 1 -5 6 -4 7.04272 2.86603 3 5 -6 -4 18.9786 10.0400 1 5 -6 -3 124.974 12.2092 1 -5 6 -3 107.846 4.82871 3 -5 -6 -3 114.756 7.74742 1 -5 6 -3 109.703 11.5126 5 -5 -6 -2 25.1206 5.66432 1 5 -6 -2 16.8425 9.20474 1 -5 6 -2 23.5538 8.90959 5 -5 6 -2 20.5564 3.87085 3 5 -6 -1 194.899 13.7086 1 -5 -6 -1 184.924 8.51050 1 -5 6 -1 199.320 14.1166 5 -5 6 0 19.9651 9.72177 5 5 -6 0 17.1959 9.05488 1 -5 -6 0 21.4866 5.07534 1 -5 -6 1 182.529 7.74672 1 -5 6 1 181.589 14.7221 5 5 -6 2 16.7573 4.46073 4 5 6 2 19.1937 5.04404 4 -5 -6 2 28.7135 4.56498 1 -5 6 2 29.3182 10.2575 5 5 6 3 111.490 7.21930 4 -5 6 3 128.337 13.9534 5 -5 6 4-2.44370 10.3454 5 5 6 4 6.04893 5.26456 4 5 6 5 192.723 9.61728 4 -5 6 5 202.400 10.3956 2 -5 6 5 214.903 18.0227 5 -5 6 6-0.95919 12.3980 5 5 6 6 2.99443 5.85093 4 -5 6 6 11.4125 6.84586 2 -5 -6 6 6.83179 4.99961 3 -5 6 7 204.996 11.5512 2 -5 6 7 230.231 20.3626 5 -5 6 8 12.4439 13.8216 5 -5 6 8 10.3604 7.72613 2 -5 6 9 121.359 17.9325 5 -5 6 9 103.960 10.2342 2 -5 6 10-0.43387 8.44908 2 -5 6 11 33.2926 9.01311 2 -5 6 12 14.1893 15.5024 5 -5 6 12 10.7669 9.18763 2 -5 6 13 30.2867 11.4046 2 -5 6 13 19.2652 16.1405 5 -5 6 14 23.0172 11.1298 2 -5 6 14 9.73472 17.0329 5 -5 6 15 55.1042 18.6070 5 -5 6 15 43.5673 12.0197 2 -5 6 16 30.9694 12.0278 2 -5 6 16 26.8726 18.2377 5 -5 6 17 22.0586 17.3634 5 -5 6 17 20.2084 13.2351 2 -5 6 18-6.12222 17.5921 5 -5 6 18-3.40958 13.3636 2 -5 6 19 12.7339 13.5863 2 -5 6 19 20.8228 18.4786 5 -5 6 20 11.6833 18.5652 5 -5 6 20-3.65318 13.8265 2 -5 -7 -17 22.5098 14.5677 1 -5 -7 -16 36.0125 13.3513 1 5 -7 -15 35.1957 14.4835 1 -5 -7 -15 36.3105 12.4893 1 -5 -7 -14 103.822 13.7342 1 5 -7 -14 66.1321 15.0275 1 -5 -7 -13 23.0585 11.7160 1 5 -7 -13-0.66188 12.9725 1 -5 -7 -12 155.403 13.3239 1 5 -7 -12 163.808 16.0770 1 5 -7 -11 34.5680 13.5575 1 -5 -7 -11 37.4826 10.8131 1 5 -7 -10 174.630 16.0479 1 -5 -7 -10 176.033 12.8838 1 5 -7 -9 5.72892 12.1606 1 -5 -7 -9 16.8279 9.10639 1 -5 -7 -8 129.532 10.6596 1 5 -7 -8 112.697 14.1901 1 5 -7 -7 153.644 14.6774 1 -5 -7 -7 159.314 10.6508 1 5 -7 -6 97.8462 12.9294 1 -5 -7 -6 80.1812 8.86491 1 -5 -7 -5 226.302 11.5948 1 5 -7 -5 245.159 17.0536 1 -5 -7 -4 148.876 9.82740 1 5 -7 -4 155.791 14.3771 1 -5 7 -3 44.5799 10.9284 5 -5 -7 -3 32.0905 7.12512 1 5 -7 -3 36.5756 11.0415 1 -5 7 -2 289.088 18.2011 5 5 -7 -2 301.304 17.3908 1 5 -7 -1 37.7606 11.2837 1 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12.2426 1 5 -8 -10 9.98184 14.6217 1 -5 -8 -10 7.89663 10.5185 1 5 -8 -9 71.2244 15.6842 1 5 -8 -8-11.8458 14.0274 1 5 -8 -7 37.7723 14.3225 1 5 -8 -6 60.3029 13.5678 1 5 -8 -5 68.8036 13.5655 1 5 -8 -4 18.9722 12.2647 1 5 -8 -3 52.8244 13.3549 1 5 -8 -2 0.65375 11.4230 1 5 -8 -1 131.019 14.7941 1 -5 8 0 65.1039 14.1480 5 5 -8 0 40.3093 12.6659 1 5 -8 1 147.821 14.9965 1 -5 8 1 206.902 18.5781 5 -5 8 2 11.0599 13.6062 5 5 -8 2-6.83596 11.4244 1 -5 8 3 70.1996 15.4551 5 5 -8 3 43.4470 12.0601 1 -5 8 4 13.1174 14.4309 5 5 -8 4 10.8993 11.1492 1 -5 8 5 40.4109 16.3260 5 -5 8 6 36.8940 15.7367 5 -5 8 7 80.7957 18.7335 5 -5 8 8 34.2738 18.5909 5 -5 8 9 66.7000 19.3448 5 -5 8 10 38.7625 19.9177 5 5 -9 -3 17.6662 13.7474 1 5 -9 -2 52.2290 14.5273 1 5 -9 -1 10.4917 13.1485 1 5 -9 0 33.5630 13.7513 1 5 -9 1 8.87679 13.2815 1 5 -9 2 38.3541 13.4692 1 5 -9 3 5.87451 12.6793 1 5 -9 4 6.55858 12.5772 1 5 -9 5-2.60904 12.3599 1 5 -9 6 11.6519 12.4955 1 5 -9 7-0.64341 12.4820 1 6 0 -26 6.87570 14.1618 1 6 0 -25 49.0353 14.0327 1 6 0 -24 48.4898 13.6127 1 6 0 -23 90.4519 13.5891 1 6 0 -22 42.6785 11.1820 1 6 0 -21 272.894 15.1257 1 6 0 -20 14.8707 9.22646 1 6 0 -19 155.214 11.8475 1 6 0 -18 185.854 11.8557 1 6 0 -17 9.73211 7.65055 1 6 0 -16 54.2271 8.17667 1 6 0 -15 72.7338 7.70798 1 6 0 -14 309.836 12.1599 1 6 0 -13 2839.87 57.4921 1 6 0 -12 962.613 23.1789 1 6 0 -11 3999.26 77.4965 1 -6 0 -11 4000.63 74.4014 5 6 0 -10 907.118 21.4601 1 6 0 -9 1687.92 35.3814 1 6 0 -8 33.6134 4.20388 1 6 0 -7 202.534 7.53142 1 6 0 -6 4830.14 91.0886 1 6 0 -5 504.772 13.1281 1 6 0 -4 1657.66 37.5178 4 6 0 -4 1617.25 33.3105 1 6 0 -3 3576.27 72.6040 4 6 0 -2 954.311 24.6202 4 6 0 -1 9082.51 171.277 4 6 0 0 2307.31 49.2994 4 6 0 1 8809.83 166.436 4 6 0 2 934.291 24.4637 4 6 0 5 446.600 12.4597 1 -6 0 8 36.7960 5.86888 3 -6 0 9 1656.01 38.3434 3 -6 0 10 912.708 24.4763 3 -6 0 10 835.807 20.4183 1 -6 0 11 3889.97 75.7189 1 -6 0 11 3921.89 79.9648 3 -6 0 12 946.060 26.5625 3 -6 0 13 2850.08 62.0219 3 -6 0 14 283.039 14.5517 3 -6 0 15 61.9680 9.64431 3 -6 0 16 45.6913 10.0240 3 -6 0 17 17.4333 9.07655 3 -6 0 21 227.007 16.7027 2 -6 0 22 54.1380 12.8699 2 -6 0 23 91.0868 14.7990 2 -6 0 24 31.7952 14.2606 2 6 -1 -27 10.5335 15.6198 1 6 -1 -26 1.00770 14.2145 1 6 -1 -25 16.0122 13.8315 1 6 1 -24-10.4953 14.6762 1 6 -1 -24 32.3368 13.2868 1 6 1 -23 5.61372 13.2087 1 6 -1 -23 23.9473 12.1681 1 6 1 -22 17.9328 12.4201 1 6 -1 -22 13.4138 12.0014 1 6 1 -21 0.86331 11.3842 1 6 -1 -21 30.3760 10.8526 1 6 1 -20 6.94203 10.6091 1 6 -1 -20 1.69130 9.83061 1 6 1 -19 17.8213 9.91038 1 6 -1 -19 12.3918 9.30563 1 6 1 -18 30.9630 9.53243 1 6 -1 -18 26.7003 9.50194 1 6 1 -17 80.9735 9.48624 1 6 -1 -17 68.0033 9.33884 1 6 1 -16 25.6166 7.68166 1 6 -1 -16 17.3200 7.67037 1 6 -1 -15 84.8137 8.72520 1 6 1 -15 118.802 8.68127 1 6 1 -14 25.6355 6.19853 1 6 -1 -14 0.31088 6.84981 1 6 -1 -13 19.3447 6.87932 1 6 1 -13 47.6728 6.12120 1 6 1 -12 83.1314 6.61912 1 6 -1 -12 83.2733 7.61244 1 -6 -1 -12 65.6110 5.03883 5 6 1 -11 131.374 6.95783 1 6 -1 -11 139.083 8.56846 1 -6 -1 -11 130.640 6.53062 5 6 1 -10 174.700 7.08412 1 6 -1 -10 170.834 8.88689 1 6 -1 -9 11.1763 4.76772 1 6 1 -9 9.12981 3.20161 1 6 -1 -8-3.23220 4.18480 1 6 1 -8 7.36401 2.80251 1 6 -1 -7 440.115 13.2918 1 6 1 -7 416.781 10.2812 1 6 -1 -6 384.403 12.5443 1 6 1 -6 387.395 9.39222 1 6 1 -5 649.405 13.9560 1 6 -1 -5 639.237 16.9142 1 6 -1 -4 333.669 12.8525 4 6 -1 -4 318.626 10.8675 1 6 1 -4 348.797 8.46215 1 6 -1 -3 188.796 9.69335 4 6 1 -3 187.895 5.69481 1 6 -1 -2 208.134 9.85192 4 6 -1 -1 282.509 11.5159 4 6 -1 0 670.371 19.2450 4 6 1 0 675.495 14.8704 1 6 1 1 281.153 8.10465 1 6 -1 1 268.994 11.3079 4 6 1 2 213.569 7.18761 1 6 -1 2 173.921 9.07622 4 6 1 3 181.328 7.14715 1 6 1 4 352.145 10.6126 1 6 1 5 643.893 16.4049 1 -6 -1 9 7.36812 3.12882 1 -6 -1 9 1.99374 5.77971 3 -6 -1 10 156.781 6.45010 1 -6 -1 10 173.390 10.2074 3 -6 -1 11 120.987 6.15095 1 -6 -1 11 122.672 9.49858 3 -6 -1 12 69.6969 8.68580 3 -6 -1 12 76.1716 5.67731 1 -6 -1 13 21.9956 4.91073 1 -6 -1 13 25.1289 7.61972 3 -6 1 14-4.02089 7.97644 3 -6 -1 14-0.85592 7.66364 3 -6 1 15 67.7862 10.2442 3 -6 -1 15 80.1658 10.1609 3 -6 1 16 12.4995 8.90055 3 -6 -1 16 3.77987 8.29576 3 -6 1 17 60.5132 11.1678 3 -6 -1 17 70.7343 10.4212 3 -6 -1 18 16.6553 9.26912 3 -6 1 21-2.59811 11.1876 2 -6 1 22 8.24396 12.1738 2 -6 -1 22 10.9779 11.3730 2 -6 1 23 28.5825 13.4721 2 -6 -1 23 10.2114 12.9043 2 -6 -1 24 2.80961 12.5781 2 6 -2 -25 38.0604 15.6230 1 6 -2 -24 39.4150 14.5835 1 6 -2 -23 72.5693 14.0580 1 6 -2 -22 38.5461 13.4363 1 -6 -2 -21 127.169 14.7041 1 6 -2 -21 178.818 14.6978 1 -6 -2 -20-11.3896 11.7359 1 6 -2 -20 5.96424 10.7233 1 6 -2 -19 130.550 12.8855 1 -6 -2 -19 150.858 13.5936 1 -6 -2 -18 38.1451 11.0873 1 6 -2 -18 58.5573 10.3979 1 6 -2 -17 55.9499 10.1126 1 -6 -2 -17 24.5225 10.0369 1 6 2 -16-25.0669 11.9130 1 -6 -2 -16 1.22271 9.28339 1 6 -2 -16-16.4096 8.84242 1 -6 -2 -15 189.790 12.4221 1 6 -2 -15 169.665 11.9148 1 6 2 -15 191.542 13.0900 1 -6 -2 -14 179.834 11.4360 1 6 -2 -14 162.959 11.0139 1 -6 -2 -13 1789.99 41.0651 1 6 -2 -13 1848.46 42.1266 1 6 2 -13 1766.21 40.5999 1 -6 -2 -12 268.576 12.1087 1 6 -2 -12 296.123 12.9485 1 -6 -2 -12 292.225 11.1316 5 -6 -2 -11 2080.23 43.7025 1 6 -2 -11 2015.64 44.7476 1 -6 -2 -11 2023.09 42.6058 5 -6 -2 -10 181.978 9.37875 1 6 -2 -10 169.052 9.95007 1 -6 2 -10 184.015 6.33236 5 -6 -2 -10 187.970 9.14778 5 6 2 -10 177.193 7.40358 1 -6 -2 -9 1228.93 28.7439 1 6 -2 -9 1262.80 30.6424 1 -6 -2 -8 4.55002 4.70875 1 6 -2 -8 7.05284 5.33364 1 6 -2 -7 692.014 19.8429 1 -6 -2 -7 716.792 17.9909 1 -6 -2 -6 1376.73 29.3013 1 6 -2 -6 1319.66 31.6765 1 6 -2 -5 1017.63 25.2135 1 6 -2 -4 343.548 12.4630 1 6 -2 -3 2804.65 58.6427 4 6 2 -3 2788.78 58.5205 4 6 -2 -2 246.725 11.1375 4 6 2 -2 259.143 11.2048 4 6 2 -2 253.705 5.66531 1 6 -2 -1 5088.88 101.807 4 6 2 -1 5251.48 95.4712 1 6 2 -1 5165.22 101.816 4 6 -2 0 503.114 16.4230 4 6 2 0 541.628 12.2851 1 6 2 0 496.457 16.3230 4 6 -2 1 5140.72 100.340 4 6 2 1 4987.52 99.9479 4 6 2 1 5157.06 95.3943 1 6 -2 2 255.836 11.3448 4 6 2 2 270.447 8.68748 1 6 2 2 273.588 11.6313 4 6 -2 3 2703.04 57.1502 4 6 2 3 2688.76 57.1421 4 6 2 3 2716.73 53.5103 1 6 2 4 375.662 11.6355 1 6 2 5 1046.98 24.7098 1 -6 2 6 1328.77 31.3591 3 -6 2 7 696.995 19.8908 3 -6 2 8 11.0603 5.47822 3 -6 2 9 1171.28 29.4809 3 -6 -2 9 1167.09 29.1898 3 -6 -2 10 185.940 5.96908 1 -6 2 10 184.860 10.6708 3 -6 -2 10 180.842 10.3993 3 -6 2 11 2026.21 45.6356 3 -6 -2 11 2003.47 44.9242 3 -6 -2 11 1955.53 38.6379 1 -6 2 12 272.815 13.6731 3 -6 -2 12 279.042 13.2038 3 -6 -2 12 264.904 8.49180 1 -6 2 13 1614.11 40.0808 3 -6 -2 13 1629.54 39.1525 3 -6 2 14 155.620 12.1326 3 -6 -2 14 171.238 11.4768 3 -6 2 15 179.764 13.2728 3 -6 -2 15 148.991 11.6983 3 -6 -2 16 7.32452 8.79078 3 -6 -2 17 41.9546 10.1292 3 -6 -2 18 42.7943 10.6196 3 -6 -2 22 13.7015 11.9762 2 -6 -2 23 56.4268 14.3681 2 -6 -2 24 21.6200 14.2806 2 6 -3 -24 48.2936 16.6057 1 6 -3 -23 39.5663 15.0011 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2.39937 7.02170 4 9 0 0 2.42864 6.97870 4 9 0 1 6.72731 7.53431 4 9 0 2-4.42992 7.59551 4 9 0 3 21.0796 8.61087 4 9 0 4 4.06472 7.46806 4 9 0 5 6.79039 8.39514 4 -9 0 10-0.96431 8.50379 3 -9 0 11 1.47952 8.68476 3 -9 0 12 5.16109 8.91865 3 -9 0 13-1.59902 9.50172 3 -9 0 14 3.77764 9.89285 3 -9 0 15 3.36144 9.89642 3 -9 0 16-1.17306 10.9647 3 -9 0 17 15.8831 12.0791 3 -9 0 18 1.88754 12.6945 3 -9 0 19 7.16519 13.1739 3 -9 0 20 11.5676 13.8271 3 -9 0 21 2.79236 14.4941 3 9 -1 -21 87.7911 13.0985 1 9 -1 -20 35.1581 11.2003 1 9 -1 -19 25.3484 10.5670 1 9 -1 -18 188.046 13.2718 1 9 -1 -17 10.4543 9.24666 1 9 1 -16 401.408 14.6944 1 9 -1 -16 313.670 15.0306 1 9 -1 -15 12.5928 8.29607 1 9 1 -15 36.3865 7.68720 1 9 -1 -14 44.7308 8.26053 1 9 1 -14 47.6027 7.53517 1 9 1 -13 392.637 12.9581 1 9 -1 -13 365.055 15.0372 1 9 -1 -12 6.56669 7.24456 1 9 1 -12 4.63011 5.22897 1 9 1 -11 871.381 20.4389 1 9 -1 -11 900.031 23.9778 1 9 1 -10 5.59147 4.25009 1 9 -1 -10 12.3058 6.67544 1 9 -1 -9 481.711 15.8729 1 9 1 -9 440.960 11.9823 1 9 -1 -8 410.381 14.5682 1 9 1 -8 417.836 11.2689 1 9 -1 -7 126.827 8.71042 1 9 1 -7 116.913 5.66987 1 9 1 -6 2184.20 43.0673 1 9 -1 -6 2181.14 47.1100 1 9 -1 -5 63.4745 6.93426 1 9 1 -5 63.8736 5.17716 1 9 -1 -4 2026.72 48.6369 4 9 1 -4 2047.51 40.7645 1 9 -1 -4 2028.66 44.1785 1 9 -1 -3 717.181 23.9707 4 9 -1 -2-4.79569 8.22034 4 9 -1 -1 1448.70 37.6507 4 9 -1 0 364.048 17.2839 4 9 1 0 437.693 12.3813 1 9 1 1 1654.08 33.8152 1 9 -1 1 1422.81 39.3559 4 9 -1 2 3.44188 7.63600 4 9 1 2 16.1468 5.15369 1 9 -1 3 760.693 24.9859 4 9 -1 4 2015.10 48.9355 4 9 -1 5 73.9362 10.1621 4 -9 -1 11 856.866 27.2075 3 -9 -1 12 11.0433 9.13783 3 -9 -1 13 352.165 17.9078 3 -9 -1 14 40.5504 10.4355 3 -9 -1 15 22.0546 10.7581 3 -9 -1 16 301.052 17.6328 3 -9 1 17 13.5663 12.4454 3 -9 -1 17 20.2532 11.5896 3 -9 1 18 162.403 15.8187 3 -9 -1 18 170.896 16.0570 3 -9 1 19 27.9656 13.5171 3 -9 -1 19 8.85998 12.9965 3 -9 1 20 11.7227 14.1574 3 -9 -1 20 3.29088 13.3426 3 -9 -1 21 63.2188 15.3758 3 9 -2 -23 16.5296 14.1568 1 9 -2 -22 21.9458 13.3686 1 9 -2 -21 22.3557 12.7700 1 9 -2 -20 2.31461 11.7146 1 9 -2 -19 6.33421 10.8416 1 9 -2 -18-3.98353 11.1672 1 9 -2 -17 76.8902 11.7800 1 9 -2 -16 10.6864 10.1840 1 9 -2 -15 58.7545 10.0790 1 9 -2 -14 7.02841 8.26342 1 9 -2 -13 59.9296 9.64827 1 9 -2 -12 135.710 10.7639 1 9 -2 -11 138.179 10.9232 1 9 -2 -10 105.488 9.96775 1 9 -2 -9 22.2601 7.62706 1 9 -2 -8 29.3137 7.52255 1 9 -2 -7 374.408 15.0490 1 9 -2 -6 66.7513 8.35482 1 9 -2 -5 711.945 21.6458 1 9 2 -4 50.6707 2.61747 1 9 -2 -4 50.8659 8.57178 4 9 2 -4 45.6006 8.67364 4 9 2 -4 35.4833 3.59435 1 9 -2 -4 43.7090 7.65689 1 9 -2 -3 73.9091 9.95275 4 9 2 -3 67.4744 9.48606 4 9 2 -3 75.0688 3.63361 1 9 2 -3 51.0598 4.80017 1 9 -2 -2 75.1898 9.67787 4 9 2 -2 84.2068 9.56943 4 9 -2 -1 556.807 20.3713 4 9 2 -1 554.606 20.0845 4 9 2 -1 482.835 14.6360 1 9 -2 0 871.090 26.6479 4 9 2 0 825.799 25.9679 4 9 2 0 820.492 21.2716 1 9 -2 1 557.486 20.8767 4 9 2 1 599.768 21.4471 4 9 2 1 583.647 17.4266 1 9 -2 2 71.1739 9.53038 4 9 2 2 86.3827 9.95907 4 9 -2 3 69.4418 9.20000 4 9 2 3 63.8263 9.51482 4 9 -2 4 66.1340 9.51338 4 9 2 4 55.2115 9.27601 4 9 -2 5 713.983 24.3532 4 9 2 5 696.794 24.2643 4 9 -2 6 66.4347 10.0492 4 9 2 6 55.2328 9.97178 4 -9 2 8 19.3027 8.67093 3 -9 2 9 31.9380 9.19006 3 -9 2 10 110.745 11.8353 3 -9 2 11 156.683 12.9892 3 -9 -2 11 150.858 12.8677 3 -9 2 12 139.586 12.9464 3 -9 -2 12 141.124 12.7040 3 -9 2 13 67.9665 11.3804 3 -9 -2 13 55.0145 10.9464 3 -9 2 14 2.22082 10.4219 3 -9 -2 14 5.14527 9.99468 3 -9 2 15 69.4691 12.5737 3 -9 -2 15 48.1669 11.5953 3 -9 2 16 19.7132 11.7828 3 -9 -2 16 12.0464 11.0252 3 -9 2 17 82.2423 13.7512 3 -9 -2 17 89.8349 13.8612 3 -9 2 18 11.0071 13.0644 3 -9 -2 18 6.48504 12.1044 3 -9 2 19-2.68595 13.2736 3 -9 -2 19 1.83499 12.7982 3 -9 -2 20 13.9808 13.7154 3 -9 -2 21 10.4959 13.7270 3 9 -3 -22 17.0908 14.4176 1 9 -3 -21 23.6496 13.9900 1 9 -3 -20 8.48469 13.6497 1 9 -3 -19-6.76223 13.3110 1 9 -3 -18 2.07079 12.9028 1 9 -3 -17 38.4713 11.2114 1 9 -3 -16 78.9345 12.8529 1 9 -3 -15 60.4903 11.2520 1 9 -3 -14 27.3681 10.4786 1 9 -3 -13 133.174 12.5066 1 9 -3 -12 146.003 12.6621 1 9 -3 -11 177.080 12.7538 1 9 -3 -10 64.4555 9.98142 1 9 -3 -9 131.709 11.2214 1 9 -3 -8 109.077 10.5353 1 9 -3 -7 274.134 14.1540 1 9 -3 -6 298.173 14.6516 1 9 -3 -5 267.892 13.6714 1 9 -3 -4 490.098 18.5230 1 9 -3 -3 437.165 18.3317 4 9 3 -3 435.212 18.1537 4 9 -3 -3 427.826 17.4675 1 9 -3 -2 194.313 12.9436 4 9 3 -2 206.990 13.1200 4 9 -3 -1 448.710 18.2640 4 9 3 -1 421.167 17.8360 4 9 3 -1 398.811 9.36134 1 9 -3 0 25.4543 8.95648 4 9 3 0 14.4704 8.05162 4 9 3 0 33.3631 3.92000 1 9 -3 1 440.523 18.6284 4 9 3 1 439.128 18.4933 4 9 3 1 461.451 12.8038 1 9 -3 2 193.952 13.3149 4 9 3 2 217.125 13.5313 4 9 3 2 238.796 9.60915 1 9 -3 3 413.224 18.1099 4 9 3 3 422.476 18.4101 4 9 3 3 463.095 14.6537 1 9 -3 4 527.435 20.4269 4 9 3 4 506.287 20.3551 4 9 -3 5 264.531 15.2047 4 9 3 5 275.306 15.4028 4 9 -3 6 273.636 15.6685 4 9 3 6 294.414 16.2759 4 9 -3 7 259.793 15.5238 4 -9 3 7 275.268 14.2730 3 -9 3 8 112.885 10.9651 3 -9 3 9 154.643 12.4175 3 -9 3 10 90.7813 11.2655 3 -9 3 11 156.853 12.9969 3 -9 -3 11 165.956 13.0290 3 -9 3 12 127.832 12.7046 3 -9 -3 12 122.999 12.0730 3 -9 3 13 146.497 13.4272 3 -9 -3 13 157.544 12.8800 3 -9 3 14 9.97552 11.1586 3 -9 -3 14 20.3015 10.0647 3 -9 3 15 57.0669 12.8235 3 -9 -3 15 43.1957 11.7748 3 -9 3 16 50.7155 13.0202 3 -9 -3 16 61.4800 12.1064 3 -9 3 17 35.5319 13.0252 3 -9 -3 17 24.3451 12.1705 3 -9 3 18 19.3795 13.3312 3 -9 -3 18 34.6068 12.8910 3 -9 -3 19 12.3510 12.9138 3 -9 -3 20 20.7070 13.3489 3 -9 -3 21 30.0351 14.3234 3 9 -4 -20 14.1378 14.6612 1 9 -4 -19-2.35086 14.8279 1 9 -4 -18 28.2772 13.1253 1 9 -4 -17 82.0956 14.4281 1 9 -4 -16 11.2089 11.6768 1 9 -4 -15 44.9458 12.4956 1 9 -4 -14-1.62371 11.1621 1 9 -4 -13 40.0858 11.4559 1 9 -4 -12 122.112 13.2996 1 9 -4 -11 61.8597 11.4590 1 9 -4 -10 87.3508 11.3997 1 9 -4 -9 8.66684 9.11699 1 9 -4 -8 53.3546 10.4238 1 -9 4 -8 54.9979 8.10034 5 9 -4 -7 274.439 15.5880 1 9 -4 -6 10.2780 9.13526 1 9 -4 -5 363.762 17.2700 1 9 -4 -4-1.02266 8.90640 1 9 -4 -3 49.8080 10.2192 1 9 -4 -2 83.5686 10.6305 4 9 4 -2 81.3188 10.3780 4 9 -4 -1 267.802 15.1300 4 9 4 -1 265.142 14.7903 4 9 -4 0 700.337 23.7652 4 9 4 0 757.204 24.4241 4 9 4 0 694.021 14.9105 1 9 -4 1 294.069 15.4270 4 9 4 1 269.872 15.0586 4 9 4 1 272.586 8.43629 1 9 4 2 79.4193 5.72245 1 9 -4 2 77.2725 10.4875 4 9 4 2 87.0437 10.8169 4 9 4 3 48.2217 5.82316 1 9 -4 3 37.4843 9.72671 4 9 4 3 35.5558 9.21347 4 9 -4 4-6.62473 8.96060 4 9 4 4-5.05353 9.09062 4 9 -4 5 425.300 18.6707 4 9 4 5 372.001 17.7418 4 -9 4 5 362.506 15.9043 3 9 -4 6 7.49678 9.45955 4 9 4 6 1.05637 9.12745 4 -9 4 6 8.76443 8.23515 3 9 -4 7 259.192 15.9800 4 9 4 7 242.441 15.6827 4 -9 4 7 253.551 13.8345 3 9 -4 8 58.3055 11.4593 4 9 4 8 48.7310 10.8687 4 -9 4 8 56.4941 9.92760 3 -9 4 9 23.9123 9.21424 3 -9 4 10 85.0894 10.9417 3 -9 -4 10 78.0506 10.1750 3 -9 4 11 71.2181 11.7462 3 -9 -4 11 62.3469 10.4730 3 -9 4 12 133.652 13.2758 3 -9 -4 12 126.677 12.0554 3 -9 4 13 53.2102 11.2261 3 -9 -4 13 45.8752 10.5196 3 -9 4 14 20.3295 11.0243 3 -9 -4 14 14.0736 10.0227 3 -9 4 15 36.8113 12.6691 3 -9 -4 15 36.0459 10.6923 3 -9 4 16 16.7097 12.6525 3 -9 -4 16 12.1502 11.4336 3 -9 -4 17 49.8495 12.4359 3 -9 -4 18 8.65009 11.8106 3 -9 -4 19 6.12572 12.3352 3 -9 -4 20 8.05677 12.5083 3 -9 -5 -18 2.36336 13.0176 1 -9 -5 -17 42.4677 13.1529 1 9 -5 -17 40.1701 14.5908 1 -9 -5 -16 9.45384 11.2997 1 9 -5 -16 11.8975 13.2604 1 -9 -5 -15 35.3484 11.2233 1 9 -5 -15 54.9298 14.0221 1 -9 -5 -14 11.4977 10.3470 1 9 -5 -14 4.20405 12.1611 1 9 -5 -13 39.4955 12.8505 1 -9 -5 -13 49.1187 10.3312 1 -9 -5 -12 240.837 12.8830 1 9 -5 -12 224.477 17.4422 1 -9 -5 -11 10.4181 8.57628 1 9 -5 -11 22.0584 12.5584 1 9 -5 -10 212.290 16.2286 1 -9 -5 -10 225.709 11.7684 1 9 -5 -9 27.5118 11.2704 1 -9 -5 -9 36.7922 7.62412 1 -9 -5 -8 16.6152 6.94755 1 9 -5 -8 16.6656 10.7736 1 9 -5 -7 235.846 16.6865 1 -9 5 -7 265.934 14.8604 5 9 -5 -6 20.6576 10.6653 1 -9 5 -6 3.65565 8.57977 5 9 -5 -5 334.896 17.9937 1 -9 5 -5 295.954 16.5332 5 9 -5 -4 29.8654 10.9000 1 9 -5 -3 132.343 13.3447 1 9 -5 -2 343.837 18.5042 1 9 -5 -1 58.7663 9.92563 4 9 5 -1 42.0325 9.88435 4 9 -5 0 300.317 15.3920 4 9 5 0 303.204 15.5137 4 9 -5 1 60.0967 10.0875 4 9 5 1 52.3809 10.0904 4 9 -5 2 322.172 16.0481 4 9 5 2 347.733 16.1103 4 -9 5 2 314.543 13.7743 3 9 -5 3 144.519 12.0526 4 9 5 3 128.288 11.9613 4 -9 5 3 137.522 10.3839 3 9 -5 4 53.8204 10.2553 4 9 5 4 57.8245 10.3814 4 -9 5 4 39.8684 8.57918 3 9 -5 5 349.403 17.0898 4 9 5 5 325.230 16.4422 4 -9 5 5 293.392 14.4753 3 9 -5 6 8.81736 9.62924 4 9 5 6 4.53632 9.23953 4 -9 5 6-6.58594 7.84400 3 9 -5 7 256.586 15.8163 4 9 5 7 242.697 15.4270 4 -9 5 7 217.319 13.3935 3 9 -5 8 8.74973 9.70805 4 9 5 8 24.2079 10.3595 4 -9 5 8 13.5432 8.54324 3 9 -5 9 25.5756 11.1611 4 9 5 9 29.6102 11.2814 4 -9 5 9 22.4934 10.1104 3 9 -5 10 222.016 16.2227 4 -9 5 10 211.313 14.2558 3 -9 -5 10 182.955 12.7260 3 -9 5 11 20.4368 10.6866 3 -9 -5 11 13.5926 9.48697 3 -9 5 12 230.328 15.5934 3 -9 -5 12 224.175 13.7066 3 -9 5 13 54.5817 11.9086 3 -9 -5 13 45.1812 10.6028 3 -9 5 14 11.6273 12.3366 3 -9 -5 14 6.66997 9.96530 3 -9 -5 15 61.6966 11.5224 3 -9 -5 16 7.12821 11.3205 3 -9 5 18 12.0300 13.2939 2 9 -6 -14 6.64083 13.6030 1 9 -6 -13-14.9262 14.0419 1 9 -6 -12 49.2934 14.7664 1 9 -6 -11 10.7309 13.4210 1 9 -6 -10 13.9667 13.0358 1 9 -6 -9 14.4572 12.3212 1 9 -6 -8 40.0396 12.0880 1 9 -6 -7 45.1613 13.6227 1 9 -6 -6 51.7523 13.4387 1 -9 6 -6 38.5517 10.7513 5 9 -6 -5 7.40720 11.7502 1 -9 6 -5 19.8265 10.8967 5 9 -6 -4 39.6472 12.4380 1 -9 6 -4 34.5594 10.8387 5 9 -6 -3 10.5982 11.0385 1 -9 6 -3 27.7924 12.2539 5 -9 6 -2 46.5981 13.2289 5 -9 6 -1 8.56265 7.42699 3 -9 6 -1 13.4085 12.0974 5 -9 6 0 165.792 10.8772 3 -9 6 0 173.816 18.7008 5 9 6 1 2.19488 8.92997 4 -9 6 1 4.64365 7.75969 3 -9 6 1 9.07851 15.0548 5 9 6 2 28.0595 9.61766 4 -9 6 2 34.2091 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20.0946 27.7078 5 -9 7 9 14.9688 28.8828 5 -9 8 -4 35.5618 13.7314 5 -9 8 -3 12.7741 14.0145 5 -9 8 -2 25.2467 15.3600 5 -9 8 -1 45.0626 16.8510 5 -9 8 0 25.6888 16.2724 5 -9 8 1 31.2973 17.2567 5 -9 8 2-1.22422 18.1918 5 -9 8 3 2.68549 21.0508 5 10 0 -16 231.680 11.9450 1 10 0 -15 111.661 9.57432 1 10 0 -14 82.7802 8.37828 1 10 0 -13-6.81667 6.71689 1 10 0 -12 19.5916 6.23833 1 10 0 -11 72.3632 7.23356 1 10 0 -10 70.1650 6.91503 1 10 0 -9 4.40326 5.65752 1 10 0 -8 479.259 14.8383 1 10 0 -7 469.441 14.6190 1 10 0 -6 1916.24 40.9896 1 10 0 -5 1537.99 34.0104 1 10 0 -4 1390.84 37.9980 4 10 0 -4 1416.30 31.9028 1 10 0 -3 653.152 23.4792 4 10 0 -2 547.910 21.5631 4 10 0 -1 429.537 18.9839 4 10 0 0 185.982 13.8709 4 10 0 1 433.574 18.9975 4 10 0 2 578.831 22.3248 4 10 0 3 639.985 23.6884 4 10 0 4 1436.82 39.5040 4 10 0 5 1510.91 41.0619 4 10 0 6 1989.54 50.6272 4 -10 0 10 65.1949 10.9906 3 -10 0 11 78.3919 12.1747 3 -10 0 12 26.7913 10.6718 3 -10 0 13 4.03710 10.2814 3 -10 0 14 84.9037 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9.57385 13.9649 4 14 3 3 21.9312 14.9347 4 14 -3 4-4.91070 14.7002 4 14 3 4 14.0748 14.6699 4 14 -3 5 56.0236 16.8281 4 14 3 5 29.7466 16.2301 4 14 -3 6 11.8038 14.9652 4 14 3 6 24.7495 16.0447 4 14 -3 7 33.8803 16.3110 4 14 3 7 12.9724 16.6108 4 14 -3 8-2.60768 15.8197 4 14 3 8-1.77724 16.3126 4 -14 3 8 8.25044 13.8227 3 14 -3 9 46.0476 16.9674 4 14 3 9 19.0267 17.1313 4 -14 3 9 26.9839 15.1540 3 -14 3 10 33.5002 15.6594 3 14 -4 -12-2.97684 12.9660 1 14 -4 -11 1.20391 13.8450 1 14 -4 -10 3.00840 13.6619 1 14 -4 -9 10.8596 12.4998 1 14 -4 -8 34.4043 13.2988 1 14 -4 -7 46.4171 15.0460 1 14 -4 -6 46.2291 13.9563 1 14 -4 -5 25.2301 13.0746 1 14 -4 -4 37.1660 13.7348 1 14 -4 -3 25.3540 13.3543 1 14 -4 -2 20.3691 13.1837 1 14 -4 -1 16.2675 14.5425 4 14 4 -1 15.2929 14.4910 4 14 -4 -1 6.09980 13.4158 1 14 -4 0 17.9371 14.2993 4 14 4 0 16.9524 13.8845 4 14 -4 1 12.6215 14.7700 4 14 4 1 21.0198 14.8730 4 14 -4 2 27.6108 15.2887 4 14 4 2 12.5546 14.5311 4 14 -4 3 35.2375 15.6051 4 14 4 3 25.2427 15.3128 4 14 -4 4 49.7941 15.3632 4 14 4 4 57.6657 16.4705 4 14 -4 5 29.5170 16.2489 4 14 4 5-2.44982 14.8851 4 14 -4 6 47.5235 16.2531 4 14 4 6 60.1495 17.4571 4 -14 4 6 75.3918 15.5708 3 14 -4 7 42.4036 16.3179 4 14 4 7 27.0544 16.6016 4 -14 4 7 38.9848 14.8596 3 14 -4 8 19.6979 16.8296 4 14 4 8 27.2678 16.5144 4 -14 4 8 18.9270 14.1178 3 -14 4 9 33.3966 15.2202 3 14 -5 0 31.4709 15.6457 4 14 5 0-1.47677 14.2900 4 14 -5 1 10.5459 14.4492 4 14 5 1 30.4365 15.4514 4 14 -5 2 32.9410 15.5406 4 14 5 2 33.8455 15.8173 4 14 -5 3 15.4288 15.7479 4 14 5 3 4.52476 14.5559 4 -14 5 3 7.87977 12.5649 3 14 -5 4 16.4138 15.0699 4 14 5 4 23.6861 15.6720 4 -14 5 4 17.4028 13.5029 3 14 -5 5 20.3882 16.0457 4 14 5 5 18.9391 15.1783 4 -14 5 5 7.56541 12.2856 3 14 -5 6 3.20953 15.9194 4 14 5 6 14.2610 15.2520 4 -14 5 6-12.0589 13.4591 3 14 -5 7 14.7503 16.2995 4 14 5 7 17.6212 15.8736 4 -14 5 7 7.33077 14.1162 3 -14 5 8 2.47231 14.2931 3 15 0 -3 11.6990 15.1658 4 15 0 -2 4.19878 15.0154 4 15 0 -1 33.0728 15.5786 4 15 0 0 18.6992 14.5247 4 15 0 1 17.2058 15.5462 4 15 0 2-7.71031 15.2957 4 15 0 3 7.08388 15.3260 4 15 0 4 3.57335 15.4863 4 15 0 5-0.91663 15.5304 4 15 0 6 1.83751 16.5261 4 15 -1 -3 32.5796 15.3453 4 15 1 -3 29.3408 16.5603 4 15 -1 -2 101.200 17.3521 4 15 1 -2 130.107 18.0812 4 15 -1 -1 24.5647 16.4988 4 15 1 -1 12.7662 15.5153 4 15 -1 0 243.925 21.4803 4 15 1 0 250.625 22.0788 4 15 -1 1 21.4332 16.4185 4 15 1 1-17.2857 15.4073 4 15 -1 2 148.222 19.0952 4 15 1 2 109.068 17.7757 4 15 -1 3 3.49503 14.5313 4 15 1 3 27.6242 16.6831 4 15 -1 4 11.5526 15.8667 4 15 1 4 8.99602 16.2066 4 15 -1 5 61.6487 18.0734 4 15 1 5 35.0999 17.7102 4 15 -1 6 6.39840 15.2783 4 15 1 6-4.63010 17.6875 4 15 -2 -5 22.8659 11.9475 1 15 -2 -4 3.44861 10.4988 1 15 -2 -3 13.7914 11.4157 1 15 -2 -2 10.0639 15.0632 4 15 2 -2 4.20415 15.3031 4 15 -2 -2 3.16097 11.5316 1 15 -2 -1 49.8527 16.7677 4 15 2 -1 50.0967 16.2216 4 15 -2 0 11.9497 16.1778 4 15 2 0 27.4749 16.9549 4 15 -2 1 49.7496 17.0420 4 15 2 1 51.1188 16.9607 4 15 -2 2-8.64728 14.9184 4 15 2 2 22.6556 16.1549 4 15 -2 3-0.85272 15.0628 4 15 2 3-6.99533 16.2339 4 15 -2 4-3.55480 15.5283 4 15 2 4 8.09694 16.1104 4 15 -2 5 13.4131 16.1335 4 15 2 5 10.0772 16.6500 4 15 -3 -7 14.3399 13.0509 1 15 -3 -6 21.5228 12.6124 1 15 -3 -5 21.8843 12.8985 1 15 -3 -4 10.8440 12.3046 1 15 -3 -3 31.2817 13.0596 1 15 -3 -2 53.7172 16.9733 4 15 3 -2 25.8997 15.9991 4 15 -3 -2 52.6528 13.7350 1 15 -3 -1 22.9480 13.5087 1 15 -3 -1 5.03273 16.1277 4 15 3 -1 3.35314 15.2137 4 15 -3 0 32.2307 16.6614 4 15 3 0 57.6323 17.1186 4 15 -3 1 11.1172 15.9445 4 15 3 1 16.2507 15.8365 4 15 -3 2 44.7770 17.0699 4 15 3 2 63.1745 17.3840 4 15 -3 3-10.3699 15.7730 4 15 3 3 7.79891 16.4642 4 15 3 4 13.2854 16.9634 4 15 -4 -9 25.1881 14.0214 1 15 -4 -8 9.26467 13.5606 1 15 -4 -7 16.3338 14.7409 1 15 -4 -6 14.8407 13.9549 1 15 -4 -5 5.24038 13.7513 1 15 -4 -4 0.65212 14.1010 1 15 -4 -3 13.3181 13.9505 1 15 -4 -2 24.5716 14.0673 1 15 -4 -1 26.5395 14.5728 1 15 -4 0-13.0696 14.5127 1 -15 5 3 12.0746 13.7100 3 16 -3 -3-4.18681 12.9599 1 16 -3 -2 1.23569 13.3734 1 16 -3 -1 18.3234 13.9440 1 16 -3 0 4.65228 13.4095 1 0 0 0 0.00 0.00 0 TITL OAT-3a in Pna2(1) REM Pna2(1) (#33, found as Pbn2(1) in ba-c setting) CELL 0.71073 12.431954 7.573554 21.005510 90.0000 90.0000 90.0000 ZERR 4.00 0.000469 0.000240 0.000775 0.0000 0.0000 0.0000 LATT -1 SYMM -x,-y, z+1/2 SYMM x+1/2,-y+1/2, z SYMM -x+1/2, y+1/2, z+1/2 SFAC C H N Se Sn UNIT 64.00 88.00 8.00 8.00 4.00 TREF HKLF 4 END ; _shelx_hkl_checksum 2959 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, y, -z-1/2' '-x-1/2, y-1/2, z-1/2' 'x-1/2, -y-1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Sn1 Sn 0.70643(3) 0.48527(4) 0.750000 0.06222(15) Uani 1 2 d S T P . . Se1 Se 0.56459(3) 0.42410(6) 0.66080(2) 0.07867(18) Uani 1 1 d . . . . . N1 N 0.7708(3) 0.5175(3) 0.62922(16) 0.0631(8) Uani 1 1 d . . . . . C1 C 0.6750(4) 0.4841(4) 0.6022(2) 0.0683(10) Uani 1 1 d . . . . . C2 C 0.6598(4) 0.4888(5) 0.5368(2) 0.0720(11) Uani 1 1 d . . . . . H2 H 0.592149 0.466255 0.519740 0.086 Uiso 1 1 calc R U . . . C3 C 0.7449(5) 0.5269(5) 0.4971(2) 0.0720(10) Uani 1 1 d . . . . . C4 C 0.8432(4) 0.5599(5) 0.5255(2) 0.0724(11) Uani 1 1 d . . . . . H4 H 0.902510 0.585384 0.500190 0.087 Uiso 1 1 calc R U . . . C5 C 0.8550(4) 0.5556(5) 0.5909(2) 0.0685(10) Uani 1 1 d . . . . . C6 C 0.7322(5) 0.5296(6) 0.4260(2) 0.0951(16) Uani 1 1 d . . . . . H6A H 0.759026 0.421232 0.408424 0.143 Uiso 1 1 calc R U . . . H6B H 0.771875 0.627145 0.408654 0.143 Uiso 1 1 calc R U . . . H6C H 0.657424 0.542293 0.415400 0.143 Uiso 1 1 calc R U . . . C7 C 0.9595(4) 0.5913(6) 0.6224(2) 0.0899(14) Uani 1 1 d . . . . . H7A H 0.947056 0.646644 0.662877 0.135 Uiso 1 1 calc R U . . . H7B H 1.001845 0.668132 0.596106 0.135 Uiso 1 1 calc R U . . . H7C H 0.997300 0.482108 0.628726 0.135 Uiso 1 1 calc R U . . . C8 C 0.7327(6) 0.7620(7) 0.750000 0.0886(18) Uani 1 2 d S T P . . H8A H 0.803640 0.786611 0.765713 0.133 Uiso 0.5 1 calc R U P . . H8B H 0.680448 0.818112 0.776890 0.133 Uiso 0.5 1 calc R U P . . H8C H 0.725884 0.806494 0.707397 0.133 Uiso 0.5 1 calc R U P . . C9 C 0.8153(5) 0.2705(7) 0.750000 0.0749(16) Uani 1 2 d S T P . . H9A H 0.826134 0.230392 0.707126 0.112 Uiso 0.5 1 calc R U P . . H9B H 0.786260 0.175961 0.775154 0.112 Uiso 0.5 1 calc R U P . . H9C H 0.882732 0.307655 0.767721 0.112 Uiso 0.5 1 calc R U P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sn1 0.0661(3) 0.0503(2) 0.0703(3) 0.000 0.000 0.00693(15) Se1 0.0649(3) 0.0877(3) 0.0834(3) 0.0062(2) -0.0053(2) -0.0020(2) N1 0.067(2) 0.0539(17) 0.068(2) -0.0009(14) -0.0094(16) 0.0004(14) C1 0.073(3) 0.052(2) 0.080(3) -0.0002(18) -0.010(2) 0.0006(17) C2 0.072(3) 0.068(2) 0.076(3) 0.002(2) -0.019(2) -0.0020(19) C3 0.089(3) 0.058(2) 0.070(3) 0.0029(18) -0.010(2) -0.001(2) C4 0.080(3) 0.064(2) 0.073(3) 0.000(2) -0.001(2) -0.006(2) C5 0.074(3) 0.0530(19) 0.078(3) -0.0031(18) -0.011(2) -0.0025(18) C6 0.115(4) 0.100(3) 0.070(3) 0.008(3) -0.015(3) -0.018(3) C7 0.081(3) 0.092(3) 0.097(3) 0.002(3) -0.019(3) -0.011(2) C8 0.130(6) 0.055(3) 0.081(4) 0.000 0.000 0.004(3) C9 0.092(4) 0.062(3) 0.071(3) 0.000 0.000 0.021(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C9 Sn1 C8 131.4(3) . . ? C9 Sn1 Se1 107.16(11) . . ? C8 Sn1 Se1 106.20(14) . . ? C9 Sn1 Se1 107.16(11) . 6_557 ? C8 Sn1 Se1 106.20(14) . 6_557 ? Se1 Sn1 Se1 91.57(2) . 6_557 ? C1 Se1 Sn1 86.22(13) . . ? C1 N1 C5 118.4(4) . . ? N1 C1 C2 122.3(4) . . ? N1 C1 Se1 114.4(3) . . ? C2 C1 Se1 123.3(3) . . ? C3 C2 C1 120.0(4) . . ? C3 C2 H2 120.0 . . ? C1 C2 H2 120.0 . . ? C2 C3 C4 117.0(4) . . ? C2 C3 C6 121.6(5) . . ? C4 C3 C6 121.4(5) . . ? C5 C4 C3 121.3(4) . . ? C5 C4 H4 119.4 . . ? C3 C4 H4 119.4 . . ? N1 C5 C4 121.0(4) . . ? N1 C5 C7 116.8(4) . . ? C4 C5 C7 122.2(4) . . ? C3 C6 H6A 109.5 . . ? C3 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C3 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C5 C7 H7A 109.5 . . ? C5 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C5 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? Sn1 C8 H8A 109.5 . . ? Sn1 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? Sn1 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? Sn1 C8 H8A 109.5(7) . 6_557 ? H8A C8 H8A 40.2 . 6_557 ? H8B C8 H8A 137.6 . 6_557 ? H8C C8 H8A 72.1 . 6_557 ? Sn1 C8 H8B 109.5(10) . 6_557 ? H8A C8 H8B 137.6 . 6_557 ? H8B C8 H8B 72.1 . 6_557 ? H8C C8 H8B 40.2 . 6_557 ? H8A C8 H8B 109.5 6_557 6_557 ? Sn1 C8 H8C 109.5(3) . 6_557 ? H8A C8 H8C 72.1 . 6_557 ? H8B C8 H8C 40.2 . 6_557 ? H8C C8 H8C 137.6 . 6_557 ? H8A C8 H8C 109.5 6_557 6_557 ? H8B C8 H8C 109.5 6_557 6_557 ? Sn1 C9 H9A 109.5 . . ? Sn1 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? Sn1 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? Sn1 C9 H9A 109.47(16) . 6_557 ? H9A C9 H9A 139.5 . 6_557 ? H9B C9 H9A 45.6 . 6_557 ? H9C C9 H9A 66.8 . 6_557 ? Sn1 C9 H9B 109.5(8) . 6_557 ? H9A C9 H9B 45.6 . 6_557 ? H9B C9 H9B 66.8 . 6_557 ? H9C C9 H9B 139.5 . 6_557 ? H9A C9 H9B 109.5 6_557 6_557 ? Sn1 C9 H9C 109.5(6) . 6_557 ? H9A C9 H9C 66.8 . 6_557 ? H9B C9 H9C 139.5 . 6_557 ? H9C C9 H9C 45.6 . 6_557 ? H9A C9 H9C 109.5 6_557 6_557 ? H9B C9 H9C 109.5 6_557 6_557 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sn1 C9 2.116(5) . ? Sn1 C8 2.121(6) . ? Sn1 Se1 2.6144(5) . ? Sn1 Se1 2.6144(5) 6_557 ? Se1 C1 1.899(5) . ? N1 C1 1.342(5) . ? N1 C5 1.352(5) . ? C1 C2 1.389(6) . ? C2 C3 1.377(7) . ? C2 H2 0.9300 . ? C3 C4 1.384(7) . ? C3 C6 1.502(7) . ? C4 C5 1.381(6) . ? C4 H4 0.9300 . ? C5 C7 1.484(6) . ? C6 H6A 0.9600 . ? C6 H6B 0.9600 . ? C6 H6C 0.9600 . ? C7 H7A 0.9600 . ? C7 H7B 0.9600 . ? C7 H7C 0.9600 . ? C8 H8A 0.9600 . ? C8 H8B 0.9600 . ? C8 H8C 0.9600 . ? C8 H8A 0.96(3) 6_557 ? C8 H8B 0.96(5) 6_557 ? C8 H8C 0.960(14) 6_557 ? C9 H9A 0.9600 . ? C9 H9B 0.9600 . ? C9 H9C 0.9600 . ? C9 H9A 0.960(7) 6_557 ? C9 H9B 0.96(4) 6_557 ? C9 H9C 0.96(3) 6_557 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 N1 C1 C2 -0.5(5) . . . . ? C5 N1 C1 Se1 177.8(2) . . . . ? Sn1 Se1 C1 N1 3.7(2) . . . . ? Sn1 Se1 C1 C2 -177.9(3) . . . . ? N1 C1 C2 C3 0.8(6) . . . . ? Se1 C1 C2 C3 -177.5(3) . . . . ? C1 C2 C3 C4 -0.3(6) . . . . ? C1 C2 C3 C6 178.7(4) . . . . ? C2 C3 C4 C5 -0.4(6) . . . . ? C6 C3 C4 C5 -179.4(4) . . . . ? C1 N1 C5 C4 -0.1(5) . . . . ? C1 N1 C5 C7 -179.8(3) . . . . ? C3 C4 C5 N1 0.6(6) . . . . ? C3 C4 C5 C7 -179.7(4) . . . . ?