#------------------------------------------------------------------------------ #$Date: 2021-10-15 02:06:48 +0300 (Fri, 15 Oct 2021) $ #$Revision: 269960 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/85/7708565.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708565 loop_ _publ_author_name 'Kramer, Eric' 'Yu, Shilin' 'Ward, Jas S.' 'Rissanen, Kari' _publ_section_title ; Dihypoiodites Stabilised by 4-ethylpyridine through O-I-N Halogen Bonds ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT03324G _journal_year 2021 _chemical_formula_moiety 'C22 H22 I2 N2 O4' _chemical_formula_sum 'C22 H22 I2 N2 O4' _chemical_formula_weight 632.21 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2021-03-06 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-08-24 deposited with the CCDC. 2021-10-14 downloaded from the CCDC. ; _cell_angle_alpha 94.664(4) _cell_angle_beta 95.181(4) _cell_angle_gamma 107.477(4) _cell_formula_units_Z 2 _cell_length_a 8.1534(3) _cell_length_b 9.6858(4) _cell_length_c 15.4795(8) _cell_measurement_reflns_used 3812 _cell_measurement_temperature 120.01(10) _cell_measurement_theta_max 76.6000 _cell_measurement_theta_min 2.8580 _cell_volume 1153.67(9) _computing_cell_refinement 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_data_collection 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_data_reduction 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 120.01(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 5.1977 _diffrn_detector_type Atlas _diffrn_measured_fraction_theta_full 0.993 _diffrn_measured_fraction_theta_max 0.989 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -65.00 33.00 1.00 1.00 -- -41.65 37.00 30.00 98 2 \w -107.00 -18.00 1.00 1.00 -- -41.65 -57.00 90.00 89 3 \w -65.00 31.00 1.00 1.00 -- -41.65 57.00-120.00 96 4 \w 46.00 98.00 1.00 1.00 -- 41.65-125.00 60.00 52 5 \w 89.00 134.00 1.00 1.00 -- 112.00 -45.00 30.00 45 6 \w 30.00 77.00 1.00 1.00 -- 112.00 -94.00 -60.00 47 7 \w 104.00 175.00 1.00 1.00 -- 112.00 77.00 30.00 71 8 \w 39.00 69.00 1.00 1.00 -- 112.00 -45.00 30.00 30 9 \w 61.00 116.00 1.00 1.00 -- 112.00 178.00 -60.00 55 10 \w 78.00 107.00 1.00 1.00 -- 112.00 -94.00 -60.00 29 11 \w 39.00 138.00 1.00 1.00 -- 112.00 -45.00 -90.00 99 12 \w 29.00 72.00 1.00 1.00 -- 112.00 -94.00 120.00 43 13 \w 75.00 106.00 1.00 1.00 -- 112.00 -94.00 120.00 31 14 \w 37.00 101.00 1.00 1.00 -- 112.00 -94.00 60.00 64 15 \w 40.00 83.00 1.00 1.00 -- 112.00-111.00-150.00 43 16 \w 38.00 109.00 1.00 1.00 -- 112.00-111.00 -90.00 71 17 \w 37.00 178.00 1.00 1.00 -- 112.00 0.00-180.00 141 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, Atlas' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.1898950000 _diffrn_orient_matrix_UB_12 0.0019810000 _diffrn_orient_matrix_UB_13 0.0015977000 _diffrn_orient_matrix_UB_21 -0.0253731000 _diffrn_orient_matrix_UB_22 -0.0317180000 _diffrn_orient_matrix_UB_23 -0.1002864000 _diffrn_orient_matrix_UB_31 0.0558244000 _diffrn_orient_matrix_UB_32 0.1648126000 _diffrn_orient_matrix_UB_33 -0.0076262000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0443 _diffrn_reflns_av_unetI/netI 0.0507 _diffrn_reflns_Laue_measured_fraction_full 0.993 _diffrn_reflns_Laue_measured_fraction_max 0.989 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 7530 _diffrn_reflns_point_group_measured_fraction_full 0.993 _diffrn_reflns_point_group_measured_fraction_max 0.989 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 72.128 _diffrn_reflns_theta_min 2.885 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 21.662 _exptl_absorpt_correction_T_max 0.718 _exptl_absorpt_correction_T_min 0.091 _exptl_absorpt_correction_type analytical _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.84a (Rigaku Oxford Diffraction, 2020) Analytical numeric absorption correction using a multifaceted crystal model based on expressions derived by R.C. Clark & J.S. Reid. (Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.820 _exptl_crystal_description plate _exptl_crystal_F_000 612 _exptl_crystal_recrystallization_method 'Re-crystallisation from solvent: DCM/TBME' _exptl_crystal_size_max 0.37 _exptl_crystal_size_mid 0.153 _exptl_crystal_size_min 0.016 _refine_diff_density_max 1.348 _refine_diff_density_min -1.286 _refine_diff_density_rms 0.169 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.039 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 273 _refine_ls_number_reflns 4475 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.039 _refine_ls_R_factor_all 0.0500 _refine_ls_R_factor_gt 0.0431 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0795P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1167 _refine_ls_wR_factor_ref 0.1270 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3833 _reflns_number_total 4475 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt03324g2.cif _cod_data_source_block 1 _cod_original_cell_volume 1153.66(9) _cod_database_code 7708565 _shelxl_version_number 2014/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _reflns_odcompleteness_completeness 98.85 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 71.98 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Secondary CH2 refined with riding coordinates: C7(H7A,H7B), C17(H17A,H17B) 2.b Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C5(H5), C6(H6), C12(H12), C13(H13), C15(H15), C16(H16), C23(H23), C24(H24), C25(H25), C26(H26) 2.c Idealised Me refined as rotating group: C8(H8A,H8B,H8C), C18(H18A,H18B,H18C) ; _shelx_res_file ; TITL oie020_numabs_ana_a.res in P-1 REM Old TITL OIE020_numabs_ana in P-1 REM SHELXT solution in P-1 REM R1 0.084, Rweak 0.003, Alpha 0.029, Orientation as input REM Formula found by SHELXT: C22 N2 O4 I2 CELL 1.54184 8.1534 9.6858 15.4795 94.664 95.181 107.477 ZERR 2 0.0003 0.0004 0.0008 0.004 0.004 0.004 LATT 1 SFAC C H I N O UNIT 44 44 4 4 8 L.S. 4 0 0 PLAN 20 BOND $H list 4 fmap 2 53 ACTA SHEL 50 0.81 REM REM REM WGHT 0.079500 FVAR 0.40136 I1 3 0.328653 0.230520 0.553939 11.00000 0.02467 0.02785 = 0.03475 0.00784 0.00651 0.00700 I2 3 0.449825 0.492945 0.856712 11.00000 0.02305 0.03764 = 0.03426 0.00049 0.00302 0.00814 O28 5 0.109092 0.223110 0.623143 11.00000 0.02901 0.04345 = 0.04470 0.01966 0.01302 0.01439 O29 5 0.132654 0.031875 0.691627 11.00000 0.03433 0.03342 = 0.04852 0.01346 0.01377 0.01215 O31 5 0.203731 0.326836 0.812283 11.00000 0.02313 0.04008 = 0.05414 -0.00704 -0.00216 0.01029 O32 5 0.059048 0.479504 0.852279 11.00000 0.02936 0.03708 = 0.05979 -0.00814 0.00171 0.01353 N1 4 0.558049 0.260098 0.472901 11.00000 0.02807 0.02547 = 0.03617 0.01112 0.00847 0.00612 N11 4 0.716844 0.658580 0.894707 11.00000 0.02758 0.04023 = 0.03112 0.00535 0.00472 0.00454 C2 1 0.578728 0.350814 0.409829 11.00000 0.02693 0.03459 = 0.04283 0.00994 0.00738 0.00571 AFIX 43 H2 2 0.495190 0.396119 0.397054 11.00000 -1.20000 AFIX 0 C3 1 0.718582 0.377417 0.364644 11.00000 0.03363 0.03640 = 0.04225 0.01739 0.00974 0.00899 AFIX 43 H3 2 0.730076 0.442540 0.322946 11.00000 -1.20000 AFIX 0 C4 1 0.845564 0.308808 0.379604 11.00000 0.02197 0.02996 = 0.03626 0.00315 0.00121 0.00497 C5 1 0.822350 0.216082 0.444766 11.00000 0.02812 0.03225 = 0.03761 0.00568 0.00253 0.01220 AFIX 43 H5 2 0.903347 0.168516 0.458154 11.00000 -1.20000 AFIX 0 C6 1 0.679162 0.194574 0.489602 11.00000 0.02760 0.02612 = 0.03885 0.00737 0.00330 0.00570 AFIX 43 H6 2 0.666283 0.132373 0.532958 11.00000 -1.20000 AFIX 0 C7 1 1.000702 0.341578 0.331514 11.00000 0.03178 0.03492 = 0.04786 0.00865 0.01079 0.00697 AFIX 23 H7A 2 0.965761 0.350129 0.271111 11.00000 -1.20000 H7B 2 1.048621 0.261277 0.332264 11.00000 -1.20000 AFIX 0 C8 1 1.140633 0.482455 0.371268 11.00000 0.03187 0.04101 = 0.04589 0.01161 0.00747 0.00167 AFIX 137 H8A 2 1.237686 0.499455 0.338325 11.00000 -1.50000 H8B 2 1.177543 0.473687 0.430678 11.00000 -1.50000 H8C 2 1.094415 0.562562 0.369728 11.00000 -1.50000 AFIX 0 C12 1 0.830430 0.640230 0.956853 11.00000 0.03667 0.04634 = 0.02982 0.00820 0.00949 0.01569 AFIX 43 H12 2 0.796100 0.561091 0.988614 11.00000 -1.20000 AFIX 0 C13 1 0.995829 0.733839 0.975529 11.00000 0.03041 0.04744 = 0.03714 0.00550 0.00464 0.00461 AFIX 43 H13 2 1.072561 0.717616 1.018783 11.00000 -1.20000 AFIX 0 C14 1 1.048059 0.854383 0.928667 11.00000 0.03708 0.03698 = 0.03952 0.00055 0.01013 -0.00200 C15 1 0.927181 0.872971 0.865024 11.00000 0.04707 0.04488 = 0.04852 0.01432 0.00883 0.00412 AFIX 43 H15 2 0.956293 0.952382 0.833133 11.00000 -1.20000 AFIX 0 C16 1 0.765472 0.773750 0.849730 11.00000 0.03589 0.05257 = 0.04659 0.01805 -0.00031 0.00863 AFIX 43 H16 2 0.686117 0.786532 0.806513 11.00000 -1.20000 AFIX 0 C17 1 1.234318 0.953752 0.942138 11.00000 0.03444 0.06288 = 0.06214 -0.00272 0.00426 -0.00230 AFIX 23 H17A 2 1.239057 1.048085 0.923707 11.00000 -1.20000 H17B 2 1.278379 0.967991 1.003617 11.00000 -1.20000 AFIX 0 C18 1 1.342810 0.888631 0.891093 11.00000 0.03632 0.06648 = 0.09102 0.00801 0.01490 0.00149 AFIX 137 H18A 2 1.298374 0.873986 0.830343 11.00000 -1.50000 H18B 2 1.340770 0.796700 0.910733 11.00000 -1.50000 H18C 2 1.459744 0.952914 0.899051 11.00000 -1.50000 AFIX 0 C21 1 -0.097772 0.131046 0.714814 11.00000 0.02562 0.02761 = 0.03272 0.01089 0.00767 0.00669 C22 1 -0.097069 0.248149 0.776220 11.00000 0.02511 0.02444 = 0.03645 0.01077 0.00305 0.00874 C23 1 -0.255603 0.253859 0.801415 11.00000 0.02838 0.03787 = 0.03584 0.00874 0.00712 0.01190 AFIX 43 H23 2 -0.257197 0.330592 0.841216 11.00000 -1.20000 AFIX 0 C24 1 -0.410353 0.148251 0.768662 11.00000 0.02456 0.04440 = 0.04272 0.01348 0.00536 0.01014 AFIX 43 H24 2 -0.514773 0.154569 0.785461 11.00000 -1.20000 AFIX 0 C25 1 -0.406626 0.032310 0.710041 11.00000 0.02634 0.03931 = 0.03269 0.00740 0.00373 0.00228 AFIX 43 H25 2 -0.509532 -0.040031 0.688432 11.00000 -1.20000 AFIX 0 C26 1 -0.251397 0.023156 0.683374 11.00000 0.03236 0.03797 = 0.02611 0.00312 -0.00184 0.00631 AFIX 43 H26 2 -0.250785 -0.055149 0.644564 11.00000 -1.20000 AFIX 0 C27 1 0.064451 0.124434 0.676917 11.00000 0.02838 0.02574 = 0.03323 0.00289 0.00380 0.00484 C30 1 0.064906 0.365203 0.816713 11.00000 0.02514 0.03010 = 0.03430 0.00769 0.00465 0.00909 HKLF 4 REM oie020_numabs_ana_a.res in P-1 REM R1 = 0.0431 for 3833 Fo > 4sig(Fo) and 0.0500 for all 4475 data REM 273 parameters refined using 0 restraints END WGHT 0.0795 0.0000 REM Highest difference peak 1.348, deepest hole -1.286, 1-sigma level 0.169 Q1 1 0.3281 0.2236 0.6179 11.00000 0.05 1.35 Q2 1 0.3360 0.2352 0.4865 11.00000 0.05 1.26 Q3 1 0.4380 0.4938 0.9226 11.00000 0.05 1.24 Q4 1 0.4595 0.4940 0.7878 11.00000 0.05 1.12 Q5 1 0.3384 0.3430 0.6088 11.00000 0.05 1.01 Q6 1 -0.5797 0.2587 0.8385 11.00000 0.05 0.81 Q7 1 0.4552 0.5979 0.9196 11.00000 0.05 0.80 Q8 1 1.3051 1.0819 0.9467 11.00000 0.05 0.76 Q9 1 0.7749 0.7963 0.7342 11.00000 0.05 0.75 Q10 1 1.0997 0.9431 0.9602 11.00000 0.05 0.75 Q11 1 -0.1983 0.0364 0.7457 11.00000 0.05 0.75 Q12 1 0.5768 0.5055 0.9541 11.00000 0.05 0.74 Q13 1 0.4314 0.3815 0.7962 11.00000 0.05 0.73 Q14 1 0.4162 0.3906 0.6777 11.00000 0.05 0.71 Q15 1 0.3412 0.5400 0.8795 11.00000 0.05 0.71 Q16 1 0.2113 0.2361 0.4437 11.00000 0.05 0.70 Q17 1 0.3168 0.1178 0.5003 11.00000 0.05 0.64 Q18 1 1.3414 0.6644 0.8810 11.00000 0.05 0.64 Q19 1 0.4651 0.4041 0.7862 11.00000 0.05 0.63 Q20 1 0.6069 0.4943 0.2993 11.00000 0.05 0.61 ; _shelx_res_checksum 42090 _shelx_hkl_file ; 0 0 1 193.06 9.63 0 0 1 158.78 7.67 0 0 2 113.96 8.56 0 0 3 2844.06 46.87 0 0 4 1726.82 35.80 0 0 5 31.26 4.97 0 0 6 417.86 17.89 0 0 7 1994.43 42.43 0 0 8 159.60 11.90 0 0 9 227.23 14.90 0 0 10 1409.02 39.81 0 0 11 9.13 3.57 0 0 12 392.39 22.46 0 0 12 479.78 29.53 0 0 13 319.84 20.83 0 0 13 378.69 26.63 0 0 14 219.26 19.84 0 0 15 4.60 4.09 0 0 16 39.50 7.91 0 0 17 359.21 21.05 0 0 18 1.01 1.32 0 0 19 50.36 5.33 0 -1 19 1.64 0.82 0 -1 18 32.44 5.45 0 -1 17 167.96 14.14 0 -1 16 14.91 5.12 0 1 -16 20.34 4.76 0 -1 15 28.78 7.46 0 1 -15 37.87 6.88 0 -1 14 939.31 41.39 0 1 -14 956.19 35.02 0 -1 13 156.98 14.67 0 1 -13 178.37 15.04 0 -1 13 187.23 18.72 0 -1 12 163.08 14.32 0 1 -12 205.02 15.72 0 -1 12 176.61 18.71 0 -1 11 579.60 26.04 0 -1 10 262.27 16.61 0 -1 9 353.89 18.76 0 -1 8 285.31 16.71 0 -1 7 1870.43 44.67 0 1 -6 64.67 3.97 0 -1 6 77.29 9.82 0 -1 5 2052.45 50.66 0 1 -5 1857.89 25.97 0 -1 4 7725.86 94.33 0 1 -4 7763.37 73.22 0 1 -3 2701.13 37.84 0 -1 3 2766.01 39.42 0 1 -2 1102.59 30.54 0 -1 2 881.41 15.49 0 1 -1 2035.88 20.17 0 1 -1 1968.26 17.40 0 1 0 696.81 9.01 0 1 0 689.03 9.08 0 1 1 78.60 4.45 0 1 1 64.89 3.49 0 1 2 313.91 15.15 0 1 2 297.48 7.86 0 1 2 302.36 7.12 0 1 3 1417.60 45.10 0 1 3 1228.25 24.65 0 1 4 4.25 2.43 0 1 5 80.24 7.67 0 1 6 1450.42 34.94 0 1 7 6.63 2.49 0 1 8 1327.16 36.67 0 1 9 19.22 4.55 0 1 10 652.77 27.57 0 1 11 21.88 5.37 0 1 12 225.07 15.75 0 1 12 198.44 15.94 0 1 12 225.28 20.37 0 1 13 473.10 25.36 0 1 13 516.30 24.21 0 1 14 -2.61 3.72 0 1 15 473.46 28.26 0 1 16 208.79 17.60 0 1 17 15.65 4.42 0 1 18 140.94 10.74 0 1 19 2.26 1.22 0 2 -19 35.61 4.40 0 -2 18 204.07 12.26 0 -2 17 25.85 5.12 0 2 -17 20.42 4.22 0 2 -16 62.75 8.25 0 -2 16 59.11 9.14 0 2 -15 267.70 18.36 0 -2 15 251.82 20.09 0 2 -14 89.62 10.91 0 -2 14 71.69 11.40 0 -2 13 69.80 9.80 0 -2 13 87.80 12.59 0 2 -13 74.17 9.93 0 2 -12 27.51 5.84 0 -2 12 19.46 5.20 0 -2 12 25.00 6.09 0 -2 11 1397.66 41.99 0 -2 10 18.74 4.69 0 -2 9 948.07 33.64 0 -2 8 1409.83 43.28 0 -2 7 410.44 26.89 0 2 -7 327.42 12.03 0 2 -6 1162.83 23.79 0 -2 6 1028.96 35.71 0 2 -5 1437.38 28.01 0 -2 5 1453.30 35.09 0 2 -4 2914.37 45.13 0 -2 4 3098.21 45.44 0 2 -3 33.07 5.63 0 -2 3 36.13 3.60 0 2 -2 25.87 2.45 0 2 -2 25.17 1.40 0 2 -2 26.36 5.90 0 2 -1 2591.72 24.97 0 2 -1 2489.63 28.03 0 2 0 336.77 8.69 0 2 0 313.24 12.80 0 2 0 315.81 7.58 0 2 1 5419.60 51.24 0 2 1 5285.57 61.17 0 2 2 7349.51 96.33 0 2 2 7162.80 67.16 0 2 3 72.01 4.88 0 2 3 79.12 12.06 0 2 4 1017.67 37.74 0 2 4 887.38 21.02 0 2 5 201.50 12.94 0 2 6 717.83 28.79 0 2 7 227.35 15.43 0 2 8 629.89 26.56 0 2 9 750.52 29.79 0 2 10 16.55 4.51 0 2 11 945.21 35.69 0 2 11 1015.46 35.17 0 2 12 139.35 15.62 0 2 12 118.56 11.97 0 2 13 34.67 6.61 0 2 13 31.99 8.25 0 2 14 372.68 20.56 0 2 14 402.45 26.21 0 2 15 48.52 7.02 0 2 15 48.41 9.06 0 2 16 76.90 10.23 0 2 17 18.32 4.49 0 2 18 225.51 12.21 0 3 -19 54.53 5.20 0 3 -18 24.72 4.59 0 3 -17 48.57 6.47 0 -3 17 46.13 6.14 0 -3 16 14.37 3.79 0 3 -16 39.90 6.84 0 -3 15 378.36 23.31 0 3 -15 420.66 23.47 0 -3 14 42.89 8.61 0 3 -14 61.38 9.52 0 -3 13 1075.20 43.31 0 3 -13 1166.97 41.52 0 -3 12 555.98 27.91 0 3 -12 606.70 30.16 0 -3 11 -0.51 2.54 0 -3 10 1352.26 43.50 0 -3 9 18.30 5.51 0 3 -8 1026.55 26.98 0 -3 8 1234.96 49.68 0 3 -7 737.15 22.20 0 -3 7 698.00 33.20 0 -3 6 128.20 11.41 0 3 -6 168.50 10.45 0 -3 5 1215.84 31.26 0 3 -5 1166.44 30.00 0 3 -4 14.63 1.26 0 3 -4 14.34 3.90 0 -3 4 19.29 3.47 0 3 -3 6257.96 52.99 0 -3 3 6365.03 68.53 0 3 -2 625.57 14.37 0 3 -2 640.90 11.55 0 3 -1 1.34 0.95 0 3 -1 0.39 0.61 0 3 -1 1.50 1.65 0 3 0 1469.26 30.07 0 3 0 1503.29 35.30 0 3 1 190.18 11.09 0 3 1 186.62 13.60 0 3 1 179.80 7.30 0 3 2 109.25 7.94 0 3 2 123.48 6.59 0 3 3 266.63 11.99 0 3 3 285.43 11.21 0 3 3 274.29 24.62 0 3 4 2347.90 61.61 0 3 4 2377.48 38.81 0 3 4 2218.23 38.09 0 3 5 348.73 16.34 0 3 6 23.46 5.70 0 3 7 1164.89 46.90 0 3 8 1.47 1.68 0 3 9 0.89 2.52 0 3 10 763.06 35.71 0 3 10 731.78 31.67 0 3 11 306.46 22.37 0 3 11 368.67 22.30 0 3 11 340.08 23.55 0 3 12 75.80 9.99 0 3 12 90.16 12.31 0 3 13 3.04 3.38 0 3 13 0.72 2.00 0 3 14 762.51 34.55 0 3 14 742.77 29.12 0 3 15 14.89 3.67 0 3 15 22.10 5.67 0 3 16 11.27 2.93 0 3 16 11.38 3.93 0 3 17 232.71 13.04 0 3 18 2.91 1.21 0 4 -18 -3.05 1.54 0 4 -17 472.68 19.82 0 4 -17 552.26 24.58 0 4 -16 86.07 9.62 0 4 -15 14.43 4.84 0 4 -14 457.22 25.91 0 4 -13 106.07 13.14 0 -4 12 139.45 14.25 0 4 -12 134.87 14.28 0 4 -11 43.86 7.14 0 4 -11 41.04 7.81 0 -4 11 38.02 7.35 0 -4 10 894.94 37.49 0 -4 9 593.97 33.23 0 -4 8 58.08 11.85 0 4 -8 36.38 6.02 0 4 -7 1338.06 35.71 0 -4 7 1188.02 45.45 0 4 -6 12.28 3.89 0 -4 6 22.47 5.34 0 -4 5 65.42 7.36 0 4 -5 66.10 8.19 0 -4 4 680.00 21.57 0 4 -4 668.25 30.38 0 4 -3 365.27 29.77 0 -4 3 305.54 12.61 0 4 -2 96.69 12.93 0 4 -2 109.31 6.60 0 4 -1 60.10 4.60 0 4 -1 56.33 8.88 0 4 0 3568.51 65.52 0 4 0 3250.81 40.73 0 4 1 541.83 22.40 0 4 1 554.36 39.38 0 4 1 533.96 14.80 0 4 2 381.55 13.36 0 4 2 360.04 26.86 0 4 2 351.36 16.95 0 4 3 3517.77 50.40 0 4 3 3289.36 55.28 0 4 4 5.32 1.84 0 4 4 10.13 2.84 0 4 5 31.81 5.06 0 4 6 364.09 20.15 0 4 7 1617.96 55.39 0 4 8 1.67 2.53 0 4 9 7.62 3.96 0 4 9 3.84 1.24 0 4 10 1175.11 45.12 0 4 10 1164.32 43.58 0 4 11 2.79 1.99 0 4 11 0.31 2.58 0 4 12 173.37 17.14 0 4 12 197.16 16.32 0 4 13 503.70 26.66 0 4 13 510.29 24.89 0 4 14 56.86 7.88 0 4 14 43.29 7.48 0 4 15 17.50 4.17 0 4 15 19.88 4.16 0 4 16 4.06 1.53 0 4 16 2.31 1.49 0 4 17 91.08 7.13 0 5 -18 149.40 9.08 0 5 -17 28.85 5.21 0 5 -16 0.83 1.84 0 5 -16 0.84 1.57 0 5 -15 3.71 2.89 0 5 -15 4.95 2.87 0 5 -14 423.59 27.85 0 5 -14 432.05 24.94 0 5 -13 129.72 12.20 0 5 -13 133.23 17.90 0 5 -13 119.78 13.82 0 5 -12 66.28 9.34 0 5 -12 74.29 11.02 0 5 -11 776.78 35.83 0 5 -11 766.63 32.88 0 -5 11 808.87 35.45 0 5 -10 21.74 6.21 0 5 -10 27.16 6.40 0 -5 10 26.96 6.76 0 5 -9 164.08 17.90 0 -5 9 176.06 18.75 0 5 -9 160.39 15.93 0 5 -9 140.86 17.52 0 5 -8 364.27 21.17 0 -5 8 466.55 34.15 0 5 -7 293.80 18.78 0 -5 7 256.69 22.18 0 -5 6 1.77 1.74 0 5 -6 3.64 2.02 0 -5 5 23.78 4.97 0 5 -5 22.02 5.77 0 5 -4 2223.98 70.88 0 -5 4 1956.95 42.31 0 5 -3 72.32 15.19 0 -5 3 108.44 8.21 0 5 -2 924.31 22.89 0 -5 2 941.62 23.06 0 5 -1 2951.99 42.19 0 5 -1 3184.12 75.80 0 5 0 132.53 13.77 0 5 0 116.37 7.36 0 5 1 343.23 20.65 0 5 1 318.77 12.50 0 5 2 78.13 6.55 0 5 2 74.58 9.09 0 5 3 1592.25 33.92 0 5 3 1487.02 40.41 0 5 4 166.29 13.00 0 5 7 26.57 7.32 0 5 8 570.30 32.48 0 5 8 581.61 37.10 0 5 9 219.05 20.70 0 5 9 228.15 18.54 0 5 10 142.99 15.70 0 5 11 109.24 12.67 0 5 12 3.18 3.02 0 5 13 266.91 16.98 0 5 14 3.15 1.55 0 5 15 157.63 10.03 0 5 15 144.38 11.48 0 5 16 101.17 7.69 0 6 -17 1.48 0.94 0 6 -16 96.49 9.67 0 6 -15 317.29 18.06 0 6 -15 309.76 19.92 0 6 -14 -1.85 2.15 0 6 -14 7.91 3.28 0 6 -14 6.92 3.65 0 6 -13 84.57 14.33 0 6 -13 83.69 10.11 0 6 -13 79.58 10.48 0 6 -12 11.94 5.18 0 6 -12 22.64 10.65 0 6 -12 14.15 4.71 0 6 -11 485.35 26.96 0 6 -11 402.24 36.11 0 6 -11 442.47 28.03 0 6 -10 1.64 2.84 0 6 -10 5.30 3.79 0 6 -10 5.80 2.59 0 6 -9 177.09 19.59 0 6 -9 200.24 19.68 0 6 -8 820.03 36.13 0 6 -8 796.94 39.02 0 6 -7 5.92 3.63 0 6 -7 -0.58 1.99 0 6 -7 2.14 2.16 0 6 -6 718.49 34.91 0 6 -5 628.50 35.71 0 6 -4 339.06 34.13 0 6 -3 238.47 28.09 0 6 -2 18.76 7.60 0 6 -1 849.38 42.96 0 6 0 134.14 15.62 0 6 1 965.63 39.94 0 6 2 1403.80 46.20 0 6 3 2.98 2.19 0 6 5 52.50 9.43 0 6 5 47.88 9.27 0 6 5 62.10 14.39 0 6 6 128.11 21.71 0 6 6 120.41 17.28 0 6 6 114.78 15.68 0 6 7 158.35 19.39 0 6 7 183.52 22.64 0 6 7 189.24 25.97 0 6 8 86.66 12.93 0 6 8 98.62 20.18 0 6 8 93.26 15.16 0 6 9 362.71 26.66 0 6 9 370.50 23.70 0 6 10 6.92 2.89 0 6 10 5.27 3.78 0 6 10 4.68 3.95 0 6 11 274.44 22.96 0 6 11 317.85 20.95 0 6 12 117.26 13.50 0 6 12 129.78 12.05 0 6 13 -0.20 1.87 0 6 13 -0.89 1.93 0 6 14 177.33 12.25 0 6 14 199.06 11.53 0 6 15 0.97 1.08 0 7 -16 1.94 1.09 0 7 -15 58.58 7.19 0 7 -14 -0.71 1.55 0 7 -14 -0.91 1.90 0 7 -14 1.41 1.76 0 7 -13 115.70 11.43 0 7 -13 138.43 16.45 0 7 -13 112.82 11.38 0 7 -12 290.74 20.53 0 7 -12 333.96 20.98 0 7 -11 21.91 6.67 0 7 -11 28.33 6.83 0 7 -11 21.25 8.24 0 7 -10 574.45 40.39 0 7 -10 545.13 30.81 0 7 -10 465.42 33.55 0 7 -9 104.49 15.72 0 7 -9 100.28 14.41 0 7 -8 89.29 17.91 0 7 -8 51.04 9.69 0 7 -7 308.80 24.66 0 7 -7 231.75 26.65 0 7 -7 286.33 20.97 0 7 -7 276.61 21.61 0 7 -7 291.98 21.51 0 7 -6 21.47 7.20 0 7 -6 23.32 6.67 0 7 -6 20.57 5.59 0 7 -6 20.26 7.22 0 7 -6 24.46 5.93 0 7 -5 245.95 22.53 0 7 -5 202.66 16.77 0 7 -5 261.66 26.76 0 7 -5 207.03 18.25 0 7 -5 212.86 16.69 0 7 -4 37.28 8.55 0 7 -4 36.84 10.37 0 7 -4 27.03 11.43 0 7 -4 41.54 8.13 0 7 -4 36.02 6.87 0 7 -4 29.42 5.81 0 7 -3 1080.96 38.05 0 7 -3 1253.38 43.21 0 7 -3 1228.65 43.88 0 7 -3 1184.37 66.57 0 7 -3 1079.79 63.73 0 7 -2 605.81 52.87 0 7 -2 696.44 46.17 0 7 -2 704.02 30.41 0 7 -2 685.19 32.35 0 7 -1 16.26 4.95 0 7 -1 13.62 4.30 0 7 -1 14.82 6.47 0 7 -1 21.33 10.51 0 7 0 1326.89 42.35 0 7 0 1395.99 46.38 0 7 0 1316.88 43.52 0 7 1 41.48 7.73 0 7 1 36.35 8.52 0 7 1 39.46 7.88 0 7 1 51.47 9.05 0 7 2 31.55 7.71 0 7 2 36.01 7.08 0 7 2 26.92 7.58 0 7 2 29.41 6.60 0 7 3 207.60 18.66 0 7 3 225.31 17.79 0 7 3 235.24 18.67 0 7 3 249.72 23.03 0 7 4 566.25 31.51 0 7 4 517.63 29.36 0 7 5 392.50 39.90 0 7 5 348.17 26.55 0 7 5 312.63 24.87 0 7 6 20.47 8.11 0 7 6 16.57 6.19 0 7 6 16.13 5.97 0 7 7 561.24 35.35 0 7 7 606.56 44.01 0 7 7 505.96 40.51 0 7 8 84.73 17.50 0 7 8 85.83 13.91 0 7 8 110.66 13.83 0 7 9 -1.62 2.24 0 7 9 -1.92 1.58 0 7 10 376.49 23.21 0 7 10 304.28 17.92 0 7 10 323.84 24.53 0 7 11 10.58 4.40 0 7 11 9.81 3.59 0 7 12 2.72 2.11 0 7 13 5.16 2.14 0 8 -14 205.91 12.62 0 8 -14 219.68 12.15 0 8 -13 16.77 4.66 0 8 -13 14.54 3.73 0 8 -12 1.88 1.37 0 8 -12 7.59 4.95 0 8 -11 72.83 13.21 0 8 -11 98.64 11.86 0 8 -10 198.40 20.33 0 8 -10 256.88 21.36 0 8 -9 224.71 23.27 0 8 -9 177.56 18.50 0 8 -8 21.31 10.82 0 8 -8 7.45 3.76 0 8 -7 670.06 32.65 0 8 -7 655.39 32.77 0 8 -6 30.68 8.79 0 8 -6 29.01 6.64 0 8 -6 36.79 7.65 0 8 -6 25.77 6.54 0 8 -5 53.49 9.67 0 8 -5 46.06 8.06 0 8 -5 57.58 11.21 0 8 -4 845.07 35.05 0 8 -4 890.13 38.71 0 8 -4 808.11 39.48 0 8 -3 3.62 2.91 0 8 -3 5.19 3.21 0 8 -3 4.06 2.78 0 8 -3 0.46 2.87 0 8 -2 -0.76 1.72 0 8 -2 -0.80 3.14 0 8 -2 3.03 2.76 0 8 -2 -5.01 2.85 0 8 -1 25.91 5.84 0 8 -1 25.12 9.76 0 8 -1 26.06 7.06 0 8 -1 23.60 5.61 0 8 0 1030.80 53.09 0 8 0 983.88 42.35 0 8 0 939.80 38.83 0 8 0 944.01 37.32 0 8 1 25.29 7.92 0 8 1 16.33 5.12 0 8 1 20.47 5.60 0 8 2 2.04 1.44 0 8 2 -1.47 2.81 0 8 3 901.22 39.52 0 8 3 1027.42 52.44 0 8 4 33.39 7.97 0 8 4 62.60 16.19 0 8 5 61.69 11.75 0 8 5 82.52 17.87 0 8 6 223.71 24.04 0 8 6 222.39 23.66 0 8 7 72.75 11.59 0 8 7 90.80 17.90 0 8 8 -0.98 3.83 0 8 8 -5.88 3.08 0 8 9 1.26 2.10 0 8 9 -1.20 2.36 0 8 10 164.40 14.02 0 8 10 168.22 11.05 0 8 11 2.09 1.77 0 8 12 40.75 4.60 0 9 -13 24.51 4.00 0 9 -12 8.64 2.71 0 9 -11 241.79 16.41 0 9 -10 23.68 6.60 0 9 -9 181.95 20.68 0 9 -8 248.46 27.75 0 9 -7 17.05 7.00 0 9 -6 -2.99 2.26 0 9 -6 1.36 1.82 0 9 -6 -2.83 3.13 0 9 -5 7.90 5.02 0 9 -5 1.58 2.07 0 9 -5 -1.17 2.91 0 9 -5 2.30 2.63 0 9 -4 292.22 20.29 0 9 -4 285.43 19.90 0 9 -4 289.64 22.97 0 9 -4 279.33 22.47 0 9 -3 -0.02 1.25 0 9 -3 3.63 3.76 0 9 -3 1.77 1.48 0 9 -3 4.06 2.44 0 9 -2 150.52 16.38 0 9 -2 121.04 13.44 0 9 -2 137.54 14.27 0 9 -2 142.97 13.94 0 9 -1 929.80 41.74 0 9 -1 939.35 36.62 0 9 -1 886.14 37.38 0 9 0 16.37 4.51 0 9 0 24.40 7.68 0 9 1 75.93 10.75 0 9 1 89.30 13.41 0 9 2 100.96 16.04 0 9 2 99.77 12.36 0 9 3 19.88 6.01 0 9 3 19.90 9.02 0 9 4 -5.14 8.27 0 9 4 4.85 3.14 0 9 5 4.60 4.02 0 9 5 11.24 4.70 0 9 6 367.77 25.03 0 9 6 451.12 34.65 0 9 7 13.40 4.37 0 9 7 5.12 3.14 0 9 8 125.42 10.56 0 9 8 122.12 12.20 0 9 9 133.44 8.62 0 9 9 122.16 10.06 0 10 -11 19.09 3.67 0 10 -10 5.99 2.67 0 10 -9 14.80 5.65 0 10 -8 276.60 25.58 0 10 -8 210.09 16.48 0 10 -7 9.78 4.38 0 10 -7 12.23 3.91 0 10 -6 170.95 14.25 0 10 -6 182.82 18.04 0 10 -5 301.16 18.88 0 10 -5 300.48 22.37 0 10 -4 12.64 3.00 0 10 -4 16.71 4.42 0 10 -4 9.35 3.73 0 10 -4 19.51 6.03 0 10 -3 126.55 12.63 0 10 -3 116.92 11.34 0 10 -3 114.79 11.55 0 10 -3 141.62 15.07 0 10 -2 156.79 13.39 0 10 -2 149.41 13.25 0 10 -2 166.19 16.47 0 10 -1 16.24 5.80 0 10 -1 14.53 4.13 0 10 0 2.15 2.13 0 10 0 1.17 2.80 0 10 1 96.02 14.03 0 10 1 73.78 9.71 0 10 2 381.73 30.22 0 10 2 304.78 20.66 0 10 3 2.95 3.74 0 10 4 189.97 18.84 0 10 5 112.26 11.96 0 10 6 6.81 2.64 0 10 7 153.13 9.58 0 11 -1 8.07 3.42 0 11 0 372.71 23.38 0 11 1 61.45 10.58 0 11 2 -0.64 2.01 0 11 3 68.26 8.26 0 11 4 54.75 6.11 -1 11 5 73.45 7.60 -1 11 4 91.53 10.18 -1 11 3 -4.20 3.56 -1 11 2 68.76 11.44 -1 11 1 64.82 9.89 -1 11 0 51.66 8.20 -1 11 -1 2.42 2.78 -1 11 -2 45.58 7.34 -1 11 -3 292.48 18.00 -1 11 -4 7.14 2.94 -1 11 -5 64.55 8.20 -1 11 -6 83.29 9.27 -1 11 -7 -2.27 2.56 -1 11 -8 21.27 4.60 -1 10 8 62.54 6.28 -1 10 7 1.98 1.47 -1 10 6 61.60 9.01 -1 10 5 -0.91 2.71 -1 10 4 141.53 19.94 -1 10 3 -1.66 4.70 -1 10 2 121.98 15.91 -1 10 1 437.31 28.13 -1 10 0 1.60 2.00 -1 10 0 5.33 3.32 -1 10 -1 368.75 24.73 -1 10 -1 354.80 22.10 -1 10 -2 167.12 16.32 -1 10 -2 166.05 15.26 -1 10 -3 4.18 2.33 -1 10 -3 4.38 3.75 -1 10 -3 2.96 2.17 -1 10 -4 14.89 5.00 -1 10 -4 12.23 4.41 -1 10 -4 9.47 4.12 -1 10 -5 67.53 9.57 -1 10 -5 55.90 10.37 -1 10 -5 62.92 9.68 -1 10 -6 141.04 14.36 -1 10 -6 128.07 16.61 -1 10 -7 -1.35 2.64 -1 10 -7 -4.16 3.38 -1 10 -8 221.07 18.41 -1 10 -8 247.29 26.88 -1 10 -9 178.40 17.60 -1 10 -9 128.64 14.11 -1 10 -10 12.47 3.72 -1 10 -10 13.85 5.20 -1 10 -11 165.98 11.50 -1 10 -11 188.81 13.06 -1 9 10 67.32 6.26 -1 9 10 88.92 7.25 -1 9 9 8.01 2.48 -1 9 9 10.83 3.17 -1 9 8 103.36 11.26 -1 9 8 86.68 10.99 -1 9 7 5.74 4.08 -1 9 7 5.09 3.49 -1 9 6 335.58 28.60 -1 9 6 299.93 25.00 -1 9 5 296.13 23.93 -1 9 5 271.39 29.25 -1 9 4 -0.18 3.77 -1 9 4 -3.80 2.67 -1 9 3 546.59 36.87 -1 9 3 456.81 25.73 -1 9 2 36.42 6.85 -1 9 2 29.01 8.14 -1 9 1 1.18 2.32 -1 9 1 -1.27 4.42 -1 9 0 213.71 19.61 -1 9 0 207.11 18.14 -1 9 -1 75.63 10.89 -1 9 -1 86.08 11.59 -1 9 -1 77.43 11.58 -1 9 -2 106.16 13.63 -1 9 -2 117.34 14.49 -1 9 -2 113.95 13.24 -1 9 -3 15.69 5.78 -1 9 -3 13.46 4.69 -1 9 -3 14.27 4.79 -1 9 -4 754.73 34.50 -1 9 -4 752.54 35.48 -1 9 -4 754.83 39.67 -1 9 -5 95.20 15.02 -1 9 -5 112.81 12.93 -1 9 -6 3.36 4.40 -1 9 -7 255.20 27.62 -1 9 -8 4.19 4.10 -1 9 -8 7.01 7.16 -1 9 -9 1.41 3.29 -1 9 -9 3.54 3.34 -1 9 -10 15.10 4.91 -1 9 -10 20.09 6.80 -1 9 -11 253.81 24.62 -1 9 -11 184.83 14.72 -1 9 -12 60.70 9.20 -1 9 -12 45.17 6.42 -1 9 -13 31.51 4.65 -1 8 12 28.52 4.17 -1 8 11 -4.38 2.28 -1 8 11 -0.24 1.31 -1 8 10 317.45 19.40 -1 8 10 270.92 19.38 -1 8 10 303.19 17.59 -1 8 9 36.29 7.05 -1 8 9 28.66 6.86 -1 8 9 34.80 7.95 -1 8 8 4.62 4.08 -1 8 8 2.13 5.46 -1 8 8 7.69 3.63 -1 8 7 261.46 23.60 -1 8 7 257.91 26.15 -1 8 7 322.95 31.21 -1 8 6 0.16 3.13 -1 8 6 1.39 3.10 -1 8 6 -0.15 2.79 -1 8 5 -0.68 3.21 -1 8 5 -2.22 2.70 -1 8 5 6.49 6.11 -1 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1.92 1 4 15 106.85 8.80 1 4 16 82.05 7.42 1 5 -17 14.77 3.32 1 5 -17 14.40 3.28 1 5 -16 18.95 4.59 1 5 -16 19.28 4.34 1 5 -15 206.84 15.45 1 5 -15 199.02 16.52 1 5 -14 5.87 2.50 1 5 -14 2.86 2.33 1 5 -13 -0.14 1.37 1 5 -13 2.21 2.18 1 5 -13 -0.03 3.48 1 5 -12 2.85 2.43 1 5 -12 6.30 2.76 1 5 -12 5.92 3.31 1 5 -11 657.70 30.71 1 5 -11 637.68 31.22 1 5 -10 124.41 13.50 1 5 -10 80.65 13.87 1 5 -9 287.71 19.67 1 5 -9 298.33 21.66 1 5 -9 244.46 21.61 1 5 -8 1372.42 43.98 1 5 -8 1479.63 54.11 1 5 -7 7.99 3.96 1 5 -6 145.93 14.52 1 5 -5 474.00 28.67 1 5 -4 486.20 36.49 1 5 -3 132.23 19.39 1 5 -2 21.41 6.92 1 5 -1 2385.33 68.87 1 5 0 31.82 7.30 1 5 0 36.17 7.93 1 5 1 1091.40 49.93 1 5 1 1132.68 39.84 1 5 2 1148.29 62.75 1 5 2 1406.45 41.60 1 5 3 91.26 9.81 1 5 3 82.84 18.44 1 5 4 137.85 19.54 1 5 6 502.43 35.21 1 5 7 -9.20 8.93 1 5 8 9.87 5.18 1 5 9 313.18 24.78 1 5 10 2.52 3.01 1 5 11 312.05 20.65 1 5 12 49.44 7.51 1 5 13 1.29 1.43 1 5 13 4.10 3.03 1 5 14 37.97 6.16 1 5 15 11.74 2.74 1 6 -16 13.54 3.17 1 6 -16 15.97 3.31 1 6 -15 215.37 12.47 1 6 -15 214.52 14.29 1 6 -15 216.34 15.11 1 6 -14 13.10 4.03 1 6 -14 17.61 4.97 1 6 -14 10.74 3.48 1 6 -13 244.21 22.88 1 6 -13 249.82 17.19 1 6 -13 222.45 16.78 1 6 -12 571.71 28.26 1 6 -12 503.39 26.84 1 6 -11 1.27 2.09 1 6 -11 -1.12 2.26 1 6 -11 3.41 2.77 1 6 -10 178.87 18.01 1 6 -10 146.57 17.83 1 6 -10 159.23 16.18 1 6 -9 35.58 8.30 1 6 -9 37.35 9.73 1 6 -9 44.05 9.65 1 6 -8 393.34 25.53 1 6 -8 406.23 26.91 1 6 -8 445.61 27.05 1 6 -7 24.64 8.88 1 6 -7 11.93 3.55 1 6 -7 11.62 4.18 1 6 -7 14.34 5.27 1 6 -6 339.19 27.77 1 6 -6 414.87 24.20 1 6 -6 426.13 25.82 1 6 -6 417.38 27.47 1 6 -5 1058.54 49.78 1 6 -4 7.03 6.25 1 6 -3 832.53 50.84 1 6 -2 500.57 35.54 1 6 -1 193.28 20.80 1 6 0 365.84 26.51 1 6 1 21.98 6.01 1 6 2 684.72 32.23 1 6 3 6.10 4.23 1 6 3 4.43 1.78 1 6 3 7.32 4.00 1 6 3 5.54 2.46 1 6 4 301.84 21.67 1 6 4 322.90 23.78 1 6 4 336.07 29.62 1 6 5 878.38 42.19 1 6 5 863.87 41.77 1 6 5 989.30 63.25 1 6 6 152.17 21.55 1 6 6 157.05 21.10 1 6 6 156.33 19.19 1 6 7 715.70 38.46 1 6 7 774.65 49.56 1 6 7 716.35 52.27 1 6 8 26.48 11.96 1 6 8 34.59 9.58 1 6 8 35.94 7.20 1 6 9 11.72 4.97 1 6 9 13.81 6.86 1 6 10 60.50 9.65 1 6 10 56.81 11.00 1 6 11 98.34 10.86 1 6 11 91.90 12.59 1 6 12 77.33 10.09 1 6 13 1.15 1.34 1 6 14 167.93 10.32 1 7 -15 4.33 1.83 1 7 -15 2.39 1.26 1 7 -14 124.53 10.05 1 7 -14 139.76 11.49 1 7 -14 148.44 11.09 1 7 -13 0.90 1.37 1 7 -13 -2.53 2.46 1 7 -12 48.24 7.99 1 7 -12 68.45 9.35 1 7 -12 62.41 12.42 1 7 -11 17.89 5.17 1 7 -11 20.28 7.22 1 7 -11 18.97 4.84 1 7 -10 314.76 24.99 1 7 -10 378.41 25.64 1 7 -9 226.39 20.10 1 7 -9 282.16 25.20 1 7 -8 47.41 9.44 1 7 -8 51.29 9.46 1 7 -8 71.89 16.76 1 7 -7 835.25 35.00 1 7 -7 838.04 37.51 1 7 -6 141.53 14.77 1 7 -6 130.25 16.92 1 7 -6 130.15 18.03 1 7 -6 128.93 15.82 1 7 -5 23.10 7.17 1 7 -5 19.44 6.57 1 7 -5 19.02 5.37 1 7 -4 349.25 24.61 1 7 -4 369.58 25.16 1 7 -4 364.18 23.29 1 7 -3 61.76 10.22 1 7 -3 73.02 15.50 1 7 -3 60.79 9.53 1 7 -2 182.54 16.38 1 7 -2 164.06 22.06 1 7 -2 159.41 16.28 1 7 -1 29.18 6.65 1 7 -1 27.65 6.85 1 7 -1 29.63 9.12 1 7 0 773.95 42.35 1 7 0 723.32 35.77 1 7 0 802.09 36.19 1 7 1 496.32 31.75 1 7 1 491.30 29.97 1 7 1 497.50 28.90 1 7 2 214.47 19.01 1 7 2 206.28 20.59 1 7 2 201.93 19.11 1 7 3 554.18 37.87 1 7 3 491.13 29.54 1 7 4 23.27 9.29 1 7 4 9.88 4.88 1 7 5 18.65 6.97 1 7 5 5.85 4.05 1 7 6 103.70 16.45 1 7 6 105.77 16.33 1 7 7 294.32 22.76 1 7 7 344.07 34.31 1 7 8 24.71 8.94 1 7 8 35.08 6.83 1 7 9 1.95 2.34 1 7 10 324.31 22.39 1 7 11 1.29 1.78 1 7 12 0.46 1.09 1 7 13 142.77 8.50 1 8 -14 165.34 10.15 1 8 -13 80.55 8.20 1 8 -12 51.37 7.38 1 8 -11 391.13 28.27 1 8 -11 355.48 21.51 1 8 -10 27.69 7.27 1 8 -10 21.81 6.16 1 8 -9 6.10 4.50 1 8 -8 67.51 15.09 1 8 -7 228.43 19.48 1 8 -7 176.81 21.53 1 8 -6 199.55 17.98 1 8 -6 197.78 19.10 1 8 -6 189.88 20.64 1 8 -5 4.39 2.97 1 8 -5 -0.79 1.91 1 8 -5 2.56 3.91 1 8 -4 531.93 29.60 1 8 -4 536.14 30.50 1 8 -4 573.09 32.28 1 8 -3 73.45 11.70 1 8 -3 78.32 10.68 1 8 -3 90.44 12.14 1 8 -2 84.56 12.52 1 8 -1 249.32 20.50 1 8 -1 241.75 21.41 1 8 0 38.22 8.80 1 8 0 18.47 5.16 1 8 1 2.00 2.16 1 8 1 5.95 4.17 1 8 2 4.48 3.18 1 8 2 4.52 3.12 1 8 3 494.79 40.70 1 8 3 415.43 27.41 1 8 4 19.87 11.41 1 8 4 13.98 5.57 1 8 5 26.17 8.94 1 8 5 23.68 8.11 1 8 6 698.23 44.00 1 8 6 642.30 34.38 1 8 7 3.49 1.85 1 8 7 5.49 4.20 1 8 8 89.44 9.15 1 8 8 85.89 12.54 1 8 9 113.38 12.02 1 8 10 45.90 6.41 1 8 11 1.98 1.42 1 9 -13 6.33 1.99 1 9 -12 27.78 4.58 1 9 -11 119.70 10.87 1 9 -10 17.41 5.25 1 9 -9 5.47 4.59 1 9 -8 348.81 30.12 1 9 -7 29.23 7.91 1 9 -6 118.66 13.53 1 9 -6 112.53 14.84 1 9 -5 284.51 20.90 1 9 -5 250.41 20.81 1 9 -5 292.03 22.45 1 9 -4 3.86 2.96 1 9 -4 3.41 3.07 1 9 -4 2.90 1.89 1 9 -3 14.21 5.15 1 9 -3 9.19 4.71 1 9 -2 -1.78 2.45 1 9 -2 3.86 3.76 1 9 -1 220.20 20.10 1 9 -1 207.83 18.31 1 9 0 2.71 3.33 1 9 1 165.27 16.02 1 9 1 164.40 19.63 1 9 2 925.23 51.73 1 9 2 789.98 35.90 1 9 3 -1.75 2.50 1 9 3 10.21 7.17 1 9 4 179.56 20.56 1 9 4 225.42 20.70 1 9 5 81.88 13.82 1 9 5 67.20 10.44 1 9 6 47.45 7.15 1 9 6 44.06 9.14 1 9 7 22.48 4.17 1 9 7 24.77 5.72 1 9 8 5.19 2.11 1 9 9 113.66 7.85 1 10 -10 74.12 7.78 1 10 -9 93.18 11.61 1 10 -8 5.35 4.06 1 10 -7 5.45 2.94 1 10 -6 45.30 7.44 1 10 -5 158.18 13.41 1 10 -4 12.92 3.89 1 10 -3 243.61 16.96 1 10 -3 240.68 18.90 1 10 -2 211.87 18.15 1 10 -2 164.80 13.92 1 10 -1 0.24 3.54 1 10 -1 0.37 2.41 1 10 0 252.88 21.71 1 10 0 192.34 15.36 1 10 1 17.18 4.85 1 10 1 15.63 6.67 1 10 2 32.50 10.31 1 10 2 34.32 6.96 1 10 3 21.80 5.97 1 10 3 18.45 5.47 1 10 4 84.91 9.71 1 10 4 67.22 10.04 1 10 5 111.46 9.03 1 10 5 65.01 7.81 -2 11 6 3.31 1.83 -2 11 5 5.36 2.98 -2 11 4 157.38 15.40 -2 11 3 2.87 2.80 -2 11 2 47.13 9.08 -2 11 1 126.02 13.18 -2 11 0 0.68 2.44 -2 11 -1 126.83 11.99 -2 11 -2 31.57 5.60 -2 11 -2 38.85 7.39 -2 11 -3 43.27 7.67 -2 11 -3 37.00 5.72 -2 11 -4 2.43 2.42 -2 11 -5 72.62 9.83 -2 11 -6 219.35 16.86 -2 11 -7 4.60 2.82 -2 11 -8 118.52 12.84 -2 11 -9 90.87 10.32 -2 10 9 23.32 3.64 -2 10 8 129.71 10.58 -2 10 7 -0.90 1.53 -2 10 6 121.12 13.65 -2 10 5 124.25 16.35 -2 10 4 0.78 3.44 -2 10 3 112.09 15.88 -2 10 2 1.92 2.65 -2 10 1 170.64 16.21 -2 10 1 162.36 16.60 -2 10 0 0.78 2.29 -2 10 0 4.59 2.41 -2 10 -1 382.83 24.26 -2 10 -1 410.54 25.16 -2 10 -2 440.41 26.31 -2 10 -2 394.27 24.14 -2 10 -3 27.79 6.32 -2 10 -3 27.58 6.87 -2 10 -4 534.07 29.25 -2 10 -5 45.13 10.77 -2 10 -5 42.46 8.37 -2 10 -6 8.59 5.08 -2 10 -6 5.35 3.53 -2 10 -7 94.77 17.11 -2 10 -7 111.63 13.81 -2 10 -8 32.44 10.71 -2 10 -8 23.66 6.40 -2 10 -9 50.38 9.01 -2 10 -9 41.11 8.68 -2 10 -10 8.10 4.15 -2 10 -11 274.35 18.25 -2 10 -12 62.90 6.27 -2 9 11 4.51 1.72 -2 9 10 201.90 12.66 -2 9 9 62.14 8.38 -2 9 8 -1.93 3.42 -2 9 7 180.52 18.40 -2 9 6 25.94 8.65 -2 9 5 116.65 20.38 -2 9 4 2.99 3.56 -2 9 3 693.57 38.99 -2 9 2 112.62 14.67 -2 9 2 127.28 19.17 -2 9 2 129.65 15.01 -2 9 1 4.18 3.29 -2 9 1 4.08 3.16 -2 9 1 5.72 5.86 -2 9 0 509.23 40.78 -2 9 0 499.42 29.27 -2 9 0 491.92 29.01 -2 9 -1 -0.52 7.38 -2 9 -1 3.39 2.76 -2 9 -1 5.66 4.65 -2 9 -2 34.68 12.84 -2 9 -2 37.01 7.60 -2 9 -2 37.63 8.69 -2 9 -2 38.73 8.10 -2 9 -3 482.62 47.30 -2 9 -3 454.95 31.26 -2 9 -3 409.25 24.71 -2 9 -3 417.23 26.38 -2 9 -4 84.61 14.46 -2 9 -4 60.51 13.57 -2 9 -4 81.14 11.80 -2 9 -5 62.47 13.04 -2 9 -5 61.45 12.05 -2 9 -6 25.89 7.85 -2 9 -6 27.43 10.55 -2 9 -7 391.67 38.27 -2 9 -7 520.87 32.06 -2 9 -8 39.93 12.88 -2 9 -8 32.31 8.47 -2 9 -9 51.88 10.79 -2 9 -9 61.02 11.84 -2 9 -10 189.12 17.05 -2 9 -10 202.30 21.99 -2 9 -11 1.29 3.35 -2 9 -11 -0.74 1.94 -2 9 -12 2.48 2.45 -2 9 -13 2.74 1.72 -2 8 12 0.14 1.27 -2 8 12 0.58 1.17 -2 8 11 93.76 9.60 -2 8 11 95.51 9.42 -2 8 10 81.65 9.96 -2 8 10 66.86 9.06 -2 8 9 34.90 7.63 -2 8 9 39.02 8.08 -2 8 8 0.83 2.17 -2 8 8 5.14 3.06 -2 8 7 514.55 34.78 -2 8 7 476.03 35.51 -2 8 6 28.00 11.28 -2 8 6 30.98 8.70 -2 8 5 24.04 6.69 -2 8 5 23.32 10.33 -2 8 4 516.46 31.17 -2 8 4 512.56 36.67 -2 8 4 571.64 36.86 -2 8 3 21.01 7.75 -2 8 3 23.51 7.61 -2 8 3 19.89 7.11 -2 8 3 25.64 6.63 -2 8 2 62.74 10.47 -2 8 2 62.77 10.75 -2 8 2 87.18 18.12 -2 8 2 68.98 13.42 -2 8 1 116.37 14.21 -2 8 1 129.05 14.54 -2 8 1 139.52 18.59 -2 8 0 614.98 31.75 -2 8 0 532.74 29.45 -2 8 0 666.39 38.42 -2 8 0 602.45 31.64 -2 8 0 687.59 43.01 -2 8 -1 58.94 9.50 -2 8 -1 55.82 9.66 -2 8 -1 60.11 9.85 -2 8 -1 60.11 13.26 -2 8 -1 68.02 11.59 -2 8 -2 137.00 22.75 -2 8 -2 137.57 14.25 -2 8 -2 124.58 15.57 -2 8 -3 968.57 37.64 -2 8 -3 1174.28 71.07 -2 8 -3 1138.21 48.59 -2 8 -4 130.16 18.42 -2 8 -4 166.67 19.67 -2 8 -4 137.30 14.91 -2 8 -5 379.84 28.14 -2 8 -5 396.70 25.94 -2 8 -5 454.91 34.94 -2 8 -6 372.10 26.06 -2 8 -6 354.70 25.63 -2 8 -6 356.72 33.35 -2 8 -7 126.39 16.15 -2 8 -7 117.58 22.36 -2 8 -8 9.36 7.30 -2 8 -8 1.17 2.07 -2 8 -9 -0.82 2.44 -2 8 -9 6.23 4.73 -2 8 -10 280.32 21.87 -2 8 -10 241.02 25.58 -2 8 -11 3.39 4.99 -2 8 -11 1.70 1.91 -2 8 -12 130.31 17.97 -2 8 -12 96.43 10.56 -2 8 -13 459.26 20.03 -2 8 -13 502.60 27.13 -2 8 -14 4.22 1.96 -2 8 -15 40.23 4.64 -2 8 -15 51.71 5.62 -2 7 14 50.77 5.54 -2 7 13 1.04 1.32 -2 7 13 0.88 1.25 -2 7 12 3.98 2.15 -2 7 12 2.12 1.99 -2 7 12 1.90 1.65 -2 7 11 491.48 25.58 -2 7 11 486.59 24.38 -2 7 10 28.24 6.89 -2 7 10 20.52 5.66 -2 7 10 17.96 5.86 -2 7 9 160.16 17.13 -2 7 9 150.75 16.51 -2 7 8 412.15 29.87 -2 7 8 494.54 32.07 -2 7 7 39.69 10.72 -2 7 7 47.36 12.62 -2 7 6 132.67 18.62 -2 7 6 150.12 23.48 -2 7 5 22.93 9.73 -2 7 5 15.78 5.93 -2 7 5 19.15 6.29 -2 7 5 21.12 5.55 -2 7 4 684.55 33.05 -2 7 4 633.28 34.87 -2 7 4 738.65 39.92 -2 7 4 593.74 28.58 -2 7 4 711.31 30.77 -2 7 4 682.27 36.80 -2 7 3 -1.79 4.38 -2 7 3 -5.38 3.36 -2 7 3 2.21 2.51 -2 7 3 6.29 2.95 -2 7 2 402.61 24.73 -2 7 2 373.05 26.34 -2 7 2 415.68 24.36 -2 7 2 420.63 21.95 -2 7 1 1378.36 40.02 -2 7 0 114.61 11.00 -2 7 -1 453.08 21.41 -2 7 -2 235.29 15.44 -2 7 -3 77.97 9.17 2 -7 3 87.64 9.62 2 -7 4 396.77 21.63 -2 7 -4 450.53 30.33 -2 7 -4 395.70 23.97 -2 7 -4 403.06 30.10 -2 7 -5 1.88 2.00 2 -7 5 2.74 2.01 -2 7 -5 8.12 3.95 -2 7 -5 6.70 2.93 2 -7 6 560.50 29.24 -2 7 -6 507.31 29.73 2 -7 7 6.60 2.72 -2 7 -7 0.61 3.98 -2 7 -7 8.37 3.85 2 -7 8 526.23 33.59 -2 7 -8 630.41 37.92 -2 7 -8 617.46 43.61 -2 7 -9 373.12 27.75 -2 7 -9 377.49 31.25 -2 7 -10 5.88 4.00 -2 7 -10 -1.72 3.49 -2 7 -11 139.73 14.41 -2 7 -11 138.94 21.58 -2 7 -12 100.57 11.30 -2 7 -12 130.01 20.51 -2 7 -13 24.82 7.20 -2 7 -14 2.19 1.84 -2 7 -15 135.97 11.26 -2 7 -16 77.38 6.98 -2 6 16 22.03 2.97 -2 6 15 214.92 11.68 -2 6 15 157.32 9.84 -2 6 14 0.55 1.74 -2 6 14 1.19 0.95 -2 6 13 104.21 10.77 -2 6 13 102.92 9.99 -2 6 12 136.40 13.46 -2 6 12 118.60 11.80 -2 6 11 53.74 9.62 -2 6 11 57.83 9.11 -2 6 10 153.77 16.44 -2 6 10 169.39 16.73 -2 6 9 36.94 8.98 -2 6 9 26.84 7.47 -2 6 8 451.60 30.75 -2 6 8 597.45 42.67 -2 6 7 3.94 4.74 -2 6 7 10.92 5.33 -2 6 6 716.87 33.01 -2 6 6 816.99 46.49 -2 6 5 712.14 29.90 -2 6 4 6.74 2.90 -2 6 3 332.83 18.56 -2 6 2 68.80 8.10 -2 6 1 44.17 6.21 -2 6 0 458.48 19.93 -2 6 -1 418.34 18.81 -2 6 -2 1101.65 30.84 -2 6 -3 0.50 0.83 2 -6 4 1383.01 37.34 2 -6 5 570.11 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300.63 17.72 4 4 -3 288.18 19.21 4 4 -2 881.59 53.51 4 4 -2 886.93 35.08 4 4 -2 910.18 32.07 4 4 -2 884.09 34.99 4 4 -1 236.68 21.56 4 4 -1 269.74 26.85 4 4 -1 246.69 18.34 4 4 -1 236.80 18.18 4 4 -1 241.38 16.27 4 4 0 3.97 1.73 4 4 0 4.11 3.12 4 4 0 3.46 1.91 4 4 0 7.97 2.74 4 4 1 10.59 3.66 4 4 1 11.52 5.09 4 4 1 11.29 3.76 4 4 1 13.80 4.93 4 4 2 827.97 34.06 4 4 2 838.77 34.70 4 4 2 877.67 37.94 4 4 3 4.72 3.31 4 4 3 1.21 1.43 4 4 3 -0.24 2.13 4 4 4 162.80 18.48 4 4 4 147.13 15.82 4 4 5 798.10 39.47 4 4 6 13.26 7.57 4 4 7 123.73 20.62 4 4 8 202.22 27.74 4 4 9 60.19 11.87 4 4 10 31.52 6.88 4 4 11 6.53 2.97 4 4 12 215.03 11.61 4 4 13 1.47 0.96 4 5 -15 -0.40 1.19 4 5 -15 3.80 1.39 4 5 -14 2.28 1.42 4 5 -14 4.99 2.44 4 5 -13 24.93 4.83 4 5 -13 26.74 5.53 4 5 -12 221.11 16.26 4 5 -11 60.05 9.23 4 5 -11 51.92 11.23 4 5 -10 195.36 17.27 4 5 -10 165.87 21.52 4 5 -9 627.80 34.52 4 5 -9 595.06 33.23 4 5 -8 141.62 18.81 4 5 -8 109.38 12.63 4 5 -7 186.24 18.37 4 5 -7 232.13 27.18 4 5 -7 201.15 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8 2 -8 64.71 10.43 8 2 -7 85.54 10.77 8 2 -6 104.82 11.28 8 2 -5 90.19 10.20 8 2 -4 353.09 20.07 8 2 -3 -1.82 2.08 8 2 -2 391.27 21.10 8 2 -1 218.26 15.77 8 2 0 -0.55 2.75 8 2 1 365.18 21.30 8 2 2 10.81 3.95 8 2 3 25.25 6.19 8 2 4 33.63 10.30 8 2 5 59.20 8.73 8 2 6 93.81 7.45 8 3 -9 108.07 11.34 8 3 -8 54.04 9.17 8 3 -7 0.13 1.30 8 3 -6 436.19 21.52 8 3 -5 89.62 9.36 8 3 -4 15.32 3.69 8 3 -3 267.63 15.84 8 3 -2 4.35 1.82 8 3 -1 12.17 3.35 8 3 0 30.60 5.50 8 3 1 211.56 15.50 8 3 2 80.73 10.65 8 3 3 14.04 5.54 8 3 4 247.07 15.65 8 4 -6 17.08 4.11 8 4 -5 9.58 2.89 8 4 -4 -0.48 1.07 8 4 -3 421.91 18.07 8 4 -2 65.90 7.17 8 4 -1 58.02 6.86 8 4 0 204.41 13.97 8 4 1 5.77 2.78 -9 8 5 12.99 3.25 -9 8 4 28.26 5.69 -9 8 3 312.76 17.04 -9 8 2 1.87 1.68 -9 8 2 0.42 1.08 -9 8 1 57.33 7.22 -9 8 0 184.91 13.98 -9 8 -1 17.79 4.68 -9 8 -2 21.04 5.84 -9 8 -3 3.31 2.06 -9 8 -4 89.34 6.73 -9 7 7 140.15 9.48 -9 7 6 0.29 1.35 -9 7 5 160.14 13.98 -9 7 4 212.29 16.97 -9 7 3 20.92 4.59 -9 7 3 15.90 3.43 -9 7 2 90.53 8.04 -9 7 2 95.06 9.33 -9 7 1 -1.05 2.14 -9 7 0 202.59 16.39 -9 7 -1 -0.94 2.06 -9 7 -2 184.09 18.22 -9 7 -3 219.92 16.47 -9 7 -4 1.10 1.61 -9 7 -5 130.21 8.16 -9 6 9 125.83 7.56 -9 6 8 14.86 3.29 -9 6 7 36.99 5.67 -9 6 6 99.77 10.87 9 -6 -5 16.53 4.97 -9 6 5 23.89 6.90 9 -6 -4 185.65 14.27 -9 6 4 206.27 16.38 9 -6 -3 -1.69 2.59 -9 6 3 1.00 1.84 9 -6 -2 452.80 20.31 -9 6 2 375.17 17.18 9 -6 -1 114.92 9.94 9 -6 0 -0.38 2.31 9 -6 1 229.18 14.58 9 -6 2 0.87 1.87 9 -6 3 27.03 4.88 9 -6 4 26.89 4.96 9 -6 5 141.29 12.51 -9 6 -6 66.43 5.61 -9 5 10 78.22 5.58 -9 5 9 78.19 6.97 -9 5 8 75.42 7.93 -9 5 7 3.00 2.24 9 -5 -6 380.43 22.80 -9 5 6 294.53 21.01 9 -5 -5 14.06 3.51 -9 5 5 24.44 7.27 9 -5 -4 44.64 6.37 -9 5 4 40.93 7.21 9 -5 -3 320.47 16.99 -9 5 3 283.30 16.40 9 -5 -2 2.89 1.18 -9 5 2 1.58 0.87 9 -5 -1 2.68 1.64 9 -5 0 15.57 3.65 9 -5 1 319.66 18.18 9 -5 2 59.20 7.75 9 -5 3 8.80 2.97 9 -5 4 330.77 19.54 9 -5 5 2.28 1.60 9 -5 6 34.97 6.87 -9 4 10 364.59 13.58 -9 4 9 17.15 3.64 -9 4 8 37.66 6.16 9 -4 -7 164.85 15.93 -9 4 7 114.65 11.76 9 -4 -6 43.42 7.04 -9 4 6 53.36 9.81 9 -4 -5 -0.98 2.20 -9 4 5 4.11 2.21 9 -4 -4 6.83 2.97 -9 4 4 7.41 3.42 9 -4 -3 304.79 17.12 -9 4 3 288.87 15.94 9 -4 -2 43.42 6.57 9 -4 -1 55.35 6.92 9 -4 0 573.33 24.35 9 -4 1 -0.06 1.99 9 -4 2 67.17 8.46 9 -4 3 63.74 8.74 9 -4 4 72.97 9.38 9 -4 5 1.11 1.50 9 -4 6 10.57 4.97 9 -4 7 223.44 12.99 -9 3 10 69.28 6.13 -9 3 9 30.48 4.76 -9 3 8 1.83 1.42 9 -3 -7 276.08 19.78 -9 3 7 186.76 15.70 9 -3 -6 1.84 1.61 -9 3 6 -8.99 5.02 9 -3 -5 150.74 12.10 -9 3 5 149.20 15.11 9 -3 -4 352.57 18.71 -9 3 4 323.57 18.21 9 -3 -3 6.77 2.53 9 -3 -2 216.73 14.46 9 -3 -1 45.28 6.66 9 -3 0 162.85 12.80 9 -3 1 35.74 5.99 9 -3 2 197.96 14.65 9 -3 3 319.98 19.12 9 -3 4 1.12 1.36 9 -3 5 128.10 14.49 9 -3 6 104.01 15.96 9 -3 7 10.45 2.87 -9 2 10 -0.61 0.93 -9 2 9 222.12 12.54 -9 2 8 91.60 9.04 9 -2 -7 -0.54 1.73 -9 2 7 -0.88 2.02 9 -2 -6 216.90 15.45 -9 2 6 212.06 21.85 9 -2 -5 0.24 1.40 -9 2 5 -0.06 1.83 9 -2 -4 80.41 8.63 -9 2 4 69.94 7.57 9 -2 -3 55.01 7.14 9 -2 -2 397.02 19.35 9 -2 -1 191.13 13.42 9 -2 0 1.44 1.74 9 -2 1 566.41 24.08 9 -2 2 52.49 7.42 9 -2 3 0.31 1.86 9 -2 4 117.92 12.52 9 -2 5 24.65 7.69 9 -2 6 19.35 5.52 9 -2 7 10.13 2.58 -9 1 10 115.76 7.12 9 -1 -9 18.63 3.55 9 -1 -8 20.74 4.28 9 -1 -7 28.74 6.52 9 -1 -7 28.75 6.93 9 -1 -6 357.76 19.29 9 -1 -6 351.83 26.90 9 -1 -5 72.55 7.88 9 -1 -5 78.08 11.01 9 -1 -4 4.86 1.53 9 -1 -4 7.41 3.03 9 -1 -3 568.15 22.11 9 -1 -3 652.24 28.73 9 -1 -2 2.60 1.37 9 -1 -2 6.44 2.54 9 -1 -1 2.34 1.00 9 -1 0 112.06 9.92 9 -1 1 116.28 10.31 9 -1 2 34.20 5.86 9 -1 3 3.43 1.91 9 -1 4 296.17 21.53 9 -1 5 14.27 4.71 9 -1 6 4.87 1.78 9 0 -9 15.41 3.17 9 0 -8 35.24 6.45 9 0 -7 539.06 32.88 9 0 -6 16.73 4.76 9 0 -6 16.96 5.05 9 0 -5 5.81 2.29 9 0 -5 6.70 2.64 9 0 -4 94.33 8.34 9 0 -4 93.98 10.16 9 0 -3 166.16 10.79 9 0 -3 170.63 13.50 9 0 -2 -0.16 1.37 9 0 -2 0.84 1.23 9 0 -1 30.67 4.69 9 0 -1 37.08 6.27 9 0 0 420.67 18.02 9 0 0 415.68 21.28 9 0 1 6.44 2.25 9 0 1 0.76 2.77 9 0 2 125.34 11.04 9 0 3 207.51 16.35 9 0 4 5.36 2.73 9 1 -8 20.13 4.14 9 1 -7 140.81 15.24 9 1 -6 -0.70 2.48 9 1 -5 90.74 9.90 9 1 -4 253.72 15.83 9 1 -3 0.49 1.87 9 1 -2 232.29 14.71 9 1 -1 142.33 11.59 9 1 0 23.62 4.77 9 1 1 6.93 2.64 9 1 2 8.68 4.32 9 2 -5 56.97 7.46 9 2 -4 28.90 5.04 9 2 -3 43.24 5.94 9 2 -2 47.71 6.24 9 2 -1 115.57 10.36 10 -5 -4 6.60 2.33 10 -5 -3 344.57 17.03 10 -5 -2 25.54 4.26 10 -5 -1 33.35 4.70 10 -5 0 356.84 15.71 10 -5 1 5.05 2.03 10 -4 -5 39.48 6.91 10 -4 -4 198.17 12.78 10 -4 -3 92.83 8.08 10 -4 -2 41.61 5.23 10 -4 -1 2.35 1.49 10 -4 0 316.93 14.85 10 -4 1 6.53 1.99 10 -4 2 57.74 6.80 10 -3 -5 -2.18 1.84 10 -3 -4 253.54 13.98 10 -3 -3 3.19 1.17 10 -3 -2 140.63 9.53 10 -3 -1 168.02 10.42 10 -3 0 -0.34 1.38 10 -3 1 195.01 11.97 10 -3 2 10.21 3.18 10 -2 -4 10.05 2.74 10 -2 -3 179.67 10.85 10 -2 -2 14.69 2.81 10 -2 -1 26.56 4.01 10 -2 0 47.21 5.53 10 -2 1 183.43 12.07 TITL OIE020_numabs_ana in P-1 REM P-1 (#2 in standard setting) CELL 1.54184 8.153375 9.685768 15.479468 94.6638 95.1811 107.4768 ZERR 2.00 0.000314 0.000437 0.000755 0.0038 0.0035 0.0037 LATT 1 SFAC C H N O I UNIT 44.00 44.00 4.00 8.00 4.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 34862 _ins_header ; TITL OIE020_numabs_ana in P-1 REM P-1 (#2 in standard setting) CELL 1.54184 8.153375 9.685768 15.479468 94.6638 95.1811 107.4768 ZERR 2.00 0.000314 0.000437 0.000755 0.0038 0.0035 0.0037 LATT 1 SFAC C H N O I UNIT 44.00 44.00 4.00 8.00 4.00 TREF HKLF 4 END ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.473 _oxdiff_exptl_absorpt_empirical_full_min 0.569 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group I1 I 0.32865(4) 0.23052(3) 0.55394(2) 0.02891(13) Uani 1 1 d . . . . . I2 I 0.44982(4) 0.49294(4) 0.85671(2) 0.03217(13) Uani 1 1 d . . . . . O28 O 0.1091(5) 0.2231(5) 0.6231(3) 0.0369(9) Uani 1 1 d . . . . . O29 O 0.1327(5) 0.0319(4) 0.6916(3) 0.0373(9) Uani 1 1 d . . . . . O31 O 0.2037(5) 0.3268(5) 0.8123(3) 0.0402(10) Uani 1 1 d . . . . . O32 O 0.0590(5) 0.4795(5) 0.8523(3) 0.0424(10) Uani 1 1 d . . . . . N1 N 0.5580(6) 0.2601(5) 0.4729(3) 0.0297(9) Uani 1 1 d . . . . . N11 N 0.7168(6) 0.6586(5) 0.8947(3) 0.0342(10) Uani 1 1 d . . . . . C2 C 0.5787(7) 0.3508(6) 0.4098(4) 0.0351(12) Uani 1 1 d . . . . . H2 H 0.4952 0.3961 0.3971 0.042 Uiso 1 1 calc R . . . . C3 C 0.7186(8) 0.3774(7) 0.3646(4) 0.0368(13) Uani 1 1 d . . . . . H3 H 0.7301 0.4425 0.3229 0.044 Uiso 1 1 calc R . . . . C4 C 0.8456(7) 0.3088(6) 0.3796(4) 0.0303(11) Uani 1 1 d . . . . . C5 C 0.8223(7) 0.2161(6) 0.4448(4) 0.0320(11) Uani 1 1 d . . . . . H5 H 0.9033 0.1685 0.4582 0.038 Uiso 1 1 calc R . . . . C6 C 0.6792(7) 0.1946(6) 0.4896(4) 0.0313(11) Uani 1 1 d . . . . . H6 H 0.6663 0.1324 0.5330 0.038 Uiso 1 1 calc R . . . . C7 C 1.0007(8) 0.3416(6) 0.3315(4) 0.0383(13) Uani 1 1 d . . . . . H7A H 0.9658 0.3501 0.2711 0.046 Uiso 1 1 calc R . . . . H7B H 1.0486 0.2613 0.3323 0.046 Uiso 1 1 calc R . . . . C8 C 1.1406(8) 0.4825(7) 0.3713(4) 0.0412(14) Uani 1 1 d . . . . . H8A H 1.2377 0.4995 0.3383 0.062 Uiso 1 1 calc GR . . . . H8B H 1.1775 0.4737 0.4307 0.062 Uiso 1 1 calc GR . . . . H8C H 1.0944 0.5626 0.3697 0.062 Uiso 1 1 calc GR . . . . C12 C 0.8304(8) 0.6402(7) 0.9569(4) 0.0364(12) Uani 1 1 d . . . . . H12 H 0.7961 0.5611 0.9886 0.044 Uiso 1 1 calc R . . . . C13 C 0.9958(8) 0.7338(7) 0.9755(4) 0.0399(13) Uani 1 1 d . . . . . H13 H 1.0726 0.7176 1.0188 0.048 Uiso 1 1 calc R . . . . C14 C 1.0481(8) 0.8544(7) 0.9287(4) 0.0407(14) Uani 1 1 d . . . . . C15 C 0.9272(9) 0.8730(7) 0.8650(5) 0.0484(16) Uani 1 1 d . . . . . H15 H 0.9563 0.9524 0.8331 0.058 Uiso 1 1 calc R . . . . C16 C 0.7655(8) 0.7738(7) 0.8497(5) 0.0458(15) Uani 1 1 d . . . . . H16 H 0.6861 0.7865 0.8065 0.055 Uiso 1 1 calc R . . . . C17 C 1.2343(9) 0.9538(9) 0.9421(6) 0.0577(19) Uani 1 1 d . . . . . H17A H 1.2391 1.0481 0.9237 0.069 Uiso 1 1 calc R . . . . H17B H 1.2784 0.9680 1.0036 0.069 Uiso 1 1 calc R . . . . C18 C 1.3428(9) 0.8886(9) 0.8911(7) 0.067(2) Uani 1 1 d . . . . . H18A H 1.2984 0.8740 0.8303 0.101 Uiso 1 1 calc GR . . . . H18B H 1.3408 0.7967 0.9107 0.101 Uiso 1 1 calc GR . . . . H18C H 1.4597 0.9529 0.8991 0.101 Uiso 1 1 calc GR . . . . C21 C -0.0978(7) 0.1310(6) 0.7148(3) 0.0283(11) Uani 1 1 d . . . . . C22 C -0.0971(7) 0.2481(6) 0.7762(4) 0.0281(11) Uani 1 1 d . . . . . C23 C -0.2556(7) 0.2539(6) 0.8014(4) 0.0332(12) Uani 1 1 d . . . . . H23 H -0.2572 0.3306 0.8412 0.040 Uiso 1 1 calc R . . . . C24 C -0.4104(7) 0.1483(7) 0.7687(4) 0.0368(13) Uani 1 1 d . . . . . H24 H -0.5148 0.1546 0.7855 0.044 Uiso 1 1 calc R . . . . C25 C -0.4066(7) 0.0323(6) 0.7100(4) 0.0343(12) Uani 1 1 d . . . . . H25 H -0.5095 -0.0400 0.6884 0.041 Uiso 1 1 calc R . . . . C26 C -0.2514(7) 0.0232(6) 0.6834(4) 0.0335(12) Uani 1 1 d . . . . . H26 H -0.2508 -0.0551 0.6446 0.040 Uiso 1 1 calc R . . . . C27 C 0.0645(7) 0.1244(6) 0.6769(4) 0.0299(11) Uani 1 1 d . . . . . C30 C 0.0649(7) 0.3652(6) 0.8167(4) 0.0294(11) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I1 0.0247(2) 0.0278(2) 0.0347(2) 0.00784(14) 0.00651(14) 0.00700(14) I2 0.0230(2) 0.0376(2) 0.0343(2) 0.00049(14) 0.00302(14) 0.00814(15) O28 0.029(2) 0.043(2) 0.045(2) 0.0197(19) 0.0130(18) 0.0144(18) O29 0.034(2) 0.033(2) 0.049(2) 0.0135(18) 0.0138(19) 0.0121(17) O31 0.0231(19) 0.040(2) 0.054(3) -0.0070(19) -0.0022(18) 0.0103(17) O32 0.029(2) 0.037(2) 0.060(3) -0.008(2) 0.002(2) 0.0135(18) N1 0.028(2) 0.025(2) 0.036(2) 0.0111(18) 0.0085(19) 0.0061(18) N11 0.028(2) 0.040(3) 0.031(2) 0.005(2) 0.0047(19) 0.005(2) C2 0.027(3) 0.035(3) 0.043(3) 0.010(2) 0.007(2) 0.006(2) C3 0.034(3) 0.036(3) 0.042(3) 0.017(2) 0.010(3) 0.009(3) C4 0.022(3) 0.030(3) 0.036(3) 0.003(2) 0.001(2) 0.005(2) C5 0.028(3) 0.032(3) 0.038(3) 0.006(2) 0.003(2) 0.012(2) C6 0.028(3) 0.026(3) 0.039(3) 0.007(2) 0.003(2) 0.006(2) C7 0.032(3) 0.035(3) 0.048(3) 0.009(3) 0.011(3) 0.007(2) C8 0.032(3) 0.041(3) 0.046(3) 0.012(3) 0.007(3) 0.002(3) C12 0.037(3) 0.046(3) 0.030(3) 0.008(2) 0.009(2) 0.016(3) C13 0.030(3) 0.047(4) 0.037(3) 0.005(3) 0.005(2) 0.005(3) C14 0.037(3) 0.037(3) 0.040(3) 0.001(2) 0.010(3) -0.002(3) C15 0.047(4) 0.045(4) 0.049(3) 0.014(3) 0.009(3) 0.004(3) C16 0.036(3) 0.053(4) 0.047(3) 0.018(3) 0.000(3) 0.009(3) C17 0.034(4) 0.063(5) 0.062(5) -0.003(4) 0.004(3) -0.002(3) C18 0.036(4) 0.066(5) 0.091(6) 0.008(5) 0.015(4) 0.001(4) C21 0.026(3) 0.028(3) 0.033(3) 0.011(2) 0.008(2) 0.007(2) C22 0.025(3) 0.024(3) 0.036(3) 0.011(2) 0.003(2) 0.009(2) C23 0.028(3) 0.038(3) 0.036(3) 0.009(2) 0.007(2) 0.012(2) C24 0.025(3) 0.044(3) 0.043(3) 0.013(3) 0.005(2) 0.010(2) C25 0.026(3) 0.039(3) 0.033(3) 0.007(2) 0.004(2) 0.002(2) C26 0.032(3) 0.038(3) 0.026(2) 0.003(2) -0.002(2) 0.006(2) C27 0.028(3) 0.026(3) 0.033(3) 0.003(2) 0.004(2) 0.005(2) C30 0.025(3) 0.030(3) 0.034(3) 0.008(2) 0.005(2) 0.009(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.3257 6.8362 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 0 -1 -10 0.0147 0 1 10 0.0010 -5 0 1 0.1697 5 -1 -1 0.1808 0 6 -2 0.0721 0 -6 2 0.0803 3 -6 1 0.1233 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O28 I1 N1 173.60(15) . . ? O31 I2 N11 175.39(16) . . ? C27 O28 I1 118.6(3) . . ? C30 O31 I2 116.9(4) . . ? C2 N1 I1 120.4(4) . . ? C6 N1 I1 121.3(4) . . ? C6 N1 C2 118.2(5) . . ? C12 N11 I2 122.1(4) . . ? C12 N11 C16 118.9(5) . . ? C16 N11 I2 118.9(4) . . ? N1 C2 H2 119.1 . . ? N1 C2 C3 121.7(5) . . ? C3 C2 H2 119.1 . . ? C2 C3 H3 119.3 . . ? C2 C3 C4 121.4(5) . . ? C4 C3 H3 119.3 . . ? C3 C4 C7 121.0(5) . . ? C5 C4 C3 116.1(5) . . ? C5 C4 C7 122.8(5) . . ? C4 C5 H5 119.9 . . ? C6 C5 C4 120.2(5) . . ? C6 C5 H5 119.9 . . ? N1 C6 C5 122.5(5) . . ? N1 C6 H6 118.8 . . ? C5 C6 H6 118.8 . . ? C4 C7 H7A 109.2 . . ? C4 C7 H7B 109.2 . . ? C4 C7 C8 112.3(5) . . ? H7A C7 H7B 107.9 . . ? C8 C7 H7A 109.2 . . ? C8 C7 H7B 109.2 . . ? C7 C8 H8A 109.5 . . ? C7 C8 H8B 109.5 . . ? C7 C8 H8C 109.5 . . ? H8A C8 H8B 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? N11 C12 H12 118.8 . . ? N11 C12 C13 122.3(6) . . ? C13 C12 H12 118.8 . . ? C12 C13 H13 120.4 . . ? C12 C13 C14 119.2(6) . . ? C14 C13 H13 120.4 . . ? C13 C14 C17 120.8(7) . . ? C15 C14 C13 117.7(6) . . ? C15 C14 C17 121.3(6) . . ? C14 C15 H15 120.3 . . ? C16 C15 C14 119.5(6) . . ? C16 C15 H15 120.3 . . ? N11 C16 C15 122.4(6) . . ? N11 C16 H16 118.8 . . ? C15 C16 H16 118.8 . . ? C14 C17 H17A 109.7 . . ? C14 C17 H17B 109.7 . . ? H17A C17 H17B 108.2 . . ? C18 C17 C14 110.0(6) . . ? C18 C17 H17A 109.7 . . ? C18 C17 H17B 109.7 . . ? C17 C18 H18A 109.5 . . ? C17 C18 H18B 109.5 . . ? C17 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C22 C21 C27 121.8(5) . . ? C26 C21 C22 120.4(5) . . ? C26 C21 C27 117.7(5) . . ? C21 C22 C30 123.6(5) . . ? C23 C22 C21 118.2(5) . . ? C23 C22 C30 118.2(5) . . ? C22 C23 H23 119.1 . . ? C24 C23 C22 121.8(5) . . ? C24 C23 H23 119.1 . . ? C23 C24 H24 120.6 . . ? C23 C24 C25 118.8(5) . . ? C25 C24 H24 120.6 . . ? C24 C25 H25 119.5 . . ? C26 C25 C24 121.0(5) . . ? C26 C25 H25 119.5 . . ? C21 C26 C25 119.8(5) . . ? C21 C26 H26 120.1 . . ? C25 C26 H26 120.1 . . ? O28 C27 C21 110.6(4) . . ? O29 C27 O28 126.7(5) . . ? O29 C27 C21 122.5(5) . . ? O31 C30 C22 113.0(5) . . ? O32 C30 O31 125.7(5) . . ? O32 C30 C22 121.2(5) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag I1 O28 2.154(4) . ? I1 N1 2.305(4) . ? I2 O31 2.172(4) . ? I2 N11 2.275(5) . ? O28 C27 1.309(6) . ? O29 C27 1.214(7) . ? O31 C30 1.299(6) . ? O32 C30 1.212(7) . ? N1 C2 1.354(7) . ? N1 C6 1.342(7) . ? N11 C12 1.334(7) . ? N11 C16 1.340(8) . ? C2 H2 0.9300 . ? C2 C3 1.361(8) . ? C3 H3 0.9300 . ? C3 C4 1.401(8) . ? C4 C5 1.393(8) . ? C4 C7 1.491(8) . ? C5 H5 0.9300 . ? C5 C6 1.383(8) . ? C6 H6 0.9300 . ? C7 H7A 0.9700 . ? C7 H7B 0.9700 . ? C7 C8 1.531(8) . ? C8 H8A 0.9600 . ? C8 H8B 0.9600 . ? C8 H8C 0.9600 . ? C12 H12 0.9300 . ? C12 C13 1.370(8) . ? C13 H13 0.9300 . ? C13 C14 1.402(9) . ? C14 C15 1.391(9) . ? C14 C17 1.519(9) . ? C15 H15 0.9300 . ? C15 C16 1.365(9) . ? C16 H16 0.9300 . ? C17 H17A 0.9700 . ? C17 H17B 0.9700 . ? C17 C18 1.478(11) . ? C18 H18A 0.9600 . ? C18 H18B 0.9600 . ? C18 H18C 0.9600 . ? C21 C22 1.418(8) . ? C21 C26 1.385(8) . ? C21 C27 1.511(7) . ? C22 C23 1.399(7) . ? C22 C30 1.503(8) . ? C23 H23 0.9300 . ? C23 C24 1.386(8) . ? C24 H24 0.9300 . ? C24 C25 1.395(8) . ? C25 H25 0.9300 . ? C25 C26 1.391(8) . ? C26 H26 0.9300 . ? loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z 0.2268 -0.5867 -9.8394 0.0262 0.9996 -0.0090 -0.2268 0.5867 9.8394 -0.0262 -0.9996 0.0090 -5.1340 0.3816 0.9261 -0.9727 0.0253 -0.2308 5.2615 -1.2643 -0.6720 0.9956 -0.0260 0.0905 -0.2140 6.0501 -1.8759 -0.0317 0.0017 0.9995 0.2018 -6.0464 1.8772 0.0293 -0.0016 -0.9996 3.4430 -5.7537 1.1233 0.6442 -0.0175 -0.7646 loop_ _hkl_oxdiff_h _hkl_oxdiff_k _hkl_oxdiff_l _hkl_oxdiff_f2 _hkl_oxdiff_sig _hkl_oxdiff_ba 0 0 1 19308.1 962.648 1 0 0 1 15879.3 767.308 2 0 0 2 11397.2 856.388 2 0 0 3 284434. 4687.40 2 0 0 4 172699. 3580.32 2 0 0 5 3125.82 497.484 2 0 0 6 41790.5 1789.46 2 0 0 7 199463. 4242.94 2 0 0 8 15961.2 1189.72 2 0 0 9 22725.5 1489.76 2 0 0 10 140916. 3981.60 2 0 0 11 912.601 357.149 2 0 0 12 39243.2 2246.22 2 0 0 12 47982.8 2953.77 17 0 0 13 31986.9 2082.88 2 0 0 13 37872.5 2663.36 17 0 0 14 21928.3 1984.44 17 0 0 15 460.469 408.689 17 0 0 16 3950.51 791.459 17 0 0 17 35924.7 2105.12 17 0 0 18 100.922 132.185 17 0 0 19 5036.90 532.860 17 0 -1 19 164.338 82.2617 17 0 -1 18 3244.49 544.914 17 0 -1 17 16798.1 1414.00 17 0 -1 16 1491.47 512.182 17 0 1 -16 2034.40 476.479 8 0 -1 15 2878.62 746.380 17 0 1 -15 3787.32 687.685 8 0 -1 14 93940.7 4139.82 17 0 1 -14 95628.9 3501.98 8 0 -1 13 15699.8 1466.82 2 0 1 -13 17839.1 1503.92 8 0 -1 13 18724.8 1872.14 17 0 -1 12 16309.7 1432.20 2 0 1 -12 20504.3 1572.25 8 0 -1 12 17662.7 1871.21 17 0 -1 11 57966.0 2604.60 2 0 -1 10 26229.8 1660.74 2 0 -1 9 35392.9 1876.35 2 0 -1 8 28534.0 1671.18 2 0 -1 7 187062. 4467.51 2 0 1 -6 6467.24 396.603 4 0 -1 6 7729.57 982.026 2 0 -1 5 205265. 5066.71 2 0 1 -5 185807. 2597.47 4 0 -1 4 772663. 9433.77 2 0 1 -4 776414. 7322.57 4 0 1 -3 270140. 3784.74 4 0 -1 3 276628. 3942.59 2 0 1 -2 110270. 3054.76 4 0 -1 2 88149.7 1549.12 2 0 1 -1 203608. 2016.82 3 0 1 -1 196845. 1739.97 1 0 1 0 69688.0 901.391 1 0 1 0 68909.8 908.291 3 0 1 1 7860.49 445.456 1 0 1 1 6489.97 349.139 4 0 1 2 31394.1 1515.25 1 0 1 2 29751.1 785.687 2 0 1 2 30239.4 711.832 4 0 1 3 141774. 4510.85 1 0 1 3 122837. 2464.91 2 0 1 4 425.279 243.221 2 0 1 5 8024.77 767.039 2 0 1 6 145056. 3494.21 2 0 1 7 663.161 249.207 2 0 1 8 132729. 3667.57 2 0 1 9 1922.32 454.979 2 0 1 10 65283.4 2757.63 2 0 1 11 2188.19 536.639 2 0 1 12 22508.9 1574.77 7 0 1 12 19846.1 1594.50 2 0 1 12 22530.1 2036.92 17 0 1 13 47314.2 2536.17 2 0 1 13 51635.2 2420.99 7 0 1 14 -261.346 372.322 17 0 1 15 47350.9 2825.94 17 0 1 16 20880.8 1760.09 17 0 1 17 1565.15 442.378 17 0 1 18 14095.1 1074.06 17 0 1 19 226.210 122.309 17 0 2 -19 3561.47 440.168 12 0 -2 18 20408.7 1226.60 17 0 -2 17 2584.86 511.981 17 0 2 -17 2041.85 422.212 8 0 2 -16 6275.75 825.441 8 0 -2 16 5911.35 914.061 17 0 2 -15 26773.0 1836.10 8 0 -2 15 25184.6 2009.07 17 0 2 -14 8962.76 1090.98 8 0 -2 14 7170.05 1139.63 17 0 -2 13 6980.77 979.830 2 0 -2 13 8780.87 1258.88 17 0 2 -13 7417.98 993.159 8 0 2 -12 2751.15 584.178 8 0 -2 12 1946.19 519.640 2 0 -2 12 2500.44 609.228 17 0 -2 11 139780. 4199.86 2 0 -2 10 1873.79 468.743 2 0 -2 9 94815.9 3363.88 2 0 -2 8 140997. 4328.38 2 0 -2 7 41048.4 2689.52 2 0 2 -7 32745.2 1202.67 4 0 2 -6 116295. 2379.32 4 0 -2 6 102906. 3571.28 2 0 2 -5 143752. 2800.99 4 0 -2 5 145344. 3509.43 2 0 2 -4 291466. 4513.27 4 0 -2 4 309852. 4543.96 2 0 2 -3 3307.36 562.736 4 0 -2 3 3613.70 359.813 2 0 2 -2 2587.32 244.537 3 0 2 -2 2517.22 139.910 1 0 2 -2 2636.03 590.456 4 0 2 -1 259198. 2496.84 1 0 2 -1 248988. 2803.16 3 0 2 0 33680.6 869.059 1 0 2 0 31327.1 1280.09 4 0 2 0 31584.1 758.103 3 0 2 1 542014. 5124.55 3 0 2 1 528609. 6117.82 4 0 2 2 735024. 9633.96 1 0 2 2 716351. 6716.22 3 0 2 3 7201.73 488.300 4 0 2 3 7912.34 1205.70 1 0 2 4 101777. 3774.50 1 0 2 4 88747.2 2102.02 2 0 2 5 20152.1 1294.02 2 0 2 6 71790.4 2879.59 2 0 2 7 22737.3 1543.03 2 0 2 8 62994.8 2655.93 2 0 2 9 75059.8 2979.68 2 0 2 10 1655.42 451.284 2 0 2 11 94530.6 3569.33 2 0 2 11 101556. 3517.62 7 0 2 12 13936.3 1562.48 17 0 2 12 11857.0 1197.08 7 0 2 13 3466.96 661.295 7 0 2 13 3199.77 825.028 17 0 2 14 37271.5 2055.73 7 0 2 14 40248.9 2621.43 17 0 2 15 4852.75 702.280 7 0 2 15 4841.47 906.082 17 0 2 16 7690.95 1022.69 17 0 2 17 1832.12 449.315 17 0 2 18 22553.7 1221.19 17 0 3 -19 5453.87 520.082 12 0 3 -18 2472.06 459.245 12 0 3 -17 4857.57 647.370 8 0 -3 17 4613.82 613.689 17 0 -3 16 1437.37 379.337 17 0 3 -16 3989.99 684.123 8 0 -3 15 37840.0 2331.42 17 0 3 -15 42070.5 2346.81 8 0 -3 14 4289.67 861.184 17 0 3 -14 6138.69 952.394 8 0 -3 13 107531. 4331.11 17 0 3 -13 116709. 4152.35 8 0 -3 12 55603.6 2791.07 2 0 3 -12 60676.4 3016.14 8 0 -3 11 -51.4761 253.649 2 0 -3 10 135239. 4350.59 2 0 -3 9 1829.75 551.263 2 0 3 -8 102665. 2698.57 4 0 -3 8 123508. 4968.81 2 0 3 -7 73722.6 2220.58 4 0 -3 7 69806.6 3320.08 2 0 -3 6 12821.1 1140.91 2 0 3 -6 16851.6 1045.30 4 0 -3 5 121596. 3126.17 2 0 3 -5 116656. 2999.92 4 0 3 -4 1463.50 126.246 1 0 3 -4 1433.75 389.815 4 0 -3 4 1929.39 347.084 2 0 3 -3 625858. 5299.51 1 0 -3 3 636566. 6853.31 2 0 3 -2 62563.6 1437.49 3 0 3 -2 64096.1 1155.44 1 0 3 -1 133.656 94.5619 1 0 3 -1 38.6986 60.6189 3 0 3 -1 150.440 165.162 4 0 3 0 146941. 3007.50 1 0 3 0 150344. 3530.51 4 0 3 1 19020.2 1109.52 4 0 3 1 18664.1 1360.12 1 0 3 1 17981.9 730.421 3 0 3 2 10926.4 794.433 4 0 3 2 12349.0 659.336 3 0 3 3 26665.7 1199.49 4 0 3 3 28546.1 1121.34 3 0 3 3 27432.2 2462.04 1 0 3 4 234813. 6161.15 1 0 3 4 237772. 3881.87 4 0 3 4 221845. 3809.02 3 0 3 5 34876.9 1634.22 3 0 3 6 2346.56 570.033 3 0 3 7 116501. 4690.73 3 0 3 8 147.166 167.671 3 0 3 9 89.3470 252.448 3 0 3 10 76313.8 3571.29 17 0 3 10 73185.3 3167.44 7 0 3 11 30649.4 2237.26 3 0 3 11 36870.5 2229.78 7 0 3 11 34010.9 2354.76 17 0 3 12 7580.77 999.252 7 0 3 12 9017.16 1230.87 17 0 3 13 304.502 337.900 17 0 3 13 72.3251 200.098 7 0 3 14 76258.9 3455.71 17 0 3 14 74284.3 2912.37 7 0 3 15 1489.35 366.541 7 0 3 15 2210.16 566.673 17 0 3 16 1127.49 293.388 7 0 3 16 1137.77 393.089 17 0 3 17 23273.5 1303.86 17 0 3 18 291.325 121.318 6 0 4 -18 -305.417 153.592 12 0 4 -17 47272.4 1982.41 8 0 4 -17 55231.1 2458.70 12 0 4 -16 8607.74 962.534 8 0 4 -15 1442.78 483.838 8 0 4 -14 45726.5 2591.05 8 0 4 -13 10608.3 1313.77 8 0 -4 12 13946.7 1424.74 2 0 4 -12 13488.4 1428.13 8 0 4 -11 4386.28 714.053 14 0 4 -11 4104.16 780.580 8 0 -4 11 3802.03 734.825 2 0 -4 10 89503.1 3749.35 2 0 -4 9 59402.8 3323.29 2 0 -4 8 5808.16 1185.05 2 0 4 -8 3638.69 602.240 4 0 4 -7 133819. 3571.59 4 0 -4 7 118814. 4545.87 2 0 4 -6 1228.48 388.730 4 0 -4 6 2247.05 534.212 2 0 -4 5 6542.43 736.034 2 0 4 -5 6610.62 819.458 4 0 -4 4 68006.5 2156.97 2 0 4 -4 66831.4 3038.59 4 0 4 -3 36530.5 2977.22 4 0 -4 3 30557.0 1261.38 2 0 4 -2 9670.06 1293.45 4 0 4 -2 10932.5 660.325 3 0 4 -1 6010.32 460.452 3 0 4 -1 5633.42 888.499 4 0 4 0 356886. 6552.32 4 0 4 0 325113. 4073.10 3 0 4 1 54188.0 2239.82 4 0 4 1 55441.6 3938.35 1 0 4 1 53401.2 1479.99 3 0 4 2 38158.6 1335.88 3 0 4 2 36007.8 2686.27 1 0 4 2 35139.8 1695.35 4 0 4 3 351812. 5040.57 3 0 4 3 328969. 5528.72 4 0 4 4 531.559 184.154 3 0 4 4 1013.56 284.317 4 0 4 5 3181.01 506.026 3 0 4 6 36413.1 2015.65 3 0 4 7 161812. 5539.60 3 0 4 8 167.155 253.017 3 0 4 9 762.498 395.738 7 0 4 9 384.022 123.793 3 0 4 10 117523. 4512.01 17 0 4 10 116444. 4358.52 7 0 4 11 279.045 199.117 17 0 4 11 30.7506 258.435 7 0 4 12 17338.5 1714.20 17 0 4 12 19717.5 1632.04 7 0 4 13 50375.2 2665.92 17 0 4 13 51034.5 2489.17 7 0 4 14 5686.07 788.504 7 0 4 14 4329.20 748.143 17 0 4 15 1749.77 417.523 17 0 4 15 1988.16 416.530 7 0 4 16 406.208 153.440 7 0 4 16 231.315 149.206 17 0 4 17 9109.30 713.316 6 0 5 -18 14941.8 908.245 12 0 5 -17 2885.28 520.968 12 0 5 -16 83.3755 183.642 8 0 5 -16 83.7915 157.162 12 0 5 -15 370.957 289.133 12 0 5 -15 494.944 286.987 8 0 5 -14 42363.3 2785.66 12 0 5 -14 43209.1 2493.95 8 0 5 -13 12973.6 1220.19 14 0 5 -13 13324.7 1789.92 12 0 5 -13 11978.8 1381.65 8 0 5 -12 6628.49 933.841 14 0 5 -12 7430.14 1101.76 8 0 5 -11 77685.2 3583.40 8 0 5 -11 76670.5 3287.98 14 0 -5 11 80894.7 3545.09 2 0 5 -10 2174.67 621.257 8 0 5 -10 2716.52 640.355 14 0 -5 10 2696.75 675.627 2 0 5 -9 16410.1 1790.34 8 0 -5 9 17607.5 1875.44 2 0 5 -9 16040.8 1593.40 14 0 5 -9 14087.0 1751.75 12 0 5 -8 36430.8 2117.63 4 0 -5 8 46659.7 3414.97 2 0 5 -7 29382.5 1878.55 4 0 -5 7 25671.7 2218.57 2 0 -5 6 177.097 174.514 2 0 5 -6 364.460 202.356 4 0 -5 5 2378.15 496.980 2 0 5 -5 2202.32 576.598 4 0 5 -4 222420. 7088.22 4 0 -5 4 195714. 4231.72 2 0 5 -3 7232.96 1519.38 4 0 -5 3 10845.2 820.840 2 0 5 -2 92440.1 2289.17 3 0 -5 2 94171.7 2306.35 2 0 5 -1 295228. 4218.93 3 0 5 -1 318444. 7580.93 4 0 5 0 13254.3 1377.39 4 0 5 0 11638.2 736.400 3 0 5 1 34325.9 2065.47 4 0 5 1 31880.2 1250.25 3 0 5 2 7813.36 655.102 3 0 5 2 7458.83 909.350 4 0 5 3 159241. 3392.10 3 0 5 3 148717. 4040.91 4 0 5 4 16630.4 1299.99 4 0 5 7 2657.62 732.316 7 0 5 8 57035.4 3247.96 16 0 5 8 58166.4 3710.30 7 0 5 9 21906.9 2070.33 7 0 5 9 22817.0 1854.53 16 0 5 10 14300.8 1569.67 7 0 5 11 10924.8 1267.58 7 0 5 12 317.579 301.584 7 0 5 13 26693.9 1697.72 7 0 5 14 315.401 155.340 7 0 5 15 15765.0 1002.84 7 0 5 15 14439.2 1147.70 6 0 5 16 10118.2 768.688 6 0 6 -17 148.382 94.3898 12 0 6 -16 9649.72 966.800 12 0 6 -15 31731.9 1806.62 8 0 6 -15 30978.6 1991.82 12 0 6 -14 -184.765 214.938 14 0 6 -14 791.047 327.548 8 0 6 -14 692.157 364.787 12 0 6 -13 8457.53 1433.05 12 0 6 -13 8369.52 1011.22 14 0 6 -13 7958.38 1048.19 8 0 6 -12 1194.34 517.736 8 0 6 -12 2263.94 1065.14 12 0 6 -12 1415.12 471.180 14 0 6 -11 48540.1 2696.70 14 0 6 -11 40228.3 3611.23 12 0 6 -11 44250.9 2803.20 8 0 6 -10 164.113 284.008 12 0 6 -10 530.330 378.616 8 0 6 -10 579.923 259.136 14 0 6 -9 17710.4 1959.08 12 0 6 -9 20026.0 1967.95 14 0 6 -8 82010.9 3613.00 4 0 6 -8 79701.9 3902.61 12 0 6 -7 591.743 362.884 14 0 6 -7 -57.6505 199.309 4 0 6 -7 214.240 216.038 12 0 6 -6 71855.7 3491.32 4 0 6 -5 62856.6 3571.66 4 0 6 -4 33908.9 3413.68 4 0 6 -3 23849.7 2809.59 4 0 6 -2 1876.43 760.142 4 0 6 -1 84946.6 4296.64 4 0 6 0 13415.5 1562.62 4 0 6 1 96572.4 3993.99 4 0 6 2 140394. 4620.61 4 0 6 3 297.904 219.469 4 0 6 5 5250.73 942.797 6 0 6 5 4788.81 927.504 7 0 6 5 6210.16 1438.75 16 0 6 6 12811.8 2170.91 16 0 6 6 12042.6 1728.22 7 0 6 6 11479.4 1568.20 6 0 6 7 15836.2 1939.34 16 0 6 7 18353.6 2264.67 6 0 6 7 18925.6 2596.84 7 0 6 8 8667.24 1292.65 16 0 6 8 9862.80 2018.27 6 0 6 8 9327.30 1516.54 7 0 6 9 36275.0 2665.89 7 0 6 9 37053.7 2369.79 16 0 6 10 691.841 289.142 16 0 6 10 526.652 377.639 7 0 6 10 468.441 394.924 6 0 6 11 27446.8 2296.66 6 0 6 11 31788.0 2094.75 7 0 6 12 11726.7 1349.94 6 0 6 12 12979.5 1205.02 7 0 6 13 -19.5390 186.561 6 0 6 13 -89.1414 192.763 7 0 6 14 17734.5 1225.56 6 0 6 14 19908.1 1153.30 7 0 6 15 97.1362 108.382 6 0 7 -16 193.569 109.043 12 0 7 -15 5858.85 719.301 12 0 7 -14 -70.8248 154.916 12 0 7 -14 -90.5871 190.241 14 0 7 -14 140.954 176.388 8 0 7 -13 11570.7 1143.32 14 0 7 -13 13844.5 1645.50 12 0 7 -13 11283.3 1138.44 8 0 7 -12 29076.8 2053.13 8 0 7 -12 33399.2 2098.27 14 0 7 -11 2191.06 667.098 8 0 7 -11 2832.87 682.830 14 0 7 -11 2125.15 824.508 12 0 7 -10 57450.2 4039.40 8 0 7 -10 54518.4 3081.48 14 0 7 -10 46546.6 3355.39 12 0 7 -9 10450.1 1572.32 14 0 7 -9 10028.9 1441.46 12 0 7 -8 8929.95 1791.01 14 0 7 -8 5104.87 968.780 12 0 7 -7 30882.9 2466.19 4 0 7 -7 23177.6 2665.34 14 0 7 -7 28635.6 2096.83 10 0 7 -7 27664.0 2161.36 12 0 7 -7 29200.7 2150.83 16 0 7 -6 2146.92 720.327 14 0 7 -6 2332.08 666.834 4 0 7 -6 2057.56 559.157 12 0 7 -6 2026.23 722.450 16 0 7 -6 2446.41 592.938 10 0 7 -5 24597.8 2253.60 14 0 7 -5 20268.2 1677.29 12 0 7 -5 26168.6 2676.65 4 0 7 -5 20705.4 1825.14 16 0 7 -5 21287.8 1669.37 10 0 7 -4 3728.64 855.371 14 0 7 -4 3683.87 1037.29 15 0 7 -4 2702.80 1142.73 4 0 7 -4 4154.61 812.685 16 0 7 -4 3602.64 687.306 10 0 7 -4 2942.50 581.069 12 0 7 -3 108107. 3805.73 12 0 7 -3 125350. 4321.50 16 0 7 -3 122877. 4388.73 14 0 7 -3 118449. 6657.86 15 0 7 -3 107990. 6373.23 4 0 7 -2 60587.2 5287.82 15 0 7 -2 69650.5 4617.91 4 0 7 -2 70408.8 3041.41 6 0 7 -2 68525.5 3235.09 16 0 7 -1 1626.08 494.894 6 0 7 -1 1361.73 429.832 16 0 7 -1 1482.38 647.138 4 0 7 -1 2132.96 1050.80 15 0 7 0 132702. 4234.99 13 0 7 0 139613. 4638.94 16 0 7 0 131701. 4352.00 6 0 7 1 4148.21 773.570 13 0 7 1 3635.68 852.501 4 0 7 1 3946.16 787.991 6 0 7 1 5147.28 905.160 16 0 7 2 3155.55 771.370 4 0 7 2 3601.84 708.037 13 0 7 2 2692.60 758.160 16 0 7 2 2941.73 660.416 6 0 7 3 20762.1 1865.75 6 0 7 3 22533.1 1779.10 7 0 7 3 23526.8 1867.39 13 0 7 3 24974.8 2303.48 16 0 7 4 56630.4 3151.26 6 0 7 4 51768.1 2936.61 7 0 7 5 39254.0 3990.89 16 0 7 5 34820.4 2654.87 7 0 7 5 31265.9 2487.27 6 0 7 6 2046.76 811.035 16 0 7 6 1657.12 619.180 7 0 7 6 1613.45 596.633 6 0 7 7 56129.2 3535.33 16 0 7 7 60662.5 4401.88 6 0 7 7 50600.6 4051.20 7 0 7 8 8474.24 1749.76 6 0 7 8 8583.48 1391.45 7 0 7 8 11067.1 1382.96 16 0 7 9 -161.595 223.588 6 0 7 9 -192.352 157.718 16 0 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