#------------------------------------------------------------------------------ #$Date: 2021-10-15 02:07:29 +0300 (Fri, 15 Oct 2021) $ #$Revision: 269961 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/85/7708569.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708569 loop_ _publ_author_name 'Ibrahim, Nourhan M.' 'Khaled, Rabaa M.' 'Ragheb, Mohamed A.' 'Radacki, Krzysztof' 'Farag, Ahmad M.' 'Mansour, Ahmed M.' _publ_section_title ; Light-activated cytotoxicity of dicarbonyl Ru(ii) complexes with a benzimidazole coligand towards breast cancer ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT02296B _journal_year 2021 _chemical_formula_moiety 'C18 H15 Cl2 N3 O4 Ru' _chemical_formula_sum 'C18 H15 Cl2 N3 O4 Ru' _chemical_formula_weight 509.30 _chemical_properties_physical Photo-sensitive _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _audit_creation_date 2020-05-11 _audit_creation_method 'CrysAlisPro 1.171.41.63a (Rigaku OD, 2020)' _audit_update_record ; 2021-05-23 deposited with the CCDC. 2021-09-28 downloaded from the CCDC. ; _cell_angle_alpha 90.0 _cell_angle_beta 92.9222(10) _cell_angle_gamma 90.0 _cell_formula_units_Z 4 _cell_length_a 7.86247(9) _cell_length_b 11.42684(13) _cell_length_c 21.9614(2) _cell_measurement_reflns_used 16184 _cell_measurement_temperature 100.03(17) _cell_measurement_theta_max 77.0920 _cell_measurement_theta_min 4.0530 _cell_volume 1970.52(4) _computing_cell_refinement 'CrysAlisPro 1.171.41.63a (Rigaku OD, 2020)' _computing_data_collection 'CrysAlisPro 1.171.41.63a (Rigaku OD, 2020)' _computing_data_reduction 'CrysAlisPro 1.171.41.63a (Rigaku OD, 2020)' _computing_molecular_graphics 'ShelXLe (Huebschle et all, 2011)' _computing_publication_material 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.03(17) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.9990 _diffrn_measured_fraction_theta_max 0.9834 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -42.00 24.00 0.50 1.00 -- -47.95 37.00 -60.00 132 2 \w -38.00 24.00 0.50 1.00 -- -47.95 4.00-125.00 124 3 \w -84.00 -16.00 0.50 1.00 -- -47.95 125.00 30.00 136 4 \w -108.00 -9.00 0.50 1.00 -- -47.95 -4.00 56.00 198 5 \w -24.00 12.00 0.50 1.00 -- 47.95 -4.00 56.00 72 6 \w -21.00 26.00 0.50 1.00 -- 47.95 -19.00 -60.00 94 7 \w 57.00 95.00 0.50 1.00 -- 47.95 4.00-125.00 76 8 \w 60.00 96.00 0.50 1.00 -- 47.95-125.00-180.00 72 9 \w -42.00 -15.00 0.50 4.00 -- -86.25 4.00-125.00 54 10 \w -66.00 -16.00 0.50 4.00 -- -86.25 61.00 -60.00 100 11 \w -99.00 -64.00 0.50 4.00 -- -86.25 -4.00 56.00 70 12 \w -157.00-123.00 0.50 4.00 -- -86.25 -4.00 56.00 68 13 \w 126.00 177.00 0.50 4.00 -- 107.75 4.00-125.00 102 14 \w 145.00 174.00 0.50 4.00 -- 107.75 45.00-120.00 58 15 \w 107.00 174.00 0.50 4.00 -- 107.75 30.00 0.00 134 16 \w 139.00 178.00 0.50 4.00 -- 107.75 30.00 60.00 78 17 \w 114.00 178.00 0.50 4.00 -- 107.75 77.00 90.00 128 18 \w 98.00 136.00 0.50 4.00 -- 107.75 30.00 60.00 76 19 \w 95.00 145.00 0.50 4.00 -- 107.75 125.00 -90.00 100 20 \w 63.00 123.00 0.50 4.00 -- 107.75 4.00-125.00 120 21 \w 57.00 91.00 0.50 4.00 -- 107.75 -77.00 -60.00 68 22 \w 80.00 106.00 0.50 4.00 -- 107.75 -77.00 0.00 52 23 \w 82.00 112.00 0.50 4.00 -- 107.75-125.00 60.00 60 24 \w 58.00 112.00 0.50 4.00 -- 107.75-125.00 30.00 108 25 \w 67.00 93.00 0.50 4.00 -- 107.75 -94.00 90.00 52 26 \w 39.00 68.00 0.50 4.00 -- 107.75-125.00 60.00 58 27 \w 41.00 66.00 0.50 4.00 -- 107.75 -94.00 60.00 50 28 \w 35.00 100.00 0.50 4.00 -- 107.75 -77.00 120.00 130 29 \w 37.00 63.00 0.50 4.00 -- 107.75 -77.00 60.00 52 30 \w 36.00 76.00 0.50 4.00 -- 107.75 -77.00 0.00 80 31 \w 35.00 100.00 0.50 4.00 -- 107.75-103.00 -84.56 130 32 \w 77.00 107.00 0.50 4.00 -- 107.75-107.00 -92.40 60 33 \w 66.00 105.00 0.50 4.00 -- 107.75 -94.00-180.00 78 34 \w 75.00 110.00 0.50 4.00 -- 107.75-125.00-180.00 70 35 \w 40.00 70.00 0.50 4.00 -- 107.75 -61.00-180.00 60 36 \w 36.00 70.00 0.50 4.00 -- 107.75 -61.00 -90.00 68 37 \w 35.00 100.00 0.50 4.00 -- 107.75 -77.00 -90.00 130 38 \w 49.00 112.00 0.50 4.00 -- 107.75-125.00 -90.00 126 39 \w 40.00 65.00 0.50 4.00 -- 107.75 -61.00 60.00 50 40 \w 37.00 71.00 0.50 4.00 -- 107.75 -61.00 150.00 68 41 \w 39.00 112.00 0.50 4.00 -- 107.75-125.00 150.00 146 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.1945209000 _diffrn_orient_matrix_UB_12 -0.0129931000 _diffrn_orient_matrix_UB_13 -0.0027759000 _diffrn_orient_matrix_UB_21 -0.0185785000 _diffrn_orient_matrix_UB_22 -0.1341204000 _diffrn_orient_matrix_UB_23 0.0018963000 _diffrn_orient_matrix_UB_31 -0.0180838000 _diffrn_orient_matrix_UB_32 -0.0030360000 _diffrn_orient_matrix_UB_33 -0.0701596000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0321 _diffrn_reflns_av_sigmaI/netI 0.0395 _diffrn_reflns_av_unetI/netI 0.0198 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.984 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_number 23678 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.984 _diffrn_reflns_theta_full 68.1328 _diffrn_reflns_theta_max 77.2565 _diffrn_reflns_theta_min 2.0143 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 9.204 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.384 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.63a (Rigaku Oxford Diffraction, 2020) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour orange _exptl_crystal_density_diffrn 1.717 _exptl_crystal_description block _exptl_crystal_F_000 1016 _exptl_crystal_size_max 0.180 _exptl_crystal_size_mid 0.091 _exptl_crystal_size_min 0.039 _refine_diff_density_max 0.448 _refine_diff_density_min -0.900 _refine_diff_density_rms 0.078 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.119 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 254 _refine_ls_number_reflns 4112 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.119 _refine_ls_R_factor_all 0.0280 _refine_ls_R_factor_gt 0.0269 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0316P)^2^+2.5560P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0708 _refine_ls_wR_factor_ref 0.0714 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3922 _reflns_number_total 4112 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt02296b2.cif _cod_data_source_block 10 _cod_original_cell_volume 1970.51(4) _cod_database_code 7708569 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.288 _shelx_estimated_absorpt_t_max 0.710 _shelx_res_file ; TITL KR1049_AhMa NM3 in P2(1)/n KR1049_AhMa_a.res created by SHELXL-2018/3 at 08:44:32 on 11-May-2020 CELL 1.54184 7.8625 11.4268 21.9614 90.000 92.922 90.000 ZERR 4.000 0.0001 0.0001 0.0002 0.000 0.001 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H N O CL RU UNIT 72.00 60.00 12.00 16.00 8.00 4.00 TEMP -173 SIZE 0.04 0.09 0.18 L.S. 10 BOND $H LIST 4 acta FMAP 2 PLAN 20 WGHT 0.031600 2.556000 FVAR 0.38798 RU1 6 0.393683 0.531288 0.674812 11.00000 0.01552 0.02501 = 0.02393 -0.00030 -0.00130 0.00185 O1 4 0.533477 0.442252 0.559044 11.00000 0.03862 0.04306 = 0.03141 -0.00173 0.00982 0.01211 C1 1 0.481031 0.477155 0.602456 11.00000 0.02259 0.02628 = 0.03367 0.00572 -0.00100 0.00389 CL1 5 0.240226 0.355079 0.686764 11.00000 0.03309 0.02781 = 0.03228 0.00150 -0.00105 -0.00520 CL2 5 0.516170 0.723050 0.667420 11.00000 0.01710 0.02775 = 0.04063 -0.00035 0.00187 0.00057 O2 4 0.705325 0.425473 0.740180 11.00000 0.03084 0.05463 = 0.04564 0.00018 -0.01299 0.02037 C2 1 0.589091 0.466493 0.715987 11.00000 0.03033 0.03350 = 0.03029 -0.00461 0.00123 -0.00020 RESI 1 LIG N1 3 0.272931 0.602813 0.754449 11.00000 0.01700 0.03029 = 0.02376 -0.00249 -0.00130 0.00096 AFIX 13 H1 2 0.299990 0.688310 0.754018 11.00000 -1.20000 AFIX 0 C2 1 0.084302 0.596648 0.745117 11.00000 0.01417 0.03827 = 0.02604 -0.00226 0.00033 0.00181 AFIX 23 H2A 2 0.029150 0.655615 0.770604 11.00000 -1.20000 H2AB 2 0.042322 0.518028 0.755903 11.00000 -1.20000 AFIX 0 C3 1 0.047133 0.621164 0.679133 11.00000 0.01482 0.02948 = 0.02687 -0.00236 -0.00157 0.00159 N4 3 0.163034 0.601925 0.638880 11.00000 0.01589 0.02706 = 0.02498 0.00019 -0.00114 0.00122 C5 1 0.087716 0.627160 0.581777 11.00000 0.01996 0.02499 = 0.02736 0.00065 -0.00255 0.00157 C6 1 0.151632 0.622959 0.523968 11.00000 0.02234 0.03280 = 0.02863 0.00162 0.00261 0.00131 AFIX 43 H6 2 0.265493 0.599269 0.518177 11.00000 -1.20000 AFIX 0 C7 1 0.043186 0.654569 0.475233 11.00000 0.03211 0.03446 = 0.02600 0.00129 0.00097 -0.00080 AFIX 43 H7 2 0.083678 0.652619 0.435222 11.00000 -1.20000 AFIX 0 C8 1 -0.125369 0.689498 0.483386 11.00000 0.03122 0.03559 = 0.02918 0.00070 -0.00798 0.00070 AFIX 43 H8 2 -0.196248 0.710487 0.448781 11.00000 -1.20000 AFIX 0 C9 1 -0.190563 0.694035 0.540692 11.00000 0.02275 0.03492 = 0.03143 0.00067 -0.00393 0.00319 AFIX 43 H9 2 -0.304535 0.717599 0.546378 11.00000 -1.20000 AFIX 0 C10 1 -0.080338 0.662237 0.589665 11.00000 0.01983 0.02855 = 0.02817 -0.00029 -0.00156 0.00067 N11 3 -0.101078 0.658147 0.652091 11.00000 0.01597 0.03733 = 0.02453 0.00006 0.00005 0.00369 AFIX 43 H11 2 -0.194100 0.676390 0.670624 11.00000 -1.20000 AFIX 0 RESI 0 RESI 2 PH C1 1 0.346306 0.560816 0.812423 11.00000 0.02140 0.03010 = 0.02189 -0.00450 -0.00328 0.00373 C2 1 0.500783 0.610850 0.831758 11.00000 0.02492 0.02750 = 0.02729 -0.00147 -0.00208 0.00096 AFIX 43 H2 2 0.547011 0.672969 0.809078 11.00000 -1.20000 AFIX 0 C3 1 0.587511 0.570324 0.884043 11.00000 0.02767 0.02868 = 0.03049 -0.00388 -0.00800 0.00228 C4 1 0.518435 0.480829 0.917989 11.00000 0.03806 0.03337 = 0.02957 0.00216 -0.00914 0.00392 AFIX 43 H4 2 0.576914 0.453381 0.954129 11.00000 -1.20000 AFIX 0 C5 1 0.363903 0.432236 0.898625 11.00000 0.04240 0.02927 = 0.03625 0.00366 -0.00188 -0.00307 AFIX 43 H5 2 0.316519 0.371295 0.921818 11.00000 -1.20000 AFIX 0 C6 1 0.276346 0.471304 0.845516 11.00000 0.03006 0.03054 = 0.03158 -0.00113 -0.00325 -0.00379 AFIX 43 H6 2 0.170682 0.437069 0.832337 11.00000 -1.20000 AFIX 0 RESI 0 RESI 3 CARB C1 1 0.756471 0.625368 0.900554 11.00000 0.02863 0.03437 = 0.03838 -0.00354 -0.00994 0.00353 O2 4 0.825185 0.695336 0.869408 11.00000 0.02995 0.05998 = 0.04792 0.00219 -0.00913 -0.01080 O3 4 0.820564 0.587828 0.954831 11.00000 0.04403 0.03555 = 0.05459 0.00345 -0.03126 -0.00308 C4 1 0.981503 0.640850 0.974257 11.00000 0.05007 0.03943 = 0.08153 0.00051 -0.04231 -0.00528 AFIX 137 H4A 2 1.068770 0.618094 0.946227 11.00000 -1.50000 H4B 2 1.015207 0.614139 1.015528 11.00000 -1.50000 H4C 2 0.969492 0.726215 0.974168 11.00000 -1.50000 RESI 0 AFIX 0 HKLF 4 REM KR1049_AhMa NM3 in P2(1)/n REM wR2 = 0.071381, GooF = S = 1.11870, Restrained GooF = 1.11870 for all data REM R1 = 0.026889 for 3922 Fo > 4sig(Fo) and 0.028035 for all 4112 data REM 254 parameters refined using 0 restraints END WGHT 0.0316 2.5563 REM Highest difference peak 0.448, deepest hole -0.900, 1-sigma level 0.078 Q1 1 0.3800 0.5356 0.6232 11.00000 0.05 0.45 Q2 1 0.6241 0.6401 0.6760 11.00000 0.05 0.43 Q3 1 0.5028 0.6192 0.6842 11.00000 0.05 0.39 Q4 1 0.3850 0.4600 0.6763 11.00000 0.05 0.38 Q5 1 0.0627 0.6158 0.7096 11.00000 0.05 0.38 Q6 1 0.5155 0.6979 0.7056 11.00000 0.05 0.38 Q7 1 0.5211 0.4615 0.6769 11.00000 0.05 0.37 Q8 1 0.4872 0.4404 0.6951 11.00000 0.05 0.37 Q9 1 0.2981 0.5877 0.7191 11.00000 0.05 0.34 Q10 1 0.3879 0.4572 0.6276 11.00000 0.05 0.34 Q11 1 0.4751 0.4638 0.6411 11.00000 0.05 0.34 Q12 1 0.4008 0.6447 0.6749 11.00000 0.05 0.32 Q13 1 0.0063 0.6269 0.5841 11.00000 0.05 0.32 Q14 1 0.3137 0.4440 0.7077 11.00000 0.05 0.32 Q15 1 0.6553 0.7186 0.6921 11.00000 0.05 0.32 Q16 1 0.4313 0.4556 0.6312 11.00000 0.05 0.31 Q17 1 0.4275 0.4654 0.7199 11.00000 0.05 0.31 Q18 1 0.1872 0.4462 0.7136 11.00000 0.05 0.31 Q19 1 0.0786 0.4842 0.7400 11.00000 0.05 0.30 Q20 1 0.7749 0.4103 0.7578 11.00000 0.05 0.30 ; _shelx_res_checksum 45532 _shelx_hkl_file ; 0 0 -1 0.06 0.37 0 0 -2 2474.73 72.58 0 0 -3 1.43 1.06 0 0 -3 1.08 1.42 0 0 -3 0.61 0.64 0 0 -4 1177.44 35.03 0 0 -4 1096.93 33.52 0 0 -5 1.54 2.91 0 0 -5 1.36 2.10 0 0 -6 5272.54 155.00 0 0 -6 5446.60 157.56 0 0 -7 0.76 3.01 0 0 -7 0.49 1.73 0 0 -7 2.16 3.07 0 0 -8 3123.45 92.78 0 0 -8 2914.91 91.48 0 0 -9 -1.05 3.72 0 0 -9 3.89 3.89 0 0 -10 367.40 17.02 0 0 -10 333.15 15.52 0 0 -11 4.15 4.69 0 0 -12 3582.84 113.50 0 0 -13 0.59 4.97 0 0 -14 4641.22 146.34 0 0 -15 -0.13 1.46 0 0 -15 -0.12 1.78 0 0 -15 1.79 1.60 0 0 -15 1.27 1.71 0 0 -16 113.91 5.17 0 0 -16 111.41 4.96 0 0 -16 100.83 5.44 0 0 -16 118.56 5.76 0 0 -16 110.91 5.55 0 0 -16 113.13 5.14 0 0 -16 119.30 5.84 0 0 -16 117.06 5.33 0 0 -17 0.69 1.66 0 0 -17 1.22 1.63 0 0 -17 -2.39 1.87 0 0 -17 0.82 2.02 0 0 -17 2.85 1.91 0 0 -17 3.90 1.57 0 0 -17 -0.17 1.90 0 0 -17 -0.35 1.82 0 0 -17 -1.67 1.91 0 0 -18 96.39 4.82 0 0 -18 83.35 4.51 0 0 -18 92.10 5.05 0 0 -18 95.71 5.33 0 0 -18 86.77 5.22 0 0 -18 93.73 4.61 0 0 -18 92.79 5.53 0 0 -19 -0.96 1.67 0 0 -19 0.52 1.93 0 0 -19 0.65 2.15 0 0 -19 1.15 2.24 0 0 -19 1.32 2.34 0 0 -19 -0.60 1.43 0 0 -19 1.82 1.97 0 0 -20 653.47 21.37 0 0 -20 665.05 21.47 0 0 -20 713.98 21.67 0 0 -20 733.97 22.14 0 0 -20 731.43 22.65 0 0 -20 740.83 22.90 0 0 -20 736.91 23.29 0 0 -21 -0.56 2.25 0 0 -21 0.13 1.95 0 0 -21 -1.59 2.20 0 0 -21 0.17 2.11 0 0 -21 0.77 1.82 0 0 -22 193.63 8.17 0 0 -22 188.20 8.28 0 0 -22 177.90 7.53 0 0 -22 199.27 8.76 0 0 -23 1.60 1.87 0 0 -23 1.28 2.34 0 0 -23 1.23 2.08 0 0 -24 20.47 2.81 0 0 -24 19.17 2.50 0 0 -25 0.68 1.56 0 1 0 0.74 0.62 0 1 -1 1528.06 45.83 0 1 1 1568.43 45.64 0 1 -2 312.97 10.46 0 1 -2 316.26 10.09 0 1 2 316.58 10.07 0 1 -3 4338.47 129.80 0 -1 -3 4572.10 130.03 0 1 3 4378.04 128.66 0 1 -3 4479.33 128.76 0 1 -4 299.70 10.93 0 1 -4 307.78 9.82 0 1 4 293.90 9.63 0 -1 -4 303.80 11.61 0 1 -5 4725.71 138.00 0 1 -5 4756.45 136.45 0 1 5 4629.03 136.18 0 -1 -5 4720.40 139.00 0 1 -6 334.72 13.15 0 1 -6 318.08 12.13 0 1 -6 330.59 13.02 0 1 6 296.59 9.81 0 -1 -6 318.26 13.20 0 -1 6 316.28 9.70 0 -1 -6 308.26 9.87 0 1 -7 2.35 3.10 0 -1 -7 6.40 3.38 0 1 -7 4.30 3.20 0 1 -7 1.77 0.86 0 1 -8 343.32 14.63 0 1 -8 349.78 15.16 0 -1 -8 341.97 15.26 0 1 -8 340.86 13.20 0 1 -9 2034.88 65.61 0 1 -9 2039.85 66.50 0 -1 -9 2163.01 67.03 0 1 -9 2078.88 63.53 0 1 -10 992.75 34.96 0 -1 -10 961.03 35.96 0 1 -10 1006.87 32.42 0 1 -11 1340.32 46.16 0 1 -11 1355.87 43.07 0 -1 -11 1419.51 48.39 0 1 -12 95.08 4.67 0 -1 -12 98.96 9.53 0 1 -12 83.63 8.12 0 -1 -13 4.66 4.90 0 1 -13 0.42 4.28 0 1 -13 3.99 2.25 0 1 -14 502.57 16.50 0 1 -14 484.29 16.25 0 -1 -14 492.14 17.13 0 -1 -14 538.50 25.05 0 1 -14 519.57 22.34 0 -1 -14 507.70 22.14 0 1 -14 497.72 16.47 0 -1 -14 485.72 16.22 0 1 -15 417.27 14.21 0 1 -15 403.78 13.70 0 -1 -15 394.17 14.42 0 1 -15 401.80 14.14 0 1 -15 416.72 14.74 0 1 -15 389.13 13.53 0 -1 -15 396.47 14.79 0 -1 -15 407.01 14.01 0 1 -15 429.78 14.16 0 -1 -15 395.10 13.70 0 -1 -15 407.50 14.12 0 -1 -15 406.93 13.87 0 -1 -15 407.72 14.12 0 1 -15 416.72 14.21 0 -1 -15 427.68 14.36 0 1 -15 390.17 14.02 0 -1 -15 446.67 22.95 0 -1 -15 433.12 20.29 0 1 -15 400.28 19.58 0 1 -15 399.43 13.76 0 1 -16 80.91 4.78 0 -1 -16 78.48 4.52 0 -1 -16 85.05 4.48 0 -1 -16 84.22 4.91 0 1 -16 77.13 4.62 0 -1 -16 86.51 4.64 0 1 -16 79.69 4.19 0 -1 -16 85.35 5.29 0 1 -16 81.85 5.18 0 1 -16 83.77 4.71 0 -1 -16 75.11 4.15 0 1 -16 71.28 3.98 0 -1 -16 83.09 4.87 0 -1 -16 78.63 4.22 0 1 -16 76.14 4.02 0 1 -16 73.91 4.49 0 -1 -16 86.43 10.21 0 1 -16 81.25 4.23 0 1 -16 72.82 4.47 0 -1 -16 78.47 4.07 0 -1 -16 89.84 8.91 0 1 -16 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1.80 0 4 -25 15.83 1.88 0 4 -26 84.53 3.45 0 4 -26 79.59 3.44 0 5 0 1.15 2.86 0 5 0 0.29 1.65 0 5 0 2.62 3.29 0 5 1 776.66 27.69 0 5 1 765.68 23.63 0 5 1 785.34 26.99 0 5 -1 763.67 27.59 0 5 2 1381.68 43.85 0 5 2 1274.16 39.40 0 5 -2 1334.69 39.52 0 5 -2 1354.39 44.11 0 5 2 1351.44 42.67 0 5 3 520.58 20.21 0 5 -3 541.16 20.57 0 5 -3 504.15 16.33 0 5 3 501.82 16.25 0 5 3 532.96 19.11 0 5 -3 549.72 21.20 0 5 4 3355.49 100.44 0 5 -4 3470.67 101.06 0 5 -4 3287.78 95.98 0 5 4 3200.13 95.83 0 5 4 3294.08 98.59 0 5 -4 3275.72 101.68 0 5 -5 648.33 24.28 0 5 5 643.08 23.67 0 5 5 607.01 19.42 0 5 -5 627.38 19.63 0 5 5 616.21 21.66 0 5 -6 173.86 10.22 0 -5 -6 173.30 10.53 0 5 6 160.50 9.47 0 5 6 162.44 6.40 0 5 -6 170.20 6.66 0 5 6 173.58 8.01 0 5 7 8.17 3.27 0 5 -7 10.91 4.15 0 5 -7 6.34 2.06 0 5 7 7.82 1.91 0 5 7 5.55 2.14 0 5 -7 12.06 5.78 0 -5 -7 10.24 4.28 0 5 8 1237.49 40.60 0 5 -8 1223.09 41.74 0 5 -8 1192.56 37.20 0 5 -8 1162.38 36.22 0 5 8 1183.20 35.90 0 5 -8 1317.98 44.49 0 5 -9 731.27 27.70 0 -5 9 742.98 26.23 0 -5 -9 648.80 27.03 0 5 9 722.75 26.50 0 5 -9 719.13 23.87 0 5 -9 748.87 30.36 0 -5 -10 1416.18 51.68 0 5 -10 1659.12 52.67 0 -5 10 1567.80 50.71 0 5 10 1562.47 51.39 0 5 -10 1764.44 56.74 0 -5 -11 644.74 20.07 0 -5 -11 562.92 19.21 0 5 -11 661.41 27.11 0 -5 -11 479.28 21.54 0 5 -11 615.31 19.47 0 -5 -11 560.94 18.78 0 5 -12 1049.22 32.51 0 -5 -12 1102.28 34.20 0 5 -12 1023.62 32.68 0 -5 -12 1008.04 33.25 0 5 -12 1162.91 41.46 0 5 -12 1084.02 33.39 0 -5 -12 1091.50 38.48 0 -5 -12 1039.82 32.80 0 5 -12 1157.56 34.56 0 5 -13 77.44 4.06 0 5 -13 80.65 4.23 0 -5 -13 84.03 5.29 0 -5 -13 78.20 4.41 0 -5 -13 78.37 4.79 0 5 -13 81.06 9.02 0 5 -13 76.65 4.77 0 -5 -13 82.03 8.07 0 -5 -13 73.84 4.46 0 5 -13 87.83 6.08 0 5 -14 153.81 6.34 0 5 -14 143.58 6.66 0 5 -14 147.75 6.95 0 -5 -14 149.98 7.69 0 5 -14 140.76 6.36 0 -5 -14 152.15 7.08 0 -5 -14 126.73 6.43 0 5 -14 135.10 11.08 0 -5 -14 158.50 11.33 0 5 -14 159.58 8.16 0 -5 -14 142.49 6.58 0 5 -15 841.47 26.34 0 5 -15 820.99 26.33 0 5 -15 841.04 26.92 0 5 -15 826.47 26.53 0 -5 -15 891.15 27.05 0 -5 -15 736.97 26.39 0 -5 -15 849.31 27.16 0 -5 -15 790.95 25.81 0 -5 -15 834.82 26.79 0 5 -15 813.56 32.92 0 -5 -15 820.83 32.89 0 -5 -15 836.00 26.46 0 5 -15 893.52 27.87 0 5 -16 588.21 18.99 0 5 -16 569.72 19.02 0 -5 -16 533.59 18.22 0 -5 -16 593.08 19.50 0 5 -16 567.82 19.20 0 -5 -16 527.83 19.09 0 -5 -16 585.11 19.62 0 -5 -16 548.76 19.22 0 -5 -16 531.08 18.77 0 5 -16 614.42 19.62 0 -5 -16 501.94 24.35 0 -5 -16 562.34 19.03 0 -5 -16 587.45 19.09 0 5 -16 630.99 20.40 0 5 -17 323.39 11.28 0 5 -17 316.09 11.81 0 5 -17 341.00 11.84 0 -5 -17 328.37 12.09 0 5 -17 332.12 12.12 0 5 -17 243.01 10.90 0 -5 -17 296.84 11.77 0 -5 -17 336.45 12.38 0 -5 -17 330.70 12.10 0 5 -17 330.98 12.21 0 -5 -17 315.60 11.66 0 -5 -17 270.02 16.49 0 -5 -17 324.96 11.70 0 -5 -17 336.73 11.93 0 5 -17 318.74 12.74 0 5 -18 405.92 14.42 0 5 -18 426.12 15.26 0 5 -18 414.47 14.98 0 -5 -18 462.05 15.42 0 5 -18 447.29 15.57 0 -5 -18 432.66 15.22 0 -5 -18 437.44 15.33 0 -5 -18 413.20 14.81 0 5 -18 447.16 15.55 0 -5 -18 433.42 14.84 0 -5 -18 434.46 15.06 0 5 -18 450.52 15.89 0 -5 -19 66.97 4.32 0 5 -19 68.25 4.64 0 -5 -19 65.93 4.46 0 -5 -19 63.86 4.94 0 5 -19 69.48 4.69 0 -5 -19 64.48 4.28 0 5 -19 59.51 4.87 0 5 -19 62.10 4.07 0 5 -19 63.93 4.36 0 -5 -19 69.33 4.57 0 -5 -19 61.02 3.90 0 -5 -20 3.67 2.58 0 5 -20 -0.14 2.64 0 -5 -20 0.91 2.08 0 -5 -20 2.12 2.18 0 5 -20 1.53 1.90 0 5 -20 -0.26 1.68 0 -5 -20 1.62 2.29 0 5 -20 0.71 2.36 0 5 -20 1.95 2.14 0 -5 -21 112.77 5.39 0 5 -21 103.68 5.14 0 5 -21 114.59 5.93 0 5 -21 102.95 5.53 0 -5 -21 111.43 5.86 0 -5 -21 108.54 5.31 0 5 -21 106.35 5.57 0 -5 -21 116.60 5.43 0 -5 -22 188.18 7.55 0 -5 -22 187.31 8.01 0 5 -22 207.78 8.19 0 5 -22 212.04 8.37 0 -5 -22 196.87 7.62 0 5 -22 194.47 8.03 0 -5 -22 204.31 7.72 0 -5 -23 146.80 5.84 0 -5 -23 138.37 6.04 0 -5 -23 153.21 5.94 0 5 -23 136.49 6.07 0 -5 -23 149.49 5.84 0 5 -23 145.58 6.25 0 5 -23 146.67 6.39 0 -5 -24 178.20 6.17 0 5 -24 171.98 6.50 0 5 -25 18.87 1.73 0 5 -26 11.58 1.02 0 6 0 133.47 9.60 0 6 0 156.31 9.43 0 6 0 140.17 5.92 0 6 1 794.44 30.28 0 6 -1 820.08 29.97 0 6 1 824.12 29.31 0 6 1 800.58 25.10 0 6 2 3.34 3.56 0 6 -2 -0.38 4.34 0 6 2 3.29 3.29 0 6 2 5.43 2.05 0 6 -3 407.14 17.97 0 6 3 388.00 17.78 0 6 3 393.37 16.23 0 6 -3 397.64 18.34 0 6 -3 383.36 13.09 0 6 3 379.21 12.99 0 6 4 95.98 7.89 0 6 -4 109.27 8.35 0 6 -4 113.50 9.28 0 6 4 93.29 6.64 0 6 4 96.83 4.78 0 6 -4 104.15 4.96 0 6 -5 2652.43 80.15 0 6 5 2478.48 78.89 0 6 5 2380.24 76.14 0 6 -5 2539.04 80.77 0 6 5 2411.63 73.13 0 6 -5 2522.19 73.39 0 6 -6 639.76 25.45 0 6 6 622.93 24.47 0 6 6 586.80 21.68 0 6 6 589.49 19.20 0 6 -6 601.63 19.54 0 6 7 2821.10 88.98 0 6 -7 2914.00 90.44 0 6 7 2811.77 82.91 0 6 -7 2812.12 83.28 0 6 -7 2765.69 83.89 0 6 8 376.92 17.25 0 6 -8 377.81 18.35 0 -6 8 366.55 16.75 0 6 -8 409.03 20.73 0 6 -8 373.60 12.93 0 6 8 367.27 12.48 0 6 -8 346.51 13.67 0 6 -9 515.94 24.29 0 6 -9 481.13 17.10 0 6 -9 474.43 15.92 0 -6 9 454.82 19.78 0 6 -9 470.21 21.55 0 6 9 457.31 20.15 0 -6 -9 421.66 20.93 0 6 -10 286.86 9.84 0 6 -10 297.59 10.71 0 6 -10 299.54 12.05 0 6 -10 325.99 18.42 0 6 10 259.21 13.89 0 -6 -10 256.60 14.50 0 -6 10 281.95 13.79 0 6 -10 303.80 15.67 0 -6 -10 270.96 10.03 0 6 -10 280.62 9.63 0 6 -10 289.58 10.75 0 -6 -10 266.55 10.56 0 6 -11 122.93 5.85 0 -6 -11 90.45 7.68 0 -6 -11 102.87 5.61 0 6 -11 125.00 11.54 0 6 -11 104.71 4.53 0 -6 -11 107.09 5.01 0 -6 -11 104.58 5.34 0 6 -11 109.72 4.83 0 6 -11 122.88 5.68 0 6 -12 54.59 3.17 0 6 -12 50.99 3.81 0 6 -12 55.35 3.39 0 -6 -12 56.20 4.04 0 6 -12 52.05 8.74 0 6 -12 58.12 4.16 0 -6 -12 42.02 5.98 0 6 -12 45.34 2.75 0 -6 -12 42.27 3.02 0 -6 -12 55.07 3.83 0 6 -13 630.31 21.12 0 -6 -13 623.11 21.19 0 -6 -13 613.07 20.62 0 -6 -13 647.49 26.25 0 6 -13 619.37 20.56 0 -6 -13 627.25 21.15 0 6 -13 677.92 29.53 0 6 -13 637.15 20.33 0 6 -14 13.81 2.84 0 -6 -14 21.03 3.03 0 6 -14 22.41 2.50 0 -6 -14 15.01 2.96 0 -6 -14 18.97 3.04 0 -6 -14 23.88 5.20 0 6 -14 24.21 4.86 0 6 -14 19.10 2.24 0 6 -14 24.03 6.33 0 6 -15 996.98 30.56 0 6 -15 995.27 31.20 0 6 -15 989.97 30.85 0 -6 -15 912.89 29.97 0 -6 -15 1006.92 31.38 0 -6 -15 917.04 30.47 0 -6 -15 991.54 30.75 0 -6 -15 859.46 35.99 0 6 -15 1062.79 32.51 0 6 -15 985.58 38.74 0 6 -16 11.07 2.28 0 -6 -16 8.95 2.04 0 -6 -16 16.58 3.07 0 -6 -16 9.84 2.30 0 -6 -16 13.92 2.91 0 -6 -16 18.07 3.03 0 -6 -16 14.08 2.60 0 -6 -16 9.56 4.04 0 6 -16 16.09 4.54 0 6 -16 12.44 2.82 0 -6 -16 7.77 2.57 0 6 -16 9.68 1.99 0 6 -16 12.44 2.27 0 6 -17 5.08 1.98 0 -6 -17 3.57 2.54 0 -6 -17 4.03 2.02 0 -6 -17 8.64 2.74 0 -6 -17 5.86 2.25 0 -6 -17 3.83 2.67 0 6 -17 10.49 3.91 0 -6 -17 2.66 2.34 0 6 -17 1.72 2.42 0 6 -17 4.08 1.99 0 6 -17 7.01 1.94 0 6 -18 14.74 2.00 0 6 -18 15.66 2.35 0 6 -18 15.22 2.36 0 -6 -18 13.17 2.93 0 -6 -18 11.92 2.38 0 -6 -18 14.38 2.94 0 -6 -18 13.08 2.47 0 6 -18 19.24 4.06 0 -6 -18 13.46 2.61 0 6 -18 17.13 2.98 0 6 -18 16.21 2.61 0 -6 -18 15.27 2.76 0 6 -19 442.02 15.57 0 6 -19 434.51 15.64 0 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10.91 0 7 3 291.97 10.78 0 7 -4 705.08 29.15 0 7 4 705.81 28.80 0 7 -4 703.41 22.89 0 7 4 703.27 22.74 0 7 -4 734.54 29.79 0 7 4 704.56 26.54 0 7 5 27.63 5.40 0 7 -5 24.24 5.48 0 7 -5 25.95 3.55 0 7 -5 27.03 3.22 0 7 5 25.12 2.96 0 7 -5 32.33 6.80 0 7 5 25.40 4.41 0 7 -5 30.79 2.29 0 7 -6 64.15 8.31 0 7 -6 53.94 7.29 0 7 6 52.35 6.82 0 7 -6 50.09 4.06 0 -7 6 55.30 3.46 0 7 -6 49.48 4.36 0 7 6 53.10 3.81 0 7 -7 10.07 3.52 0 -7 -7 9.12 1.68 0 7 7 8.20 2.37 0 -7 7 6.89 1.71 0 -7 -7 8.54 2.09 0 7 -7 7.87 2.75 0 -7 7 6.38 3.13 0 7 -7 7.61 4.85 0 -7 -7 3.97 3.72 0 7 7 9.38 4.09 0 -7 -8 304.33 11.59 0 -7 -8 336.50 11.93 0 7 -8 323.62 11.08 0 7 8 300.38 16.53 0 7 -8 318.20 17.90 0 -7 -8 291.63 17.71 0 -7 8 294.21 15.92 0 -7 -8 305.68 12.09 0 7 8 336.49 11.82 0 -7 8 354.83 11.76 0 7 -8 325.17 12.98 0 -7 -9 8.21 1.99 0 -7 -9 4.96 2.01 0 -7 -9 3.82 1.71 0 7 -9 7.31 3.97 0 7 -9 7.36 6.72 0 7 -9 6.22 1.54 0 7 -9 10.44 4.61 0 7 9 4.89 3.28 0 -7 9 1.44 2.39 0 -7 -9 4.84 3.15 0 7 -10 1208.53 36.49 0 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15.58 0 8 -5 263.98 16.44 0 -8 -5 229.01 16.71 0 -8 5 215.56 14.40 0 -8 -6 59.66 3.57 0 8 6 57.78 4.41 0 8 -6 67.83 4.91 0 -8 6 63.55 3.99 0 8 -6 64.78 5.14 0 -8 -6 53.41 4.33 0 8 -6 58.72 8.95 0 -8 -6 55.49 8.25 0 8 -6 64.04 8.43 0 8 6 59.05 7.79 0 -8 6 49.70 6.76 0 8 6 64.25 3.75 0 8 7 184.17 7.41 0 -8 -7 193.97 7.58 0 -8 -7 136.29 12.69 0 8 7 157.87 12.40 0 -8 7 153.96 11.76 0 8 -7 180.26 13.95 0 -8 7 186.08 7.75 0 8 -7 178.28 8.79 0 -8 -7 164.10 8.13 0 8 -7 178.68 7.13 0 8 -7 196.84 15.08 0 -8 -8 67.19 4.04 0 -8 -8 50.17 3.76 0 8 -8 66.45 5.60 0 -8 8 69.27 4.07 0 -8 -8 59.70 4.36 0 8 -8 61.90 3.54 0 8 8 50.53 7.20 0 -8 8 43.06 6.12 0 -8 -8 48.22 7.47 0 8 -8 59.15 8.49 0 8 -9 171.63 6.88 0 -8 -9 162.92 7.36 0 -8 -9 182.07 7.77 0 -8 9 188.10 7.43 0 -8 -9 164.08 7.59 0 8 -9 185.45 9.13 0 8 -9 176.16 14.95 0 -8 9 151.57 11.25 0 8 9 161.31 12.40 0 8 -9 156.16 13.17 0 -8 -10 18.56 4.51 0 -8 -10 23.52 3.00 0 -8 -10 30.66 3.14 0 8 -10 31.86 4.92 0 8 -10 31.49 8.10 0 -8 -10 27.69 2.91 0 -8 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20.24 0 9 8 363.85 13.62 0 9 -8 412.57 13.68 0 -9 -9 2.80 1.95 0 -9 9 4.64 1.80 0 -9 -9 2.57 1.74 0 9 -9 2.73 1.77 0 9 -9 3.42 4.18 0 -9 -9 2.15 3.14 0 -9 -10 473.52 18.45 0 -9 -10 562.72 18.69 0 9 -10 577.43 18.28 0 -9 -10 558.26 19.19 0 -9 -10 519.44 18.46 0 -9 -10 621.92 19.52 0 9 -10 602.59 20.48 0 9 -10 605.94 30.31 0 9 -11 0.98 1.75 0 -9 -11 1.15 2.38 0 -9 -11 1.70 2.03 0 -9 -11 0.18 1.87 0 9 -11 4.46 6.48 0 9 -11 8.92 4.67 0 -9 -11 0.96 2.59 0 9 -11 -0.55 1.57 0 -9 -11 0.26 1.84 0 9 -12 4.75 1.83 0 -9 -12 6.96 2.57 0 -9 -12 5.48 2.21 0 -9 -12 6.60 2.18 0 9 -12 5.21 5.60 0 9 -12 15.64 4.65 0 -9 -12 7.84 2.06 0 9 -12 2.72 1.54 0 -9 -12 4.82 2.53 0 -9 -13 0.18 2.00 0 -9 -13 1.81 2.53 0 9 -13 4.46 4.27 0 9 -13 4.30 1.82 0 -9 -13 4.06 2.36 0 -9 -13 1.24 2.04 0 -9 -14 169.53 7.81 0 -9 -14 158.54 7.14 0 9 -14 173.31 7.25 0 -9 -14 157.56 7.39 0 9 -14 180.56 9.06 0 9 -15 1.36 3.69 0 -9 -15 1.79 2.28 0 9 -15 -0.40 1.76 0 -9 -15 1.51 1.98 0 -9 -15 -1.24 2.52 0 -9 -16 265.73 10.05 0 9 -16 260.34 9.98 0 -9 -16 265.21 10.45 0 -9 -16 265.54 10.07 0 -9 -16 265.85 9.70 0 -9 -17 1.66 1.80 0 9 -17 0.78 1.66 0 -9 -17 0.90 1.90 0 9 -17 1.08 1.58 0 -9 -17 0.22 1.88 0 -9 -17 2.68 2.07 0 -9 -18 227.99 8.89 0 -9 -18 234.20 8.25 0 -9 -18 224.39 8.42 0 9 -18 231.38 8.59 0 -9 -18 235.92 8.60 0 9 -18 237.80 8.80 0 -9 -19 3.55 1.50 0 9 -19 3.15 1.38 0 -9 -19 2.61 1.45 0 9 -19 2.67 1.38 0 9 -19 1.98 2.24 0 -9 -20 14.53 1.69 0 9 -20 12.98 1.49 0 9 -20 15.26 1.48 0 9 -20 15.40 1.69 0 9 -21 3.76 0.99 0 -10 0 222.18 9.81 0 10 0 182.45 13.89 0 10 0 187.86 15.02 0 -10 0 176.07 15.20 0 -10 1 690.38 23.25 0 10 -1 646.59 29.58 0 10 1 638.50 28.66 0 -10 1 613.41 31.37 0 10 1 677.40 31.31 0 10 2 67.45 4.29 0 -10 2 60.49 8.73 0 10 -2 59.83 9.14 0 10 2 48.73 8.28 0 10 -2 57.18 8.46 0 10 2 54.58 7.39 0 -10 2 69.89 4.98 0 -10 -3 21.04 3.58 0 -10 3 18.24 2.90 0 10 -3 20.87 2.68 0 10 -3 20.94 3.13 0 10 -3 16.01 5.84 0 -10 3 7.09 3.67 0 -10 -3 12.81 5.55 0 10 3 11.39 5.60 0 10 -3 13.49 6.09 0 10 3 17.08 2.55 0 10 4 29.50 3.00 0 10 -4 25.93 7.24 0 -10 -4 26.28 3.80 0 -10 4 30.75 3.35 0 -10 -4 12.69 5.23 0 10 -4 40.72 7.86 0 10 4 24.98 6.47 0 -10 4 19.79 5.29 0 10 -4 28.55 3.66 0 -10 -5 249.60 19.43 0 10 5 284.64 19.01 0 10 -5 267.91 19.31 0 -10 5 289.78 18.45 0 10 -5 319.26 20.05 0 -10 5 335.75 12.49 0 -10 -5 303.76 12.95 0 10 -5 346.08 12.38 0 -10 -6 145.11 14.36 0 10 -6 184.28 15.46 0 10 6 169.77 14.33 0 -10 6 164.87 13.51 0 10 -6 189.99 15.79 0 10 -6 219.40 8.46 0 -10 6 221.58 9.13 0 -10 -6 211.17 9.64 0 10 -6 213.59 9.27 0 -10 -7 710.67 25.85 0 10 -7 837.27 24.96 0 -10 7 796.53 25.53 0 -10 -7 745.81 25.08 0 -10 -7 592.83 32.96 0 -10 7 676.72 32.17 0 10 -7 855.91 36.70 0 10 -7 818.44 25.90 0 -10 -8 363.40 14.13 0 -10 8 392.38 13.88 0 10 -8 399.89 13.36 0 -10 -8 358.04 13.67 0 10 -8 384.67 23.22 0 10 -8 416.67 14.76 0 10 -9 41.48 4.70 0 -10 -9 31.26 3.39 0 10 -9 37.20 3.00 0 -10 -9 39.14 3.42 0 -10 9 32.23 3.00 0 -10 -9 27.03 3.10 0 10 -10 123.97 7.17 0 -10 -10 117.27 5.94 0 -10 -10 110.75 5.70 0 10 -10 123.81 5.65 0 -10 -10 113.15 5.95 0 -10 -10 110.95 5.66 0 10 -10 118.83 5.40 0 10 -11 276.55 11.30 0 -10 -11 259.11 9.78 0 -10 -11 243.51 9.81 0 10 -11 248.27 9.58 0 -10 -11 250.59 9.99 0 10 -11 245.65 9.21 0 -10 -11 246.64 9.52 0 10 -12 48.42 5.06 0 -10 -12 38.41 3.56 0 -10 -12 42.78 3.38 0 10 -12 39.88 3.11 0 -10 -12 45.21 3.65 0 10 -12 41.57 2.85 0 -10 -13 850.48 28.53 0 10 -13 959.32 29.81 0 10 -13 898.23 28.30 0 -10 -13 906.09 28.57 0 -10 -13 907.50 28.20 0 -10 -14 73.49 4.31 0 -10 -14 70.64 4.59 0 -10 -14 75.19 4.30 0 10 -14 77.85 4.22 0 -10 -14 83.89 4.55 0 10 -14 88.04 5.75 0 -10 -15 120.68 5.19 0 -10 -15 108.87 5.29 0 10 -15 112.34 5.22 0 10 -15 122.36 6.54 0 10 -16 7.29 2.95 0 10 -16 7.77 1.72 0 -10 -16 10.86 1.98 0 10 -17 26.62 3.04 0 10 -17 24.22 2.16 0 -10 -17 26.04 2.30 0 10 -18 8.83 1.48 0 10 -18 7.35 1.10 0 10 -18 8.40 1.38 0 -10 -18 7.20 1.45 0 10 -19 284.46 9.76 0 -10 -19 296.69 9.70 0 -10 -20 21.08 1.31 0 11 0 1.43 2.18 0 -11 0 -0.22 2.67 0 -11 0 -0.93 3.80 0 11 0 0.80 4.32 0 11 1 172.40 7.58 0 11 -1 172.75 7.50 0 -11 1 160.17 8.32 0 11 -2 483.01 16.25 0 11 2 484.41 16.40 0 -11 2 475.29 17.31 0 11 -2 362.57 23.56 0 11 2 397.21 23.87 0 11 3 626.73 21.23 0 11 -3 658.89 21.16 0 -11 -3 601.89 22.55 0 -11 3 660.14 22.27 0 -11 4 500.29 17.59 0 -11 -4 463.51 17.96 0 11 4 487.87 16.84 0 -11 5 317.35 11.88 0 11 5 294.05 11.14 0 -11 -5 287.63 12.15 0 11 -5 282.55 11.00 0 11 6 212.69 8.58 0 -11 6 223.79 9.21 0 11 -6 219.66 8.62 0 -11 -6 206.98 9.51 0 11 -6 210.46 8.83 0 -11 7 3.68 1.92 0 -11 -7 2.51 2.12 0 11 -7 2.87 1.95 0 11 7 4.64 1.85 0 -11 -7 0.89 2.20 0 11 -7 4.06 2.90 0 -11 -7 0.62 1.78 0 11 -8 321.46 11.15 0 -11 8 299.69 11.36 0 11 8 302.27 10.75 0 -11 -8 274.99 11.52 0 -11 -8 342.42 11.76 0 11 -8 320.09 11.87 0 -11 -8 293.22 11.08 0 11 -9 454.19 15.85 0 11 -9 442.65 14.89 0 -11 -9 453.46 15.34 0 -11 -9 456.50 15.19 0 -11 -9 415.32 15.01 0 11 -9 446.42 14.90 0 11 -10 437.47 15.15 0 -11 -10 409.40 14.20 0 11 -10 411.32 13.89 0 -11 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4 4 156.43 7.18 8 -4 4 151.61 6.74 -8 -4 -4 144.13 6.77 -8 4 -4 160.12 6.49 8 -4 5 21.51 2.68 8 4 5 29.00 3.30 -8 -4 -5 23.99 2.78 -8 4 -5 23.20 2.49 -8 4 -5 22.38 2.36 -8 -4 -6 3.03 2.03 8 4 6 3.53 2.31 8 -4 6 2.54 1.87 -8 4 -6 3.16 1.48 -8 -4 -7 82.57 4.41 8 -4 7 80.51 4.11 8 4 7 79.37 4.42 -8 4 -7 76.63 3.68 -8 -4 -8 177.39 6.97 8 -4 8 165.87 6.37 8 4 8 157.54 6.49 -8 4 -8 171.26 6.27 -8 4 -9 93.14 4.19 -8 -4 -9 106.01 4.79 -8 -4 -10 193.80 7.42 -8 4 -10 199.18 7.27 -8 -4 -11 57.94 3.21 -8 4 -11 60.20 3.11 -8 -4 -12 4.93 1.54 -8 4 -12 5.86 1.24 -8 -4 -13 9.01 1.26 8 -5 -14 125.15 4.29 -8 5 14 124.42 4.24 8 -5 -13 163.61 5.73 -8 -5 13 174.57 5.80 8 -5 -12 4.70 1.18 8 5 -12 4.31 1.10 -8 -5 12 7.84 1.29 8 -5 -11 0.42 1.22 8 5 -11 0.30 1.07 8 -5 -10 237.13 7.60 8 5 -10 224.13 7.49 8 -5 -9 211.03 7.12 -8 5 9 198.96 6.67 -8 5 8 200.04 7.12 -8 5 8 212.89 7.11 8 5 -8 191.26 7.15 8 5 -7 295.29 10.30 8 -5 -7 299.69 10.07 -8 5 7 304.67 9.77 8 5 -6 26.00 2.81 8 -5 -6 22.08 2.34 -8 5 6 22.46 2.00 8 5 -6 22.85 1.99 8 -5 -5 0.95 1.75 -8 5 5 2.47 1.35 8 5 -5 3.50 2.26 8 5 -4 147.74 6.68 8 -5 -4 149.46 6.35 -8 5 4 145.78 5.89 -8 -5 4 139.94 6.60 -8 5 3 313.08 10.58 -8 -5 3 284.67 11.20 8 -5 -2 846.54 26.91 -8 5 2 885.19 26.55 -8 -5 2 814.95 27.20 8 -5 -1 387.63 13.00 -8 -5 1 352.07 12.48 -8 5 1 384.06 12.59 -8 -5 1 338.52 13.12 8 -5 0 120.12 5.65 -8 5 0 117.35 5.22 -8 -5 0 107.80 5.83 8 -5 1 31.30 3.01 -8 -5 -1 28.58 3.29 8 5 2 67.28 4.43 8 -5 2 67.53 4.03 8 5 3 225.30 9.41 8 -5 3 241.73 9.13 -8 5 -3 252.16 8.91 -8 -5 -3 235.20 9.36 8 5 4 372.74 12.83 8 -5 4 353.77 12.35 -8 5 -4 341.53 12.03 -8 -5 -4 352.34 12.63 8 5 5 222.81 8.84 8 -5 5 221.26 8.46 -8 5 -5 236.04 8.32 -8 -5 -5 220.94 8.76 8 5 6 319.46 11.25 8 -5 6 303.84 10.87 -8 5 -6 310.07 10.71 -8 -5 -6 334.42 11.39 -8 -5 -7 40.11 3.01 8 5 7 34.03 2.84 -8 5 -8 2.80 1.27 -8 -5 -8 5.96 1.87 -8 5 -9 3.63 1.22 -8 -5 -9 4.09 1.73 -8 5 -10 253.39 8.62 -8 -5 -10 259.49 8.97 -8 -5 -11 295.93 10.17 -8 5 -11 323.60 10.00 -8 -5 -11 298.90 10.13 -8 5 -12 426.54 13.19 -8 6 12 3.10 0.71 -8 -6 12 2.03 0.80 8 -6 -12 1.18 0.72 -8 6 11 398.35 11.37 8 -6 -11 366.57 11.12 8 6 -10 1.30 0.99 -8 6 10 2.64 0.97 8 -6 -10 2.24 1.05 8 6 -9 8.43 1.27 8 -6 -9 9.81 1.38 8 6 -8 7.55 1.32 -8 6 8 7.58 1.02 8 -6 -8 8.38 1.38 8 6 -7 197.12 7.21 8 -6 -7 222.59 7.37 -8 6 7 212.31 7.15 -8 -6 6 28.26 2.63 8 6 -6 25.76 1.92 8 6 -6 26.42 2.54 8 -6 -6 29.75 2.26 -8 6 6 27.44 1.92 -8 -6 5 448.88 15.45 8 -6 -5 476.99 15.16 8 6 -5 453.64 15.36 -8 6 5 468.09 14.74 -8 -6 4 7.44 2.18 8 -6 -4 9.42 1.91 -8 6 4 11.40 1.58 -8 6 3 221.54 8.12 -8 -6 3 235.87 9.08 -8 6 3 242.59 8.30 -8 -6 2 27.29 3.08 -8 6 2 35.75 2.45 -8 -6 1 24.49 2.95 8 -6 -1 21.80 2.49 -8 6 1 26.73 2.27 8 -6 0 55.40 3.51 -8 6 0 61.70 3.30 8 -6 1 517.46 16.76 -8 6 -1 545.89 16.55 8 -6 2 16.87 2.24 -8 -6 -2 11.84 2.44 -8 -6 -3 825.58 25.11 8 -6 3 820.66 24.73 8 6 3 838.83 25.10 -8 6 -4 16.74 1.43 8 6 4 18.36 2.57 -8 -6 -4 14.83 2.38 8 -6 4 16.64 2.12 -8 6 -4 18.30 1.93 8 6 5 10.73 2.20 -8 -6 -5 9.58 2.09 -8 6 -5 10.05 1.58 -8 6 -5 11.62 1.27 -8 6 -6 14.06 1.61 8 -6 6 13.15 1.67 8 6 6 15.73 2.09 -8 -6 -6 14.63 2.12 -8 6 -6 15.86 1.43 8 6 7 224.44 8.28 -8 -6 -7 302.56 9.18 -8 6 -7 282.89 8.34 8 -6 7 214.47 8.20 -8 6 -8 32.60 1.86 -8 -6 -8 30.10 2.37 -8 6 -9 448.96 13.89 -8 -6 -9 452.98 14.40 -8 -6 -10 7.87 1.30 -8 -6 -10 5.78 1.30 -8 -7 10 120.64 4.39 -8 7 10 125.48 4.29 -8 7 9 1.09 0.69 -8 -7 9 2.12 0.98 8 -7 -8 174.06 5.93 -8 -7 8 211.70 6.73 -8 7 7 34.04 1.68 8 -7 -7 37.82 1.87 -8 7 7 41.33 2.12 -8 -7 7 43.25 2.52 8 7 -7 35.69 1.90 8 -7 -6 43.83 2.15 -8 7 6 49.32 2.18 -8 7 6 49.02 2.42 -8 -7 6 50.61 2.88 8 7 -6 41.31 2.15 8 -7 -6 48.42 2.59 8 -7 -5 13.54 1.32 8 -7 -5 14.75 1.66 -8 7 5 15.23 1.33 -8 7 5 11.56 1.33 8 7 -5 12.52 1.92 -8 -7 5 13.94 1.95 -8 -7 4 70.90 3.80 -8 7 4 69.99 3.16 -8 7 4 77.93 3.21 8 -7 -4 71.55 3.01 8 7 -4 69.32 3.72 8 7 -3 12.92 2.03 -8 -7 3 11.91 2.04 -8 7 3 11.46 1.37 -8 -7 2 285.33 10.57 -8 7 2 313.15 10.02 8 7 -1 -0.69 1.99 -8 -7 1 -1.43 1.74 -8 7 1 2.45 1.15 8 7 0 152.29 6.28 -8 7 0 148.84 5.42 8 7 1 8.70 2.00 -8 -7 -1 5.70 1.88 -8 7 -1 10.37 1.46 8 7 2 3.91 1.86 -8 -7 -2 3.81 1.70 -8 7 -2 7.23 1.32 8 -7 3 9.66 1.49 8 7 3 6.52 1.86 -8 -7 -3 6.47 1.80 8 -7 4 188.06 7.21 -8 -7 -4 197.55 7.44 8 7 4 196.61 7.39 8 -7 5 8.98 1.27 -8 7 -5 11.26 1.31 8 7 5 10.80 1.70 -8 -7 -5 13.43 1.77 -8 -7 -6 72.61 3.47 -8 -7 -7 1.26 1.24 -8 -7 -8 31.29 1.93 -8 -8 7 29.84 1.61 -8 8 6 0.39 0.51 -8 -8 6 0.99 0.86 8 -8 -5 97.70 3.62 -8 -8 5 101.15 3.79 -8 8 5 96.24 3.39 8 8 -4 5.95 1.28 -8 -8 4 6.63 1.26 8 -8 -4 7.20 1.07 -8 8 3 148.37 4.98 -8 -8 3 144.86 5.47 -8 8 2 35.90 1.80 -8 -8 2 34.32 2.23 8 -8 -1 20.36 1.67 -8 8 1 22.39 1.41 -8 -8 1 18.37 1.76 8 8 -1 18.67 1.86 8 -8 0 34.34 2.11 -8 8 0 36.68 1.89 -8 -8 0 29.25 2.16 8 8 0 34.72 2.33 -8 -8 -1 87.92 3.86 8 -8 1 92.62 3.79 8 8 1 91.39 3.91 8 8 2 9.97 1.46 8 -8 2 8.81 1.19 8 8 3 95.82 3.83 8 -8 3 97.36 3.74 9 0 -13 2.50 0.67 9 0 -12 0.31 0.70 -9 0 11 24.05 1.45 -9 0 10 -0.41 0.97 -9 0 9 373.86 11.95 -9 0 8 -0.53 1.21 -9 0 7 101.36 4.18 -9 0 7 89.89 3.84 9 0 -6 2.09 1.52 -9 0 6 -0.08 1.35 -9 0 6 0.56 1.04 9 0 -5 150.12 6.08 -9 0 5 148.80 5.88 -9 0 5 150.07 5.71 9 0 -4 3.36 1.79 -9 0 4 1.69 1.16 -9 0 3 512.92 16.41 9 0 -2 0.62 1.81 -9 0 2 -0.60 1.56 -9 0 2 0.09 1.28 9 0 -1 161.19 6.49 -9 0 1 154.67 6.14 -9 0 1 147.24 6.05 -9 0 0 2.57 1.46 9 0 0 2.29 1.86 -9 0 -1 87.07 4.15 -9 0 -1 90.95 4.31 9 0 2 0.40 1.69 -9 0 -2 1.04 1.34 9 0 3 457.49 14.75 -9 0 -3 431.23 14.48 -9 0 -4 0.44 1.38 -9 0 -4 1.77 1.28 9 0 4 -0.65 1.63 -9 0 -5 451.00 14.13 9 0 5 446.05 14.59 -9 0 -6 0.60 1.18 9 0 6 0.88 1.20 -9 0 -7 1.30 1.21 -9 0 -8 0.06 1.12 -9 0 -9 201.26 6.78 9 -1 -12 162.99 5.49 9 1 -12 180.27 5.71 9 -1 -11 74.99 3.18 -9 1 11 71.60 2.82 9 -1 -10 80.85 3.52 -9 1 10 87.46 3.36 -9 -1 10 84.80 3.46 -9 1 9 14.09 1.41 -9 -1 9 13.78 1.54 9 -1 -8 49.90 2.62 -9 1 8 52.75 2.67 -9 -1 8 52.89 2.78 -9 1 7 69.48 3.32 -9 -1 7 72.45 3.46 -9 1 6 379.30 11.87 -9 -1 6 366.95 11.88 9 -1 -6 342.09 11.88 9 1 -6 361.14 11.98 -9 1 6 348.45 11.62 -9 1 5 209.09 7.41 9 -1 -5 197.39 7.55 9 1 -5 212.65 7.72 -9 1 5 197.89 7.25 -9 1 4 104.55 4.47 9 -1 -4 101.06 4.68 9 1 -4 100.68 4.74 -9 1 4 101.06 4.33 -9 -1 4 94.77 4.26 -9 -1 3 98.72 4.40 -9 1 3 92.35 4.19 -9 -1 3 93.07 4.21 -9 -1 2 129.66 5.28 9 -1 -2 125.28 5.50 9 1 -2 124.71 5.60 -9 1 2 121.30 5.11 -9 -1 2 120.80 5.14 -9 1 1 96.78 4.44 -9 -1 1 102.17 4.52 9 -1 -1 101.72 4.82 9 1 -1 104.39 4.95 -9 1 1 97.19 4.43 -9 -1 1 97.71 4.47 9 -1 0 793.94 25.11 9 1 0 793.71 25.17 -9 1 0 830.36 24.84 -9 -1 0 789.35 24.75 -9 1 -1 178.95 6.68 -9 1 -1 175.59 6.75 -9 -1 -1 179.17 6.83 9 -1 1 169.82 6.96 9 1 1 178.23 7.14 -9 1 -2 288.37 9.52 -9 1 -2 272.22 9.27 9 -1 2 268.85 9.65 9 1 2 270.77 9.72 -9 -1 -2 250.07 8.82 -9 1 -3 136.51 5.54 9 -1 3 142.95 5.83 9 1 3 138.88 5.81 -9 -1 -3 130.65 5.14 -9 1 -4 13.75 1.79 -9 -1 -4 14.18 1.77 9 -1 4 14.31 2.05 9 1 4 15.15 2.04 -9 -1 -5 1.12 1.37 9 -1 5 0.08 1.48 9 1 5 1.67 1.56 -9 1 -6 324.12 10.38 9 1 6 311.51 10.73 9 -1 6 313.07 10.70 -9 1 -7 84.06 3.51 -9 -1 -7 96.76 3.90 -9 1 -8 225.41 7.65 -9 -1 -8 248.36 7.99 -9 -1 -9 31.44 1.98 -9 -2 11 124.21 4.27 9 -2 -11 116.30 4.22 -9 2 10 144.74 4.94 9 -2 -10 157.24 5.19 -9 -2 9 130.48 4.61 -9 2 9 118.80 4.33 9 -2 -9 129.05 4.51 -9 -2 8 89.18 3.64 -9 2 8 86.66 3.45 9 -2 -8 83.08 3.50 -9 2 7 30.79 1.96 -9 -2 7 28.28 2.09 -9 2 6 8.22 1.38 -9 -2 6 8.05 1.59 -9 2 6 4.12 1.18 9 -2 -6 6.94 1.55 9 2 -6 5.84 1.66 -9 2 5 200.53 7.10 -9 2 5 193.06 6.97 9 2 -5 187.06 7.33 9 -2 -5 207.33 7.38 -9 2 4 126.35 5.11 -9 -2 4 134.06 5.26 -9 2 4 120.34 5.00 9 2 -4 130.07 5.53 9 -2 -4 130.08 5.39 -9 2 3 261.30 9.24 -9 2 3 272.12 9.32 -9 -2 3 278.74 9.41 -9 -2 2 331.09 10.67 9 2 -2 330.57 11.09 9 -2 -2 306.38 10.82 -9 -2 1 48.12 2.90 -9 2 1 45.24 2.79 9 2 -1 47.63 3.31 9 -2 -1 49.11 3.16 -9 2 0 42.13 2.69 9 2 0 45.74 3.29 9 -2 0 47.38 3.11 -9 2 -1 59.82 3.14 -9 2 -1 51.54 3.06 9 2 1 62.15 3.63 9 -2 1 59.56 3.47 -9 2 -2 3.53 1.30 9 -2 2 6.86 1.81 9 2 2 4.56 1.98 -9 2 -2 4.36 1.40 9 2 3 342.21 11.61 9 -2 3 335.13 11.47 -9 2 -3 335.92 11.26 -9 -2 -4 115.49 4.65 9 2 4 116.31 5.02 9 -2 4 109.15 4.81 -9 -2 -5 119.28 4.69 9 2 5 111.69 4.75 9 -2 5 110.45 4.70 9 2 6 31.25 2.20 9 -2 6 27.81 2.10 -9 -2 -7 1.89 1.27 -9 -2 -8 5.43 1.32 -9 -2 -9 54.74 2.59 -9 -3 11 11.63 1.00 -9 -3 10 5.21 0.99 -9 -3 9 28.27 1.77 -9 3 9 22.88 1.39 -9 -3 8 69.76 3.11 -9 3 8 67.39 2.87 -9 -3 7 182.34 6.54 -9 3 7 186.13 6.38 -9 3 6 327.37 10.26 9 3 -6 300.22 10.41 9 -3 -6 312.39 10.39 -9 -3 5 53.23 2.78 -9 3 5 48.46 2.57 -9 3 5 42.86 2.48 9 3 -5 52.39 2.98 9 -3 -5 46.83 2.79 -9 -3 4 112.03 4.48 -9 3 4 105.95 4.32 -9 3 4 98.25 4.23 9 3 -4 107.74 4.77 9 -3 -4 103.69 4.57 -9 3 3 2.15 1.16 -9 3 3 2.76 1.23 -9 -3 3 3.40 1.42 -9 -3 2 20.70 1.92 -9 3 2 19.51 1.84 -9 3 2 16.30 1.71 9 3 -2 20.82 2.43 9 -3 -2 22.06 2.20 -9 3 1 99.11 4.30 9 3 -1 112.00 4.92 9 -3 -1 100.68 4.62 -9 3 0 275.52 9.23 9 3 0 261.80 9.58 9 -3 0 270.58 9.50 -9 3 -1 86.07 3.75 -9 3 -1 78.46 3.69 9 3 1 87.29 4.23 9 -3 1 74.63 3.89 -9 3 -2 279.26 9.07 -9 3 -2 259.74 9.02 9 3 2 263.96 9.44 9 -3 2 257.61 9.25 9 -3 3 13.72 1.84 9 3 3 16.79 2.14 -9 3 -3 14.20 1.57 9 3 4 -1.41 1.60 9 -3 4 -0.15 1.39 9 3 5 10.11 1.59 9 -3 5 13.11 1.54 9 3 6 61.58 2.88 9 -3 6 59.95 2.82 -9 -3 -7 18.53 1.67 -9 3 -8 253.12 8.10 -9 -3 -8 242.04 8.14 -9 3 -9 2.07 0.69 9 -4 -10 64.72 2.56 -9 -4 10 69.61 2.61 9 -4 -9 249.99 8.14 -9 -4 9 261.10 8.20 9 -4 -8 23.91 1.60 -9 4 8 21.37 1.31 9 -4 -7 148.71 5.24 -9 4 7 145.37 5.05 -9 -4 6 18.59 1.59 -9 4 6 16.56 1.36 -9 -4 5 13.37 1.47 -9 4 5 14.37 1.35 9 -4 -5 12.87 1.53 9 4 -5 13.95 1.72 -9 -4 4 142.87 5.05 -9 4 4 150.68 5.01 9 -4 -4 138.30 5.17 9 4 -4 143.95 5.36 -9 -4 3 422.36 12.51 -9 4 3 453.58 12.61 -9 4 2 161.34 5.55 9 -4 -2 150.93 5.77 -9 4 1 232.78 7.65 9 -4 -1 227.73 7.90 9 4 -1 242.90 8.15 -9 -4 0 3.25 1.07 9 4 0 5.33 1.73 9 -4 0 2.92 1.44 -9 -4 -1 3.49 1.04 -9 4 -1 3.38 1.14 9 4 1 4.47 1.67 9 -4 1 3.16 1.44 -9 4 -2 95.22 3.75 9 -4 2 92.12 3.94 9 4 2 96.54 4.14 -9 4 -3 284.01 8.64 9 -4 3 266.58 8.80 9 4 3 274.40 8.95 9 -4 4 117.44 4.42 9 4 4 122.85 4.60 9 4 5 312.49 10.06 9 -4 5 314.26 10.00 -9 4 -6 10.87 1.04 -9 -4 -6 12.09 1.36 -9 -4 -7 80.14 3.25 -9 -5 7 80.04 3.02 9 -5 -7 77.57 2.97 -9 -5 6 81.39 3.12 -9 5 6 76.15 2.93 9 -5 -6 84.25 3.14 -9 -5 5 150.86 5.34 -9 5 5 159.16 5.32 9 -5 -5 162.17 5.42 9 5 -5 156.55 5.55 -9 5 4 211.37 6.37 9 -5 -4 210.81 6.57 9 5 -4 195.38 6.59 -9 -5 3 43.10 2.16 -9 5 3 55.35 2.38 -9 -5 2 10.74 1.20 -9 5 2 16.32 1.34 -9 5 1 27.41 1.67 9 -5 -1 25.72 1.87 9 5 -1 28.51 2.13 9 -5 0 94.50 3.81 9 5 0 96.52 3.96 9 -5 1 266.02 8.48 9 5 1 278.57 8.62 -9 5 -2 71.77 2.78 9 -5 2 62.81 2.85 9 5 2 63.88 3.00 -9 -5 -3 26.30 1.61 9 5 3 29.61 1.91 -9 5 -3 32.00 1.68 -9 6 2 257.89 8.09 9 6 -1 4.28 1.01 -9 6 1 2.70 0.64 9 -6 -1 2.74 0.80 9 6 0 16.90 1.38 9 -6 0 14.63 1.25 0 0 0 0.00 0.00 TITL KR1049_AhMa in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 1.54184 7.862475 11.426837 21.961359 90.0000 92.9222 90.0000 ZERR 4.00 0.000089 0.000129 0.000212 0.0000 0.0010 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N O Cl Ru UNIT 72.00 60.00 12.00 16.00 8.00 4.00 REM CrysAlisPro recorded range (K): Min=99.9; max=100.2; aver:100.0 TEMP -173 SIZE 0.04 0.09 0.18 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 2738 _cell_oxdiff_length_a 7.86031(14) _cell_oxdiff_length_b 11.4300(2) _cell_oxdiff_length_c 21.9606(3) _cell_oxdiff_angle_alpha 89.9660(14) _cell_oxdiff_angle_beta 92.8841(14) _cell_oxdiff_angle_gamma 90.0433(15) _cell_oxdiff_volume 1970.51(6) _cell_oxdiff_measurement_reflns_used 16184 _oxdiff_exptl_absorpt_empirical_full_min 0.765 _oxdiff_exptl_absorpt_empirical_full_max 1.371 _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _diffrn_oxdiff_digest_frames ; 019956cb4477bb4c3782c734a2ab398e97036888fc5 ; _diffrn_oxdiff_digest_hkl ; 01de7ee9863bf338703b956a064cb097f2edfa ; _reflns_odcompleteness_completeness 99.90 _reflns_odcompleteness_theta 68.13 _reflns_odcompleteness_iscentric 1 _chemical_oxdiff_formula 'C18 H15 Cl2 N3 O4 Ru' _chemical_oxdiff_usercomment 'Objekttraeger NM3' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ru1 Ru 0.39368(2) 0.53129(2) 0.67481(2) 0.02157(7) Uani 1 1 d . . . . . O1 O 0.5335(3) 0.44225(19) 0.55904(9) 0.0374(5) Uani 1 1 d . . . . . C1 C 0.4810(3) 0.4772(2) 0.60246(12) 0.0276(5) Uani 1 1 d . . . . . Cl1 Cl 0.24023(8) 0.35508(5) 0.68676(3) 0.03115(14) Uani 1 1 d . . . . . Cl2 Cl 0.51617(7) 0.72305(5) 0.66742(3) 0.02848(13) Uani 1 1 d . . . . . O2 O 0.7053(3) 0.4255(2) 0.74018(10) 0.0442(5) Uani 1 1 d . . . . . C2 C 0.5891(4) 0.4665(2) 0.71599(13) 0.0314(6) Uani 1 1 d . . . . . N1_1 N 0.2729(2) 0.60281(19) 0.75445(9) 0.0238(4) Uani 1 1 d . . . . . H1_1 H 0.299990 0.688310 0.754018 0.029 Uiso 1 1 calc R U . . . C2_1 C 0.0843(3) 0.5966(2) 0.74512(11) 0.0262(5) Uani 1 1 d . . . . . H2A_1 H 0.029150 0.655615 0.770604 0.031 Uiso 1 1 calc R U . . . H2AB_1 H 0.042322 0.518028 0.755903 0.031 Uiso 1 1 calc R U . . . C3_1 C 0.0471(3) 0.6212(2) 0.67913(11) 0.0238(5) Uani 1 1 d . . . . . N4_1 N 0.1630(2) 0.60192(18) 0.63888(9) 0.0227(4) Uani 1 1 d . . . . . C5_1 C 0.0877(3) 0.6272(2) 0.58178(11) 0.0242(5) Uani 1 1 d . . . . . C6_1 C 0.1516(3) 0.6230(2) 0.52397(12) 0.0279(5) Uani 1 1 d . . . . . H6_1 H 0.265493 0.599269 0.518177 0.033 Uiso 1 1 calc R U . . . C7_1 C 0.0432(3) 0.6546(2) 0.47523(12) 0.0309(5) Uani 1 1 d . . . . . H7_1 H 0.083678 0.652619 0.435222 0.037 Uiso 1 1 calc R U . . . C8_1 C -0.1254(4) 0.6895(3) 0.48339(12) 0.0323(6) Uani 1 1 d . . . . . H8_1 H -0.196248 0.710487 0.448781 0.039 Uiso 1 1 calc R U . . . C9_1 C -0.1906(3) 0.6940(2) 0.54069(12) 0.0299(5) Uani 1 1 d . . . . . H9_1 H -0.304535 0.717599 0.546378 0.036 Uiso 1 1 calc R U . . . C10_1 C -0.0803(3) 0.6622(2) 0.58966(11) 0.0256(5) Uani 1 1 d . . . . . N11_1 N -0.1011(3) 0.6581(2) 0.65209(9) 0.0260(4) Uani 1 1 d . . . . . H11_1 H -0.194100 0.676390 0.670624 0.031 Uiso 1 1 calc R U . . . C1_2 C 0.3463(3) 0.5608(2) 0.81242(11) 0.0246(5) Uani 1 1 d . . . . . C2_2 C 0.5008(3) 0.6108(2) 0.83176(11) 0.0267(5) Uani 1 1 d . . . . . H2_2 H 0.547011 0.672969 0.809078 0.032 Uiso 1 1 calc R U . . . C3_2 C 0.5875(3) 0.5703(2) 0.88404(12) 0.0293(5) Uani 1 1 d . . . . . C4_2 C 0.5184(4) 0.4808(3) 0.91799(13) 0.0340(6) Uani 1 1 d . . . . . H4_2 H 0.576914 0.453381 0.954129 0.041 Uiso 1 1 calc R U . . . C5_2 C 0.3639(4) 0.4322(3) 0.89863(13) 0.0361(6) Uani 1 1 d . . . . . H5_2 H 0.316519 0.371295 0.921818 0.043 Uiso 1 1 calc R U . . . C6_2 C 0.2763(4) 0.4713(2) 0.84552(13) 0.0309(6) Uani 1 1 d . . . . . H6_2 H 0.170682 0.437069 0.832337 0.037 Uiso 1 1 calc R U . . . C1_3 C 0.7565(4) 0.6254(3) 0.90055(13) 0.0342(6) Uani 1 1 d . . . . . O2_3 O 0.8252(3) 0.6953(2) 0.86941(10) 0.0463(5) Uani 1 1 d . . . . . O3_3 O 0.8206(3) 0.58783(19) 0.95483(11) 0.0459(5) Uani 1 1 d . . . . . C4_3 C 0.9815(5) 0.6408(3) 0.9743(2) 0.0586(11) Uani 1 1 d . . . . . H4A_3 H 1.068770 0.618094 0.946227 0.088 Uiso 1 1 calc R U . . . H4B_3 H 1.015207 0.614139 1.015528 0.088 Uiso 1 1 calc R U . . . H4C_3 H 0.969492 0.726215 0.974168 0.088 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ru1 0.01552(10) 0.02501(11) 0.02393(11) -0.00030(6) -0.00130(7) 0.00185(6) O1 0.0386(11) 0.0431(11) 0.0314(10) -0.0017(8) 0.0098(8) 0.0121(9) C1 0.0226(12) 0.0263(12) 0.0337(13) 0.0057(10) -0.0010(10) 0.0039(9) Cl1 0.0331(3) 0.0278(3) 0.0323(3) 0.0015(2) -0.0010(2) -0.0052(2) Cl2 0.0171(2) 0.0277(3) 0.0406(3) -0.0004(2) 0.0019(2) 0.0006(2) O2 0.0308(11) 0.0546(13) 0.0456(12) 0.0002(10) -0.0130(9) 0.0204(10) C2 0.0303(14) 0.0335(14) 0.0303(13) -0.0046(10) 0.0012(11) -0.0002(11) N1_1 0.0170(9) 0.0303(11) 0.0238(9) -0.0025(8) -0.0013(7) 0.0010(8) C2_1 0.0142(10) 0.0383(14) 0.0260(12) -0.0023(10) 0.0003(9) 0.0018(10) C3_1 0.0148(10) 0.0295(12) 0.0269(12) -0.0024(9) -0.0016(9) 0.0016(9) N4_1 0.0159(9) 0.0271(10) 0.0250(10) 0.0002(8) -0.0011(7) 0.0012(8) C5_1 0.0200(11) 0.0250(12) 0.0274(12) 0.0007(9) -0.0025(9) 0.0016(9) C6_1 0.0223(12) 0.0328(13) 0.0286(12) 0.0016(10) 0.0026(9) 0.0013(10) C7_1 0.0321(13) 0.0345(14) 0.0260(12) 0.0013(10) 0.0010(10) -0.0008(11) C8_1 0.0312(13) 0.0356(14) 0.0292(13) 0.0007(11) -0.0080(10) 0.0007(11) C9_1 0.0227(12) 0.0349(14) 0.0314(13) 0.0007(11) -0.0039(10) 0.0032(10) C10_1 0.0198(11) 0.0285(12) 0.0282(12) -0.0003(10) -0.0016(9) 0.0007(9) N11_1 0.0160(9) 0.0373(12) 0.0245(10) 0.0001(9) 0.0001(7) 0.0037(8) C1_2 0.0214(11) 0.0301(12) 0.0219(11) -0.0045(9) -0.0033(9) 0.0037(10) C2_2 0.0249(12) 0.0275(12) 0.0273(12) -0.0015(10) -0.0021(9) 0.0010(10) C3_2 0.0277(13) 0.0287(13) 0.0305(13) -0.0039(10) -0.0080(10) 0.0023(10) C4_2 0.0381(15) 0.0334(14) 0.0296(13) 0.0022(11) -0.0091(11) 0.0039(12) C5_2 0.0424(16) 0.0293(14) 0.0362(14) 0.0037(11) -0.0019(12) -0.0031(12) C6_2 0.0301(13) 0.0305(14) 0.0316(13) -0.0011(10) -0.0033(11) -0.0038(10) C1_3 0.0286(13) 0.0344(14) 0.0384(14) -0.0035(12) -0.0099(11) 0.0035(11) O2_3 0.0299(10) 0.0600(15) 0.0479(12) 0.0022(11) -0.0091(9) -0.0108(10) O3_3 0.0440(12) 0.0356(11) 0.0546(13) 0.0035(10) -0.0313(10) -0.0031(9) C4_3 0.050(2) 0.0394(17) 0.082(3) 0.0005(17) -0.0423(19) -0.0053(15) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru 0.0552 3.2960 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 0 -1 2 0.0544 0 1 -2 0.0288 0 0 -1 0.0269 0 0 1 0.0760 -1 -1 3 0.0562 -1 -1 4 0.0498 -1 1 3 0.0217 0 -2 1 0.0535 1 -4 -3 0.0381 1 -1 -4 0.0092 4 -4 -3 0.0413 3 5 -1 0.0371 3 1 -4 0.0334 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 Ru1 C2 87.26(11) . . ? C1 Ru1 N4_1 98.94(9) . . ? C2 Ru1 N4_1 173.30(10) . . ? C1 Ru1 N1_1 174.73(9) . . ? C2 Ru1 N1_1 97.98(10) . . ? N4_1 Ru1 N1_1 75.86(8) . . ? C1 Ru1 Cl1 91.39(8) . . ? C2 Ru1 Cl1 91.16(9) . . ? N4_1 Ru1 Cl1 86.18(6) . . ? N1_1 Ru1 Cl1 89.13(6) . . ? C1 Ru1 Cl2 94.50(8) . . ? C2 Ru1 Cl2 94.05(9) . . ? N4_1 Ru1 Cl2 88.02(6) . . ? N1_1 Ru1 Cl2 84.56(6) . . ? Cl1 Ru1 Cl2 172.31(2) . . ? O1 C1 Ru1 178.7(2) . . ? O2 C2 Ru1 178.6(3) . . ? C1_2 N1_1 C2_1 117.0(2) . . ? C1_2 N1_1 Ru1 114.06(15) . . ? C2_1 N1_1 Ru1 109.99(14) . . ? C1_2 N1_1 H1_1 104.8 . . ? C2_1 N1_1 H1_1 104.8 . . ? Ru1 N1_1 H1_1 104.8 . . ? N1_1 C2_1 C3_1 105.64(19) . . ? N1_1 C2_1 H2A_1 110.6 . . ? C3_1 C2_1 H2A_1 110.6 . . ? N1_1 C2_1 H2AB_1 110.6 . . ? C3_1 C2_1 H2AB_1 110.6 . . ? H2A_1 C2_1 H2AB_1 108.7 . . ? N4_1 C3_1 N11_1 111.6(2) . . ? N4_1 C3_1 C2_1 120.8(2) . . ? N11_1 C3_1 C2_1 127.5(2) . . ? C3_1 N4_1 C5_1 107.03(19) . . ? C3_1 N4_1 Ru1 115.12(16) . . ? C5_1 N4_1 Ru1 137.60(16) . . ? N4_1 C5_1 C6_1 131.3(2) . . ? N4_1 C5_1 C10_1 108.0(2) . . ? C6_1 C5_1 C10_1 120.7(2) . . ? C7_1 C6_1 C5_1 117.4(2) . . ? C7_1 C6_1 H6_1 121.3 . . ? C5_1 C6_1 H6_1 121.3 . . ? C6_1 C7_1 C8_1 121.6(2) . . ? C6_1 C7_1 H7_1 119.2 . . ? C8_1 C7_1 H7_1 119.2 . . ? C9_1 C8_1 C7_1 121.5(2) . . ? C9_1 C8_1 H8_1 119.3 . . ? C7_1 C8_1 H8_1 119.3 . . ? C8_1 C9_1 C10_1 116.6(2) . . ? C8_1 C9_1 H9_1 121.7 . . ? C10_1 C9_1 H9_1 121.7 . . ? N11_1 C10_1 C9_1 132.1(2) . . ? N11_1 C10_1 C5_1 105.7(2) . . ? C9_1 C10_1 C5_1 122.2(2) . . ? C3_1 N11_1 C10_1 107.6(2) . . ? C3_1 N11_1 H11_1 126.2 . . ? C10_1 N11_1 H11_1 126.2 . . ? C6_2 C1_2 C2_2 120.5(2) . . ? C6_2 C1_2 N1_1 123.6(2) . . ? C2_2 C1_2 N1_1 115.7(2) . . ? C3_2 C2_2 C1_2 120.1(2) . . ? C3_2 C2_2 H2_2 119.9 . . ? C1_2 C2_2 H2_2 119.9 . . ? C2_2 C3_2 C4_2 120.0(2) . . ? C2_2 C3_2 C1_3 117.0(3) . . ? C4_2 C3_2 C1_3 123.0(2) . . ? C5_2 C4_2 C3_2 119.4(3) . . ? C5_2 C4_2 H4_2 120.3 . . ? C3_2 C4_2 H4_2 120.3 . . ? C4_2 C5_2 C6_2 121.1(3) . . ? C4_2 C5_2 H5_2 119.5 . . ? C6_2 C5_2 H5_2 119.5 . . ? C1_2 C6_2 C5_2 118.8(3) . . ? C1_2 C6_2 H6_2 120.6 . . ? C5_2 C6_2 H6_2 120.6 . . ? O2_3 C1_3 O3_3 124.1(3) . . ? O2_3 C1_3 C3_2 124.2(3) . . ? O3_3 C1_3 C3_2 111.7(3) . . ? C1_3 O3_3 C4_3 114.3(3) . . ? O3_3 C4_3 H4A_3 109.5 . . ? O3_3 C4_3 H4B_3 109.5 . . ? H4A_3 C4_3 H4B_3 109.5 . . ? O3_3 C4_3 H4C_3 109.5 . . ? H4A_3 C4_3 H4C_3 109.5 . . ? H4B_3 C4_3 H4C_3 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ru1 C1 1.868(3) . ? Ru1 C2 1.893(3) . ? Ru1 N4_1 2.1017(19) . ? Ru1 N1_1 2.190(2) . ? Ru1 Cl1 2.3688(6) . ? Ru1 Cl2 2.4024(6) . ? O1 C1 1.131(3) . ? O2 C2 1.135(3) . ? N1_1 C1_2 1.452(3) . ? N1_1 C2_1 1.488(3) . ? N1_1 H1_1 1.0000 . ? C2_1 C3_1 1.490(3) . ? C2_1 H2A_1 0.9900 . ? C2_1 H2AB_1 0.9900 . ? C3_1 N4_1 1.320(3) . ? C3_1 N11_1 1.349(3) . ? N4_1 C5_1 1.390(3) . ? C5_1 C6_1 1.390(4) . ? C5_1 C10_1 1.400(3) . ? C6_1 C7_1 1.382(4) . ? C6_1 H6_1 0.9500 . ? C7_1 C8_1 1.404(4) . ? C7_1 H7_1 0.9500 . ? C8_1 C9_1 1.384(4) . ? C8_1 H8_1 0.9500 . ? C9_1 C10_1 1.395(3) . ? C9_1 H9_1 0.9500 . ? C10_1 N11_1 1.390(3) . ? N11_1 H11_1 0.8800 . ? C1_2 C6_2 1.385(4) . ? C1_2 C2_2 1.389(4) . ? C2_2 C3_2 1.385(4) . ? C2_2 H2_2 0.9500 . ? C3_2 C4_2 1.392(4) . ? C3_2 C1_3 1.498(4) . ? C4_2 C5_2 1.383(4) . ? C4_2 H4_2 0.9500 . ? C5_2 C6_2 1.397(4) . ? C5_2 H5_2 0.9500 . ? C6_2 H6_2 0.9500 . ? C1_3 O2_3 1.199(4) . ? C1_3 O3_3 1.341(3) . ? O3_3 C4_3 1.447(4) . ? C4_3 H4A_3 0.9800 . ? C4_3 H4B_3 0.9800 . ? C4_3 H4C_3 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C1_2 N1_1 C2_1 C3_1 -168.8(2) . . . . ? Ru1 N1_1 C2_1 C3_1 -36.5(2) . . . . ? N1_1 C2_1 C3_1 N4_1 24.1(3) . . . . ? N1_1 C2_1 C3_1 N11_1 -159.3(3) . . . . ? N11_1 C3_1 N4_1 C5_1 -0.2(3) . . . . ? C2_1 C3_1 N4_1 C5_1 176.9(2) . . . . ? N11_1 C3_1 N4_1 Ru1 -175.41(17) . . . . ? C2_1 C3_1 N4_1 Ru1 1.7(3) . . . . ? C3_1 N4_1 C5_1 C6_1 179.4(3) . . . . ? Ru1 N4_1 C5_1 C6_1 -7.0(5) . . . . ? C3_1 N4_1 C5_1 C10_1 -0.3(3) . . . . ? Ru1 N4_1 C5_1 C10_1 173.33(19) . . . . ? N4_1 C5_1 C6_1 C7_1 -179.6(3) . . . . ? C10_1 C5_1 C6_1 C7_1 0.0(4) . . . . ? C5_1 C6_1 C7_1 C8_1 -0.1(4) . . . . ? C6_1 C7_1 C8_1 C9_1 0.1(4) . . . . ? C7_1 C8_1 C9_1 C10_1 0.0(4) . . . . ? C8_1 C9_1 C10_1 N11_1 178.9(3) . . . . ? C8_1 C9_1 C10_1 C5_1 -0.1(4) . . . . ? N4_1 C5_1 C10_1 N11_1 0.6(3) . . . . ? C6_1 C5_1 C10_1 N11_1 -179.2(2) . . . . ? N4_1 C5_1 C10_1 C9_1 179.8(2) . . . . ? C6_1 C5_1 C10_1 C9_1 0.1(4) . . . . ? N4_1 C3_1 N11_1 C10_1 0.6(3) . . . . ? C2_1 C3_1 N11_1 C10_1 -176.3(3) . . . . ? C9_1 C10_1 N11_1 C3_1 -179.8(3) . . . . ? C5_1 C10_1 N11_1 C3_1 -0.7(3) . . . . ? C2_1 N1_1 C1_2 C6_2 31.4(3) . . . . ? Ru1 N1_1 C1_2 C6_2 -98.9(3) . . . . ? C2_1 N1_1 C1_2 C2_2 -152.8(2) . . . . ? Ru1 N1_1 C1_2 C2_2 76.9(2) . . . . ? C6_2 C1_2 C2_2 C3_2 0.9(4) . . . . ? N1_1 C1_2 C2_2 C3_2 -175.0(2) . . . . ? C1_2 C2_2 C3_2 C4_2 -1.2(4) . . . . ? C1_2 C2_2 C3_2 C1_3 177.6(2) . . . . ? C2_2 C3_2 C4_2 C5_2 0.7(4) . . . . ? C1_3 C3_2 C4_2 C5_2 -178.1(3) . . . . ? C3_2 C4_2 C5_2 C6_2 0.2(5) . . . . ? C2_2 C1_2 C6_2 C5_2 0.0(4) . . . . ? N1_1 C1_2 C6_2 C5_2 175.5(2) . . . . ? C4_2 C5_2 C6_2 C1_2 -0.5(4) . . . . ? C2_2 C3_2 C1_3 O2_3 -5.4(4) . . . . ? C4_2 C3_2 C1_3 O2_3 173.4(3) . . . . ? C2_2 C3_2 C1_3 O3_3 173.8(2) . . . . ? C4_2 C3_2 C1_3 O3_3 -7.4(4) . . . . ? O2_3 C1_3 O3_3 C4_3 1.1(5) . . . . ? C3_2 C1_3 O3_3 C4_3 -178.1(3) . . . . ? loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z 0.0007 -1.0006 1.9956 0.0076 0.1380 -0.1370 -0.0007 1.0006 -1.9956 -0.0076 -0.1380 0.1370 0.0001 0.0008 -0.9993 0.0028 -0.0020 0.0701 -0.0001 -0.0008 0.9993 -0.0028 0.0020 -0.0701 -0.9984 -1.0034 2.9937 -0.1895 0.1588 -0.1889 -0.9985 -1.0042 3.9930 -0.1923 0.1608 -0.2590 -1.0002 0.9946 2.9999 -0.2158 -0.1091 -0.1954 0.0018 -1.9988 0.9931 0.0236 0.2699 -0.0636 1.0030 -3.9917 -3.0092 0.2553 0.5110 0.2051 1.0003 -0.9939 -3.9992 0.2186 0.1071 0.2655 4.0000 -3.9856 -3.0056 0.8382 0.4545 0.1506 2.9925 5.0020 -0.9802 0.5198 -0.7283 -0.0005 2.9965 1.0083 -3.9906 0.5809 -0.1985 0.2227