#------------------------------------------------------------------------------ #$Date: 2021-10-16 01:59:07 +0300 (Sat, 16 Oct 2021) $ #$Revision: 269973 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/85/7708570.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708570 loop_ _publ_author_name 'Swaminathan, Srividya' 'Haribabu, Jebiti' 'Mohamed Kasim, Mohamed Subarkhan' 'dasararaju, gayathri' 'Balakrishnan, Nithya' 'Bhuvanesh, Nattamai' 'Echeverria, Cesar' 'Karvembu, R.' _publ_section_title ; Impact of aliphatic acyl and aromatic thioamide substituents on the anticancer activity of Ru(II)-p-cymene complexes carrying acylthiourea ligands -- In vitro and in vivo studies ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT02611A _journal_year 2021 _chemical_formula_moiety 'C30 H40 Cl2 N2 O Ru S' _chemical_formula_sum 'C30 H40 Cl2 N2 O Ru S' _chemical_formula_weight 648.67 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _audit_creation_date 2020-01-13 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-09-18 deposited with the CCDC. 2021-10-15 downloaded from the CCDC. ; _cell_angle_alpha 112.455(3) _cell_angle_beta 95.919(3) _cell_angle_gamma 91.536(3) _cell_formula_units_Z 4 _cell_length_a 10.4538(10) _cell_length_b 16.6161(15) _cell_length_c 18.7518(17) _cell_measurement_reflns_used 9794 _cell_measurement_temperature 110.0 _cell_measurement_theta_max 33.056 _cell_measurement_theta_min 2.223 _cell_volume 2986.4(5) _computing_cell_refinement 'SAINT V8.38 Bruker AXS Inc., Madison, WI, USA.' _computing_data_collection 'APEX 3 (Bruker AXS)' _computing_data_reduction 'SAINT V8.38 Bruker AXS Inc., Madison, WI, USA.' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 110.0 _diffrn_detector 'Bruker APEX2 area detector' _diffrn_detector_area_resol_mean 7.9 _diffrn_detector_type 'CCD area detector' _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker PHOTON II' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator 'mirror optics' _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0399 _diffrn_reflns_av_unetI/netI 0.0141 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_number 223947 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 26.000 _diffrn_reflns_theta_max 27.500 _diffrn_reflns_theta_min 2.095 _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_type 'Incoatec I\ms' _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.800 _exptl_absorpt_correction_T_max 0.4353 _exptl_absorpt_correction_T_min 0.3959 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1017 before and 0.0651 after correction. The Ratio of minimum to maximum transmission is 0.9095. The \l/2 correction factor is Not present.' _exptl_crystal_colour brown _exptl_crystal_colour_primary brown _exptl_crystal_density_diffrn 1.443 _exptl_crystal_description block _exptl_crystal_F_000 1344 _exptl_crystal_size_max 0.325 _exptl_crystal_size_mid 0.221 _exptl_crystal_size_min 0.153 _refine_diff_density_max 1.186 _refine_diff_density_min -0.712 _refine_diff_density_rms 0.074 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.057 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 724 _refine_ls_number_reflns 13730 _refine_ls_number_restraints 393 _refine_ls_restrained_S_all 1.074 _refine_ls_R_factor_all 0.0348 _refine_ls_R_factor_gt 0.0302 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0249P)^2^+5.3126P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0698 _refine_ls_wR_factor_ref 0.0746 _reflns_Friedel_coverage 0.000 _reflns_number_gt 12502 _reflns_number_total 13730 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt02611a2.cif _cod_data_source_block svpncnap _cod_database_code 7708570 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.887 _shelx_estimated_absorpt_t_min 0.781 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All C(H,H,H,H) groups, All N(H) groups, All N(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances C13B-C15B = C14B-C16B = C15B-C17B = C16B-C18B = C17B-C19B = C18B-C20B = C19B- C21B = C13C-C15C = C14C-C16C = C15C-C17C = C16C-C18C = C17C-C19C = C18C-C20C = C19C-C21C 2.5 with sigma of 0.005 C15-C17 = C16-C18 = C17-C19 = C18-C20 = C19-C21 = C15A-C17A = C16A-C18A = C17A-C19A = C18A-C20A = C19A-C21A 2.5 with sigma of 0.005 C13B-O1B \\sim C13C-O1C with sigma of 0.005 C13B-C14B \\sim C14B-C15B \\sim C15B-C16B \\sim C16B-C17B \\sim C17B-C18B \\sim C18B-C19B \\sim C19B- C20B \\sim C20B-C21B \\sim C13C-C14C \\sim C14C-C15C \\sim C15C-C16C \\sim C16C-C17C \\sim C17C-C18C ~ C18C-C19C \\sim C19C-C20C \\sim C20C-C21C with sigma of 0.005 C15-C16 \\sim C16-C17 \\sim C17-C18 \\sim C18-C19 \\sim C19-C20 \\sim C20-C21 \\sim C15A-C16A \\sim C16A- C17A \\sim C17A-C18A \\sim C18A-C19A \\sim C19A-C20A \\sim C20A-C21A with sigma of 0.005 3. Uiso/Uaniso restraints and constraints O1B \\sim C13B \\sim C14B \\sim C15B \\sim C16B \\sim C17B \\sim C18B \\sim C19B \\sim C20B \\sim C21B: within 2A with sigma of 0.005 and sigma for terminal atoms of 0.01 C15 \\sim C16 \\sim C17 \\sim C18 \\sim C19 \\sim C20 \\sim C21: within 2A with sigma of 0.005 and sigma for terminal atoms of 0.01 Uanis(O1B) = Uanis(O1C) Uanis(C13B) = Uanis(C13C) Uanis(C15C) = Uanis(C15B) Uanis(C16C) = Uanis(C16B) Uanis(C17C) = Uanis(C17B) Uanis(C18C) = Uanis(C18B) Uanis(C19B) = Uanis(C19C) Uanis(C20B) = Uanis(C20C) Uanis(C21C) = Uanis(C21B) Uanis(C21) = Uanis(C21A) Uanis(C20) = Uanis(C20A) Uanis(C19) = Uanis(C19A) Uanis(C18) = Uanis(C18A) Uanis(C17) = Uanis(C17A) Uanis(C16) = Uanis(C16A) Uanis(C15) = Uanis(C15A) Uanis(C14C) = Uanis(C14B) 4. Rigid body (RIGU) restrains O1B, C13B, C14B, C15B, C16B, C17B, C18B, C19B, C20B, C21B with sigma for 1-2 distances of 0.005 and sigma for 1-3 distances of 0.005 C15, C16, C17, C18, C19, C20, C21 with sigma for 1-2 distances of 0.005 and sigma for 1-3 distances of 0.005 5. Same fragment restrains {O1B, C13B, C14B, C15B, C16B, C17B, C18B, C19B, C20B, C21B} sigma for 1-2: 0.005, 1-3: 0.04 as {O1C, C13C, C14C, C15C, C16C, C17C, C18C, C19C, C20C, C21C} 6. Others Sof(H2BA)=Sof(O1C)=Sof(C13C)=Sof(C14C)=Sof(H14C)=Sof(H14D)=Sof(C15C)= Sof(H15C)=Sof(H15D)=Sof(C16C)=Sof(H16C)=Sof(H16D)=Sof(C17C)=Sof(H17C)= Sof(H17D)=Sof(C18C)=Sof(H18C)=Sof(H18D)=Sof(C19C)=Sof(H19C)=Sof(H19D)= Sof(C20C)=Sof(H20C)=Sof(H20D)=Sof(C21C)=Sof(H21D)=Sof(H21E)=Sof(H21F)=1-FVAR(1) Sof(H2B)=Sof(O1B)=Sof(C13B)=Sof(C14B)=Sof(H14A)=Sof(H14B)=Sof(C15B)=Sof(H15A)= Sof(H15B)=Sof(C16B)=Sof(H16A)=Sof(H16B)=Sof(C17B)=Sof(H17A)=Sof(H17B)= Sof(C18B)=Sof(H18A)=Sof(H18B)=Sof(C19B)=Sof(H19A)=Sof(H19B)=Sof(C20B)= Sof(H20A)=Sof(H20B)=Sof(C21B)=Sof(H21A)=Sof(H21B)=Sof(H21C)=FVAR(1) Sof(H14G)=Sof(H14H)=Sof(C15A)=Sof(H15G)=Sof(H15H)=Sof(C16A)=Sof(H16G)= Sof(H16H)=Sof(C17A)=Sof(H17G)=Sof(H17H)=Sof(C18A)=Sof(H18G)=Sof(H18H)= Sof(C19A)=Sof(H19G)=Sof(H19H)=Sof(C20A)=Sof(H20G)=Sof(H20H)=Sof(C21A)= Sof(H21J)=Sof(H21K)=Sof(H21L)=1-FVAR(2) Sof(H14E)=Sof(H14F)=Sof(C15)=Sof(H15E)=Sof(H15F)=Sof(C16)=Sof(H16E)=Sof(H16F)= Sof(C17)=Sof(H17E)=Sof(H17F)=Sof(C18)=Sof(H18E)=Sof(H18F)=Sof(C19)=Sof(H19E)= Sof(H19F)=Sof(C20)=Sof(H20E)=Sof(H20F)=Sof(C21)=Sof(H21G)=Sof(H21H)=Sof(H21I)= FVAR(2) Fixed U11: C14(0.051277) Fixed U12: C14(0.010607) Fixed U13: C14(0.016499) Fixed U22: C14(0.060761) Fixed U23: C14(-0.002736) Fixed U33: C14(0.02717) 7.a Ternary CH refined with riding coordinates: C28(H28), C28B(H28B) 7.b Secondary CH2 refined with riding coordinates: C14(H14E,H14F), C14(H14G,H14H), C15(H15E,H15F), C16(H16E,H16F), C17(H17E, H17F), C18(H18E,H18F), C19(H19E,H19F), C20(H20E,H20F), C15A(H15G,H15H), C16A(H16G,H16H), C17A(H17G,H17H), C18A(H18G,H18H), C19A(H19G,H19H), C20A(H20G, H20H), C14B(H14A,H14B), C15B(H15A,H15B), C16B(H16A,H16B), C17B(H17A,H17B), C18B(H18A,H18B), C19B(H19A,H19B), C20B(H20A,H20B), C14C(H14C,H14D), C15C(H15C, H15D), C16C(H16C,H16D), C17C(H17C,H17D), C18C(H18C,H18D), C19C(H19C,H19D), C20C(H20C,H20D) 7.c Aromatic/amide H refined with riding coordinates: N1(H1), N2(H2), C4(H4), C5(H5), C6(H6), C9(H9), C10(H10), C11(H11), C12(H12), C23(H23), C24(H24), C26(H26), C27(H27), N1B(H1B), N2B(H2B), N2B(H2BA), C4B(H4B), C5B(H5B), C6B(H6B), C9B(H9B), C10B(H10B), C11B(H11B), C12B(H12B), C23B(H23B), C24B(H24B), C26B(H26B), C27B(H27B) 7.d Idealised Me refined as rotating group: C21(H21G,H21H,H21I), C21A(H21J,H21K,H21L), C29(H29D,H29E,H29F), C30(H30D,H30E, H30F), C31(H31D,H31E,H31F), C21B(H21A,H21B,H21C), C21C(H21D,H21E,H21F), C29B(H29A,H29B,H29C), C30B(H30A,H30B,H30C), C31B(H31A,H31B,H31C) ; _shelx_res_file ; TITL svpncnap_a.res in P-1 svpncnap.res created by SHELXL-2018/3 at 09:16:08 on 13-Jan-2020 REM Old TITL SVPNCNAP in P-1 #2 REM SHELXT solution in P-1 REM R1 0.131, Rweak 0.005, Alpha 0.048, Orientation as input REM Formula found by SHELXT: C50 N11 O3 S Cl5 Ru2 REM Instructions for potential hydrogen bonds CELL 0.71073 10.4538 16.6161 18.7518 112.455 95.919 91.536 ZERR 4 0.001 0.0015 0.0017 0.003 0.003 0.003 LATT 1 SFAC C H Cl N O Ru S UNIT 120 160 8 8 4 4 4 EQIV $1 2-X,-Y,1-Z DFIX 2.5 0.005 C13B C15B C14B C16B C15B C17B C16B C18B C17B C19B C18B C20B = C19B C21B C13C C15C C14C C16C C15C C17C C16C C18C C17C C19C C18C C20C C19C = C21C DFIX 2.5 0.005 C15 C17 C16 C18 C17 C19 C18 C20 C19 C21 C15A C17A C16A C18A = C17A C19A C18A C20A C19A C21A SADI 0.005 C13B O1B C13C O1C SADI 0.005 C13B C14B C14B C15B C15B C16B C16B C17B C17B C18B C18B C19B C19B = C20B C20B C21B C13C C14C C14C C15C C15C C16C C16C C17C C17C C18C C18C C19C = C19C C20C C20C C21C SADI 0.005 C15 C16 C16 C17 C17 C18 C18 C19 C19 C20 C20 C21 C15A C16A C16A = C17A C17A C18A C18A C19A C19A C20A C20A C21A SIMU 0.005 0.01 2 O1B > C21B SIMU 0.005 0.01 2 C15 > C21 RIGU 0.005 0.005 O1B > C21B RIGU 0.005 0.005 C15 > C21 EADP O1B O1C EADP C13B C13C EADP C15C C15B EADP C16C C16B EADP C17C C17B EADP C18C C18B EADP C19B C19C EADP C20B C20C EADP C21C C21B EADP C21 C21A EADP C20 C20A EADP C19 C19A EADP C18 C18A EADP C17 C17A EADP C16 C16A EADP C15 C15A EADP C14C C14B L.S. 10 PLAN 20 SIZE 0.153 0.221 0.325 TEMP -163.15 HTAB N1 O1 HTAB N2 Cl2 HTAB N1B O1B HTAB N1B O1B_$1 HTAB N1B O1C HTAB N1B O1C_$1 HTAB N2B Cl1B HTAB N2B Cl2B BOND $H acta wpdb -1 htab MORE -1 CONF fmap 2 acta 52 OMIT -4 55 OMIT -1 1 1 OMIT -1 0 1 OMIT -1 0 2 OMIT -1 -1 2 OMIT 1 0 2 OMIT 1 -1 1 OMIT 2 -3 4 OMIT 1 -8 8 OMIT 5 -4 4 OMIT 0 5 0 OMIT -1 -4 2 OMIT -2 -4 4 REM REM REM WGHT 0.024900 5.312600 FVAR 0.36658 0.53105 0.68048 RU1 6 0.417522 0.157708 0.106065 11.00000 0.01599 0.01454 = 0.01388 0.00130 0.00026 0.00220 CL1 3 0.643625 0.169972 0.089045 11.00000 0.01726 0.02150 = 0.02311 0.00397 0.00117 0.00221 CL2 3 0.366632 0.159999 -0.022411 11.00000 0.02489 0.02388 = 0.01521 0.00377 -0.00096 0.00187 S1 7 0.407221 0.314506 0.164523 11.00000 0.02150 0.01543 = 0.01755 0.00241 0.00314 0.00280 O1 5 0.701863 0.439366 0.069985 11.00000 0.06763 0.04838 = 0.04610 0.00101 0.03270 -0.01546 N1 4 0.539305 0.457593 0.170818 11.00000 0.02577 0.01876 = 0.02000 0.00329 0.00707 0.00017 AFIX 43 H1 2 0.589272 0.482438 0.148905 11.00000 -1.20000 AFIX 0 N2 4 0.553037 0.333131 0.062751 11.00000 0.03506 0.02118 = 0.01805 0.00200 0.00598 0.00356 AFIX 43 H2 2 0.515920 0.281773 0.031637 11.00000 -1.20000 AFIX 0 C2 1 0.504858 0.372937 0.132034 11.00000 0.02094 0.02023 = 0.01839 0.00398 0.00129 0.00351 C3 1 0.503179 0.511920 0.244352 11.00000 0.02457 0.01449 = 0.01950 0.00364 0.00450 0.00202 C4 1 0.376387 0.518152 0.255637 11.00000 0.02292 0.02032 = 0.02251 0.00500 0.00169 0.00071 AFIX 43 H4 2 0.311554 0.486284 0.214138 11.00000 -1.20000 AFIX 0 C5 1 0.341015 0.571505 0.328385 11.00000 0.02359 0.02149 = 0.02842 0.00720 0.00779 0.00499 AFIX 43 H5 2 0.252580 0.574274 0.336101 11.00000 -1.20000 AFIX 0 C6 1 0.433268 0.619373 0.388013 11.00000 0.02940 0.02005 = 0.02059 0.00320 0.00722 0.00618 AFIX 43 H6 2 0.408613 0.654648 0.437114 11.00000 -1.20000 AFIX 0 C7 1 0.564862 0.616692 0.377055 11.00000 0.02692 0.01977 = 0.02148 0.00358 0.00167 0.00342 C8 1 0.602571 0.562064 0.303969 11.00000 0.02363 0.01795 = 0.02205 0.00512 0.00320 0.00298 C9 1 0.662075 0.667093 0.438020 11.00000 0.03467 0.03283 = 0.02416 -0.00185 -0.00003 0.00188 AFIX 43 H9 2 0.638363 0.702951 0.487210 11.00000 -1.20000 AFIX 0 C10 1 0.788487 0.664515 0.426674 11.00000 0.03105 0.05127 = 0.03506 -0.00497 -0.00634 -0.00434 AFIX 43 H10 2 0.852242 0.699105 0.467711 11.00000 -1.20000 AFIX 0 C11 1 0.825515 0.610849 0.354415 11.00000 0.02275 0.05407 = 0.04237 0.00011 0.00083 -0.00064 AFIX 43 H11 2 0.914192 0.609610 0.347239 11.00000 -1.20000 AFIX 0 C12 1 0.735398 0.560456 0.294397 11.00000 0.02394 0.03278 = 0.02986 0.00214 0.00455 0.00268 AFIX 43 H12 2 0.761961 0.524268 0.246145 11.00000 -1.20000 AFIX 0 C13 1 0.653827 0.365127 0.036546 11.00000 0.04267 0.03968 = 0.02536 0.00743 0.01345 0.00426 C14 1 0.700299 0.300509 -0.035828 11.00000 10.05548 10.05378 = 10.02717 10.00799 10.01963 10.01848 PART 1 AFIX 23 H14E 2 0.774009 0.328862 -0.048721 31.00000 -1.20000 H14F 2 0.732193 0.250569 -0.024481 31.00000 -1.20000 AFIX 23 PART 0 PART 2 H14G 2 0.789301 0.287721 -0.022096 -31.00000 -1.20000 H14H 2 0.645377 0.245362 -0.053370 -31.00000 -1.20000 AFIX 0 PART 0 PART 1 C15 1 0.601210 0.266696 -0.104709 31.00000 0.04940 0.03772 = 0.02725 0.01035 0.01180 0.00079 AFIX 23 H15E 2 0.536050 0.228975 -0.094986 31.00000 -1.20000 H15F 2 0.643149 0.229137 -0.149614 31.00000 -1.20000 AFIX 0 C16 1 0.531818 0.332637 -0.127613 31.00000 0.05446 0.04328 = 0.03669 0.01643 0.00648 -0.00114 AFIX 23 H16E 2 0.507734 0.378938 -0.080185 31.00000 -1.20000 H16F 2 0.591702 0.360213 -0.150650 31.00000 -1.20000 AFIX 0 C17 1 0.412966 0.295937 -0.184279 31.00000 0.05065 0.06108 = 0.04500 0.02302 0.00572 0.00715 AFIX 23 H17E 2 0.354675 0.266880 -0.161589 31.00000 -1.20000 H17F 2 0.368283 0.345059 -0.190511 31.00000 -1.20000 AFIX 0 C18 1 0.433161 0.232424 -0.262816 31.00000 0.05056 0.06464 = 0.04471 0.02099 0.00137 0.00176 AFIX 23 H18E 2 0.480571 0.184156 -0.256829 31.00000 -1.20000 H18F 2 0.488100 0.261959 -0.286814 31.00000 -1.20000 AFIX 0 C19 1 0.311810 0.194565 -0.316760 31.00000 0.05376 0.07516 = 0.04966 0.02058 0.00343 0.00485 AFIX 23 H19E 2 0.259599 0.161990 -0.294062 31.00000 -1.20000 H19F 2 0.261777 0.243195 -0.319684 31.00000 -1.20000 AFIX 0 C20 1 0.329438 0.135090 -0.397299 31.00000 0.06330 0.07607 = 0.05929 0.01637 -0.00681 0.00862 AFIX 23 H20E 2 0.386404 0.166221 -0.418921 31.00000 -1.20000 H20F 2 0.244657 0.121559 -0.429762 31.00000 -1.20000 AFIX 0 C21 1 0.385287 0.051405 -0.403580 31.00000 0.08216 0.09217 = 0.06963 0.02343 -0.00872 0.02163 AFIX 137 H21G 2 0.388966 0.014896 -0.458439 31.00000 -1.50000 H21H 2 0.331111 0.020630 -0.381018 31.00000 -1.50000 H21I 2 0.472510 0.063657 -0.375414 31.00000 -1.50000 AFIX 0 PART 0 PART 2 C15A 1 0.699792 0.327945 -0.099119 -31.00000 0.04940 0.03772 = 0.02725 0.01035 0.01180 0.00079 AFIX 23 H15G 2 0.722043 0.277782 -0.144391 -31.00000 -1.20000 H15H 2 0.770575 0.374060 -0.085280 -31.00000 -1.20000 AFIX 0 C16A 1 0.581052 0.361824 -0.125471 -31.00000 0.05446 0.04328 = 0.03669 0.01643 0.00648 -0.00114 AFIX 23 H16G 2 0.548622 0.404997 -0.079221 -31.00000 -1.20000 H16H 2 0.604681 0.392962 -0.158446 -31.00000 -1.20000 AFIX 0 C17A 1 0.474534 0.294434 -0.169850 -31.00000 0.05065 0.06108 = 0.04500 0.02302 0.00572 0.00715 AFIX 23 H17G 2 0.394692 0.324188 -0.173206 -31.00000 -1.20000 H17H 2 0.459838 0.257345 -0.140422 -31.00000 -1.20000 AFIX 0 C18A 1 0.497640 0.237014 -0.250082 -31.00000 0.05056 0.06464 = 0.04471 0.02099 0.00137 0.00176 AFIX 23 H18G 2 0.575778 0.205637 -0.246757 -31.00000 -1.20000 H18H 2 0.514953 0.274092 -0.279142 -31.00000 -1.20000 AFIX 0 C19A 1 0.388075 0.171459 -0.294811 -31.00000 0.05376 0.07516 = 0.04966 0.02058 0.00343 0.00485 AFIX 23 H19G 2 0.372251 0.133107 -0.266706 -31.00000 -1.20000 H19H 2 0.309275 0.202550 -0.297159 -31.00000 -1.20000 AFIX 0 C20A 1 0.411862 0.116170 -0.375796 -31.00000 0.06330 0.07607 = 0.05929 0.01637 -0.00681 0.00862 AFIX 23 H20G 2 0.492927 0.087302 -0.373503 -31.00000 -1.20000 H20H 2 0.423688 0.154330 -0.404594 -31.00000 -1.20000 AFIX 0 C21A 1 0.305250 0.047828 -0.419582 -31.00000 0.08216 0.09217 = 0.06963 0.02343 -0.00872 0.02163 AFIX 137 H21J 2 0.320514 0.019734 -0.474064 -31.00000 -1.50000 H21K 2 0.222879 0.075016 -0.416809 -31.00000 -1.50000 H21L 2 0.302500 0.003955 -0.396563 -31.00000 -1.50000 AFIX 0 PART 0 C22 1 0.223987 0.105984 0.110881 11.00000 0.01733 0.02083 = 0.02356 0.00667 0.00109 0.00000 C23 1 0.283495 0.158216 0.186664 11.00000 0.02174 0.01949 = 0.02115 0.00504 0.00578 0.00298 AFIX 43 H23 2 0.239943 0.205548 0.218786 11.00000 -1.20000 AFIX 0 C24 1 0.406951 0.141712 0.216059 11.00000 0.02477 0.02054 = 0.01623 0.00565 0.00146 0.00020 AFIX 43 H24 2 0.443525 0.177060 0.267568 11.00000 -1.20000 AFIX 0 C25 1 0.474956 0.073162 0.169006 11.00000 0.02164 0.02010 = 0.02161 0.00954 0.00104 0.00239 C26 1 0.416761 0.020028 0.092360 11.00000 0.02499 0.01393 = 0.02224 0.00367 0.00361 0.00260 AFIX 43 H26 2 0.460706 -0.026921 0.060031 11.00000 -1.20000 AFIX 0 C27 1 0.294770 0.036953 0.064614 11.00000 0.02238 0.01623 = 0.02073 0.00236 -0.00059 -0.00218 AFIX 43 H27 2 0.258094 0.001187 0.013239 11.00000 -1.20000 AFIX 0 C28 1 0.091068 0.121386 0.079707 11.00000 0.02021 0.02708 = 0.02755 0.00461 -0.00158 0.00304 AFIX 13 H28 2 0.073832 0.081843 0.023518 11.00000 -1.20000 AFIX 0 C29 1 0.078922 0.214641 0.085804 11.00000 0.02754 0.03208 = 0.03180 0.00863 -0.00012 0.00788 AFIX 137 H29D 2 0.096402 0.254722 0.140447 11.00000 -1.50000 H29E 2 -0.008629 0.220635 0.065024 11.00000 -1.50000 H29F 2 0.141158 0.228715 0.055873 11.00000 -1.50000 AFIX 0 C30 1 -0.009933 0.095757 0.123280 11.00000 0.01948 0.03414 = 0.04735 0.01300 0.00309 0.00149 AFIX 137 H30D 2 -0.004797 0.034185 0.115387 11.00000 -1.50000 H30E 2 -0.096378 0.104686 0.103178 11.00000 -1.50000 H30F 2 0.007263 0.132130 0.178935 11.00000 -1.50000 AFIX 0 C31 1 0.606564 0.056431 0.198763 11.00000 0.02537 0.02961 = 0.03257 0.01449 -0.00048 0.00606 AFIX 137 H31D 2 0.661210 0.039766 0.156675 11.00000 -1.50000 H31E 2 0.598860 0.009085 0.217418 11.00000 -1.50000 H31F 2 0.645376 0.109538 0.241583 11.00000 -1.50000 AFIX 0 RU1B 6 0.790764 0.314567 0.394795 11.00000 0.01379 0.02353 = 0.01462 -0.00168 -0.00026 0.00467 CL1B 3 0.873953 0.362075 0.530729 11.00000 0.02070 0.06005 = 0.01437 -0.00152 -0.00053 -0.00297 CL2B 3 0.619595 0.223833 0.413658 11.00000 0.02670 0.02341 = 0.02175 0.00529 -0.00206 0.00140 S1B 7 0.929454 0.194925 0.362384 11.00000 0.04236 0.04786 = 0.02351 0.01561 0.01465 0.03055 N1B 4 1.019405 0.080397 0.418001 11.00000 0.04854 0.05190 = 0.02806 0.01734 0.01276 0.02864 AFIX 43 H1B 2 1.017529 0.054144 0.450747 11.00000 -1.20000 AFIX 0 N2B 4 0.860545 0.160105 0.481714 11.00000 0.05230 0.07065 = 0.02699 0.02538 0.01879 0.04302 PART 1 AFIX 43 H2B 2 0.806372 0.200520 0.484449 21.00000 -1.20000 AFIX 43 PART 0 PART 2 H2BA 2 0.801434 0.196742 0.481438 -21.00000 -1.20000 AFIX 0 PART 0 C2B 1 0.937106 0.141616 0.423838 11.00000 0.04677 0.05527 = 0.02302 0.01668 0.01227 0.03113 C3B 1 1.111185 0.053416 0.362786 11.00000 0.03333 0.03279 = 0.03510 0.01368 0.00746 0.01219 C4B 1 1.237174 0.077557 0.386816 11.00000 0.03559 0.03896 = 0.04949 0.01984 -0.00217 0.00928 AFIX 43 H4B 2 1.262776 0.117609 0.438672 11.00000 -1.20000 AFIX 0 C5B 1 1.332193 0.044873 0.336928 11.00000 0.02585 0.04975 = 0.11524 0.05348 0.01464 0.00616 AFIX 43 H5B 2 1.420595 0.063535 0.354491 11.00000 -1.20000 AFIX 0 C6B 1 1.294340 -0.015071 0.261671 11.00000 0.05334 0.04316 = 0.07646 0.03746 0.03439 0.01618 AFIX 43 H6B 2 1.357462 -0.039180 0.227948 11.00000 -1.20000 AFIX 0 C7B 1 1.164563 -0.039887 0.235546 11.00000 0.05747 0.02358 = 0.04578 0.01806 0.03037 0.01521 C8B 1 1.069234 -0.005916 0.286578 11.00000 0.04597 0.02549 = 0.03507 0.01336 0.01482 0.00783 C9B 1 1.117535 -0.099266 0.158179 11.00000 0.10116 0.03255 = 0.04619 0.01934 0.03274 0.02476 AFIX 43 H9B 2 1.178148 -0.122395 0.122427 11.00000 -1.20000 AFIX 0 C10B 1 0.991387 -0.123944 0.133609 11.00000 0.12112 0.03551 = 0.04030 0.01087 0.00151 -0.00025 AFIX 43 H10B 2 0.964682 -0.163701 0.081783 11.00000 -1.20000 AFIX 0 C11B 1 0.903315 -0.091600 0.183390 11.00000 0.09139 0.04003 = 0.04021 0.01799 -0.01489 -0.01125 AFIX 43 H11B 2 0.814845 -0.109623 0.165391 11.00000 -1.20000 AFIX 0 C12B 1 0.935700 -0.034735 0.257651 11.00000 0.04330 0.03983 = 0.03612 0.02111 0.00541 0.00364 AFIX 43 H12B 2 0.870681 -0.013790 0.290726 11.00000 -1.20000 AFIX 0 PART 1 O1B 5 0.949643 0.086008 0.548151 21.00000 0.05015 0.06729 = 0.04363 0.03952 0.02315 0.02774 C13B 1 0.856521 0.125719 0.534193 21.00000 0.06012 0.09026 = 0.02217 0.03145 0.01822 0.04396 C14B 1 0.757743 0.154052 0.588288 21.00000 0.07396 0.08873 = 0.02369 0.02024 0.02269 0.03817 AFIX 23 H14A 2 0.679710 0.165239 0.559767 21.00000 -1.20000 H14B 2 0.734056 0.104957 0.603087 21.00000 -1.20000 AFIX 0 C15B 1 0.792912 0.231330 0.659443 21.00000 0.07680 0.09021 = 0.04730 0.01932 0.01303 0.04464 AFIX 23 H15A 2 0.724695 0.236327 0.693508 21.00000 -1.20000 H15B 2 0.791178 0.282960 0.645309 21.00000 -1.20000 AFIX 0 C16B 1 0.917629 0.236857 0.705652 21.00000 0.06591 0.07553 = 0.06808 0.02882 0.00816 0.01400 AFIX 23 H16A 2 0.986862 0.247023 0.677154 21.00000 -1.20000 H16B 2 0.929109 0.179738 0.709693 21.00000 -1.20000 AFIX 0 C17B 1 0.934614 0.305421 0.784900 21.00000 0.07679 0.07419 = 0.06817 0.02583 0.00813 0.00937 AFIX 23 H17A 2 0.907499 0.360625 0.781541 21.00000 -1.20000 H17B 2 0.875579 0.289335 0.816115 21.00000 -1.20000 AFIX 0 C18B 1 1.065682 0.321983 0.827037 21.00000 0.07804 0.07189 = 0.06946 0.02773 -0.00249 -0.00364 AFIX 23 H18A 2 1.121611 0.348639 0.801242 21.00000 -1.20000 H18B 2 1.099195 0.265163 0.822074 21.00000 -1.20000 AFIX 0 C19B 1 1.077518 0.379149 0.910744 21.00000 0.07342 0.08292 = 0.05973 0.03261 0.00190 -0.00889 AFIX 23 H19A 2 1.060633 0.439183 0.915384 21.00000 -1.20000 H19B 2 1.009439 0.359170 0.934469 21.00000 -1.20000 AFIX 0 C20B 1 1.202477 0.382479 0.955976 21.00000 0.07696 0.07157 = 0.06644 0.02548 -0.00137 0.00139 AFIX 23 H20A 2 1.268815 0.409151 0.936063 21.00000 -1.20000 H20B 2 1.224244 0.321765 0.945792 21.00000 -1.20000 AFIX 0 C21B 1 1.212079 0.430470 1.040762 21.00000 0.10003 0.09229 = 0.06687 0.02973 -0.02815 0.02481 AFIX 137 H21A 2 1.203935 0.492718 1.052468 21.00000 -1.50000 H21B 2 1.295807 0.422532 1.065024 21.00000 -1.50000 H21C 2 1.142884 0.408099 1.061224 21.00000 -1.50000 AFIX 0 SAME 0.005 0.04 O1B > C21B PART 0 PART 2 O1C 5 0.913211 0.059058 0.538393 -21.00000 0.05015 0.06729 = 0.04363 0.03952 0.02315 0.02774 C13C 1 0.862107 0.128224 0.543871 -21.00000 0.06012 0.09026 = 0.02217 0.03145 0.01822 0.04396 C14C 1 0.775628 0.173487 0.602471 -21.00000 0.07396 0.08873 = 0.02369 0.02024 0.02269 0.03817 AFIX 23 H14C 2 0.731727 0.217160 0.586618 -21.00000 -1.20000 H14D 2 0.708422 0.130158 0.602105 -21.00000 -1.20000 AFIX 0 C15C 1 0.840093 0.218165 0.682918 -21.00000 0.07680 0.09021 = 0.04730 0.01932 0.01303 0.04464 AFIX 23 H15C 2 0.773124 0.238704 0.718198 -21.00000 -1.20000 H15D 2 0.887776 0.175175 0.697842 -21.00000 -1.20000 AFIX 0 C16C 1 0.930654 0.293276 0.695008 -21.00000 0.06591 0.07553 = 0.06808 0.02882 0.00816 0.01400 AFIX 23 H16C 2 1.012146 0.270364 0.675469 -21.00000 -1.20000 H16D 2 0.894068 0.324081 0.662519 -21.00000 -1.20000 AFIX 0 C17C 1 0.962132 0.357895 0.775348 -21.00000 0.07679 0.07419 = 0.06817 0.02583 0.00813 0.00937 AFIX 23 H17C 2 1.021536 0.404810 0.774431 -21.00000 -1.20000 H17D 2 0.881787 0.384623 0.793299 -21.00000 -1.20000 AFIX 0 C18C 1 1.020919 0.325718 0.833016 -21.00000 0.07804 0.07189 = 0.06946 0.02773 -0.00249 -0.00364 AFIX 23 H18C 2 1.091474 0.289289 0.810651 -21.00000 -1.20000 H18D 2 0.955217 0.287259 0.841386 -21.00000 -1.20000 AFIX 0 C19C 1 1.073856 0.392717 0.909862 -21.00000 0.07342 0.08292 = 0.05973 0.03261 0.00190 -0.00889 AFIX 23 H19C 2 1.141604 0.430314 0.902097 -21.00000 -1.20000 H19D 2 1.004152 0.430067 0.932190 -21.00000 -1.20000 AFIX 0 C20C 1 1.129173 0.357322 0.966472 -21.00000 0.07696 0.07157 = 0.06644 0.02548 -0.00137 0.00139 AFIX 23 H20C 2 1.062578 0.316883 0.971386 -21.00000 -1.20000 H20D 2 1.201511 0.322413 0.944818 -21.00000 -1.20000 AFIX 0 C21C 1 1.176805 0.421055 1.044946 -21.00000 0.10003 0.09229 = 0.06687 0.02973 -0.02815 0.02481 AFIX 137 H21D 2 1.234192 0.466415 1.041035 -21.00000 -1.50000 H21E 2 1.224291 0.391360 1.074427 -21.00000 -1.50000 H21F 2 1.103656 0.447838 1.071642 -21.00000 -1.50000 AFIX 0 PART 0 C22B 1 0.899775 0.371405 0.329479 11.00000 0.01709 0.02293 = 0.02604 -0.00174 0.00477 0.00001 C23B 1 0.796226 0.312891 0.278617 11.00000 0.02075 0.01890 = 0.01754 0.00119 0.00211 0.00029 AFIX 43 H23B 2 0.813954 0.267414 0.232147 11.00000 -1.20000 AFIX 0 C24B 1 0.669057 0.321728 0.296391 11.00000 0.01687 0.02094 = 0.02010 0.00627 -0.00227 -0.00012 AFIX 43 H24B 2 0.602090 0.281540 0.262189 11.00000 -1.20000 AFIX 0 C25B 1 0.638471 0.390265 0.365182 11.00000 0.01600 0.02284 = 0.02741 0.00894 0.00316 0.00414 C26B 1 0.739945 0.447532 0.415019 11.00000 0.02225 0.02065 = 0.02693 -0.00195 0.00694 0.00345 AFIX 43 H26B 2 0.722075 0.493360 0.461226 11.00000 -1.20000 AFIX 0 C27B 1 0.869595 0.438037 0.397407 11.00000 0.01941 0.02478 = 0.03006 -0.00645 0.00348 -0.00353 AFIX 43 H27B 2 0.936713 0.477489 0.432249 11.00000 -1.20000 AFIX 0 C28B 1 1.035284 0.360574 0.307294 11.00000 0.01840 0.03226 = 0.03958 -0.01104 0.01054 -0.00257 AFIX 13 H28B 2 1.042076 0.297450 0.274941 11.00000 -1.20000 AFIX 0 C29B 1 1.139176 0.387409 0.377139 11.00000 0.01482 0.06546 = 0.05757 -0.01883 0.00018 -0.00018 AFIX 137 H29A 2 1.142029 0.450695 0.406114 11.00000 -1.50000 H29B 2 1.223098 0.371314 0.359091 11.00000 -1.50000 H29C 2 1.119125 0.357453 0.411071 11.00000 -1.50000 AFIX 0 C30B 1 1.053902 0.412391 0.256497 11.00000 0.04156 0.03372 = 0.06468 -0.00462 0.03377 -0.00800 AFIX 137 H30A 2 0.987345 0.392051 0.211431 11.00000 -1.50000 H30B 2 1.139261 0.403712 0.238668 11.00000 -1.50000 H30C 2 1.047021 0.474589 0.286863 11.00000 -1.50000 AFIX 0 C31B 1 0.503126 0.396950 0.385555 11.00000 0.01677 0.03041 = 0.03252 0.01214 0.00477 0.00711 AFIX 137 H31A 2 0.461020 0.338231 0.369224 11.00000 -1.50000 H31B 2 0.455141 0.429356 0.358873 11.00000 -1.50000 H31C 2 0.504744 0.427633 0.441884 11.00000 -1.50000 AFIX 0 HKLF 4 REM svpncnap_a.res in P-1 REM wR2 = 0.074629, GooF = S = 1.05690, Restrained GooF = 1.07443 for all data REM R1 = 0.030161 for 12502 Fo > 4sig(Fo) and 0.034813 for all 13730 data REM 724 parameters refined using 393 restraints END WGHT 0.0249 5.3128 REM Instructions for potential hydrogen bonds HTAB N1 O1 HTAB N2 Cl2 HTAB N1B O1B HTAB N1B O1B_$1 HTAB N1B O1C HTAB N1B O1C_$1 HTAB N2B Cl1B HTAB N2B Cl2B HTAB N2B Cl1B HTAB N2B Cl2B REM Highest difference peak 1.186, deepest hole -0.712, 1-sigma level 0.074 Q1 1 0.9425 0.0397 0.3813 11.00000 0.05 1.19 Q2 1 1.0300 0.3867 0.8311 11.00000 0.05 1.06 Q3 1 0.9992 0.0039 0.3158 11.00000 0.05 1.05 Q4 1 0.7922 0.1893 0.6773 11.00000 0.05 1.01 Q5 1 1.1410 0.0081 0.3213 11.00000 0.05 0.89 Q6 1 0.8096 0.2747 0.7376 11.00000 0.05 0.87 Q7 1 0.8816 0.1672 0.3295 11.00000 0.05 0.77 Q8 1 1.3994 0.0061 0.3071 11.00000 0.05 0.73 Q9 1 0.8735 0.3523 0.8042 11.00000 0.05 0.73 Q10 1 1.3538 0.0670 0.3898 11.00000 0.05 0.69 Q11 1 0.9854 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0 100.19 5.40 4 -2 0 102.39 6.80 4 -2 0 107.89 6.10 4 -2 0 80.09 6.00 4 -2 0 109.29 5.60 4 -2 0 111.79 7.00 -4 2 0 109.49 6.90 -4 2 0 106.29 7.00 -4 2 0 107.49 6.50 -4 2 0 105.89 5.60 -4 2 0 94.39 5.90 -4 2 0 104.99 5.70 -4 2 0 106.99 6.20 -4 2 0 105.09 6.60 -4 2 0 107.59 6.00 3 -2 0 74.69 4.60 3 -2 0 74.99 4.30 3 -2 0 70.49 4.40 3 -2 0 79.39 4.60 3 -2 0 77.49 4.90 3 -2 0 80.09 4.20 3 -2 0 74.29 5.00 -3 2 0 81.49 5.10 -3 2 0 70.29 4.90 -3 2 0 78.29 5.10 -3 2 0 80.69 5.10 -3 2 0 76.99 4.60 -3 2 0 69.89 4.40 -3 2 0 74.49 4.40 -3 2 0 77.79 4.50 -3 2 0 81.49 4.20 2 -2 0 1393.96 42.10 2 -2 0 1479.65 42.40 2 -2 0 1494.15 42.50 2 -2 0 1405.66 40.40 2 -2 0 1453.05 40.30 2 -2 0 1503.85 42.50 2 -2 0 1481.35 41.50 -2 2 0 1436.66 41.70 -2 2 0 1438.46 42.40 -2 2 0 1437.16 43.10 -2 2 0 1430.96 43.30 -2 2 0 1408.26 42.20 -2 2 0 1418.06 42.40 -2 2 0 1415.96 42.30 -2 2 0 1455.05 41.40 -2 2 0 1410.46 42.20 1 -2 0 3766.12 102.29 -1 2 0 3477.95 102.29 0 -2 0 1246.98 37.90 0 -2 0 1325.57 37.70 0 2 0 1348.77 38.20 0 2 0 1305.57 37.90 0 2 0 1384.06 38.50 -1 -2 0 994.30 29.70 -1 -2 0 1012.30 29.50 -1 -2 0 965.40 29.50 -1 -2 0 1017.40 29.20 1 2 0 979.40 28.60 1 2 0 963.80 29.20 1 2 0 975.00 29.00 -2 -2 0 2567.24 73.39 -2 -2 0 2473.35 72.09 -2 -2 0 2564.84 73.29 -2 -2 0 2498.85 72.49 -2 -2 0 2465.95 71.09 -2 -2 0 2452.45 72.49 2 2 0 2383.86 70.69 2 2 0 2473.15 72.29 2 2 0 2756.22 72.99 2 2 0 2784.72 73.29 2 2 0 2487.55 71.59 2 2 0 2320.07 72.89 -3 -2 0 1.40 0.70 -3 -2 0 0.30 0.80 -3 -2 0 0.30 0.80 -3 -2 0 -0.80 1.10 -3 -2 0 2.70 1.10 -3 -2 0 1.80 1.30 3 2 0 0.50 1.00 3 2 0 0.70 1.00 3 2 0 0.90 0.70 3 2 0 0.90 1.10 3 2 0 -0.50 1.10 3 2 0 0.40 0.40 -4 -2 0 1970.00 54.59 -4 -2 0 1978.90 58.39 -4 -2 0 1947.01 59.99 -4 -2 0 1929.31 55.89 -4 -2 0 1900.51 60.09 -4 -2 0 1938.11 58.89 -4 -2 0 1935.71 57.09 -4 -2 0 1963.60 60.29 -4 -2 0 1922.41 56.29 4 2 0 1924.01 57.99 4 2 0 1613.74 59.19 4 2 0 1906.31 56.49 4 2 0 1875.41 57.29 4 2 0 2111.99 59.59 4 2 0 1880.31 54.59 4 2 0 1932.21 56.49 -5 -2 0 2309.07 69.79 -5 -2 0 2330.87 73.59 -5 -2 0 2370.46 70.29 -5 -2 0 2355.36 68.59 -5 -2 0 2327.77 68.19 -5 -2 0 2358.56 67.19 -5 -2 0 2369.96 72.29 -5 -2 0 2315.77 71.19 -5 -2 0 2268.87 70.29 -5 -2 0 2432.66 71.49 5 2 0 2359.06 70.79 5 2 0 2424.16 70.69 5 2 0 2442.16 69.89 5 2 0 2323.87 72.39 5 2 0 2368.16 70.69 5 2 0 2268.07 68.99 -6 -2 0 348.27 16.60 -6 -2 0 330.47 13.60 -6 -2 0 332.57 13.00 -6 -2 0 345.07 12.50 -6 -2 0 323.47 13.40 -6 -2 0 349.87 13.00 -6 -2 0 332.07 14.40 -6 -2 0 321.27 17.30 -6 -2 0 361.46 16.10 -6 -2 0 341.47 17.60 6 2 0 350.46 16.80 6 2 0 310.57 13.70 6 2 0 400.66 18.90 6 2 0 353.46 13.10 6 2 0 346.87 12.50 6 2 0 329.67 14.70 6 2 0 349.27 14.10 6 2 0 321.47 13.70 6 2 0 322.17 11.90 -7 -2 0 524.45 24.50 -7 -2 0 487.45 19.90 -7 -2 0 496.65 19.10 -7 -2 0 515.65 19.20 -7 -2 0 524.55 18.70 -7 -2 0 501.55 24.00 -7 -2 0 501.85 20.90 -7 -2 0 512.75 22.70 -7 -2 0 500.25 18.10 -7 -2 0 500.65 21.40 -7 -2 0 488.45 17.60 -7 -2 0 503.95 21.80 7 2 0 498.95 19.90 7 2 0 463.45 17.40 7 2 0 514.35 19.50 7 2 0 463.95 21.40 7 2 0 557.34 21.90 7 2 0 532.65 18.50 7 2 0 490.75 16.90 7 2 0 499.25 19.10 7 2 0 479.15 19.00 7 2 0 559.64 25.20 7 2 0 549.65 23.70 -8 -2 0 241.58 11.70 -8 -2 0 256.47 11.40 -8 -2 0 268.17 17.10 -8 -2 0 245.38 12.20 -8 -2 0 260.97 17.00 -8 -2 0 241.58 13.00 -8 -2 0 250.97 15.50 -8 -2 0 253.07 14.60 -8 -2 0 272.87 14.40 -8 -2 0 256.27 11.30 -8 -2 0 270.37 12.60 -8 -2 0 267.07 15.00 8 2 0 265.37 14.00 8 2 0 251.87 12.70 8 2 0 281.87 16.50 8 2 0 238.18 11.00 8 2 0 251.57 10.10 8 2 0 259.37 14.50 8 2 0 304.27 18.40 8 2 0 255.67 12.80 8 2 0 265.07 15.20 8 2 0 238.48 11.20 -9 -2 0 79.99 8.20 -9 -2 0 78.29 8.90 -9 -2 0 85.69 8.70 -9 -2 0 79.99 7.40 -9 -2 0 74.19 9.40 -9 -2 0 85.39 8.90 -9 -2 0 91.69 11.10 -9 -2 0 82.99 8.70 -9 -2 0 75.09 6.60 -9 -2 0 71.89 6.50 -9 -2 0 83.79 6.20 9 2 0 68.89 9.90 9 2 0 84.59 6.30 9 2 0 70.99 6.40 9 2 0 85.39 10.40 9 2 0 88.79 8.60 9 2 0 78.49 7.90 9 2 0 64.09 8.40 9 2 0 84.49 7.20 9 2 0 73.59 6.20 9 2 0 79.99 8.90 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5.90 -13 -2 0 60.29 10.90 -13 -2 0 46.20 8.10 -13 -2 0 67.69 12.50 -13 -2 0 52.79 8.80 -13 -2 0 49.99 10.70 -13 -2 0 54.69 8.60 -13 -2 0 61.29 10.20 13 2 0 58.19 12.10 13 2 0 63.19 13.80 13 2 0 63.99 3.30 13 2 0 74.79 11.20 13 2 0 58.89 11.30 13 2 0 62.09 9.00 -14 -2 0 -4.50 4.10 -14 -2 0 0.00 7.20 -14 -2 0 -0.90 4.30 -14 -2 0 -4.90 4.00 14 2 0 1.80 5.00 14 2 0 3.60 7.10 14 2 0 2.50 3.90 -15 -2 0 123.19 15.10 -15 -2 0 126.89 14.60 15 2 0 92.49 13.70 15 -3 0 153.18 14.90 15 -3 0 123.79 12.00 15 -3 0 154.78 13.90 -15 3 0 133.19 13.10 -15 3 0 112.79 14.20 -15 3 0 122.89 12.60 14 -3 0 -4.40 6.80 14 -3 0 -9.70 3.70 14 -3 0 -4.60 4.10 14 -3 0 2.40 3.90 -14 3 0 -1.80 4.60 -14 3 0 -5.10 4.40 -14 3 0 -3.00 4.80 -14 3 0 -8.40 7.20 13 -3 0 -1.00 5.90 13 -3 0 -0.90 5.00 13 -3 0 -4.60 5.80 13 -3 0 7.60 4.10 13 -3 0 8.00 6.10 13 -3 0 10.10 7.40 13 -3 0 6.80 5.70 -13 3 0 6.70 4.50 -13 3 0 7.10 6.40 -13 3 0 9.50 7.70 -13 3 0 4.10 5.50 -13 3 0 13.80 6.30 -13 3 0 -0.60 3.70 -13 3 0 -2.50 3.90 -13 3 0 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0 151.78 11.90 10 -3 0 171.98 13.90 -10 3 0 159.88 9.60 -10 3 0 154.18 11.50 -10 3 0 157.28 12.30 -10 3 0 149.79 12.10 -10 3 0 149.59 11.70 -10 3 0 130.09 12.10 -10 3 0 157.98 13.10 -10 3 0 172.98 14.20 -10 3 0 147.79 10.30 -10 3 0 159.98 11.30 -10 3 0 141.19 12.90 -10 3 0 141.29 10.10 -10 3 0 157.18 10.40 9 -3 0 81.89 9.00 9 -3 0 73.39 7.00 9 -3 0 97.19 9.60 9 -3 0 74.79 5.70 9 -3 0 74.59 6.60 9 -3 0 68.99 6.50 9 -3 0 64.49 8.40 9 -3 0 68.19 6.30 9 -3 0 80.69 9.10 9 -3 0 77.19 8.50 9 -3 0 75.49 7.20 9 -3 0 76.49 7.80 9 -3 0 76.79 8.00 9 -3 0 66.79 8.40 -9 3 0 73.79 9.00 -9 3 0 71.69 8.40 -9 3 0 56.79 7.90 -9 3 0 65.59 8.40 -9 3 0 70.69 9.30 -9 3 0 76.29 6.30 -9 3 0 63.09 6.50 -9 3 0 79.39 7.30 -9 3 0 60.29 8.80 -9 3 0 71.49 6.80 -9 3 0 76.59 8.10 -9 3 0 77.09 5.90 -9 3 0 75.89 8.20 -9 3 0 70.39 6.50 -9 3 0 61.29 6.50 -9 3 0 67.39 6.60 8 -3 0 181.38 11.60 8 -3 0 163.98 9.50 8 -3 0 165.58 12.40 8 -3 0 165.08 9.90 8 -3 0 183.88 8.90 8 -3 0 185.18 12.20 8 -3 0 187.98 11.20 8 -3 0 177.28 11.70 8 -3 0 175.68 10.10 8 -3 0 177.48 10.30 8 -3 0 190.38 12.30 8 -3 0 179.98 11.50 8 -3 0 184.88 13.20 8 -3 0 166.28 8.90 -8 3 0 167.88 10.00 -8 3 0 162.68 9.90 -8 3 0 177.08 11.80 -8 3 0 191.88 10.70 -8 3 0 188.18 10.20 -8 3 0 175.08 12.90 -8 3 0 163.78 11.30 -8 3 0 175.18 11.10 -8 3 0 198.48 13.20 -8 3 0 198.28 12.30 -8 3 0 169.28 10.10 -8 3 0 178.48 11.30 -8 3 0 186.38 10.30 -8 3 0 170.38 8.80 -8 3 0 179.18 9.00 -8 3 0 182.68 12.00 7 -3 0 140.59 10.20 7 -3 0 141.39 8.20 7 -3 0 170.28 10.70 7 -3 0 150.48 8.80 7 -3 0 159.18 7.90 7 -3 0 163.98 9.80 7 -3 0 157.38 10.80 7 -3 0 160.88 11.30 7 -3 0 128.29 8.60 7 -3 0 138.19 7.50 7 -3 0 146.69 8.50 7 -3 0 148.99 9.20 7 -3 0 162.18 10.30 -7 3 0 159.18 10.90 -7 3 0 149.59 7.70 -7 3 0 148.29 8.70 -7 3 0 157.28 8.50 -7 3 0 140.09 8.70 -7 3 0 145.79 8.90 -7 3 0 164.48 11.40 -7 3 0 142.29 9.30 -7 3 0 141.09 9.70 -7 3 0 148.99 8.80 -7 3 0 136.79 8.30 -7 3 0 153.78 10.30 -7 3 0 144.39 7.60 -7 3 0 147.29 10.40 -7 3 0 150.88 9.50 6 -3 0 1451.25 46.10 6 -3 0 1538.25 48.90 6 -3 0 1603.44 47.90 6 -3 0 1567.94 47.70 6 -3 0 1640.54 51.09 6 -3 0 1710.83 52.29 6 -3 0 1531.35 47.80 6 -3 0 1553.04 46.60 6 -3 0 1567.34 50.39 6 -3 0 1598.54 49.30 6 -3 0 1670.93 50.29 6 -3 0 1650.23 49.10 6 -3 0 1594.84 49.60 -6 3 0 1476.05 47.30 -6 3 0 1567.04 51.39 -6 3 0 1475.55 47.50 -6 3 0 1486.05 50.19 -6 3 0 1475.15 47.50 -6 3 0 1519.65 49.50 -6 3 0 1530.15 50.99 -6 3 0 1533.45 48.00 -6 3 0 1455.35 46.50 -6 3 0 1523.85 49.40 -6 3 0 1504.25 48.40 -6 3 0 1559.74 50.69 -6 3 0 1428.06 48.60 -6 3 0 1481.45 48.90 5 -3 0 236.28 11.60 5 -3 0 212.28 10.00 5 -3 0 199.78 9.40 5 -3 0 204.98 9.20 5 -3 0 200.38 11.30 5 -3 0 200.18 10.10 5 -3 0 202.78 10.00 5 -3 0 222.28 11.20 -5 3 0 191.38 10.00 -5 3 0 194.98 10.10 -5 3 0 209.88 9.30 -5 3 0 210.18 9.90 -5 3 0 187.78 10.90 -5 3 0 203.58 11.10 -5 3 0 191.68 10.00 -5 3 0 203.28 9.90 -5 3 0 199.28 10.70 -5 3 0 221.28 11.00 -5 3 0 203.18 10.90 -5 3 0 190.18 9.50 4 -3 0 252.27 11.70 4 -3 0 229.38 10.40 4 -3 0 233.48 9.60 4 -3 0 254.07 10.60 4 -3 0 237.28 9.60 4 -3 0 235.88 10.50 4 -3 0 225.18 11.00 4 -3 0 245.48 10.30 4 -3 0 229.78 10.90 -4 3 0 227.88 10.50 -4 3 0 231.68 11.00 -4 3 0 226.18 10.50 -4 3 0 237.78 9.70 -4 3 0 244.18 9.80 -4 3 0 252.57 10.40 -4 3 0 234.68 11.60 -4 3 0 222.38 10.90 -4 3 0 246.28 9.70 -4 3 0 252.57 10.40 -4 3 0 231.88 11.30 3 -3 0 1543.25 45.90 3 -3 0 1499.35 45.70 3 -3 0 1574.14 45.70 3 -3 0 1479.05 42.80 3 -3 0 1547.75 42.60 3 -3 0 1580.44 44.50 3 -3 0 1442.86 46.70 3 -3 0 1515.95 44.80 3 -3 0 1643.24 46.10 -3 3 0 1451.95 44.60 -3 3 0 1533.75 45.80 -3 3 0 1519.95 47.30 -3 3 0 1499.55 45.70 -3 3 0 1473.05 45.50 -3 3 0 1506.85 46.90 -3 3 0 1487.85 45.70 -3 3 0 1486.15 44.30 -3 3 0 1479.15 45.40 2 -3 0 315.97 11.40 2 -3 0 347.37 12.30 2 -3 0 334.67 11.80 2 -3 0 340.17 10.70 2 -3 0 333.17 12.00 2 -3 0 313.17 12.90 2 -3 0 313.17 10.90 2 -3 0 363.46 11.10 -2 3 0 335.17 10.90 -2 3 0 344.47 11.60 -2 3 0 335.17 11.90 -2 3 0 338.07 13.10 -2 3 0 344.67 12.20 -2 3 0 322.47 13.20 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36.60 -4 -3 0 1138.09 35.80 -4 -3 0 1152.28 37.40 -4 -3 0 1165.58 35.30 -4 -3 0 1163.68 38.30 -4 -3 0 1197.88 37.40 4 3 0 1215.98 37.90 4 3 0 1155.88 36.20 4 3 0 1144.59 38.00 4 3 0 1218.88 38.70 4 3 0 1088.59 39.20 4 3 0 1137.99 34.00 4 3 0 1168.98 36.20 -5 -3 0 179.78 9.70 -5 -3 0 176.38 9.10 -5 -3 0 165.58 10.20 -5 -3 0 183.38 8.10 -5 -3 0 173.68 7.80 -5 -3 0 171.08 9.80 -5 -3 0 176.48 11.20 -5 -3 0 167.88 8.30 -5 -3 0 177.68 11.30 -5 -3 0 167.88 7.90 -5 -3 0 167.18 9.70 5 3 0 180.18 9.80 5 3 0 172.78 11.20 5 3 0 176.38 9.80 5 3 0 165.98 8.40 5 3 0 171.68 9.20 5 3 0 181.38 10.50 5 3 0 172.88 8.70 5 3 0 168.18 7.40 5 3 0 188.28 10.80 -6 -3 0 57.29 4.80 -6 -3 0 56.19 4.60 -6 -3 0 58.69 5.80 -6 -3 0 55.09 6.60 -6 -3 0 52.39 4.90 -6 -3 0 52.69 4.50 -6 -3 0 55.49 5.70 -6 -3 0 54.69 3.20 -6 -3 0 56.89 7.10 -6 -3 0 53.69 5.50 -6 -3 0 66.49 7.00 -6 -3 0 54.29 4.30 6 3 0 50.69 4.60 6 3 0 57.99 5.00 6 3 0 49.90 3.30 6 3 0 61.49 7.10 6 3 0 52.89 3.20 6 3 0 43.90 5.90 6 3 0 50.49 4.40 6 3 0 48.90 5.40 6 3 0 45.70 6.00 -7 -3 0 125.09 7.60 -7 -3 0 122.99 7.00 -7 -3 0 127.99 6.00 -7 -3 0 129.89 7.80 -7 -3 0 134.09 10.30 -7 -3 0 121.29 9.20 -7 -3 0 135.99 11.40 -7 -3 0 122.99 9.50 -7 -3 0 123.09 8.30 -7 -3 0 128.39 8.90 -7 -3 0 126.39 11.00 -7 -3 0 131.99 7.30 7 3 0 123.29 9.30 7 3 0 143.49 8.40 7 3 0 128.69 9.10 7 3 0 128.09 8.10 7 3 0 128.39 10.30 7 3 0 113.69 10.90 7 3 0 126.29 5.80 7 3 0 132.29 7.30 7 3 0 115.29 8.10 -8 -3 0 43.90 5.20 -8 -3 0 45.60 4.60 -8 -3 0 56.99 5.30 -8 -3 0 51.99 5.90 -8 -3 0 39.00 6.20 -8 -3 0 40.10 5.60 -8 -3 0 37.50 7.30 -8 -3 0 43.30 7.70 -8 -3 0 29.20 6.50 -8 -3 0 38.80 4.80 -8 -3 0 45.00 6.10 8 3 0 63.89 8.50 8 3 0 44.60 4.40 8 3 0 41.30 5.30 8 3 0 62.59 5.80 8 3 0 58.69 6.20 8 3 0 44.30 6.40 8 3 0 49.60 5.10 8 3 0 49.70 7.20 8 3 0 51.79 6.50 -9 -3 0 537.95 21.50 -9 -3 0 585.74 25.10 -9 -3 0 556.44 28.30 -9 -3 0 532.75 23.20 -9 -3 0 506.15 25.70 -9 -3 0 538.05 23.00 -9 -3 0 541.55 27.70 -9 -3 0 523.45 20.80 -9 -3 0 526.45 21.40 -9 -3 0 588.34 25.60 9 3 0 556.84 22.90 9 3 0 493.45 24.40 9 3 0 538.85 26.70 9 3 0 564.74 28.90 9 3 0 518.85 21.90 9 3 0 525.35 22.00 9 3 0 533.75 24.10 -10 -3 0 158.88 11.50 -10 -3 0 153.68 13.70 -10 -3 0 186.28 15.80 -10 -3 0 168.48 13.20 -10 -3 0 159.68 12.40 -10 -3 0 178.28 11.40 -10 -3 0 161.18 10.90 -10 -3 0 167.98 13.20 -10 -3 0 145.09 14.70 10 3 0 172.98 16.00 10 3 0 174.78 14.80 10 3 0 162.28 10.90 10 3 0 161.38 12.50 10 3 0 139.99 9.20 10 3 0 159.18 13.10 10 3 0 164.28 10.80 10 3 0 180.48 13.50 10 3 0 169.28 15.50 -11 -3 0 139.29 10.30 -11 -3 0 141.99 11.00 -11 -3 0 145.79 14.40 -11 -3 0 157.28 12.80 -11 -3 0 144.29 11.20 -11 -3 0 143.49 12.70 -11 -3 0 125.69 11.70 -11 -3 0 129.49 9.20 11 3 0 137.19 12.90 11 3 0 128.99 12.20 11 3 0 125.89 10.20 11 3 0 124.49 14.50 11 3 0 120.69 10.70 -12 -3 0 152.58 15.30 -12 -3 0 150.28 11.00 -12 -3 0 136.79 13.50 -12 -3 0 131.39 15.30 -12 -3 0 150.98 14.30 -12 -3 0 153.68 15.40 -12 -3 0 162.08 12.00 -12 -3 0 142.39 12.20 12 3 0 152.38 14.20 12 3 0 151.88 11.70 12 3 0 117.39 15.00 12 3 0 152.98 15.60 12 3 0 147.89 13.90 12 3 0 161.78 10.20 12 3 0 121.19 15.20 -13 -3 0 7.60 4.50 -13 -3 0 1.00 6.80 -13 -3 0 13.00 4.50 -13 -3 0 9.90 5.70 -13 -3 0 10.90 4.70 13 3 0 8.20 3.20 13 3 0 0.30 4.70 13 3 0 7.30 3.70 13 3 0 8.20 6.40 -14 -3 0 -2.20 4.60 -14 -3 0 0.10 7.70 -14 -3 0 -0.90 4.10 14 3 0 -0.80 3.90 14 3 0 -10.10 4.40 14 3 0 -3.20 6.20 -15 -3 0 58.89 11.30 -15 -3 0 40.80 8.30 -15 -3 0 23.10 7.20 15 3 0 33.00 7.40 15 3 0 30.80 8.80 15 -4 0 18.10 5.90 15 -4 0 17.60 6.40 -15 4 0 18.20 6.10 -15 4 0 36.50 9.50 -15 4 0 15.40 7.40 14 -4 0 4.40 4.10 14 -4 0 3.50 4.60 14 -4 0 2.10 6.70 14 -4 0 -7.30 3.60 -14 4 0 1.90 4.80 -14 4 0 -6.90 4.10 -14 4 0 -0.60 7.70 -14 4 0 -7.90 4.60 13 -4 0 384.96 24.40 13 -4 0 406.36 20.80 13 -4 0 417.26 24.50 13 -4 0 383.66 20.30 13 -4 0 384.56 25.70 13 -4 0 404.16 23.60 13 -4 0 369.66 22.80 13 -4 0 374.96 22.30 -13 4 0 367.96 22.90 -13 4 0 429.76 25.70 -13 4 0 393.96 25.60 -13 4 0 398.56 22.40 -13 4 0 360.16 25.30 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1.50 1.30 8 -4 0 3.20 2.30 8 -4 0 1.50 3.20 8 -4 0 7.40 3.20 8 -4 0 6.70 3.80 8 -4 0 1.90 2.50 8 -4 0 5.20 2.40 8 -4 0 3.40 1.90 8 -4 0 6.60 3.40 8 -4 0 4.10 1.80 8 -4 0 7.90 3.60 -8 4 0 6.40 2.70 -8 4 0 2.80 3.30 -8 4 0 2.40 1.90 -8 4 0 5.00 2.00 -8 4 0 2.40 2.20 -8 4 0 4.50 2.30 -8 4 0 4.20 2.80 -8 4 0 0.00 2.80 -8 4 0 2.10 1.90 -8 4 0 6.00 4.30 -8 4 0 4.70 2.00 -8 4 0 1.30 1.70 -8 4 0 -0.10 3.00 -8 4 0 3.10 2.70 -8 4 0 3.80 3.20 7 -4 0 150.48 9.50 7 -4 0 155.18 8.70 7 -4 0 150.98 10.80 7 -4 0 145.69 7.80 7 -4 0 128.99 10.60 7 -4 0 142.69 8.40 7 -4 0 143.59 8.70 7 -4 0 146.29 9.20 7 -4 0 149.88 9.90 7 -4 0 175.88 11.20 7 -4 0 158.58 10.90 7 -4 0 149.19 10.70 7 -4 0 134.49 8.40 7 -4 0 151.28 7.60 -7 4 0 143.49 9.30 -7 4 0 163.68 9.90 -7 4 0 162.98 11.40 -7 4 0 159.18 8.30 -7 4 0 148.79 8.60 -7 4 0 139.29 7.40 -7 4 0 153.68 10.90 -7 4 0 139.19 8.70 -7 4 0 171.08 9.70 -7 4 0 170.38 11.20 -7 4 0 140.99 9.70 -7 4 0 155.98 11.10 -7 4 0 151.48 8.70 -7 4 0 150.88 10.80 -7 4 0 145.79 8.60 -7 4 0 146.29 9.40 6 -4 0 44.30 3.90 6 -4 0 37.30 5.00 6 -4 0 41.80 3.90 6 -4 0 35.50 3.80 6 -4 0 36.90 3.90 6 -4 0 46.80 5.70 6 -4 0 46.70 8.80 6 -4 0 34.20 4.40 6 -4 0 46.60 4.50 6 -4 0 37.90 5.10 6 -4 0 37.90 4.20 6 -4 0 43.60 3.60 6 -4 0 41.20 5.10 -6 4 0 42.80 5.60 -6 4 0 36.00 5.40 -6 4 0 43.20 3.50 -6 4 0 41.90 4.70 -6 4 0 46.30 4.10 -6 4 0 46.70 4.20 -6 4 0 46.50 4.20 -6 4 0 42.50 4.80 -6 4 0 33.80 4.40 -6 4 0 32.80 5.00 -6 4 0 45.20 5.60 -6 4 0 42.70 4.70 -6 4 0 34.80 4.20 -6 4 0 51.29 6.10 -6 4 0 35.50 4.00 5 -4 0 491.55 18.10 5 -4 0 522.25 18.10 5 -4 0 556.24 20.40 5 -4 0 510.25 19.40 5 -4 0 504.05 18.60 5 -4 0 547.15 21.40 5 -4 0 523.05 18.10 5 -4 0 508.25 19.60 5 -4 0 541.25 20.60 5 -4 0 482.55 21.10 5 -4 0 519.25 19.20 -5 4 0 507.85 19.50 -5 4 0 532.25 20.40 -5 4 0 497.55 20.80 -5 4 0 481.35 19.40 -5 4 0 498.65 20.00 -5 4 0 490.55 18.70 -5 4 0 509.85 18.00 -5 4 0 488.45 18.40 -5 4 0 494.95 21.10 -5 4 0 479.25 17.70 -5 4 0 462.85 19.10 -5 4 0 489.65 18.00 -5 4 0 486.55 18.10 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781.42 27.70 -6 7 0 746.23 26.80 -6 7 0 752.32 28.70 -6 7 0 767.02 26.10 -6 7 0 767.32 29.60 -6 7 0 728.63 31.80 -6 7 0 762.62 25.90 -6 7 0 740.63 26.40 -6 7 0 748.23 24.90 -6 7 0 726.13 25.60 -6 7 0 772.82 31.60 5 -7 0 259.37 12.30 5 -7 0 229.48 10.20 5 -7 0 240.18 9.90 5 -7 0 249.97 11.70 5 -7 0 273.17 11.00 5 -7 0 241.68 12.60 5 -7 0 247.08 11.10 5 -7 0 256.17 11.70 5 -7 0 222.98 9.80 -5 7 0 256.57 13.20 -5 7 0 235.18 13.00 -5 7 0 243.78 11.80 -5 7 0 250.87 12.20 -5 7 0 246.28 10.60 -5 7 0 253.57 10.30 -5 7 0 244.58 11.30 -5 7 0 226.28 12.70 -5 7 0 240.08 11.40 -5 7 0 250.17 12.90 -5 7 0 228.48 14.70 -5 7 0 228.58 11.50 -5 7 0 248.28 12.40 -5 7 0 259.17 10.60 4 -7 0 1.20 1.50 4 -7 0 0.20 1.60 4 -7 0 0.80 1.20 4 -7 0 -1.10 1.30 4 -7 0 0.40 1.10 4 -7 0 1.30 1.70 4 -7 0 1.90 1.60 4 -7 0 1.50 1.20 4 -7 0 -1.50 1.10 4 -7 0 -0.10 1.00 -4 7 0 0.70 1.30 -4 7 0 0.40 1.10 -4 7 0 3.20 1.20 -4 7 0 1.20 1.80 -4 7 0 1.70 1.60 -4 7 0 -0.10 1.20 -4 7 0 0.90 1.00 -4 7 0 0.60 1.50 -4 7 0 0.10 1.20 -4 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8.00 12 -8 0 46.10 10.80 12 -8 0 37.90 9.20 12 -8 0 38.40 7.40 12 -8 0 45.30 7.30 12 -8 0 41.10 9.60 12 -8 0 68.19 12.90 -12 8 0 33.50 6.80 -12 8 0 36.70 7.80 -12 8 0 70.79 10.90 -12 8 0 49.40 7.60 -12 8 0 25.00 8.70 -12 8 0 39.40 9.60 -12 8 0 48.20 9.20 -12 8 0 43.20 7.50 -12 8 0 49.60 13.20 -12 8 0 42.50 9.60 11 -8 0 4.90 3.20 11 -8 0 -3.70 5.10 11 -8 0 5.90 3.70 11 -8 0 5.50 5.60 11 -8 0 5.80 3.20 11 -8 0 -0.20 3.20 11 -8 0 1.20 4.70 11 -8 0 7.80 4.90 11 -8 0 6.50 3.40 11 -8 0 9.20 5.50 11 -8 0 -0.70 5.30 -11 8 0 1.10 3.80 -11 8 0 6.60 5.30 -11 8 0 3.10 3.10 -11 8 0 9.50 7.10 -11 8 0 0.30 6.00 -11 8 0 2.40 4.80 -11 8 0 -0.40 5.10 -11 8 0 1.30 3.50 -11 8 0 4.70 3.30 -11 8 0 -1.20 3.50 -11 8 0 2.90 5.20 -11 8 0 -0.20 5.00 10 -8 0 12.10 5.40 10 -8 0 12.10 4.40 10 -8 0 5.00 2.70 10 -8 0 11.90 4.20 10 -8 0 2.50 3.50 10 -8 0 7.70 4.50 10 -8 0 4.50 6.10 10 -8 0 4.50 2.40 10 -8 0 7.40 4.30 10 -8 0 10.50 3.80 10 -8 0 19.80 6.90 10 -8 0 9.10 5.00 -10 8 0 7.00 4.00 -10 8 0 1.80 5.40 -10 8 0 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8.10 1 12 -4 89.59 5.80 1 12 -4 84.29 9.50 1 12 -4 96.99 9.00 1 12 -4 87.49 6.60 1 12 -4 83.59 7.70 1 12 -4 94.39 7.70 1 12 -4 94.69 8.00 1 12 -4 86.49 7.40 1 12 -4 93.29 7.20 -1 -12 4 88.69 5.60 -1 -12 4 77.19 7.10 -1 -12 4 94.49 7.70 -1 -12 4 97.29 9.00 -1 -12 4 92.59 7.90 -1 -12 4 113.49 9.50 -1 -12 4 94.39 7.10 -1 -12 4 92.19 6.70 -1 -12 4 99.09 7.50 0 12 -4 196.38 11.20 0 12 -4 190.58 9.60 0 12 -4 179.48 12.40 0 12 -4 175.48 11.40 0 12 -4 201.18 11.70 0 12 -4 198.98 10.70 0 12 -4 194.98 10.20 0 12 -4 217.18 14.10 0 12 -4 191.18 7.70 0 12 -4 196.58 12.40 0 12 -4 179.68 10.90 0 12 -4 212.08 14.10 0 -12 4 188.28 11.70 0 -12 4 191.98 10.80 0 -12 4 190.78 12.40 0 -12 4 197.68 13.60 0 -12 4 201.78 9.90 0 -12 4 191.18 12.50 0 -12 4 179.28 11.80 0 -12 4 203.88 11.80 0 -12 4 204.78 10.80 -1 12 -4 22.20 3.80 -1 12 -4 23.30 5.40 -1 12 -4 22.70 5.00 -1 12 -4 30.60 5.10 -1 12 -4 23.80 4.90 -1 12 -4 27.30 3.90 -1 12 -4 22.30 4.70 -1 12 -4 20.80 4.20 -1 12 -4 24.90 4.70 -1 12 -4 32.90 6.50 -1 12 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4 17.10 5.00 6 -12 4 22.70 6.70 6 -12 4 6.50 3.30 6 -12 4 23.90 3.60 6 -12 4 13.90 3.50 -7 12 -4 397.06 21.70 -7 12 -4 421.26 17.60 -7 12 -4 425.46 22.70 -7 12 -4 390.86 19.50 -7 12 -4 414.26 18.60 -7 12 -4 401.16 20.40 -7 12 -4 391.26 21.60 -7 12 -4 381.66 24.20 -7 12 -4 413.86 21.30 -7 12 -4 422.06 25.10 -7 12 -4 406.36 19.30 7 -12 4 416.56 22.10 7 -12 4 393.76 23.90 7 -12 4 388.66 21.30 7 -12 4 441.56 19.40 7 -12 4 404.96 17.60 7 -12 4 383.46 16.90 7 -12 4 403.96 19.50 7 -12 4 448.36 22.20 7 -12 4 436.36 21.00 -8 12 -4 211.48 15.80 -8 12 -4 244.98 17.20 -8 12 -4 235.28 13.50 -8 12 -4 232.78 15.10 -8 12 -4 196.98 17.50 -8 12 -4 262.77 19.60 -8 12 -4 238.98 16.30 -8 12 -4 242.48 14.30 -8 12 -4 239.98 15.80 -8 12 -4 250.67 16.80 -8 12 -4 245.18 14.80 8 -12 4 238.08 10.80 8 -12 4 232.48 14.30 8 -12 4 234.58 14.10 8 -12 4 244.38 19.00 8 -12 4 240.48 16.40 8 -12 4 244.78 14.60 8 -12 4 232.38 15.90 8 -12 4 244.58 15.40 8 -12 4 218.98 13.50 8 -12 4 223.88 11.30 -9 12 -4 3.40 4.90 -9 12 -4 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356.96 15.90 7 4 -9 330.27 15.90 7 4 -9 341.77 17.10 7 4 -9 334.77 17.10 7 4 -9 337.77 14.60 7 4 -9 374.46 15.60 7 4 -9 346.27 15.90 7 4 -9 357.86 15.20 7 4 -9 308.37 15.00 -7 -4 9 332.97 15.60 -7 -4 9 351.66 18.70 -7 -4 9 338.27 15.70 -7 -4 9 343.07 18.90 -7 -4 9 362.06 17.90 -7 -4 9 332.87 17.30 -7 -4 9 319.87 13.30 -7 -4 9 336.97 15.70 -7 -4 9 333.17 14.20 -7 -4 9 355.46 17.50 -7 -4 9 349.47 13.90 -7 -4 9 383.86 20.70 -7 -4 9 382.26 18.10 6 4 -9 33.00 4.90 6 4 -9 41.50 5.00 6 4 -9 27.00 3.90 6 4 -9 33.50 4.30 6 4 -9 36.00 4.30 6 4 -9 36.90 4.30 6 4 -9 43.60 4.50 6 4 -9 37.50 5.20 6 4 -9 44.50 4.10 6 4 -9 40.60 4.50 -6 -4 9 28.90 3.50 -6 -4 9 36.40 5.30 -6 -4 9 23.60 5.50 -6 -4 9 36.80 4.50 -6 -4 9 36.30 5.70 -6 -4 9 49.00 5.50 -6 -4 9 37.30 5.10 -6 -4 9 27.00 5.20 -6 -4 9 34.10 3.40 -6 -4 9 47.30 4.70 -6 -4 9 32.60 5.40 -6 -4 9 43.90 4.60 5 4 -9 -2.10 0.90 5 4 -9 -0.40 1.70 5 4 -9 -0.60 1.50 5 4 -9 2.60 2.20 5 4 -9 -0.20 1.80 5 4 -9 1.20 1.50 5 4 -9 -0.90 0.80 5 4 -9 -1.90 1.70 5 4 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10.90 8 12 -21 19.50 9.00 8 12 -21 53.29 9.20 8 12 -21 64.29 11.20 8 12 -21 46.10 11.00 -8 -12 21 45.30 11.30 -8 -12 21 71.69 15.50 -8 -12 21 59.49 11.70 -8 -12 21 54.59 8.60 7 12 -21 22.10 5.90 7 12 -21 23.60 5.70 7 12 -21 14.80 6.60 7 12 -21 23.20 5.30 7 12 -21 22.10 7.60 7 12 -21 31.80 6.80 -7 -12 21 13.80 6.10 -7 -12 21 18.70 4.70 -7 -12 21 21.40 5.80 -7 -12 21 20.80 6.60 6 12 -21 32.90 8.20 6 12 -21 28.80 9.20 6 12 -21 33.90 7.30 6 12 -21 46.50 7.70 6 12 -21 27.10 7.80 6 12 -21 30.70 7.90 6 12 -21 7.30 6.10 -6 -12 21 32.40 7.60 -6 -12 21 46.10 6.40 -6 -12 21 68.79 14.60 -6 -12 21 21.40 7.90 -6 -12 21 26.20 7.10 -6 -12 21 22.70 5.50 5 12 -21 159.58 12.40 5 12 -21 136.19 14.20 5 12 -21 112.49 13.60 5 12 -21 137.19 14.60 5 12 -21 146.69 13.20 5 12 -21 123.69 10.50 5 12 -21 147.69 12.00 5 12 -21 129.99 15.60 -5 -12 21 135.39 13.40 -5 -12 21 120.89 13.70 -5 -12 21 132.29 15.90 -5 -12 21 126.89 15.80 -5 -12 21 144.19 11.20 -5 -12 21 135.49 12.10 -5 -12 21 124.19 10.20 4 12 -21 31.00 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104.59 10.90 3 7 -21 87.29 8.80 3 7 -21 95.29 8.60 -3 -7 21 76.09 9.20 -3 -7 21 82.59 10.00 -3 -7 21 74.49 10.80 -3 -7 21 90.69 8.10 -3 -7 21 99.29 8.60 -3 -7 21 98.79 10.20 -3 -7 21 73.59 11.40 2 7 -21 81.59 7.80 2 7 -21 91.29 7.90 2 7 -21 87.89 10.30 2 7 -21 100.09 12.00 2 7 -21 88.49 9.00 2 7 -21 76.39 8.40 2 7 -21 88.19 10.30 2 7 -21 74.09 8.70 -2 -7 21 76.19 10.70 -2 -7 21 85.49 9.20 -2 -7 21 87.09 7.70 -2 -7 21 89.09 9.10 -2 -7 21 72.59 10.50 -2 -7 21 81.99 7.30 -2 -7 21 71.29 8.90 1 7 -21 22.20 5.50 1 7 -21 7.30 4.80 1 7 -21 24.40 5.60 1 7 -21 12.80 3.40 1 7 -21 18.00 6.00 1 7 -21 25.60 5.40 1 7 -21 12.00 6.90 1 7 -21 13.20 4.00 -1 -7 21 13.90 5.80 -1 -7 21 14.50 4.70 -1 -7 21 17.00 4.90 -1 -7 21 28.00 4.80 -1 -7 21 13.70 5.80 -1 -7 21 7.00 2.70 -1 -7 21 25.00 5.90 0 7 -21 128.69 13.60 0 7 -21 125.09 10.50 0 7 -21 126.19 12.30 0 7 -21 139.09 12.80 0 7 -21 131.69 10.90 0 -7 21 109.99 11.40 0 -7 21 148.19 11.00 0 -7 21 154.28 11.60 0 -7 21 163.48 14.00 -1 7 -21 21.50 6.60 -1 7 -21 16.10 6.20 -1 7 -21 12.90 3.70 -1 7 -21 32.90 6.30 1 -7 21 20.50 6.50 1 -7 21 23.40 5.50 1 -7 21 7.00 5.00 -2 7 -21 73.19 8.70 -2 7 -21 92.59 10.80 -2 7 -21 88.79 9.30 -2 7 -21 107.09 10.20 -2 7 -21 80.89 10.00 -2 7 -21 76.59 7.10 2 -7 21 119.79 12.00 2 -7 21 88.29 8.60 2 -7 21 98.79 11.10 -3 7 -21 279.67 15.70 -3 7 -21 264.27 14.50 -3 7 -21 276.77 19.20 -3 7 -21 269.17 16.50 -3 7 -21 280.87 17.20 -3 7 -21 257.47 18.30 3 -7 21 290.37 17.70 3 -7 21 293.37 16.50 3 -7 21 260.67 18.10 3 -7 21 265.87 20.20 -4 7 -21 37.10 5.80 -4 7 -21 40.20 7.90 -4 7 -21 16.70 5.00 -4 7 -21 40.50 8.80 4 -7 21 14.60 6.40 4 -7 21 17.10 8.70 4 -7 21 27.10 7.60 4 -7 21 19.10 6.30 4 -7 21 37.40 6.90 -5 7 -21 143.69 14.90 -5 7 -21 130.59 12.80 -5 7 -21 166.98 14.90 -5 7 -21 152.48 11.80 -5 7 -21 152.88 12.90 5 -7 21 138.99 13.50 5 -7 21 158.58 12.70 5 -7 21 182.28 14.80 5 -7 21 133.09 15.70 5 -7 21 154.08 13.90 -6 7 -21 9.60 5.20 -6 7 -21 10.70 4.20 -6 7 -21 10.50 6.30 -6 7 -21 16.30 6.30 -6 7 -21 16.10 4.50 -6 7 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19.10 6.00 9 6 -21 9.50 4.00 9 6 -21 2.10 8.10 -9 -6 21 15.60 6.00 -9 -6 21 13.10 7.10 -9 -6 21 17.50 7.20 -9 -6 21 11.10 5.60 -9 -6 21 12.50 9.90 8 6 -21 147.79 15.00 8 6 -21 136.39 11.60 8 6 -21 131.29 12.10 8 6 -21 138.49 12.90 8 6 -21 133.39 14.80 8 6 -21 127.89 11.80 -8 -6 21 136.59 12.00 -8 -6 21 131.79 12.20 -8 -6 21 123.59 15.70 -8 -6 21 149.69 12.60 -8 -6 21 162.78 19.00 -8 -6 21 138.89 14.80 7 6 -21 49.99 7.70 7 6 -21 38.30 9.90 7 6 -21 60.19 10.30 7 6 -21 54.29 10.10 7 6 -21 43.60 9.30 7 6 -21 40.10 8.10 7 6 -21 44.90 7.50 7 6 -21 62.89 8.20 7 6 -21 58.19 8.70 -7 -6 21 67.79 8.10 -7 -6 21 37.70 8.20 -7 -6 21 49.30 7.50 -7 -6 21 33.90 8.10 -7 -6 21 45.40 8.50 -7 -6 21 62.39 14.20 -7 -6 21 58.39 11.80 6 6 -21 14.00 6.30 6 6 -21 9.30 4.10 6 6 -21 6.90 5.60 6 6 -21 3.00 5.20 6 6 -21 11.00 3.50 6 6 -21 9.20 4.10 6 6 -21 19.80 6.30 6 6 -21 -0.80 3.20 6 6 -21 4.10 5.50 -6 -6 21 8.70 5.10 -6 -6 21 -1.30 6.90 -6 -6 21 3.00 6.10 -6 -6 21 4.90 4.70 -6 -6 21 3.20 3.20 -6 -6 21 3.80 3.60 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10.70 3.70 2 6 -21 6.10 4.80 2 6 -21 12.30 4.60 2 6 -21 23.70 5.10 2 6 -21 14.80 6.40 -2 -6 21 7.50 3.20 -2 -6 21 10.10 4.10 -2 -6 21 12.00 3.30 -2 -6 21 17.20 5.40 -2 -6 21 11.70 6.00 -2 -6 21 8.90 4.70 -2 -6 21 2.90 2.80 1 6 -21 0.70 2.80 1 6 -21 6.30 3.10 1 6 -21 2.80 4.30 1 6 -21 3.70 4.20 1 6 -21 4.10 3.60 1 6 -21 6.90 5.60 -1 -6 21 6.90 4.80 -1 -6 21 4.80 2.50 -1 -6 21 3.60 3.30 -1 -6 21 9.70 5.20 -1 -6 21 3.90 3.80 0 6 -21 171.58 14.30 0 6 -21 169.18 15.00 0 6 -21 158.58 12.00 0 6 -21 171.48 11.80 0 6 -21 170.88 13.90 0 -6 21 168.08 11.60 0 -6 21 170.98 14.40 0 -6 21 153.58 13.80 0 -6 21 159.58 11.50 0 -6 21 159.68 12.20 -1 6 -21 35.00 7.00 -1 6 -21 51.59 8.80 -1 6 -21 45.70 6.60 -1 6 -21 41.90 7.00 -1 6 -21 51.79 6.50 -1 6 -21 39.70 7.40 1 -6 21 36.20 6.40 1 -6 21 33.60 6.30 1 -6 21 66.19 9.60 1 -6 21 40.10 8.50 -2 6 -21 52.09 9.00 -2 6 -21 51.69 8.80 -2 6 -21 54.59 7.80 -2 6 -21 55.69 7.60 -2 6 -21 54.79 6.20 2 -6 21 62.79 9.40 2 -6 21 57.39 7.10 2 -6 21 63.19 9.70 -3 6 -21 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4.20 -9 -4 21 10.40 7.40 8 4 -21 19.70 7.60 8 4 -21 8.80 4.60 8 4 -21 13.40 8.10 8 4 -21 7.10 4.60 8 4 -21 16.20 5.90 8 4 -21 2.50 6.80 8 4 -21 9.60 3.80 8 4 -21 16.50 6.80 8 4 -21 2.70 3.80 -8 -4 21 8.40 6.40 -8 -4 21 8.10 4.80 -8 -4 21 26.20 8.40 -8 -4 21 4.20 6.50 -8 -4 21 8.10 4.70 -8 -4 21 11.70 4.70 -8 -4 21 -5.50 9.10 7 4 -21 396.96 23.60 7 4 -21 380.86 28.50 7 4 -21 398.66 23.60 7 4 -21 375.76 21.90 7 4 -21 384.46 22.40 7 4 -21 398.06 21.40 7 4 -21 416.46 21.30 7 4 -21 404.06 21.20 7 4 -21 360.56 22.50 -7 -4 21 406.56 22.70 -7 -4 21 386.56 22.50 -7 -4 21 393.56 21.00 -7 -4 21 398.26 21.20 -7 -4 21 335.67 24.70 -7 -4 21 409.46 23.80 -7 -4 21 355.76 24.60 -7 -4 21 425.86 24.50 6 4 -21 20.50 6.50 6 4 -21 10.80 4.30 6 4 -21 8.80 5.70 6 4 -21 12.50 5.70 6 4 -21 8.30 3.90 6 4 -21 14.70 6.10 6 4 -21 9.10 3.30 6 4 -21 4.70 3.90 6 4 -21 9.70 5.60 -6 -4 21 14.80 4.20 -6 -4 21 13.00 4.50 -6 -4 21 14.70 6.60 -6 -4 21 6.00 5.40 -6 -4 21 14.30 6.20 -6 -4 21 12.50 8.40 -6 -4 21 16.50 6.90 -6 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3.50 -2 -4 21 14.40 6.30 -2 -4 21 3.10 2.60 -2 -4 21 8.20 4.70 -2 -4 21 8.70 4.30 -2 -4 21 6.50 3.10 -2 -4 21 18.70 6.00 -2 -4 21 5.50 3.20 -2 -4 21 25.90 5.30 1 4 -21 9.50 6.10 1 4 -21 10.40 4.40 1 4 -21 19.20 5.90 1 4 -21 11.70 4.10 1 4 -21 6.50 3.40 1 4 -21 8.30 5.50 1 4 -21 9.40 4.60 -1 -4 21 4.00 3.30 -1 -4 21 16.20 5.20 -1 -4 21 5.70 4.90 -1 -4 21 13.30 5.70 -1 -4 21 4.50 3.10 -1 -4 21 9.30 3.30 -1 -4 21 9.40 4.30 0 4 -21 67.39 8.30 0 4 -21 78.29 9.50 0 4 -21 87.19 12.20 0 4 -21 68.39 9.90 0 4 -21 76.19 9.90 0 4 -21 69.59 8.20 0 -4 21 81.89 9.30 0 -4 21 71.29 10.00 0 -4 21 64.39 7.80 0 -4 21 60.39 9.30 0 -4 21 53.69 6.90 -1 4 -21 22.50 4.00 -1 4 -21 11.70 5.00 -1 4 -21 13.50 4.80 -1 4 -21 7.80 7.50 -1 4 -21 5.90 4.80 -1 4 -21 11.40 3.90 -1 4 -21 9.40 3.70 1 -4 21 14.90 4.20 1 -4 21 10.90 5.80 1 -4 21 15.30 5.80 1 -4 21 8.30 4.40 1 -4 21 4.80 3.20 -2 4 -21 341.87 16.50 -2 4 -21 315.17 18.60 -2 4 -21 335.47 20.80 -2 4 -21 328.67 17.10 -2 4 -21 323.97 19.60 -2 4 -21 354.06 18.70 2 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9.70 6 3 -21 58.09 8.80 6 3 -21 61.49 8.60 6 3 -21 39.90 8.20 6 3 -21 47.70 9.70 -6 -3 21 53.79 10.90 -6 -3 21 37.80 9.30 -6 -3 21 46.10 8.60 -6 -3 21 40.20 8.90 -6 -3 21 58.89 8.30 -6 -3 21 58.29 10.10 -6 -3 21 56.79 8.00 -6 -3 21 47.70 11.60 5 3 -21 102.79 12.20 5 3 -21 84.69 11.00 5 3 -21 121.89 13.00 5 3 -21 105.59 10.30 5 3 -21 91.59 11.00 5 3 -21 119.19 13.30 5 3 -21 103.19 11.60 5 3 -21 119.49 11.00 -5 -3 21 119.69 11.30 -5 -3 21 101.69 11.10 -5 -3 21 109.39 11.40 -5 -3 21 85.69 14.00 -5 -3 21 113.09 10.20 -5 -3 21 107.59 11.90 -5 -3 21 106.39 13.20 4 3 -21 7.90 3.40 4 3 -21 4.30 3.10 4 3 -21 6.80 5.90 4 3 -21 14.40 5.90 4 3 -21 0.80 5.00 4 3 -21 1.90 2.80 -4 -3 21 13.50 6.10 -4 -3 21 11.60 4.70 -4 -3 21 7.60 3.40 -4 -3 21 6.80 4.00 -4 -3 21 16.50 5.50 -4 -3 21 -7.00 6.40 -4 -3 21 3.00 3.30 3 3 -21 9.30 4.10 3 3 -21 6.00 3.70 3 3 -21 7.60 5.30 3 3 -21 4.30 3.10 3 3 -21 9.10 5.50 3 3 -21 5.40 2.80 3 3 -21 9.00 5.10 -3 -3 21 5.00 3.10 -3 -3 21 1.10 3.70 -3 -3 21 0.20 5.00 -3 -3 21 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10.70 5 20 -22 -5.00 6.30 5 20 -22 2.10 5.10 -5 -20 22 1.60 5.90 4 20 -22 11.70 5.60 4 20 -22 6.60 5.50 -4 -20 22 5.50 6.70 3 20 -22 57.99 12.70 3 20 -22 38.60 13.40 3 20 -22 75.59 13.20 -3 -20 22 59.89 12.40 2 20 -22 35.90 9.50 2 20 -22 50.59 11.90 2 20 -22 61.69 13.50 -2 -20 22 32.20 8.30 1 20 -22 6.80 5.50 1 20 -22 7.00 5.30 1 20 -22 13.80 8.50 -1 -20 22 7.80 6.00 0 20 -22 14.70 5.80 0 20 -22 8.70 6.20 0 -20 22 15.70 6.70 -1 20 -22 -4.20 4.90 -1 20 -22 0.20 4.60 1 -20 22 2.60 5.10 -2 20 -22 128.59 15.20 -2 20 -22 131.29 15.60 2 -20 22 124.29 13.80 -3 20 -22 91.79 14.90 -3 20 -22 98.19 13.60 3 -20 22 92.19 11.90 -4 20 -22 26.70 6.90 -4 20 -22 20.20 8.10 -4 20 -22 21.20 7.40 4 -20 22 28.10 7.10 4 -20 22 27.60 6.90 -5 20 -22 7.40 5.60 -5 20 -22 6.30 6.70 5 -20 22 -7.20 6.00 7 19 -22 -1.10 5.20 7 19 -22 -4.40 6.00 6 19 -22 22.00 7.10 6 19 -22 67.59 12.80 -6 -19 22 23.10 8.00 5 19 -22 1.50 6.40 5 19 -22 9.80 6.00 -5 -19 22 0.20 5.80 4 19 -22 -4.00 4.30 4 19 -22 8.60 4.60 4 19 -22 8.40 7.10 -4 -19 22 4.50 5.50 3 19 -22 -4.40 4.20 3 19 -22 10.50 8.40 3 19 -22 12.10 5.10 3 19 -22 -4.80 5.60 -3 -19 22 -8.10 4.50 2 19 -22 29.00 8.00 2 19 -22 27.10 7.20 -2 -19 22 47.00 10.20 1 19 -22 80.39 13.40 1 19 -22 83.79 19.00 1 19 -22 93.19 15.70 -1 -19 22 65.59 11.70 0 19 -22 34.60 10.40 0 19 -22 44.40 10.90 0 19 -22 40.20 10.10 0 -19 22 55.99 10.60 -1 19 -22 4.10 5.70 -1 19 -22 8.60 5.60 1 -19 22 18.80 6.50 -2 19 -22 22.50 7.40 -2 19 -22 9.50 6.30 2 -19 22 24.80 6.50 -3 19 -22 1.60 5.40 -3 19 -22 7.50 5.70 3 -19 22 12.20 12.40 3 -19 22 -4.50 4.60 -4 19 -22 119.69 14.90 -4 19 -22 98.99 13.70 -4 19 -22 119.69 16.50 4 -19 22 102.09 12.90 -5 19 -22 6.60 5.70 -5 19 -22 -2.70 6.50 -5 19 -22 0.90 4.80 5 -19 22 12.00 6.20 5 -19 22 -5.30 5.10 6 -19 22 -8.30 6.70 6 -19 22 -12.00 5.30 8 18 -22 2.00 7.70 8 18 -22 9.80 5.40 -8 -18 22 6.60 5.10 7 18 -22 15.20 6.50 7 18 -22 19.50 7.50 -7 -18 22 26.70 8.60 6 18 -22 20.00 7.30 6 18 -22 16.70 6.10 -6 -18 22 15.70 7.70 5 18 -22 4.90 4.80 5 18 -22 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7.20 14.90 4 -18 22 -0.10 5.00 -5 18 -22 -0.80 4.80 -5 18 -22 0.60 7.10 -5 18 -22 5.70 5.20 5 -18 22 -2.20 5.10 5 -18 22 0.90 4.70 -6 18 -22 55.69 10.50 -6 18 -22 79.89 10.80 -6 18 -22 83.99 15.30 -6 18 -22 76.49 13.90 6 -18 22 90.39 11.70 6 -18 22 56.19 11.40 6 -18 22 77.19 12.80 8 17 -22 -4.90 5.60 8 17 -22 -4.10 5.00 8 17 -22 -2.30 4.60 -8 -17 22 0.60 6.30 -8 -17 22 1.90 4.30 7 17 -22 -8.60 4.40 7 17 -22 3.00 4.90 -7 -17 22 8.60 6.00 6 17 -22 3.50 11.70 6 17 -22 11.80 10.90 6 17 -22 4.30 5.70 6 17 -22 -3.80 4.40 -6 -17 22 4.20 5.70 -6 -17 22 -0.40 8.10 -6 -17 22 12.00 10.80 5 17 -22 -2.50 8.90 5 17 -22 12.30 4.70 5 17 -22 4.20 4.50 5 17 -22 -5.60 7.10 5 17 -22 -6.20 3.60 -5 -17 22 -3.70 5.40 -5 -17 22 -6.00 8.70 4 17 -22 21.60 6.10 4 17 -22 7.70 4.90 4 17 -22 11.00 5.00 -4 -17 22 3.60 5.60 3 17 -22 7.20 4.60 3 17 -22 2.80 7.60 3 17 -22 -3.20 6.50 3 17 -22 1.00 4.50 3 17 -22 13.70 7.00 2 17 -22 55.29 11.10 2 17 -22 34.10 9.30 2 17 -22 44.50 8.40 2 17 -22 51.09 11.40 2 17 -22 44.60 10.20 2 17 -22 28.70 9.60 -2 -17 22 59.59 14.40 1 17 -22 25.30 6.90 1 17 -22 23.90 6.40 1 17 -22 17.60 7.00 1 17 -22 33.40 10.10 -1 -17 22 33.20 9.00 -1 -17 22 29.80 10.80 0 17 -22 37.20 9.40 0 17 -22 21.70 9.30 0 17 -22 33.70 7.60 0 -17 22 32.00 8.10 -1 17 -22 142.29 16.30 -1 17 -22 127.79 15.50 -1 17 -22 96.69 13.00 -1 17 -22 108.89 13.00 -2 17 -22 137.99 15.80 -2 17 -22 89.79 15.60 -2 17 -22 95.99 12.70 -2 17 -22 65.59 13.90 2 -17 22 105.89 14.30 2 -17 22 110.49 12.10 2 -17 22 73.09 16.00 -3 17 -22 13.10 6.10 -3 17 -22 27.10 6.90 -3 17 -22 13.60 9.30 3 -17 22 10.40 12.20 3 -17 22 12.90 7.70 3 -17 22 24.10 6.10 -4 17 -22 31.00 7.60 -4 17 -22 26.10 11.40 -4 17 -22 26.40 8.70 -4 17 -22 47.50 9.60 -4 17 -22 74.99 13.50 4 -17 22 47.50 9.00 4 -17 22 27.00 10.80 4 -17 22 36.30 7.40 -5 17 -22 22.40 12.20 -5 17 -22 44.90 7.90 -5 17 -22 18.50 5.90 -5 17 -22 10.70 6.10 5 -17 22 42.00 9.80 5 -17 22 36.30 9.10 5 -17 22 17.30 6.40 -6 17 -22 176.78 15.00 -6 17 -22 173.48 17.10 6 -17 22 165.88 15.30 6 -17 22 147.49 15.40 6 -17 22 170.58 15.10 -7 17 -22 2.80 5.60 -7 17 -22 6.50 5.20 7 -17 22 0.30 6.00 7 -17 22 2.10 5.70 9 16 -22 8.40 5.40 9 16 -22 -5.10 6.10 9 16 -22 18.20 10.10 -9 -16 22 19.40 6.60 8 16 -22 14.70 6.00 8 16 -22 5.60 6.60 8 16 -22 20.00 6.30 -8 -16 22 19.10 5.70 -8 -16 22 15.50 8.40 7 16 -22 0.90 5.40 7 16 -22 -2.40 5.00 -7 -16 22 -2.70 5.90 -7 -16 22 5.50 4.00 -7 -16 22 15.10 9.10 -7 -16 22 -19.50 11.90 6 16 -22 -6.10 9.70 6 16 -22 15.10 5.90 6 16 -22 18.30 6.50 6 16 -22 16.00 8.10 6 16 -22 18.50 9.70 -6 -16 22 60.79 11.60 -6 -16 22 17.30 10.30 5 16 -22 20.60 6.60 5 16 -22 1.60 10.40 5 16 -22 21.00 5.80 5 16 -22 21.80 6.10 5 16 -22 26.50 10.10 -5 -16 22 18.90 9.20 -5 -16 22 8.10 9.70 -5 -16 22 27.10 7.70 4 16 -22 2.90 4.30 4 16 -22 0.20 7.00 4 16 -22 25.50 10.00 4 16 -22 16.30 10.90 4 16 -22 10.30 7.70 4 16 -22 9.70 6.50 4 16 -22 7.20 4.30 -4 -16 22 1.50 8.50 -4 -16 22 20.00 8.30 -4 -16 22 6.60 5.80 3 16 -22 59.39 10.50 3 16 -22 57.59 12.70 3 16 -22 38.90 9.00 3 16 -22 55.29 12.50 3 16 -22 39.30 8.00 3 16 -22 47.10 10.40 -3 -16 22 28.70 8.70 -3 -16 22 37.80 8.70 -3 -16 22 43.40 12.00 2 16 -22 241.38 20.10 2 16 -22 248.58 17.70 2 16 -22 205.78 17.00 2 16 -22 215.78 18.40 2 16 -22 262.87 16.80 -2 -16 22 194.88 19.20 -2 -16 22 227.08 17.60 1 16 -22 3.20 6.40 1 16 -22 12.30 4.80 1 16 -22 14.30 8.20 -1 -16 22 4.40 4.60 -1 -16 22 5.70 7.50 0 16 -22 -9.90 6.00 0 16 -22 1.40 4.40 0 16 -22 0.10 4.30 0 -16 22 0.90 4.00 0 -16 22 -2.90 6.50 -1 16 -22 9.90 4.90 -1 16 -22 9.50 5.50 1 -16 22 19.90 6.00 1 -16 22 11.60 7.50 -2 16 -22 70.19 13.10 -2 16 -22 82.09 11.30 -2 16 -22 92.19 12.30 2 -16 22 75.99 16.30 -3 16 -22 118.19 15.80 -3 16 -22 108.69 14.80 -3 16 -22 91.19 12.40 -3 16 -22 78.29 13.20 3 -16 22 83.39 16.50 3 -16 22 98.39 13.70 3 -16 22 106.49 14.10 3 -16 22 69.09 15.00 -4 16 -22 6.40 10.90 -4 16 -22 8.00 6.00 -4 16 -22 17.50 6.50 4 -16 22 10.90 6.40 4 -16 22 15.30 8.50 4 -16 22 16.60 6.10 4 -16 22 12.00 16.20 -5 16 -22 16.90 6.90 -5 16 -22 -4.00 8.10 -5 16 -22 3.90 11.50 -5 16 -22 12.80 4.90 -5 16 -22 9.60 4.70 -5 16 -22 14.60 5.10 5 -16 22 15.00 8.80 5 -16 22 32.00 8.30 5 -16 22 10.60 6.20 5 -16 22 7.30 5.90 -6 16 -22 -0.40 4.30 -6 16 -22 4.60 6.00 -6 16 -22 -5.60 4.30 6 -16 22 -1.40 4.50 6 -16 22 -1.60 5.20 6 -16 22 0.70 5.30 -7 16 -22 8.80 5.40 -7 16 -22 2.80 4.90 -7 16 -22 7.70 5.50 7 -16 22 -10.30 5.10 7 -16 22 3.00 4.60 9 15 -22 -3.40 4.50 9 15 -22 -7.90 5.30 -9 -15 22 3.00 4.30 -9 -15 22 -2.70 7.20 -9 -15 22 4.10 4.90 8 15 -22 74.69 11.60 8 15 -22 32.50 8.00 8 15 -22 52.89 10.30 -8 -15 22 62.19 13.70 -8 -15 22 58.19 9.20 -8 -15 22 37.10 10.00 -8 -15 22 25.60 9.30 7 15 -22 15.80 6.00 7 15 -22 18.70 10.90 7 15 -22 20.70 5.90 7 15 -22 19.90 6.40 -7 -15 22 -8.00 8.80 -7 -15 22 15.40 6.90 -7 -15 22 39.90 9.20 -7 -15 22 36.80 8.50 6 15 -22 28.30 7.20 6 15 -22 24.60 12.60 6 15 -22 32.10 7.70 6 15 -22 35.20 9.30 6 15 -22 33.60 8.40 6 15 -22 22.10 6.00 -6 -15 22 37.90 7.30 -6 -15 22 37.40 12.30 -6 -15 22 55.59 11.40 5 15 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14.60 7 -14 22 156.38 14.20 -8 14 -22 116.09 15.10 -8 14 -22 112.99 13.00 -8 14 -22 120.69 13.20 8 -14 22 101.49 13.10 8 -14 22 111.29 13.20 10 13 -22 -4.10 4.90 -10 -13 22 -6.00 4.60 -10 -13 22 2.50 8.00 9 13 -22 22.70 6.70 9 13 -22 11.30 5.90 9 13 -22 11.20 5.60 -9 -13 22 25.60 6.60 -9 -13 22 29.10 7.00 -9 -13 22 20.30 8.50 8 13 -22 3.80 4.90 8 13 -22 6.80 5.80 8 13 -22 -3.20 7.20 8 13 -22 8.20 5.50 -8 -13 22 1.80 6.80 -8 -13 22 -0.70 4.50 -8 -13 22 2.50 4.90 -8 -13 22 12.60 6.60 7 13 -22 2.10 6.80 7 13 -22 5.60 5.90 7 13 -22 4.30 7.80 7 13 -22 6.80 3.70 7 13 -22 1.00 3.30 7 13 -22 4.80 8.20 7 13 -22 5.80 4.80 -7 -13 22 9.30 4.10 -7 -13 22 6.10 7.20 -7 -13 22 -9.60 5.90 -7 -13 22 9.10 4.70 6 13 -22 54.59 11.50 6 13 -22 45.40 10.40 6 13 -22 37.60 8.60 6 13 -22 59.29 9.60 6 13 -22 48.70 12.00 6 13 -22 39.70 8.50 6 13 -22 45.60 7.50 -6 -13 22 63.69 7.60 -6 -13 22 30.10 8.00 -6 -13 22 59.69 11.40 -6 -13 22 54.39 9.70 5 13 -22 15.60 6.00 5 13 -22 21.60 7.20 5 13 -22 11.00 4.00 5 13 -22 9.60 4.40 5 13 -22 19.10 9.00 5 13 -22 9.20 7.10 5 13 -22 12.40 8.70 5 13 -22 34.40 8.20 5 13 -22 16.60 4.90 -5 -13 22 19.80 8.50 -5 -13 22 9.70 5.80 -5 -13 22 14.70 4.60 -5 -13 22 8.50 9.20 -5 -13 22 7.20 3.90 -5 -13 22 4.40 5.20 4 13 -22 29.70 7.30 4 13 -22 45.80 9.50 4 13 -22 30.50 7.00 4 13 -22 45.30 8.80 4 13 -22 34.30 9.80 4 13 -22 31.70 7.00 4 13 -22 32.00 9.80 4 13 -22 51.59 9.00 -4 -13 22 41.90 9.10 -4 -13 22 35.40 6.60 -4 -13 22 16.50 7.70 3 13 -22 9.20 4.50 3 13 -22 13.20 6.60 3 13 -22 26.30 6.10 3 13 -22 8.00 4.40 3 13 -22 11.80 6.40 3 13 -22 2.60 6.00 -3 -13 22 19.70 7.70 -3 -13 22 13.70 5.60 -3 -13 22 10.10 3.90 -3 -13 22 1.30 6.60 2 13 -22 9.20 6.80 2 13 -22 13.00 4.60 2 13 -22 12.20 5.50 2 13 -22 19.00 4.60 2 13 -22 9.90 9.20 2 13 -22 10.40 4.00 2 13 -22 8.20 5.90 -2 -13 22 11.50 4.80 -2 -13 22 14.00 7.10 -2 -13 22 26.20 5.30 -2 -13 22 9.20 6.70 -2 -13 22 13.10 6.40 1 13 -22 26.80 7.80 1 13 -22 23.20 5.60 1 13 -22 23.30 5.60 1 13 -22 25.20 6.80 -1 -13 22 35.00 7.70 -1 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37.40 9.80 -7 -12 22 21.50 7.40 -7 -12 22 38.30 8.50 6 12 -22 42.80 10.40 6 12 -22 72.29 9.40 6 12 -22 43.40 11.20 6 12 -22 42.50 9.60 6 12 -22 48.00 9.10 6 12 -22 77.09 11.60 6 12 -22 59.39 9.00 6 12 -22 61.49 8.10 -6 -12 22 73.69 13.00 -6 -12 22 51.89 7.50 -6 -12 22 49.40 13.20 -6 -12 22 56.79 8.80 -6 -12 22 29.50 7.70 5 12 -22 28.40 9.50 5 12 -22 25.80 6.60 5 12 -22 0.00 5.90 5 12 -22 19.70 6.30 5 12 -22 10.30 6.80 5 12 -22 14.40 4.40 5 12 -22 11.30 4.60 5 12 -22 13.60 4.80 -5 -12 22 19.70 7.20 -5 -12 22 11.20 4.20 -5 -12 22 13.70 5.50 -5 -12 22 3.50 3.60 -5 -12 22 3.20 5.00 4 12 -22 122.09 13.60 4 12 -22 94.29 9.80 4 12 -22 93.39 9.90 4 12 -22 93.79 12.00 4 12 -22 147.89 13.40 4 12 -22 109.79 11.50 4 12 -22 119.69 15.00 4 12 -22 100.79 12.70 -4 -12 22 117.09 16.80 -4 -12 22 106.89 23.00 -4 -12 22 112.69 13.20 -4 -12 22 109.59 12.00 -4 -12 22 111.69 12.00 -4 -12 22 113.79 9.30 3 12 -22 27.00 7.30 3 12 -22 21.90 8.50 3 12 -22 20.80 7.20 3 12 -22 24.00 7.60 3 12 -22 41.80 8.90 3 12 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6.80 -5 6 -22 12.40 7.20 5 -6 22 15.10 5.10 5 -6 22 26.80 7.90 5 -6 22 29.20 10.20 -6 6 -22 12.90 4.40 -6 6 -22 15.20 7.50 -6 6 -22 15.80 5.50 6 -6 22 8.80 5.40 6 -6 22 7.50 6.70 -7 6 -22 57.09 9.00 -7 6 -22 54.89 10.90 7 -6 22 47.30 10.10 7 -6 22 34.00 12.00 -8 6 -22 2.10 4.70 -8 6 -22 5.30 6.20 -8 6 -22 3.80 5.60 8 -6 22 9.10 5.00 8 -6 22 2.60 6.10 11 5 -22 4.80 5.20 11 5 -22 -2.10 4.70 11 5 -22 4.90 5.10 -11 -5 22 4.10 5.00 -11 -5 22 -1.00 4.70 -11 -5 22 -3.50 4.80 10 5 -22 0.50 4.20 10 5 -22 -4.70 4.00 10 5 -22 -4.00 4.10 -10 -5 22 9.90 9.90 -10 -5 22 -0.40 3.80 -10 -5 22 -4.10 4.60 -10 -5 22 -0.80 4.30 9 5 -22 -0.60 3.90 9 5 -22 -0.50 3.30 9 5 -22 -2.50 3.50 9 5 -22 -3.70 4.00 9 5 -22 5.10 7.90 -9 -5 22 11.30 7.00 -9 -5 22 6.90 4.30 -9 -5 22 11.20 4.80 -9 -5 22 1.40 4.30 8 5 -22 102.69 10.80 8 5 -22 92.19 13.70 8 5 -22 114.89 12.50 8 5 -22 113.19 12.70 8 5 -22 106.09 14.30 8 5 -22 81.99 12.30 8 5 -22 105.49 11.40 8 5 -22 100.49 11.00 -8 -5 22 114.79 18.40 -8 -5 22 115.89 13.30 -8 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5 -22 10.90 5.80 4 5 -22 6.50 5.10 4 5 -22 5.00 3.60 4 5 -22 6.90 3.60 4 5 -22 7.20 5.60 4 5 -22 10.50 4.90 4 5 -22 5.70 3.50 4 5 -22 5.40 3.70 4 5 -22 6.00 6.00 -4 -5 22 8.50 5.40 -4 -5 22 -2.40 4.50 -4 -5 22 8.10 3.20 -4 -5 22 11.30 4.80 -4 -5 22 15.00 6.50 -4 -5 22 2.90 3.20 -4 -5 22 6.00 3.80 -4 -5 22 6.70 7.50 3 5 -22 12.10 5.90 3 5 -22 0.40 2.60 3 5 -22 2.10 4.40 3 5 -22 2.20 4.70 3 5 -22 0.90 3.20 3 5 -22 -1.90 5.00 3 5 -22 -0.60 4.40 3 5 -22 4.40 3.00 -3 -5 22 5.30 4.00 -3 -5 22 1.50 2.60 -3 -5 22 5.70 3.10 -3 -5 22 -1.90 6.10 -3 -5 22 6.20 5.10 -3 -5 22 1.30 2.70 -3 -5 22 -0.20 5.00 -3 -5 22 1.50 4.00 2 5 -22 9.40 5.70 2 5 -22 15.70 4.10 2 5 -22 5.70 7.80 2 5 -22 11.40 3.50 2 5 -22 11.30 5.70 2 5 -22 12.60 6.00 2 5 -22 18.50 7.80 -2 -5 22 11.10 3.50 -2 -5 22 9.70 5.60 -2 -5 22 17.10 6.00 -2 -5 22 10.80 5.30 -2 -5 22 8.20 4.40 -2 -5 22 16.90 6.80 -2 -5 22 8.20 3.60 1 5 -22 1.00 4.90 1 5 -22 -2.80 2.60 1 5 -22 -3.50 2.50 1 5 -22 1.20 6.20 1 5 -22 -0.10 4.20 1 5 -22 2.10 5.00 1 5 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7.20 6 15 -23 25.80 9.40 -6 -15 23 84.19 15.40 5 15 -23 -6.10 3.90 5 15 -23 2.20 4.20 5 15 -23 -3.70 9.00 5 15 -23 2.50 3.50 -5 -15 23 0.30 5.30 -5 -15 23 -0.30 10.70 4 15 -23 7.10 10.10 4 15 -23 13.00 5.90 4 15 -23 10.30 6.50 4 15 -23 17.10 9.40 4 15 -23 22.50 8.10 4 15 -23 37.90 8.70 -4 -15 23 21.60 11.50 -4 -15 23 41.30 9.80 3 15 -23 50.49 8.80 3 15 -23 55.69 10.80 3 15 -23 43.00 10.00 3 15 -23 59.59 12.20 3 15 -23 64.89 10.10 3 15 -23 49.40 10.40 -3 -15 23 57.49 10.80 -3 -15 23 20.60 9.80 -3 -15 23 42.80 9.80 2 15 -23 -15.00 5.60 2 15 -23 5.60 7.00 2 15 -23 -5.50 3.70 2 15 -23 -1.70 3.60 -2 -15 23 5.80 7.20 -2 -15 23 -13.90 8.10 -2 -15 23 -2.90 3.90 1 15 -23 174.38 15.00 1 15 -23 157.18 16.90 1 15 -23 163.38 14.50 -1 -15 23 183.38 15.00 -1 -15 23 154.58 16.70 -1 -15 23 154.68 15.60 0 15 -23 12.10 9.10 0 15 -23 10.20 5.00 0 15 -23 13.90 5.90 0 -15 23 7.50 8.00 0 -15 23 8.90 5.60 0 -15 23 10.10 6.50 -1 15 -23 101.39 13.80 -1 15 -23 104.59 12.20 -1 15 -23 101.09 13.40 1 -15 23 104.89 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-14 23 7.50 6.20 6 14 -23 35.00 8.00 6 14 -23 25.00 12.80 6 14 -23 32.40 10.90 6 14 -23 61.99 10.20 6 14 -23 22.70 9.00 6 14 -23 20.60 6.00 6 14 -23 40.70 10.60 -6 -14 23 31.20 8.00 -6 -14 23 27.90 7.80 -6 -14 23 39.20 7.50 -6 -14 23 19.70 9.70 5 14 -23 -10.70 7.40 5 14 -23 -2.80 6.80 5 14 -23 -0.40 4.50 5 14 -23 7.20 6.70 5 14 -23 -1.40 3.80 -5 -14 23 1.70 3.70 4 14 -23 64.49 11.80 4 14 -23 69.29 9.50 4 14 -23 32.90 9.60 4 14 -23 58.59 10.20 4 14 -23 62.79 9.30 4 14 -23 92.49 18.80 4 14 -23 41.20 10.10 -4 -14 23 49.00 12.20 -4 -14 23 54.39 8.30 -4 -14 23 55.39 11.70 -4 -14 23 60.09 11.10 3 14 -23 21.40 5.00 3 14 -23 35.60 8.80 3 14 -23 13.80 7.10 3 14 -23 33.00 8.00 3 14 -23 21.40 7.50 3 14 -23 20.70 6.20 3 14 -23 23.40 9.90 -3 -14 23 21.80 7.80 -3 -14 23 58.49 12.90 -3 -14 23 21.20 5.80 2 14 -23 108.29 12.80 2 14 -23 66.09 11.10 2 14 -23 100.19 11.50 2 14 -23 95.99 10.70 -2 -14 23 91.49 12.90 -2 -14 23 99.49 12.10 -2 -14 23 79.69 13.60 1 14 -23 83.79 11.90 1 14 -23 66.39 10.10 1 14 -23 78.79 11.10 -1 -14 23 73.09 12.50 -1 -14 23 88.39 13.20 -1 -14 23 71.49 10.10 0 14 -23 15.70 4.90 0 14 -23 11.20 8.50 0 14 -23 19.20 5.90 0 -14 23 19.00 5.70 0 -14 23 20.00 6.90 0 -14 23 14.50 7.90 -1 14 -23 189.18 17.20 -1 14 -23 163.28 14.20 -1 14 -23 189.88 15.30 -1 14 -23 172.38 18.50 1 -14 23 153.28 15.70 1 -14 23 158.88 14.60 1 -14 23 177.68 14.40 -2 14 -23 9.10 5.90 -2 14 -23 4.40 7.10 -2 14 -23 18.70 8.00 2 -14 23 12.90 6.50 2 -14 23 4.30 6.70 2 -14 23 12.10 4.70 -3 14 -23 57.19 10.20 -3 14 -23 73.89 12.00 -3 14 -23 61.79 13.50 -3 14 -23 44.60 11.20 3 -14 23 79.69 18.30 3 -14 23 48.50 10.90 -4 14 -23 87.09 12.50 -4 14 -23 70.39 11.80 -4 14 -23 78.29 18.00 4 -14 23 53.09 12.40 4 -14 23 88.89 10.80 -5 14 -23 15.10 6.20 -5 14 -23 16.20 5.20 -5 14 -23 14.70 8.50 5 -14 23 17.90 5.50 5 -14 23 23.80 11.10 5 -14 23 10.60 6.40 -6 14 -23 36.80 9.10 -6 14 -23 47.10 10.90 6 -14 23 44.10 9.50 6 -14 23 27.70 6.90 -7 14 -23 64.29 10.20 -7 14 -23 62.89 12.10 -7 14 -23 61.89 9.50 7 -14 23 41.40 9.90 7 -14 23 45.90 10.40 7 -14 23 44.80 11.20 10 13 -23 -12.80 5.80 10 13 -23 -7.70 4.90 9 13 -23 -5.40 5.10 9 13 -23 3.70 5.00 9 13 -23 -0.90 4.80 -9 -13 23 -2.00 6.30 -9 -13 23 5.80 4.70 -9 -13 23 -5.90 4.30 8 13 -23 2.00 5.00 8 13 -23 2.40 4.90 8 13 -23 6.40 5.60 -8 -13 23 10.80 6.60 -8 -13 23 -3.70 4.50 -8 -13 23 5.70 4.50 7 13 -23 56.69 14.10 7 13 -23 106.79 12.90 7 13 -23 80.29 10.70 7 13 -23 99.29 12.40 7 13 -23 88.29 11.00 -7 -13 23 94.39 15.80 -7 -13 23 99.39 15.70 -7 -13 23 101.69 11.50 -7 -13 23 113.19 11.00 6 13 -23 64.19 11.90 6 13 -23 60.19 10.10 6 13 -23 44.00 10.20 6 13 -23 56.49 13.70 6 13 -23 56.39 9.70 6 13 -23 74.89 10.00 6 13 -23 49.80 11.00 -6 -13 23 61.69 8.20 -6 -13 23 31.10 7.70 -6 -13 23 50.49 8.70 -6 -13 23 53.89 12.40 5 13 -23 7.30 4.80 5 13 -23 10.00 4.50 5 13 -23 -1.00 5.60 5 13 -23 10.20 4.70 5 13 -23 14.10 7.10 5 13 -23 -1.30 7.60 5 13 -23 17.50 7.60 5 13 -23 16.80 8.50 5 13 -23 6.40 4.10 -5 -13 23 4.50 5.30 -5 -13 23 11.30 6.20 -5 -13 23 4.80 4.20 4 13 -23 71.49 12.60 4 13 -23 73.19 9.00 4 13 -23 75.89 9.70 4 13 -23 77.09 10.40 4 13 -23 53.29 10.50 4 13 -23 73.39 14.00 4 13 -23 77.69 11.60 -4 -13 23 93.09 14.50 -4 -13 23 72.19 9.30 -4 -13 23 82.19 11.50 3 13 -23 2.90 6.80 3 13 -23 -1.00 6.20 3 13 -23 7.20 8.50 3 13 -23 -0.90 3.20 3 13 -23 -1.80 3.40 -3 -13 23 -0.30 5.90 -3 -13 23 2.80 4.40 2 13 -23 135.09 13.40 2 13 -23 114.39 12.40 2 13 -23 127.69 12.20 2 13 -23 125.49 11.70 -2 -13 23 141.69 17.80 -2 -13 23 153.68 13.80 -2 -13 23 135.59 14.10 1 13 -23 102.09 14.10 1 13 -23 120.59 13.40 1 13 -23 119.69 11.60 1 13 -23 122.49 12.40 -1 -13 23 108.59 11.60 -1 -13 23 124.09 14.50 -1 -13 23 113.09 12.60 0 13 -23 -2.60 3.00 0 13 -23 -3.70 5.70 0 13 -23 -2.90 3.40 0 13 -23 9.20 5.90 0 -13 23 -11.30 5.60 0 -13 23 6.40 5.90 0 -13 23 -1.20 3.50 -1 13 -23 -3.50 4.20 -1 13 -23 -4.90 6.40 -1 13 -23 2.90 3.80 1 -13 23 5.40 7.00 1 -13 23 12.20 6.70 1 -13 23 8.90 4.70 -2 13 -23 4.20 3.90 -2 13 -23 0.20 7.70 -2 13 -23 3.10 5.70 -2 13 -23 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7.20 8.00 -7 -10 23 13.00 4.60 -7 -10 23 28.30 7.20 6 10 -23 28.30 7.50 6 10 -23 46.20 10.70 6 10 -23 50.89 9.10 6 10 -23 29.60 8.00 6 10 -23 33.10 8.10 6 10 -23 32.90 9.40 6 10 -23 32.00 8.30 6 10 -23 37.40 7.80 -6 -10 23 47.80 10.90 -6 -10 23 39.40 8.80 -6 -10 23 36.20 6.60 -6 -10 23 53.49 11.70 -6 -10 23 34.30 7.50 -6 -10 23 37.40 8.00 5 10 -23 57.29 11.40 5 10 -23 44.50 9.30 5 10 -23 54.99 12.10 5 10 -23 56.59 7.90 5 10 -23 74.49 9.90 5 10 -23 62.19 8.40 5 10 -23 64.89 8.50 5 10 -23 31.50 9.50 -5 -10 23 66.29 9.90 -5 -10 23 68.69 11.50 -5 -10 23 57.19 8.00 -5 -10 23 71.79 11.50 -5 -10 23 65.59 7.70 4 10 -23 20.40 6.60 4 10 -23 27.70 7.10 4 10 -23 33.20 6.90 4 10 -23 21.40 7.30 4 10 -23 39.80 9.90 4 10 -23 20.80 6.30 4 10 -23 28.60 7.40 4 10 -23 26.10 5.90 4 10 -23 42.20 7.70 -4 -10 23 17.50 4.30 -4 -10 23 31.90 6.10 -4 -10 23 30.50 7.50 -4 -10 23 15.90 7.50 -4 -10 23 18.30 5.90 -4 -10 23 26.10 6.90 3 10 -23 369.86 23.80 3 10 -23 350.66 23.10 3 10 -23 375.56 20.70 3 10 -23 351.56 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23 6.80 6.10 7 9 -23 137.09 12.20 7 9 -23 117.89 12.70 7 9 -23 125.99 15.40 7 9 -23 134.89 16.30 7 9 -23 142.49 17.70 7 9 -23 130.29 14.50 7 9 -23 150.98 13.20 7 9 -23 117.89 12.20 -7 -9 23 131.39 13.30 -7 -9 23 132.99 17.00 -7 -9 23 162.98 12.90 -7 -9 23 141.19 15.40 -7 -9 23 133.69 12.60 6 9 -23 163.28 12.80 6 9 -23 172.28 16.70 6 9 -23 156.38 13.20 6 9 -23 170.08 16.00 6 9 -23 199.48 15.50 6 9 -23 160.18 14.60 6 9 -23 177.68 15.60 6 9 -23 179.78 13.30 -6 -9 23 178.78 16.00 -6 -9 23 187.58 15.10 -6 -9 23 152.48 16.80 -6 -9 23 162.48 14.40 -6 -9 23 177.28 13.20 -6 -9 23 179.58 12.90 5 9 -23 44.80 9.60 5 9 -23 35.10 8.80 5 9 -23 30.30 9.80 5 9 -23 40.70 6.90 5 9 -23 39.80 7.40 5 9 -23 51.69 9.90 5 9 -23 25.50 6.20 5 9 -23 46.90 7.50 -5 -9 23 41.10 10.00 -5 -9 23 51.49 8.80 -5 -9 23 35.20 6.20 -5 -9 23 35.60 7.00 -5 -9 23 39.10 8.60 4 9 -23 -3.70 6.00 4 9 -23 -5.30 5.30 4 9 -23 1.30 3.00 4 9 -23 -2.20 3.20 4 9 -23 5.20 6.80 4 9 -23 -5.80 3.00 4 9 -23 -1.30 5.70 4 9 -23 6.20 4.90 4 9 -23 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14.60 -1 10 -25 87.79 11.50 -1 10 -25 123.89 12.70 1 -10 25 85.59 13.90 1 -10 25 115.19 11.70 -2 10 -25 1.10 5.10 -2 10 -25 0.20 9.10 -2 10 -25 0.20 3.90 -2 10 -25 -2.00 5.80 2 -10 25 3.50 6.50 -3 10 -25 50.69 11.20 -3 10 -25 64.19 10.00 3 -10 25 52.99 12.40 3 -10 25 55.79 10.00 -4 10 -25 6.50 4.80 4 -10 25 11.10 5.20 -5 10 -25 -0.70 4.70 -5 10 -25 11.00 5.10 5 -10 25 4.40 4.80 -6 10 -25 144.59 15.20 -6 10 -25 144.59 13.20 6 -10 25 132.79 13.70 9 9 -25 14.00 6.00 9 9 -25 2.60 5.40 9 9 -25 4.90 4.70 -9 -9 25 -7.20 5.20 -9 -9 25 -5.70 7.50 -9 -9 25 -1.70 4.50 8 9 -25 34.00 7.60 8 9 -25 60.89 11.00 8 9 -25 26.00 7.00 8 9 -25 47.30 9.60 -8 -9 25 44.70 9.30 -8 -9 25 14.70 8.30 -8 -9 25 40.50 9.10 7 9 -25 31.70 7.60 7 9 -25 44.70 8.90 7 9 -25 23.00 6.20 7 9 -25 44.70 10.50 7 9 -25 32.10 7.20 -7 -9 25 48.00 8.90 -7 -9 25 15.20 7.90 -7 -9 25 25.20 6.10 6 9 -25 8.20 4.10 6 9 -25 3.80 4.30 6 9 -25 3.80 6.20 6 9 -25 26.10 8.60 6 9 -25 13.70 7.70 6 9 -25 8.20 4.50 -6 -9 25 4.70 6.60 -6 -9 25 2.00 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12.70 7.80 -2 8 -25 71.89 11.90 -2 8 -25 85.89 11.10 2 -8 25 112.19 12.30 2 -8 25 109.89 13.60 -3 8 -25 4.80 4.30 -3 8 -25 -5.90 5.70 -4 8 -25 0.90 3.90 4 -8 25 -2.40 3.80 -5 8 -25 19.90 5.80 -5 8 -25 12.30 6.50 5 -8 25 14.90 5.50 -6 8 -25 84.59 13.00 6 -8 25 71.19 11.20 9 7 -25 -7.80 3.50 9 7 -25 -9.60 4.80 9 7 -25 -5.60 4.70 -9 -7 25 -5.80 4.70 -9 -7 25 6.30 4.70 8 7 -25 -7.80 3.90 8 7 -25 -2.30 4.70 8 7 -25 -4.60 3.90 8 7 -25 -2.80 4.20 -8 -7 25 -2.70 7.80 -8 -7 25 0.30 4.40 -8 -7 25 1.00 4.20 7 7 -25 7.90 5.00 7 7 -25 3.90 4.40 7 7 -25 6.50 5.20 7 7 -25 10.50 5.20 -7 -7 25 5.10 7.60 -7 -7 25 13.20 5.20 -7 -7 25 11.30 4.60 6 7 -25 206.88 16.70 6 7 -25 192.28 14.90 6 7 -25 190.58 17.50 6 7 -25 191.88 21.10 6 7 -25 144.49 18.00 -6 -7 25 223.58 17.80 -6 -7 25 193.68 16.50 -6 -7 25 172.18 17.10 -6 -7 25 208.88 16.90 5 7 -25 41.50 10.40 5 7 -25 45.20 10.40 5 7 -25 37.20 8.20 5 7 -25 48.90 9.00 5 7 -25 48.70 10.00 5 7 -25 57.09 11.50 5 7 -25 47.00 9.30 -5 -7 25 59.69 12.10 -5 -7 25 49.50 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6.10 0 0 26 14.90 5.30 -1 0 -26 122.69 13.00 4 -1 -26 -8.90 6.60 3 -1 -26 15.30 6.10 -3 1 26 14.90 6.30 -3 1 26 22.40 7.10 -2 1 26 191.18 15.10 -2 1 26 182.88 15.90 -1 1 26 15.40 6.00 2 17 -27 5.70 5.70 0 17 -27 -4.10 6.10 4 16 -27 -6.20 4.60 3 16 -27 18.90 6.10 3 16 -27 18.50 9.90 -3 -16 27 6.50 7.20 2 16 -27 19.50 6.10 2 16 -27 15.40 6.20 -2 -16 27 7.70 7.30 1 16 -27 68.99 13.40 1 16 -27 61.99 13.10 -1 -16 27 68.59 12.30 0 16 -27 111.39 15.80 0 16 -27 93.09 15.30 0 -16 27 70.89 14.90 -1 16 -27 11.70 7.30 5 15 -27 -5.20 5.70 5 15 -27 -0.50 4.10 5 15 -27 -1.90 6.30 4 15 -27 6.40 4.50 4 15 -27 -2.10 7.70 -4 -15 27 -6.60 4.90 3 15 -27 -0.80 3.90 3 15 -27 -5.60 4.50 -3 -15 27 -0.60 5.40 2 15 -27 14.50 6.00 2 15 -27 16.40 7.00 -2 -15 27 7.20 5.90 1 15 -27 64.99 12.10 1 15 -27 62.59 11.60 -1 -15 27 76.49 11.80 0 15 -27 -7.20 5.20 0 15 -27 5.10 4.60 0 -15 27 -2.30 4.90 -1 15 -27 -12.00 5.30 -1 15 -27 -7.30 3.90 1 -15 27 3.00 5.30 -2 15 -27 15.80 8.30 5 14 -27 5.90 5.10 5 14 -27 9.00 7.00 -5 -14 27 9.50 5.40 -5 -14 27 7.50 7.20 4 14 -27 22.60 7.00 4 14 -27 16.70 6.30 -4 -14 27 26.70 7.90 3 14 -27 -2.20 4.60 3 14 -27 -1.50 4.40 -3 -14 27 -7.00 5.40 2 14 -27 2.70 4.50 2 14 -27 -3.70 4.70 -2 -14 27 -8.10 4.60 1 14 -27 15.90 5.80 1 14 -27 17.30 6.60 -1 -14 27 19.00 6.60 0 14 -27 2.20 5.10 0 14 -27 -0.80 4.30 0 -14 27 -9.80 5.30 -1 14 -27 41.20 10.60 -1 14 -27 31.70 8.20 1 -14 27 33.00 7.60 -2 14 -27 -2.60 5.00 -2 14 -27 3.60 7.20 2 -14 27 6.00 4.80 6 13 -27 -7.90 5.20 6 13 -27 4.60 5.10 -6 -13 27 -3.50 4.70 -6 -13 27 -7.20 6.60 5 13 -27 14.40 6.70 5 13 -27 17.40 5.80 5 13 -27 30.60 8.10 -5 -13 27 48.80 12.10 -5 -13 27 25.60 6.40 4 13 -27 -2.90 3.90 4 13 -27 -0.80 4.40 -4 -13 27 -0.50 6.20 3 13 -27 -1.40 4.90 3 13 -27 2.40 4.30 -3 -13 27 -8.50 5.30 2 13 -27 28.70 7.00 2 13 -27 42.00 10.00 -2 -13 27 29.50 7.80 1 13 -27 9.20 4.90 1 13 -27 3.40 4.60 -1 -13 27 5.40 5.40 0 13 -27 4.60 5.10 0 13 -27 5.30 6.00 0 -13 27 2.80 5.10 -1 13 -27 0.40 5.00 -1 13 -27 -7.90 4.10 1 -13 27 -2.00 5.00 -2 13 -27 -1.90 6.60 -2 13 -27 1.60 5.00 2 -13 27 -0.70 5.00 3 -13 27 66.69 12.40 6 12 -27 13.80 6.10 6 12 -27 10.70 6.60 -6 -12 27 11.20 5.70 -6 -12 27 -0.10 7.20 5 12 -27 17.90 7.10 5 12 -27 17.00 5.70 5 12 -27 28.80 7.90 -5 -12 27 58.39 13.50 -5 -12 27 25.00 6.70 4 12 -27 6.00 4.40 4 12 -27 -0.80 4.30 -4 -12 27 -8.60 5.20 3 12 -27 152.18 15.30 3 12 -27 141.29 14.10 -3 -12 27 130.19 15.90 2 12 -27 2.50 4.80 2 12 -27 -0.40 3.90 -2 -12 27 5.60 6.00 1 12 -27 -5.20 3.80 1 12 -27 -8.50 4.30 -1 -12 27 -1.80 5.00 0 12 -27 9.90 5.30 0 12 -27 17.20 5.60 0 -12 27 5.80 5.70 -1 12 -27 -8.00 5.10 -1 12 -27 0.60 4.50 -2 12 -27 7.00 6.70 -2 12 -27 9.20 5.00 2 -12 27 11.30 6.00 -3 12 -27 5.00 5.70 3 -12 27 -1.80 5.00 6 11 -27 96.79 20.20 6 11 -27 58.29 11.30 6 11 -27 97.69 12.20 6 11 -27 90.09 12.50 -6 -11 27 55.49 13.80 -6 -11 27 88.09 11.90 5 11 -27 70.99 12.10 5 11 -27 73.69 12.40 5 11 -27 76.89 11.70 -5 -11 27 52.49 10.70 -5 -11 27 89.09 14.80 4 11 -27 9.90 4.80 4 11 -27 17.70 6.20 -4 -11 27 10.40 6.10 3 11 -27 9.50 5.70 3 11 -27 17.30 13.90 3 11 -27 11.70 5.90 -3 -11 27 10.50 6.70 2 11 -27 48.70 10.60 2 11 -27 16.30 5.90 -2 -11 27 23.00 7.40 1 11 -27 8.30 5.50 1 11 -27 8.70 5.00 0 11 -27 10.50 5.30 0 11 -27 4.90 5.30 0 -11 27 11.80 5.50 -1 11 -27 3.10 4.00 -1 11 -27 -8.20 5.40 1 -11 27 1.80 4.80 -2 11 -27 105.29 13.00 -2 11 -27 95.39 13.60 2 -11 27 120.09 13.30 -3 11 -27 154.78 15.50 3 -11 27 158.88 16.00 7 10 -27 57.09 11.80 7 10 -27 28.60 8.70 7 10 -27 59.69 11.70 -7 -10 27 68.99 14.70 6 10 -27 -6.70 4.50 6 10 -27 0.00 5.10 6 10 -27 -7.30 3.90 6 10 -27 -6.50 5.00 -6 -10 27 -4.70 4.20 -6 -10 27 -4.00 3.90 -6 -10 27 -11.50 6.00 5 10 -27 3.50 4.50 5 10 -27 4.70 6.00 5 10 -27 0.20 4.60 -5 -10 27 -2.00 4.50 -5 -10 27 10.20 8.00 4 10 -27 37.70 9.80 4 10 -27 45.80 10.70 -4 -10 27 46.70 11.80 3 10 -27 184.98 16.60 3 10 -27 226.78 17.10 -3 -10 27 229.88 18.50 2 10 -27 1.50 4.70 2 10 -27 2.10 4.10 -2 -10 27 -0.20 5.40 1 10 -27 19.00 5.90 1 10 -27 22.20 6.40 -1 -10 27 17.80 6.50 0 10 -27 40.10 9.60 0 10 -27 22.20 6.20 0 -10 27 53.59 11.80 -1 10 -27 45.20 10.50 -1 10 -27 4.20 4.60 1 -10 27 14.90 5.80 -2 10 -27 125.79 14.20 2 -10 27 118.59 13.20 -3 10 -27 20.50 6.20 3 -10 27 25.60 7.20 7 9 -27 153.28 19.30 7 9 -27 139.39 14.30 7 9 -27 147.79 14.50 7 9 -27 132.29 14.40 -7 -9 27 138.49 21.10 -7 -9 27 146.59 14.00 -7 -9 27 152.48 15.30 6 9 -27 37.00 7.90 6 9 -27 57.69 12.50 6 9 -27 37.20 9.70 6 9 -27 64.69 11.10 -6 -9 27 46.50 11.10 -6 -9 27 55.29 9.50 -6 -9 27 90.79 14.90 5 9 -27 6.80 5.10 5 9 -27 2.20 5.40 5 9 -27 4.70 5.80 5 9 -27 0.20 4.30 -5 -9 27 4.80 5.10 -5 -9 27 7.80 6.70 4 9 -27 35.90 9.70 4 9 -27 10.10 6.00 -4 -9 27 22.30 7.70 3 9 -27 3.10 4.30 3 9 -27 0.40 4.80 -3 -9 27 3.30 6.30 2 9 -27 3.10 4.90 2 9 -27 -1.20 4.30 -2 -9 27 0.10 5.40 1 9 -27 119.79 12.70 1 9 -27 109.29 12.90 -1 -9 27 114.89 14.20 0 9 -27 2.90 4.50 0 9 -27 5.50 4.80 0 -9 27 1.60 5.70 -1 9 -27 1.20 4.30 -1 9 -27 -7.10 5.70 1 -9 27 3.60 5.20 -2 9 -27 25.50 6.20 2 -9 27 37.80 9.60 -3 9 -27 8.70 4.90 3 -9 27 17.60 6.40 7 8 -27 41.60 10.90 7 8 -27 97.79 13.80 7 8 -27 84.69 11.00 7 8 -27 94.99 15.70 -7 -8 27 61.79 24.00 -7 -8 27 72.89 11.30 -7 -8 27 85.19 12.60 6 8 -27 -6.80 4.50 6 8 -27 -1.60 5.60 6 8 -27 9.30 5.50 6 8 -27 8.70 4.10 -6 -8 27 6.40 5.30 -6 -8 27 1.30 8.40 -6 -8 27 0.50 4.30 5 8 -27 -3.30 4.30 5 8 -27 4.10 5.10 5 8 -27 3.50 5.40 5 8 -27 4.70 6.00 -5 -8 27 -3.40 7.80 -5 -8 27 2.20 4.80 -5 -8 27 6.40 4.50 4 8 -27 25.60 7.00 4 8 -27 27.80 6.80 -4 -8 27 24.80 9.70 3 8 -27 52.99 10.30 3 8 -27 20.10 6.40 2 8 -27 -1.80 10.40 2 8 -27 2.70 4.40 2 8 -27 6.70 5.00 1 8 -27 11.20 5.80 1 8 -27 22.40 6.40 -1 -8 27 19.90 7.60 0 8 -27 1.90 4.80 0 8 -27 -3.00 4.90 0 -8 27 0.00 5.80 -1 8 -27 68.09 10.70 1 -8 27 76.39 11.60 -2 8 -27 27.00 6.80 2 -8 27 29.20 7.40 -3 8 -27 10.80 5.80 3 -8 27 13.60 7.00 7 7 -27 12.10 6.70 7 7 -27 4.60 6.50 7 7 -27 9.30 8.30 7 7 -27 11.90 6.00 6 7 -27 -1.40 5.50 6 7 -27 -0.40 5.20 6 7 -27 3.10 4.70 6 7 -27 4.20 4.70 -6 -7 27 5.20 4.60 -6 -7 27 -2.00 5.10 5 7 -27 166.28 15.20 5 7 -27 137.69 13.50 5 7 -27 156.28 14.80 5 7 -27 160.98 14.20 -5 -7 27 135.99 12.40 -5 -7 27 166.68 13.90 4 7 -27 -3.50 4.10 4 7 -27 7.50 4.40 3 7 -27 -0.30 3.90 3 7 -27 3.40 4.90 -3 -7 27 -4.40 7.20 2 7 -27 6.40 5.20 2 7 -27 21.90 12.00 2 7 -27 22.20 6.20 -2 -7 27 13.30 8.70 1 7 -27 24.30 6.30 1 7 -27 20.40 6.80 0 7 -27 7.80 7.50 0 7 -27 9.50 5.00 0 -7 27 10.80 7.30 -1 7 -27 -1.00 4.20 1 -7 27 4.20 6.00 -2 7 -27 4.40 4.60 2 -7 27 2.30 4.70 -3 7 -27 18.20 6.30 3 -7 27 9.10 6.20 6 6 -27 10.50 6.00 6 6 -27 7.20 5.40 6 6 -27 4.80 5.50 6 6 -27 12.00 5.40 -6 -6 27 7.30 5.30 -6 -6 27 38.80 9.20 5 6 -27 17.30 5.70 5 6 -27 13.60 5.70 5 6 -27 6.20 6.50 5 6 -27 12.80 5.80 -5 -6 27 12.80 5.20 -5 -6 27 37.70 9.80 4 6 -27 6.80 4.70 4 6 -27 7.20 4.70 4 6 -27 4.50 4.60 -4 -6 27 -3.30 3.90 3 6 -27 70.59 11.80 3 6 -27 73.79 11.10 3 6 -27 88.79 11.20 2 6 -27 4.10 5.00 2 6 -27 8.10 5.30 1 6 -27 -5.20 3.80 1 6 -27 8.60 5.40 0 6 -27 -1.50 3.60 0 6 -27 6.70 7.40 -1 6 -27 64.29 10.50 1 -6 27 37.70 9.90 -2 6 -27 -1.70 4.40 2 -6 27 0.20 5.50 -3 6 -27 -8.90 4.50 3 -6 27 -1.20 6.60 6 5 -27 139.79 14.60 -6 -5 27 132.99 12.90 -6 -5 27 144.59 14.20 5 5 -27 181.88 15.30 5 5 -27 181.68 16.40 5 5 -27 193.08 16.10 5 5 -27 178.78 14.90 -5 -5 27 170.38 14.40 -5 -5 27 161.98 14.50 4 5 -27 14.20 5.40 4 5 -27 3.50 5.90 4 5 -27 11.00 5.50 -4 -5 27 32.80 7.90 3 5 -27 4.40 4.30 3 5 -27 -6.90 5.40 3 5 -27 -4.10 4.20 -3 -5 27 1.00 5.30 2 5 -27 5.30 4.10 2 5 -27 -1.20 4.60 1 5 -27 50.79 11.70 1 5 -27 50.39 10.10 0 5 -27 74.79 11.30 -1 5 -27 -3.90 3.60 -2 5 -27 11.50 5.50 -3 5 -27 61.19 12.20 6 4 -27 57.79 11.10 -6 -4 27 82.29 12.10 -6 -4 27 79.19 11.30 5 4 -27 -4.20 5.80 5 4 -27 6.50 5.30 5 4 -27 1.80 5.30 5 4 -27 -6.40 4.50 -5 -4 27 -8.10 3.60 -5 -4 27 -2.60 4.30 4 4 -27 84.69 12.00 4 4 -27 75.19 12.80 4 4 -27 79.69 11.80 -4 -4 27 70.39 11.00 3 4 -27 131.29 13.90 3 4 -27 129.49 13.50 -3 -4 27 134.99 12.10 2 4 -27 -1.70 4.30 2 4 -27 -0.90 4.10 1 4 -27 -2.20 4.30 1 4 -27 -1.80 4.90 0 4 -27 3.70 4.50 -1 4 -27 -3.60 4.70 -2 4 -27 202.28 16.60 5 3 -27 19.20 6.20 5 3 -27 18.50 6.10 5 3 -27 23.30 7.40 -5 -3 27 16.50 6.90 -5 -3 27 24.80 6.40 -5 -3 27 17.60 5.80 4 3 -27 42.30 10.60 4 3 -27 34.20 11.60 -4 -3 27 54.59 10.70 -4 -3 27 50.29 9.30 3 3 -27 2.40 5.30 3 3 -27 0.10 4.00 -3 -3 27 2.60 4.50 2 3 -27 30.80 7.20 2 3 -27 52.89 9.70 -2 -3 27 37.40 9.40 1 3 -27 122.39 13.50 1 3 -27 146.89 14.80 0 3 -27 74.99 10.70 -1 3 -27 1.60 4.90 4 2 -27 0.90 5.30 -4 -2 27 3.90 4.30 -4 -2 27 3.90 4.40 -3 -2 27 15.60 5.30 -3 -2 27 -6.60 4.10 2 2 -27 28.60 10.90 2 2 -27 46.20 12.10 -2 -2 27 38.60 9.50 1 2 -27 -9.60 5.10 1 2 -27 -0.50 4.60 2 1 -27 -2.30 5.40 -2 -1 27 13.20 5.70 1 15 -28 15.80 10.40 -3 -14 28 -4.30 6.80 2 14 -28 2.00 5.80 -2 -14 28 -2.60 6.40 1 14 -28 -6.30 5.30 -1 -14 28 -1.80 5.80 0 14 -28 3.90 5.30 4 13 -28 2.50 5.10 -4 -13 28 6.00 7.20 3 13 -28 28.00 7.60 3 13 -28 21.90 6.40 -3 -13 28 7.50 7.80 2 13 -28 -3.30 4.80 2 13 -28 -2.50 4.50 -2 -13 28 4.80 6.50 1 13 -28 9.30 5.40 1 13 -28 14.10 6.10 -1 -13 28 11.60 6.50 0 13 -28 6.50 5.80 0 -13 28 4.40 5.40 -1 13 -28 6.10 5.90 4 12 -28 -0.40 7.60 4 12 -28 7.90 5.00 -4 -12 28 -3.80 7.10 3 12 -28 12.80 6.10 3 12 -28 12.40 6.10 -3 -12 28 2.80 8.00 2 12 -28 3.80 4.70 2 12 -28 -0.60 4.70 -2 -12 28 -4.70 5.60 1 12 -28 10.60 5.90 1 12 -28 16.20 5.80 -1 -12 28 27.40 7.50 0 12 -28 -2.50 5.40 0 12 -28 -4.70 4.30 0 -12 28 -5.70 5.60 -1 12 -28 4.80 6.30 1 -12 28 -2.90 4.90 5 11 -28 7.10 5.00 5 11 -28 -7.90 7.70 -5 -11 28 3.50 7.20 4 11 -28 125.49 15.90 4 11 -28 124.29 14.00 -4 -11 28 110.09 16.60 3 11 -28 20.40 7.00 3 11 -28 21.20 6.50 -3 -11 28 18.10 7.40 2 11 -28 -5.60 5.20 2 11 -28 -5.10 4.00 -2 -11 28 11.10 6.70 1 11 -28 28.20 7.00 1 11 -28 22.90 7.10 -1 -11 28 27.90 7.70 0 11 -28 -2.10 4.00 0 11 -28 0.50 5.30 0 -11 28 -5.40 4.90 -1 11 -28 22.80 7.50 1 -11 28 28.20 7.70 2 -11 28 77.99 11.90 5 10 -28 -1.80 6.80 -5 -10 28 11.70 8.40 4 10 -28 -1.50 5.00 4 10 -28 -3.80 4.30 -4 -10 28 -5.50 6.30 3 10 -28 74.49 10.90 -3 -10 28 21.30 8.30 2 10 -28 29.40 7.30 2 10 -28 65.99 10.20 -2 -10 28 32.70 8.50 1 10 -28 87.49 13.00 1 10 -28 60.89 11.00 -1 -10 28 67.89 12.10 0 10 -28 -0.20 4.30 0 10 -28 -9.10 5.30 0 -10 28 -2.50 6.00 -1 10 -28 25.80 7.00 1 -10 28 17.20 6.90 2 -10 28 17.00 6.10 5 9 -28 -2.00 6.30 -5 -9 28 5.60 8.40 4 9 -28 65.79 12.40 4 9 -28 25.00 6.60 -4 -9 28 40.60 9.90 3 9 -28 -7.70 3.80 3 9 -28 0.90 4.80 -3 -9 28 -4.80 6.70 2 9 -28 18.30 6.10 2 9 -28 4.30 4.60 -2 -9 28 9.90 6.30 1 9 -28 2.50 5.40 1 9 -28 11.30 5.10 -1 -9 28 -2.90 5.40 0 9 -28 6.70 5.30 0 9 -28 23.00 7.20 0 -9 28 21.40 7.10 -1 9 -28 62.79 15.10 1 -9 28 61.09 11.30 2 -9 28 29.60 8.00 5 8 -28 -5.30 6.60 5 8 -28 1.40 7.40 4 8 -28 -0.80 5.20 4 8 -28 -2.80 5.30 -4 -8 28 -15.90 6.60 3 8 -28 3.50 4.80 -3 -8 28 -1.90 6.50 2 8 -28 67.99 11.60 2 8 -28 38.70 9.60 -2 -8 28 42.90 9.60 1 8 -28 8.10 6.50 1 8 -28 21.10 5.90 -1 -8 28 9.70 6.50 0 8 -28 5.40 5.90 0 8 -28 4.00 4.50 0 -8 28 -3.60 5.80 1 -8 28 15.30 6.50 5 7 -28 20.70 8.10 5 7 -28 16.80 7.90 -5 -7 28 18.50 5.80 4 7 -28 0.10 5.40 3 7 -28 53.29 12.70 3 7 -28 28.10 7.50 2 7 -28 14.30 6.10 2 7 -28 8.70 5.40 1 7 -28 -2.30 5.20 1 7 -28 2.20 4.10 -1 -7 28 -4.60 7.40 0 7 -28 10.10 6.70 0 7 -28 19.80 6.80 0 -7 28 0.10 7.10 1 -7 28 18.30 7.50 4 6 -28 -0.60 5.80 4 6 -28 1.90 5.90 3 6 -28 -8.30 5.00 2 6 -28 1.10 5.00 2 6 -28 -4.00 5.10 1 6 -28 9.40 6.40 0 6 -28 24.00 8.50 4 5 -28 46.70 13.70 4 5 -28 26.10 8.70 3 5 -28 4.50 5.10 2 5 -28 -8.20 4.20 1 5 -28 8.10 6.30 2 4 -28 77.49 13.40 2 4 -28 64.79 12.80 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 82287 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ru1 Ru 0.41752(2) 0.15771(2) 0.10606(2) 0.01617(4) Uani 1 1 d . . . . . Cl1 Cl 0.64363(5) 0.16997(3) 0.08905(3) 0.02211(10) Uani 1 1 d . . . . . Cl2 Cl 0.36663(5) 0.16000(3) -0.02241(3) 0.02273(10) Uani 1 1 d . . . . . S1 S 0.40722(5) 0.31451(3) 0.16452(3) 0.01928(10) Uani 1 1 d . . . . . O1 O 0.7019(2) 0.43937(15) 0.06998(13) 0.0577(7) Uani 1 1 d . . . . . N1 N 0.53930(18) 0.45759(12) 0.17082(10) 0.0225(4) Uani 1 1 d . . . . . H1 H 0.589272 0.482438 0.148905 0.027 Uiso 1 1 calc R . . . . N2 N 0.5530(2) 0.33313(13) 0.06275(11) 0.0262(4) Uani 1 1 d . . . . . H2 H 0.515920 0.281773 0.031637 0.031 Uiso 1 1 calc R . . . . C2 C 0.5049(2) 0.37294(14) 0.13203(12) 0.0210(4) Uani 1 1 d . . . . . C3 C 0.5032(2) 0.51192(13) 0.24435(12) 0.0203(4) Uani 1 1 d . . . . . C4 C 0.3764(2) 0.51815(14) 0.25564(13) 0.0230(4) Uani 1 1 d . . . . . H4 H 0.311554 0.486284 0.214138 0.028 Uiso 1 1 calc R . . . . C5 C 0.3410(2) 0.57151(14) 0.32839(13) 0.0248(4) Uani 1 1 d . . . . . H5 H 0.252580 0.574274 0.336101 0.030 Uiso 1 1 calc R . . . . C6 C 0.4333(2) 0.61937(14) 0.38801(13) 0.0244(4) Uani 1 1 d . . . . . H6 H 0.408613 0.654648 0.437114 0.029 Uiso 1 1 calc R . . . . C7 C 0.5649(2) 0.61669(14) 0.37705(13) 0.0241(4) Uani 1 1 d . . . . . C8 C 0.6026(2) 0.56206(14) 0.30397(13) 0.0219(4) Uani 1 1 d . . . . . C9 C 0.6621(3) 0.66709(17) 0.43802(15) 0.0347(6) Uani 1 1 d . . . . . H9 H 0.638363 0.702951 0.487210 0.042 Uiso 1 1 calc R . . . . C10 C 0.7885(3) 0.6645(2) 0.42667(17) 0.0466(7) Uani 1 1 d . . . . . H10 H 0.852242 0.699105 0.467711 0.056 Uiso 1 1 calc R . . . . C11 C 0.8255(3) 0.6108(2) 0.35441(18) 0.0456(7) Uani 1 1 d . . . . . H11 H 0.914192 0.609610 0.347239 0.055 Uiso 1 1 calc R . . . . C12 C 0.7354(2) 0.56046(17) 0.29440(15) 0.0318(5) Uani 1 1 d . . . . . H12 H 0.761961 0.524268 0.246145 0.038 Uiso 1 1 calc R . . . . C13 C 0.6538(3) 0.36513(18) 0.03655(15) 0.0367(6) Uani 1 1 d . . . . . C14 C 0.7003(3) 0.3005(2) -0.03583(16) 0.046 Uani 1 1 d . . . . . H14E H 0.774009 0.328862 -0.048721 0.056 Uiso 0.680(3) 1 calc R . P A 1 H14F H 0.732193 0.250569 -0.024481 0.056 Uiso 0.680(3) 1 calc R . P A 1 H14G H 0.789301 0.287721 -0.022096 0.056 Uiso 0.320(3) 1 calc R . P A 2 H14H H 0.645377 0.245362 -0.053370 0.056 Uiso 0.320(3) 1 calc R . P A 2 C15 C 0.6012(4) 0.2667(3) -0.1047(2) 0.0383(8) Uani 0.680(3) 1 d D U P A 1 H15E H 0.536050 0.228975 -0.094986 0.046 Uiso 0.680(3) 1 calc R . P A 1 H15F H 0.643149 0.229137 -0.149614 0.046 Uiso 0.680(3) 1 calc R . P A 1 C16 C 0.5318(4) 0.3326(3) -0.1276(2) 0.0445(9) Uani 0.680(3) 1 d D U P A 1 H16E H 0.507734 0.378938 -0.080185 0.053 Uiso 0.680(3) 1 calc R . P A 1 H16F H 0.591702 0.360213 -0.150650 0.053 Uiso 0.680(3) 1 calc R . P A 1 C17 C 0.4130(4) 0.2959(3) -0.1843(2) 0.0514(10) Uani 0.680(3) 1 d D U P A 1 H17E H 0.354675 0.266880 -0.161589 0.062 Uiso 0.680(3) 1 calc R . P A 1 H17F H 0.368283 0.345059 -0.190511 0.062 Uiso 0.680(3) 1 calc R . P A 1 C18 C 0.4332(4) 0.2324(3) -0.2628(2) 0.0537(10) Uani 0.680(3) 1 d D U P A 1 H18E H 0.480571 0.184156 -0.256829 0.064 Uiso 0.680(3) 1 calc R . P A 1 H18F H 0.488100 0.261959 -0.286814 0.064 Uiso 0.680(3) 1 calc R . P A 1 C19 C 0.3118(4) 0.1946(3) -0.3168(2) 0.0608(11) Uani 0.680(3) 1 d D U P A 1 H19E H 0.259599 0.161990 -0.294062 0.073 Uiso 0.680(3) 1 calc R . P A 1 H19F H 0.261777 0.243195 -0.319684 0.073 Uiso 0.680(3) 1 calc R . P A 1 C20 C 0.3294(6) 0.1351(3) -0.3973(2) 0.0702(13) Uani 0.680(3) 1 d D U P A 1 H20E H 0.386404 0.166221 -0.418921 0.084 Uiso 0.680(3) 1 calc R . P A 1 H20F H 0.244657 0.121559 -0.429762 0.084 Uiso 0.680(3) 1 calc R . P A 1 C21 C 0.3853(8) 0.0514(4) -0.4036(4) 0.0848(18) Uani 0.680(3) 1 d D U P A 1 H21G H 0.388966 0.014896 -0.458439 0.127 Uiso 0.680(3) 1 calc GR . P A 1 H21H H 0.331111 0.020630 -0.381018 0.127 Uiso 0.680(3) 1 calc GR . P A 1 H21I H 0.472510 0.063657 -0.375414 0.127 Uiso 0.680(3) 1 calc GR . P A 1 C15A C 0.6998(7) 0.3279(6) -0.0991(4) 0.0383(8) Uani 0.320(3) 1 d D . P A 2 H15G H 0.722043 0.277782 -0.144391 0.046 Uiso 0.320(3) 1 calc R . P A 2 H15H H 0.770575 0.374060 -0.085280 0.046 Uiso 0.320(3) 1 calc R . P A 2 C16A C 0.5811(7) 0.3618(4) -0.1255(5) 0.0445(9) Uani 0.320(3) 1 d D . P A 2 H16G H 0.548622 0.404997 -0.079221 0.053 Uiso 0.320(3) 1 calc R . P A 2 H16H H 0.604681 0.392962 -0.158446 0.053 Uiso 0.320(3) 1 calc R . P A 2 C17A C 0.4745(7) 0.2944(6) -0.1698(4) 0.0514(10) Uani 0.320(3) 1 d D . P A 2 H17G H 0.394692 0.324188 -0.173206 0.062 Uiso 0.320(3) 1 calc R . P A 2 H17H H 0.459838 0.257345 -0.140422 0.062 Uiso 0.320(3) 1 calc R . P A 2 C18A C 0.4976(8) 0.2370(7) -0.2501(4) 0.0537(10) Uani 0.320(3) 1 d D . P A 2 H18G H 0.575778 0.205637 -0.246757 0.064 Uiso 0.320(3) 1 calc R . P A 2 H18H H 0.514953 0.274092 -0.279142 0.064 Uiso 0.320(3) 1 calc R . P A 2 C19A C 0.3881(8) 0.1715(7) -0.2948(4) 0.0608(11) Uani 0.320(3) 1 d D . P A 2 H19G H 0.372251 0.133107 -0.266706 0.073 Uiso 0.320(3) 1 calc R . P A 2 H19H H 0.309275 0.202550 -0.297159 0.073 Uiso 0.320(3) 1 calc R . P A 2 C20A C 0.4119(10) 0.1162(8) -0.3758(5) 0.0702(13) Uani 0.320(3) 1 d D . P A 2 H20G H 0.492927 0.087302 -0.373503 0.084 Uiso 0.320(3) 1 calc R . P A 2 H20H H 0.423688 0.154330 -0.404594 0.084 Uiso 0.320(3) 1 calc R . P A 2 C21A C 0.3052(12) 0.0478(8) -0.4196(6) 0.0848(18) Uani 0.320(3) 1 d D . P A 2 H21J H 0.320514 0.019734 -0.474064 0.127 Uiso 0.320(3) 1 calc GR . P A 2 H21K H 0.222879 0.075016 -0.416809 0.127 Uiso 0.320(3) 1 calc GR . P A 2 H21L H 0.302500 0.003955 -0.396563 0.127 Uiso 0.320(3) 1 calc GR . P A 2 C22 C 0.2240(2) 0.10598(14) 0.11088(13) 0.0213(4) Uani 1 1 d . . . . . C23 C 0.2835(2) 0.15822(14) 0.18666(12) 0.0214(4) Uani 1 1 d . . . . . H23 H 0.239943 0.205548 0.218786 0.026 Uiso 1 1 calc R . . . . C24 C 0.4070(2) 0.14171(14) 0.21606(12) 0.0211(4) Uani 1 1 d . . . . . H24 H 0.443525 0.177060 0.267568 0.025 Uiso 1 1 calc R . . . . C25 C 0.4750(2) 0.07316(14) 0.16901(12) 0.0208(4) Uani 1 1 d . . . . . C26 C 0.4168(2) 0.02003(13) 0.09236(12) 0.0213(4) Uani 1 1 d . . . . . H26 H 0.460706 -0.026921 0.060031 0.026 Uiso 1 1 calc R . . . . C27 C 0.2948(2) 0.03695(13) 0.06461(12) 0.0215(4) Uani 1 1 d . . . . . H27 H 0.258094 0.001187 0.013239 0.026 Uiso 1 1 calc R . . . . C28 C 0.0911(2) 0.12139(15) 0.07971(14) 0.0271(5) Uani 1 1 d . . . . . H28 H 0.073832 0.081843 0.023518 0.032 Uiso 1 1 calc R . . . . C29 C 0.0789(2) 0.21464(16) 0.08580(15) 0.0318(5) Uani 1 1 d . . . . . H29D H 0.096402 0.254722 0.140447 0.048 Uiso 1 1 calc GR . . . . H29E H -0.008629 0.220635 0.065024 0.048 Uiso 1 1 calc GR . . . . H29F H 0.141158 0.228715 0.055873 0.048 Uiso 1 1 calc GR . . . . C30 C -0.0099(2) 0.09576(17) 0.12328(17) 0.0346(6) Uani 1 1 d . . . . . H30D H -0.004797 0.034185 0.115387 0.052 Uiso 1 1 calc GR . . . . H30E H -0.096378 0.104686 0.103178 0.052 Uiso 1 1 calc GR . . . . H30F H 0.007263 0.132130 0.178935 0.052 Uiso 1 1 calc GR . . . . C31 C 0.6066(2) 0.05643(16) 0.19876(15) 0.0287(5) Uani 1 1 d . . . . . H31D H 0.661210 0.039766 0.156675 0.043 Uiso 1 1 calc GR . . . . H31E H 0.598860 0.009085 0.217418 0.043 Uiso 1 1 calc GR . . . . H31F H 0.645376 0.109538 0.241583 0.043 Uiso 1 1 calc GR . . . . Ru1B Ru 0.79076(2) 0.31457(2) 0.39479(2) 0.02013(5) Uani 1 1 d . . . . . Cl1B Cl 0.87395(5) 0.36207(5) 0.53073(3) 0.03682(15) Uani 1 1 d . . . . . Cl2B Cl 0.61960(5) 0.22383(3) 0.41366(3) 0.02538(11) Uani 1 1 d . . . . . S1B S 0.92945(7) 0.19493(5) 0.36238(4) 0.03603(15) Uani 1 1 d . . . . . N1B N 1.0194(2) 0.08040(17) 0.41800(13) 0.0412(6) Uani 1 1 d . . . . . H1B H 1.017529 0.054144 0.450747 0.049 Uiso 1 1 calc R . . . . N2B N 0.8605(2) 0.16010(18) 0.48171(13) 0.0462(7) Uani 1 1 d . . . . . H2B H 0.806372 0.200520 0.484449 0.055 Uiso 0.531(4) 1 calc R . P B 1 H2BA H 0.801434 0.196742 0.481438 0.055 Uiso 0.469(4) 1 calc R . P B 2 C2B C 0.9371(3) 0.1416(2) 0.42384(15) 0.0401(7) Uani 1 1 d . . . . . C3B C 1.1112(3) 0.05342(17) 0.36279(15) 0.0331(5) Uani 1 1 d . . . . . C4B C 1.2372(3) 0.07756(19) 0.38682(18) 0.0410(6) Uani 1 1 d . . . . . H4B H 1.262776 0.117609 0.438672 0.049 Uiso 1 1 calc R . . . . C5B C 1.3322(3) 0.0449(2) 0.3369(3) 0.0566(10) Uani 1 1 d . . . . . H5B H 1.420595 0.063535 0.354491 0.068 Uiso 1 1 calc R . . . . C6B C 1.2943(3) -0.0151(2) 0.2617(2) 0.0511(8) Uani 1 1 d . . . . . H6B H 1.357462 -0.039180 0.227948 0.061 Uiso 1 1 calc R . . . . C7B C 1.1646(3) -0.03989(16) 0.23555(17) 0.0388(6) Uani 1 1 d . . . . . C8B C 1.0692(3) -0.00592(16) 0.28658(16) 0.0342(5) Uani 1 1 d . . . . . C9B C 1.1175(4) -0.0993(2) 0.1582(2) 0.0565(10) Uani 1 1 d . . . . . H9B H 1.178148 -0.122395 0.122427 0.068 Uiso 1 1 calc R . . . . C10B C 0.9914(5) -0.1239(2) 0.1336(2) 0.0675(11) Uani 1 1 d . . . . . H10B H 0.964682 -0.163701 0.081783 0.081 Uiso 1 1 calc R . . . . C11B C 0.9033(4) -0.0916(2) 0.18339(19) 0.0585(10) Uani 1 1 d . . . . . H11B H 0.814845 -0.109623 0.165391 0.070 Uiso 1 1 calc R . . . . C12B C 0.9357(3) -0.03474(18) 0.25765(16) 0.0378(6) Uani 1 1 d . . . . . H12B H 0.870681 -0.013790 0.290726 0.045 Uiso 1 1 calc R . . . . O1B O 0.9496(7) 0.0860(5) 0.5482(6) 0.0465(16) Uani 0.531(4) 1 d D U P B 1 C13B C 0.8565(16) 0.1257(10) 0.5342(4) 0.0528(10) Uani 0.531(4) 1 d D U P B 1 C14B C 0.7577(9) 0.1541(6) 0.5883(4) 0.0607(11) Uani 0.531(4) 1 d D U P B 1 H14A H 0.679710 0.165239 0.559767 0.073 Uiso 0.531(4) 1 calc R . P B 1 H14B H 0.734056 0.104957 0.603087 0.073 Uiso 0.531(4) 1 calc R . P B 1 C15B C 0.7929(6) 0.2313(5) 0.6594(3) 0.0725(14) Uani 0.531(4) 1 d D U P B 1 H15A H 0.724695 0.236327 0.693508 0.087 Uiso 0.531(4) 1 calc R . P B 1 H15B H 0.791178 0.282960 0.645309 0.087 Uiso 0.531(4) 1 calc R . P B 1 C16B C 0.9176(6) 0.2369(5) 0.7057(3) 0.0694(13) Uani 0.531(4) 1 d D U P B 1 H16A H 0.986862 0.247023 0.677154 0.083 Uiso 0.531(4) 1 calc R . P B 1 H16B H 0.929109 0.179738 0.709693 0.083 Uiso 0.531(4) 1 calc R . P B 1 C17B C 0.9346(6) 0.3054(5) 0.7849(3) 0.0735(14) Uani 0.531(4) 1 d D U P B 1 H17A H 0.907499 0.360625 0.781541 0.088 Uiso 0.531(4) 1 calc R . P B 1 H17B H 0.875579 0.289335 0.816115 0.088 Uiso 0.531(4) 1 calc R . P B 1 C18B C 1.0657(6) 0.3220(6) 0.8270(3) 0.0741(15) Uani 0.531(4) 1 d D U P B 1 H18A H 1.121611 0.348639 0.801242 0.089 Uiso 0.531(4) 1 calc R . P B 1 H18B H 1.099195 0.265163 0.822074 0.089 Uiso 0.531(4) 1 calc R . P B 1 C19B C 1.0775(10) 0.3791(7) 0.9107(4) 0.0713(12) Uani 0.531(4) 1 d D U P B 1 H19A H 1.060633 0.439183 0.915384 0.086 Uiso 0.531(4) 1 calc R . P B 1 H19B H 1.009439 0.359170 0.934469 0.086 Uiso 0.531(4) 1 calc R . P B 1 C20B C 1.2025(7) 0.3825(6) 0.9560(4) 0.0729(15) Uani 0.531(4) 1 d D U P B 1 H20A H 1.268815 0.409151 0.936063 0.087 Uiso 0.531(4) 1 calc R . P B 1 H20B H 1.224244 0.321765 0.945792 0.087 Uiso 0.531(4) 1 calc R . P B 1 C21B C 1.2121(14) 0.4305(10) 1.0408(4) 0.089(3) Uani 0.531(4) 1 d D U P B 1 H21A H 1.203935 0.492718 1.052468 0.134 Uiso 0.531(4) 1 calc GR . P B 1 H21B H 1.295807 0.422532 1.065024 0.134 Uiso 0.531(4) 1 calc GR . P B 1 H21C H 1.142884 0.408099 1.061224 0.134 Uiso 0.531(4) 1 calc GR . P B 1 O1C O 0.9132(9) 0.0591(6) 0.5384(7) 0.0465(16) Uani 0.469(4) 1 d D . P B 2 C13C C 0.8621(19) 0.1282(11) 0.5439(5) 0.0528(10) Uani 0.469(4) 1 d D . P B 2 C14C C 0.7756(10) 0.1735(7) 0.6025(5) 0.0607(11) Uani 0.469(4) 1 d D . P B 2 H14C H 0.731727 0.217160 0.586618 0.073 Uiso 0.469(4) 1 calc R . P B 2 H14D H 0.708422 0.130158 0.602105 0.073 Uiso 0.469(4) 1 calc R . P B 2 C15C C 0.8401(8) 0.2182(4) 0.6829(4) 0.0725(14) Uani 0.469(4) 1 d D . P B 2 H15C H 0.773124 0.238704 0.718198 0.087 Uiso 0.469(4) 1 calc R . P B 2 H15D H 0.887776 0.175175 0.697842 0.087 Uiso 0.469(4) 1 calc R . P B 2 C16C C 0.9307(7) 0.2933(5) 0.6950(3) 0.0694(13) Uani 0.469(4) 1 d D . P B 2 H16C H 1.012146 0.270364 0.675469 0.083 Uiso 0.469(4) 1 calc R . P B 2 H16D H 0.894068 0.324081 0.662519 0.083 Uiso 0.469(4) 1 calc R . P B 2 C17C C 0.9621(8) 0.3579(4) 0.7753(3) 0.0735(14) Uani 0.469(4) 1 d D . P B 2 H17C H 1.021536 0.404810 0.774431 0.088 Uiso 0.469(4) 1 calc R . P B 2 H17D H 0.881787 0.384623 0.793299 0.088 Uiso 0.469(4) 1 calc R . P B 2 C18C C 1.0209(11) 0.3257(6) 0.8330(4) 0.0741(15) Uani 0.469(4) 1 d D . P B 2 H18C H 1.091474 0.289289 0.810651 0.089 Uiso 0.469(4) 1 calc R . P B 2 H18D H 0.955217 0.287259 0.841386 0.089 Uiso 0.469(4) 1 calc R . P B 2 C19C C 1.0739(15) 0.3927(6) 0.9099(5) 0.0713(12) Uani 0.469(4) 1 d D . P B 2 H19C H 1.141604 0.430314 0.902097 0.086 Uiso 0.469(4) 1 calc R . P B 2 H19D H 1.004152 0.430067 0.932190 0.086 Uiso 0.469(4) 1 calc R . P B 2 C20C C 1.1292(10) 0.3573(6) 0.9665(4) 0.0729(15) Uani 0.469(4) 1 d D . P B 2 H20C H 1.062578 0.316883 0.971386 0.087 Uiso 0.469(4) 1 calc R . P B 2 H20D H 1.201511 0.322413 0.944818 0.087 Uiso 0.469(4) 1 calc R . P B 2 C21C C 1.1768(18) 0.4211(11) 1.0449(5) 0.089(3) Uani 0.469(4) 1 d D . P B 2 H21D H 1.234192 0.466415 1.041035 0.134 Uiso 0.469(4) 1 calc GR . P B 2 H21E H 1.224291 0.391360 1.074427 0.134 Uiso 0.469(4) 1 calc GR . P B 2 H21F H 1.103656 0.447838 1.071642 0.134 Uiso 0.469(4) 1 calc GR . P B 2 C22B C 0.8998(2) 0.37141(15) 0.32948(13) 0.0253(5) Uani 1 1 d . . . . . C23B C 0.7962(2) 0.31289(14) 0.27862(12) 0.0209(4) Uani 1 1 d . . . . . H23B H 0.813954 0.267414 0.232147 0.025 Uiso 1 1 calc R . . . . C24B C 0.6691(2) 0.32173(14) 0.29639(12) 0.0202(4) Uani 1 1 d . . . . . H24B H 0.602090 0.281540 0.262189 0.024 Uiso 1 1 calc R . . . . C25B C 0.6385(2) 0.39027(14) 0.36518(13) 0.0222(4) Uani 1 1 d . . . . . C26B C 0.7399(2) 0.44753(15) 0.41502(14) 0.0263(5) Uani 1 1 d . . . . . H26B H 0.722075 0.493360 0.461226 0.032 Uiso 1 1 calc R . . . . C27B C 0.8696(2) 0.43804(15) 0.39741(14) 0.0300(5) Uani 1 1 d . . . . . H27B H 0.936713 0.477489 0.432249 0.036 Uiso 1 1 calc R . . . . C28B C 1.0353(2) 0.36057(17) 0.30729(16) 0.0372(6) Uani 1 1 d . . . . . H28B H 1.042076 0.297450 0.274941 0.045 Uiso 1 1 calc R . . . . C29B C 1.1392(2) 0.3874(2) 0.3771(2) 0.0592(10) Uani 1 1 d . . . . . H29A H 1.142029 0.450695 0.406114 0.089 Uiso 1 1 calc GR . . . . H29B H 1.223098 0.371314 0.359091 0.089 Uiso 1 1 calc GR . . . . H29C H 1.119125 0.357453 0.411071 0.089 Uiso 1 1 calc GR . . . . C30B C 1.0539(3) 0.41239(19) 0.2565(2) 0.0519(9) Uani 1 1 d . . . . . H30A H 0.987345 0.392051 0.211431 0.078 Uiso 1 1 calc GR . . . . H30B H 1.139261 0.403712 0.238668 0.078 Uiso 1 1 calc GR . . . . H30C H 1.047021 0.474589 0.286863 0.078 Uiso 1 1 calc GR . . . . C31B C 0.5031(2) 0.39695(16) 0.38555(14) 0.0263(5) Uani 1 1 d . . . . . H31A H 0.461020 0.338231 0.369224 0.040 Uiso 1 1 calc GR . . . . H31B H 0.455141 0.429356 0.358873 0.040 Uiso 1 1 calc GR . . . . H31C H 0.504744 0.427633 0.441884 0.040 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ru1 0.01599(8) 0.01454(8) 0.01388(8) 0.00130(6) 0.00026(6) 0.00220(6) Cl1 0.0173(2) 0.0215(2) 0.0231(2) 0.00397(19) 0.00117(18) 0.00221(18) Cl2 0.0249(2) 0.0239(2) 0.0152(2) 0.00377(18) -0.00096(18) 0.00187(19) S1 0.0215(2) 0.0154(2) 0.0176(2) 0.00241(18) 0.00314(18) 0.00280(18) O1 0.0676(15) 0.0484(13) 0.0461(12) 0.0010(10) 0.0327(11) -0.0155(11) N1 0.0258(9) 0.0188(8) 0.0200(9) 0.0033(7) 0.0071(7) 0.0002(7) N2 0.0351(11) 0.0212(9) 0.0181(9) 0.0020(7) 0.0060(8) 0.0036(8) C2 0.0209(10) 0.0202(10) 0.0184(10) 0.0040(8) 0.0013(8) 0.0035(8) C3 0.0246(10) 0.0145(9) 0.0195(10) 0.0036(8) 0.0045(8) 0.0020(8) C4 0.0229(10) 0.0203(10) 0.0225(10) 0.0050(8) 0.0017(8) 0.0007(8) C5 0.0236(10) 0.0215(10) 0.0284(11) 0.0072(9) 0.0078(9) 0.0050(8) C6 0.0294(11) 0.0201(10) 0.0206(10) 0.0032(8) 0.0072(9) 0.0062(8) C7 0.0269(11) 0.0198(10) 0.0215(10) 0.0036(8) 0.0017(8) 0.0034(8) C8 0.0236(10) 0.0179(10) 0.0220(10) 0.0051(8) 0.0032(8) 0.0030(8) C9 0.0347(13) 0.0328(13) 0.0242(12) -0.0018(10) 0.0000(10) 0.0019(10) C10 0.0311(14) 0.0513(17) 0.0351(14) -0.0050(13) -0.0063(11) -0.0043(12) C11 0.0228(12) 0.0541(18) 0.0424(16) 0.0001(13) 0.0008(11) -0.0006(12) C12 0.0239(11) 0.0328(13) 0.0299(12) 0.0021(10) 0.0045(9) 0.0027(9) C13 0.0427(15) 0.0397(14) 0.0254(12) 0.0074(11) 0.0134(11) 0.0043(12) C14 0.055 0.054 0.027 0.008 0.020 0.018 C15 0.049(2) 0.0377(18) 0.0272(16) 0.0104(14) 0.0118(14) 0.0008(15) C16 0.054(2) 0.043(2) 0.0367(16) 0.0164(16) 0.0065(18) -0.0011(17) C17 0.051(3) 0.061(2) 0.045(2) 0.0230(17) 0.0057(19) 0.007(2) C18 0.051(3) 0.065(2) 0.045(2) 0.0210(17) 0.001(2) 0.002(2) C19 0.054(2) 0.075(3) 0.050(2) 0.021(2) 0.0034(19) 0.005(2) C20 0.063(3) 0.076(3) 0.059(3) 0.016(2) -0.007(2) 0.009(2) C21 0.082(4) 0.092(4) 0.070(4) 0.023(3) -0.009(3) 0.022(4) C15A 0.049(2) 0.0377(18) 0.0272(16) 0.0104(14) 0.0118(14) 0.0008(15) C16A 0.054(2) 0.043(2) 0.0367(16) 0.0164(16) 0.0065(18) -0.0011(17) C17A 0.051(3) 0.061(2) 0.045(2) 0.0230(17) 0.0057(19) 0.007(2) C18A 0.051(3) 0.065(2) 0.045(2) 0.0210(17) 0.001(2) 0.002(2) C19A 0.054(2) 0.075(3) 0.050(2) 0.021(2) 0.0034(19) 0.005(2) C20A 0.063(3) 0.076(3) 0.059(3) 0.016(2) -0.007(2) 0.009(2) C21A 0.082(4) 0.092(4) 0.070(4) 0.023(3) -0.009(3) 0.022(4) C22 0.0173(9) 0.0208(10) 0.0236(10) 0.0067(8) 0.0011(8) 0.0000(8) C23 0.0217(10) 0.0195(10) 0.0211(10) 0.0050(8) 0.0058(8) 0.0030(8) C24 0.0248(10) 0.0205(10) 0.0162(9) 0.0057(8) 0.0015(8) 0.0002(8) C25 0.0216(10) 0.0201(10) 0.0216(10) 0.0095(8) 0.0010(8) 0.0024(8) C26 0.0250(10) 0.0139(9) 0.0222(10) 0.0037(8) 0.0036(8) 0.0026(8) C27 0.0224(10) 0.0162(9) 0.0207(10) 0.0024(8) -0.0006(8) -0.0022(8) C28 0.0202(10) 0.0271(11) 0.0276(11) 0.0046(9) -0.0016(9) 0.0030(8) C29 0.0275(12) 0.0321(13) 0.0318(12) 0.0086(10) -0.0001(10) 0.0079(10) C30 0.0195(11) 0.0341(13) 0.0473(15) 0.0130(12) 0.0031(10) 0.0015(9) C31 0.0254(11) 0.0296(12) 0.0326(12) 0.0145(10) -0.0005(9) 0.0061(9) Ru1B 0.01379(8) 0.02353(9) 0.01462(8) -0.00168(6) -0.00026(6) 0.00467(6) Cl1B 0.0207(3) 0.0601(4) 0.0144(2) -0.0015(2) -0.00053(19) -0.0030(2) Cl2B 0.0267(3) 0.0234(2) 0.0218(2) 0.0053(2) -0.00206(19) 0.0014(2) S1B 0.0424(3) 0.0479(4) 0.0235(3) 0.0156(3) 0.0147(3) 0.0306(3) N1B 0.0485(14) 0.0519(14) 0.0281(11) 0.0173(10) 0.0128(10) 0.0286(11) N2B 0.0523(15) 0.0706(17) 0.0270(11) 0.0254(12) 0.0188(10) 0.0430(13) C2B 0.0468(15) 0.0553(17) 0.0230(12) 0.0167(12) 0.0123(11) 0.0311(13) C3B 0.0333(13) 0.0328(13) 0.0351(13) 0.0137(11) 0.0075(10) 0.0122(10) C4B 0.0356(14) 0.0390(15) 0.0495(16) 0.0198(13) -0.0022(12) 0.0093(11) C5B 0.0259(13) 0.0497(18) 0.115(3) 0.053(2) 0.0146(16) 0.0062(12) C6B 0.0533(18) 0.0432(17) 0.076(2) 0.0375(17) 0.0344(17) 0.0162(14) C7B 0.0575(17) 0.0236(12) 0.0458(15) 0.0181(11) 0.0304(14) 0.0152(11) C8B 0.0460(15) 0.0255(12) 0.0351(13) 0.0134(10) 0.0148(11) 0.0078(10) C9B 0.101(3) 0.0325(15) 0.0462(18) 0.0193(14) 0.0327(19) 0.0248(17) C10B 0.121(4) 0.0355(17) 0.0403(18) 0.0109(14) 0.002(2) 0.000(2) C11B 0.091(3) 0.0400(17) 0.0402(17) 0.0180(14) -0.0149(17) -0.0113(17) C12B 0.0433(15) 0.0398(14) 0.0361(14) 0.0211(12) 0.0054(11) 0.0036(12) O1B 0.050(4) 0.067(4) 0.044(3) 0.040(3) 0.023(3) 0.028(3) C13B 0.060(2) 0.090(2) 0.0222(19) 0.0315(19) 0.0182(19) 0.0440(18) C14B 0.074(3) 0.089(3) 0.024(2) 0.020(2) 0.0227(18) 0.038(2) C15B 0.077(3) 0.090(3) 0.047(3) 0.019(2) 0.013(2) 0.045(3) C16B 0.066(3) 0.076(3) 0.068(3) 0.029(2) 0.008(2) 0.014(3) C17B 0.077(3) 0.074(3) 0.068(3) 0.026(2) 0.008(2) 0.009(3) C18B 0.078(4) 0.072(2) 0.069(2) 0.028(2) -0.002(3) -0.004(3) C19B 0.073(2) 0.083(3) 0.060(2) 0.033(2) 0.0019(18) -0.009(2) C20B 0.077(4) 0.072(3) 0.066(3) 0.025(2) -0.001(3) 0.001(3) C21B 0.100(7) 0.092(4) 0.067(3) 0.030(3) -0.028(3) 0.025(5) O1C 0.050(4) 0.067(4) 0.044(3) 0.040(3) 0.023(3) 0.028(3) C13C 0.060(2) 0.090(2) 0.0222(19) 0.0315(19) 0.0182(19) 0.0440(18) C14C 0.074(3) 0.089(3) 0.024(2) 0.020(2) 0.0227(18) 0.038(2) C15C 0.077(3) 0.090(3) 0.047(3) 0.019(2) 0.013(2) 0.045(3) C16C 0.066(3) 0.076(3) 0.068(3) 0.029(2) 0.008(2) 0.014(3) C17C 0.077(3) 0.074(3) 0.068(3) 0.026(2) 0.008(2) 0.009(3) C18C 0.078(4) 0.072(2) 0.069(2) 0.028(2) -0.002(3) -0.004(3) C19C 0.073(2) 0.083(3) 0.060(2) 0.033(2) 0.0019(18) -0.009(2) C20C 0.077(4) 0.072(3) 0.066(3) 0.025(2) -0.001(3) 0.001(3) C21C 0.100(7) 0.092(4) 0.067(3) 0.030(3) -0.028(3) 0.025(5) C22B 0.0171(10) 0.0229(11) 0.0260(11) -0.0017(9) 0.0048(8) 0.0000(8) C23B 0.0207(10) 0.0189(10) 0.0175(9) 0.0012(8) 0.0021(8) 0.0003(8) C24B 0.0169(9) 0.0209(10) 0.0201(10) 0.0063(8) -0.0023(7) -0.0001(8) C25B 0.0160(9) 0.0228(10) 0.0274(11) 0.0089(9) 0.0032(8) 0.0041(8) C26B 0.0223(11) 0.0206(10) 0.0269(11) -0.0020(9) 0.0069(9) 0.0034(8) C27B 0.0194(10) 0.0248(11) 0.0301(12) -0.0065(9) 0.0035(9) -0.0035(8) C28B 0.0184(11) 0.0323(13) 0.0396(14) -0.0110(11) 0.0105(10) -0.0026(9) C29B 0.0148(12) 0.065(2) 0.0576(19) -0.0188(16) 0.0002(12) -0.0002(12) C30B 0.0416(16) 0.0337(14) 0.065(2) -0.0046(14) 0.0338(15) -0.0080(12) C31B 0.0168(10) 0.0304(12) 0.0325(12) 0.0121(10) 0.0048(9) 0.0071(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cl2 Ru1 Cl1 87.266(19) . . ? S1 Ru1 Cl1 92.693(18) . . ? S1 Ru1 Cl2 90.314(19) . . ? C22 Ru1 Cl1 163.16(6) . . ? C22 Ru1 Cl2 95.09(6) . . ? C22 Ru1 S1 103.95(6) . . ? C22 Ru1 C25 81.57(8) . . ? C22 Ru1 C26 68.51(8) . . ? C23 Ru1 Cl1 145.20(6) . . ? C23 Ru1 Cl2 127.19(6) . . ? C23 Ru1 S1 83.47(6) . . ? C23 Ru1 C22 37.87(8) . . ? C23 Ru1 C24 38.22(8) . . ? C23 Ru1 C25 68.38(8) . . ? C23 Ru1 C26 80.29(8) . . ? C23 Ru1 C27 67.79(8) . . ? C24 Ru1 Cl1 108.11(6) . . ? C24 Ru1 Cl2 163.95(6) . . ? C24 Ru1 S1 93.44(6) . . ? C24 Ru1 C22 68.86(8) . . ? C24 Ru1 C25 37.33(8) . . ? C24 Ru1 C26 67.49(8) . . ? C25 Ru1 Cl1 86.69(6) . . ? C25 Ru1 Cl2 143.78(6) . . ? C25 Ru1 S1 125.62(6) . . ? C26 Ru1 Cl1 94.87(6) . . ? C26 Ru1 Cl2 107.57(6) . . ? C26 Ru1 S1 160.86(6) . . ? C26 Ru1 C25 37.73(8) . . ? C27 Ru1 Cl1 125.80(6) . . ? C27 Ru1 Cl2 87.23(6) . . ? C27 Ru1 S1 141.20(6) . . ? C27 Ru1 C22 38.01(8) . . ? C27 Ru1 C24 80.07(8) . . ? C27 Ru1 C25 67.97(8) . . ? C27 Ru1 C26 37.38(8) . . ? C2 S1 Ru1 115.37(7) . . ? C2 N1 H1 116.8 . . ? C2 N1 C3 126.41(19) . . ? C3 N1 H1 116.8 . . ? C2 N2 H2 116.6 . . ? C2 N2 C13 126.9(2) . . ? C13 N2 H2 116.6 . . ? N1 C2 S1 123.43(16) . . ? N1 C2 N2 116.5(2) . . ? N2 C2 S1 120.06(16) . . ? C4 C3 N1 120.53(19) . . ? C4 C3 C8 121.31(19) . . ? C8 C3 N1 118.10(19) . . ? C3 C4 H4 119.8 . . ? C3 C4 C5 120.4(2) . . ? C5 C4 H4 119.8 . . ? C4 C5 H5 119.8 . . ? C6 C5 C4 120.4(2) . . ? C6 C5 H5 119.8 . . ? C5 C6 H6 119.8 . . ? C5 C6 C7 120.4(2) . . ? C7 C6 H6 119.8 . . ? C6 C7 C8 120.0(2) . . ? C6 C7 C9 121.2(2) . . ? C9 C7 C8 118.8(2) . . ? C3 C8 C7 117.5(2) . . ? C12 C8 C3 123.6(2) . . ? C12 C8 C7 118.9(2) . . ? C7 C9 H9 119.6 . . ? C10 C9 C7 120.7(2) . . ? C10 C9 H9 119.6 . . ? C9 C10 H10 119.8 . . ? C9 C10 C11 120.4(2) . . ? C11 C10 H10 119.8 . . ? C10 C11 H11 119.6 . . ? C12 C11 C10 120.9(3) . . ? C12 C11 H11 119.6 . . ? C8 C12 H12 119.9 . . ? C11 C12 C8 120.3(2) . . ? C11 C12 H12 119.9 . . ? O1 C13 N2 122.2(2) . . ? O1 C13 C14 122.9(3) . . ? N2 C13 C14 114.9(2) . . ? C13 C14 H14E 108.6 . . ? C13 C14 H14F 108.6 . . ? C13 C14 H14G 108.4 . . ? C13 C14 H14H 108.4 . . ? H14E C14 H14F 107.6 . . ? H14G C14 H14H 107.5 . . ? C15 C14 C13 114.5(3) . . ? C15 C14 H14E 108.6 . . ? C15 C14 H14F 108.6 . . ? C15A C14 C13 115.3(4) . . ? C15A C14 H14G 108.4 . . ? C15A C14 H14H 108.4 . . ? C14 C15 H15E 108.0 . . ? C14 C15 H15F 108.0 . . ? C14 C15 C16 117.2(3) . . ? H15E C15 H15F 107.2 . . ? C16 C15 H15E 108.0 . . ? C16 C15 H15F 108.0 . . ? C15 C16 H16E 108.7 . . ? C15 C16 H16F 108.7 . . ? H16E C16 H16F 107.6 . . ? C17 C16 C15 114.3(3) . . ? C17 C16 H16E 108.7 . . ? C17 C16 H16F 108.7 . . ? C16 C17 H17E 108.3 . . ? C16 C17 H17F 108.3 . . ? H17E C17 H17F 107.4 . . ? C18 C17 C16 116.0(3) . . ? C18 C17 H17E 108.3 . . ? C18 C17 H17F 108.3 . . ? C17 C18 H18E 108.6 . . ? C17 C18 H18F 108.6 . . ? C17 C18 C19 114.5(4) . . ? H18E C18 H18F 107.6 . . ? C19 C18 H18E 108.6 . . ? C19 C18 H18F 108.6 . . ? C18 C19 H19E 108.4 . . ? C18 C19 H19F 108.4 . . ? H19E C19 H19F 107.4 . . ? C20 C19 C18 115.6(4) . . ? C20 C19 H19E 108.4 . . ? C20 C19 H19F 108.4 . . ? C19 C20 H20E 108.6 . . ? C19 C20 H20F 108.6 . . ? C19 C20 C21 114.7(4) . . ? H20E C20 H20F 107.6 . . ? C21 C20 H20E 108.6 . . ? C21 C20 H20F 108.6 . . ? C20 C21 H21G 109.5 . . ? C20 C21 H21H 109.5 . . ? C20 C21 H21I 109.5 . . ? H21G C21 H21H 109.5 . . ? H21G C21 H21I 109.5 . . ? H21H C21 H21I 109.5 . . ? C14 C15A H15G 107.4 . . ? C14 C15A H15H 107.4 . . ? C14 C15A C16A 119.7(6) . . ? H15G C15A H15H 106.9 . . ? C16A C15A H15G 107.4 . . ? C16A C15A H15H 107.4 . . ? C15A C16A H16G 108.5 . . ? C15A C16A H16H 108.5 . . ? H16G C16A H16H 107.5 . . ? C17A C16A C15A 115.2(5) . . ? C17A C16A H16G 108.5 . . ? C17A C16A H16H 108.5 . . ? C16A C17A H17G 108.6 . . ? C16A C17A H17H 108.6 . . ? C16A C17A C18A 114.8(5) . . ? H17G C17A H17H 107.5 . . ? C18A C17A H17G 108.6 . . ? C18A C17A H17H 108.6 . . ? C17A C18A H18G 108.7 . . ? C17A C18A H18H 108.7 . . ? C17A C18A C19A 114.2(5) . . ? H18G C18A H18H 107.6 . . ? C19A C18A H18G 108.7 . . ? C19A C18A H18H 108.7 . . ? C18A C19A H19G 108.9 . . ? C18A C19A H19H 108.9 . . ? H19G C19A H19H 107.7 . . ? C20A C19A C18A 113.3(5) . . ? C20A C19A H19G 108.9 . . ? C20A C19A H19H 108.9 . . ? C19A C20A H20G 108.9 . . ? C19A C20A H20H 108.9 . . ? C19A C20A C21A 113.5(5) . . ? H20G C20A H20H 107.7 . . ? C21A C20A H20G 108.9 . . ? C21A C20A H20H 108.9 . . ? C20A C21A H21J 109.5 . . ? C20A C21A H21K 109.5 . . ? C20A C21A H21L 109.5 . . ? H21J C21A H21K 109.5 . . ? H21J C21A H21L 109.5 . . ? H21K C21A H21L 109.5 . . ? C23 C22 Ru1 69.58(12) . . ? C23 C22 C27 116.74(19) . . ? C23 C22 C28 122.30(19) . . ? C27 C22 Ru1 70.11(12) . . ? C27 C22 C28 120.96(19) . . ? C28 C22 Ru1 131.43(16) . . ? Ru1 C23 H23 128.8 . . ? C22 C23 Ru1 72.54(12) . . ? C22 C23 H23 119.1 . . ? C22 C23 C24 121.81(19) . . ? C24 C23 Ru1 71.99(12) . . ? C24 C23 H23 119.1 . . ? Ru1 C24 H24 130.9 . . ? C23 C24 Ru1 69.79(12) . . ? C23 C24 H24 119.9 . . ? C25 C24 Ru1 72.13(12) . . ? C25 C24 C23 120.26(19) . . ? C25 C24 H24 119.9 . . ? C24 C25 Ru1 70.53(12) . . ? C24 C25 C26 118.73(19) . . ? C24 C25 C31 120.7(2) . . ? C26 C25 Ru1 70.76(12) . . ? C26 C25 C31 120.55(19) . . ? C31 C25 Ru1 130.35(16) . . ? Ru1 C26 H26 130.9 . . ? C25 C26 Ru1 71.51(12) . . ? C25 C26 H26 119.9 . . ? C27 C26 Ru1 70.36(12) . . ? C27 C26 C25 120.18(19) . . ? C27 C26 H26 119.9 . . ? Ru1 C27 H27 129.6 . . ? C22 C27 Ru1 71.88(12) . . ? C22 C27 H27 118.9 . . ? C26 C27 Ru1 72.26(12) . . ? C26 C27 C22 122.27(19) . . ? C26 C27 H27 118.9 . . ? C22 C28 H28 108.0 . . ? C22 C28 C29 113.20(19) . . ? C22 C28 C30 108.7(2) . . ? C29 C28 H28 108.0 . . ? C29 C28 C30 110.8(2) . . ? C30 C28 H28 108.0 . . ? C28 C29 H29D 109.5 . . ? C28 C29 H29E 109.5 . . ? C28 C29 H29F 109.5 . . ? H29D C29 H29E 109.5 . . ? H29D C29 H29F 109.5 . . ? H29E C29 H29F 109.5 . . ? C28 C30 H30D 109.5 . . ? C28 C30 H30E 109.5 . . ? C28 C30 H30F 109.5 . . ? H30D C30 H30E 109.5 . . ? H30D C30 H30F 109.5 . . ? H30E C30 H30F 109.5 . . ? C25 C31 H31D 109.5 . . ? C25 C31 H31E 109.5 . . ? C25 C31 H31F 109.5 . . ? H31D C31 H31E 109.5 . . ? H31D C31 H31F 109.5 . . ? H31E C31 H31F 109.5 . . ? Cl1B Ru1B Cl2B 89.73(2) . . ? S1B Ru1B Cl1B 90.49(2) . . ? S1B Ru1B Cl2B 90.92(2) . . ? C22B Ru1B Cl1B 114.19(6) . . ? C22B Ru1B Cl2B 156.08(6) . . ? C22B Ru1B S1B 89.06(6) . . ? C22B Ru1B C25B 81.59(8) . . ? C23B Ru1B Cl1B 152.45(6) . . ? C23B Ru1B Cl2B 117.82(6) . . ? C23B Ru1B S1B 88.53(6) . . ? C23B Ru1B C22B 38.27(8) . . ? C23B Ru1B C24B 37.60(8) . . ? C23B Ru1B C25B 68.43(8) . . ? C23B Ru1B C26B 80.32(8) . . ? C24B Ru1B Cl1B 154.64(6) . . ? C24B Ru1B Cl2B 89.72(6) . . ? C24B Ru1B S1B 114.87(6) . . ? C24B Ru1B C22B 68.74(8) . . ? C24B Ru1B C25B 38.06(8) . . ? C24B Ru1B C26B 67.67(8) . . ? C25B Ru1B Cl1B 116.59(6) . . ? C25B Ru1B Cl2B 87.69(6) . . ? C25B Ru1B S1B 152.87(6) . . ? C26B Ru1B Cl1B 89.47(7) . . ? C26B Ru1B Cl2B 113.73(6) . . ? C26B Ru1B S1B 155.34(6) . . ? C26B Ru1B C22B 68.59(8) . . ? C26B Ru1B C25B 37.21(8) . . ? C27B Ru1B Cl1B 88.23(7) . . ? C27B Ru1B Cl2B 151.89(6) . . ? C27B Ru1B S1B 117.12(6) . . ? C27B Ru1B C22B 37.55(8) . . ? C27B Ru1B C23B 67.94(8) . . ? C27B Ru1B C24B 80.50(9) . . ? C27B Ru1B C25B 68.38(9) . . ? C27B Ru1B C26B 38.23(8) . . ? C2B S1B Ru1B 114.75(9) . . ? C2B N1B H1B 117.2 . . ? C2B N1B C3B 125.6(2) . . ? C3B N1B H1B 117.2 . . ? C2B N2B H2B 115.6 . . ? C2B N2B H2BA 115.3 . . ? C2B N2B C13C 129.5(5) . . ? C13B N2B H2B 115.6 . . ? C13B N2B C2B 128.8(4) . . ? C13C N2B H2BA 115.3 . . ? N1B C2B S1B 121.4(2) . . ? N1B C2B N2B 116.9(2) . . ? N2B C2B S1B 121.7(2) . . ? C4B C3B N1B 119.6(3) . . ? C4B C3B C8B 121.0(3) . . ? C8B C3B N1B 119.0(2) . . ? C3B C4B H4B 119.2 . . ? C3B C4B C5B 121.6(3) . . ? C5B C4B H4B 119.2 . . ? C4B C5B H5B 120.6 . . ? C6B C5B C4B 118.9(3) . . ? C6B C5B H5B 120.6 . . ? C5B C6B H6B 119.9 . . ? C7B C6B C5B 120.3(3) . . ? C7B C6B H6B 119.9 . . ? C6B C7B C8B 120.3(3) . . ? C6B C7B C9B 123.6(3) . . ? C8B C7B C9B 116.1(3) . . ? C3B C8B C7B 117.9(3) . . ? C3B C8B C12B 123.5(2) . . ? C7B C8B C12B 118.5(3) . . ? C7B C9B H9B 118.4 . . ? C10B C9B C7B 123.2(3) . . ? C10B C9B H9B 118.4 . . ? C9B C10B H10B 120.3 . . ? C9B C10B C11B 119.4(3) . . ? C11B C10B H10B 120.3 . . ? C10B C11B H11B 118.6 . . ? C12B C11B C10B 122.8(4) . . ? C12B C11B H11B 118.6 . . ? C8B C12B H12B 120.1 . . ? C11B C12B C8B 119.9(3) . . ? C11B C12B H12B 120.1 . . ? N2B C13B C14B 117.8(8) . . ? O1B C13B N2B 119.7(11) . . ? O1B C13B C14B 120.7(9) . . ? C13B C14B H14A 108.1 . . ? C13B C14B H14B 108.1 . . ? H14A C14B H14B 107.3 . . ? C15B C14B C13B 116.8(5) . . ? C15B C14B H14A 108.1 . . ? C15B C14B H14B 108.1 . . ? C14B C15B H15A 107.7 . . ? C14B C15B H15B 107.7 . . ? C14B C15B C16B 118.5(5) . . ? H15A C15B H15B 107.1 . . ? C16B C15B H15A 107.7 . . ? C16B C15B H15B 107.7 . . ? C15B C16B H16A 108.4 . . ? C15B C16B H16B 108.4 . . ? C15B C16B C17B 115.6(4) . . ? H16A C16B H16B 107.4 . . ? C17B C16B H16A 108.4 . . ? C17B C16B H16B 108.4 . . ? C16B C17B H17A 108.2 . . ? C16B C17B H17B 108.2 . . ? H17A C17B H17B 107.4 . . ? C18B C17B C16B 116.3(4) . . ? C18B C17B H17A 108.2 . . ? C18B C17B H17B 108.2 . . ? C17B C18B H18A 108.3 . . ? C17B C18B H18B 108.3 . . ? C17B C18B C19B 115.9(5) . . ? H18A C18B H18B 107.4 . . ? C19B C18B H18A 108.3 . . ? C19B C18B H18B 108.3 . . ? C18B C19B H19A 108.3 . . ? C18B C19B H19B 108.3 . . ? H19A C19B H19B 107.4 . . ? C20B C19B C18B 115.8(5) . . ? C20B C19B H19A 108.3 . . ? C20B C19B H19B 108.3 . . ? C19B C20B H20A 108.1 . . ? C19B C20B H20B 108.1 . . ? C19B C20B C21B 116.9(5) . . ? H20A C20B H20B 107.3 . . ? C21B C20B H20A 108.1 . . ? C21B C20B H20B 108.1 . . ? C20B C21B H21A 109.5 . . ? C20B C21B H21B 109.5 . . ? C20B C21B H21C 109.5 . . ? H21A C21B H21B 109.5 . . ? H21A C21B H21C 109.5 . . ? H21B C21B H21C 109.5 . . ? N2B C13C C14C 113.2(8) . . ? O1C C13C N2B 120.8(8) . . ? O1C C13C C14C 124.7(13) . . ? C13C C14C H14C 108.5 . . ? C13C C14C H14D 108.5 . . ? H14C C14C H14D 107.5 . . ? C15C C14C C13C 115.1(5) . . ? C15C C14C H14C 108.5 . . ? C15C C14C H14D 108.5 . . ? C14C C15C H15C 108.6 . . ? C14C C15C H15D 108.6 . . ? H15C C15C H15D 107.5 . . ? C16C C15C C14C 114.9(5) . . ? C16C C15C H15C 108.6 . . ? C16C C15C H15D 108.6 . . ? C15C C16C H16C 108.0 . . ? C15C C16C H16D 108.0 . . ? H16C C16C H16D 107.3 . . ? C17C C16C C15C 117.0(4) . . ? C17C C16C H16C 108.0 . . ? C17C C16C H16D 108.0 . . ? C16C C17C H17C 108.1 . . ? C16C C17C H17D 108.1 . . ? H17C C17C H17D 107.3 . . ? C18C C17C C16C 116.8(4) . . ? C18C C17C H17C 108.1 . . ? C18C C17C H17D 108.1 . . ? C17C C18C H18C 108.1 . . ? C17C C18C H18D 108.1 . . ? C17C C18C C19C 116.6(5) . . ? H18C C18C H18D 107.3 . . ? C19C C18C H18C 108.1 . . ? C19C C18C H18D 108.1 . . ? C18C C19C H19C 108.6 . . ? C18C C19C H19D 108.6 . . ? H19C C19C H19D 107.6 . . ? C20C C19C C18C 114.6(5) . . ? C20C C19C H19C 108.6 . . ? C20C C19C H19D 108.6 . . ? C19C C20C H20C 108.1 . . ? C19C C20C H20D 108.1 . . ? H20C C20C H20D 107.3 . . ? C21C C20C C19C 116.8(5) . . ? C21C C20C H20C 108.1 . . ? C21C C20C H20D 108.1 . . ? C20C C21C H21D 109.5 . . ? C20C C21C H21E 109.5 . . ? C20C C21C H21F 109.5 . . ? H21D C21C H21E 109.5 . . ? H21D C21C H21F 109.5 . . ? H21E C21C H21F 109.5 . . ? C23B C22B Ru1B 70.22(13) . . ? C23B C22B C28B 119.21(19) . . ? C27B C22B Ru1B 70.43(14) . . ? C27B C22B C23B 117.83(19) . . ? C27B C22B C28B 122.9(2) . . ? C28B C22B Ru1B 131.94(19) . . ? Ru1B C23B H23B 130.4 . . ? C22B C23B Ru1B 71.52(13) . . ? C22B C23B H23B 119.5 . . ? C24B C23B Ru1B 71.20(12) . . ? C24B C23B C22B 120.95(19) . . ? C24B C23B H23B 119.5 . . ? Ru1B C24B H24B 129.5 . . ? C23B C24B Ru1B 71.20(12) . . ? C23B C24B H24B 119.5 . . ? C23B C24B C25B 121.07(19) . . ? C25B C24B Ru1B 72.30(12) . . ? C25B C24B H24B 119.5 . . ? C24B C25B Ru1B 69.64(12) . . ? C24B C25B C31B 120.73(19) . . ? C26B C25B Ru1B 70.41(13) . . ? C26B C25B C24B 117.96(19) . . ? C26B C25B C31B 121.2(2) . . ? C31B C25B Ru1B 128.32(16) . . ? Ru1B C26B H26B 130.4 . . ? C25B C26B Ru1B 72.38(13) . . ? C25B C26B H26B 119.5 . . ? C25B C26B C27B 121.0(2) . . ? C27B C26B Ru1B 70.39(14) . . ? C27B C26B H26B 119.5 . . ? Ru1B C27B H27B 129.7 . . ? C22B C27B Ru1B 72.02(14) . . ? C22B C27B C26B 121.2(2) . . ? C22B C27B H27B 119.4 . . ? C26B C27B Ru1B 71.38(14) . . ? C26B C27B H27B 119.4 . . ? C22B C28B H28B 107.9 . . ? C22B C28B C29B 113.4(2) . . ? C22B C28B C30B 107.7(2) . . ? C29B C28B H28B 107.9 . . ? C29B C28B C30B 111.8(3) . . ? C30B C28B H28B 107.9 . . ? C28B C29B H29A 109.5 . . ? C28B C29B H29B 109.5 . . ? C28B C29B H29C 109.5 . . ? H29A C29B H29B 109.5 . . ? H29A C29B H29C 109.5 . . ? H29B C29B H29C 109.5 . . ? C28B C30B H30A 109.5 . . ? C28B C30B H30B 109.5 . . ? C28B C30B H30C 109.5 . . ? H30A C30B H30B 109.5 . . ? H30A C30B H30C 109.5 . . ? H30B C30B H30C 109.5 . . ? C25B C31B H31A 109.5 . . ? C25B C31B H31B 109.5 . . ? C25B C31B H31C 109.5 . . ? H31A C31B H31B 109.5 . . ? H31A C31B H31C 109.5 . . ? H31B C31B H31C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ru1 Cl1 2.4310(6) . ? Ru1 Cl2 2.4280(6) . ? Ru1 S1 2.4205(6) . ? Ru1 C22 2.201(2) . ? Ru1 C23 2.162(2) . ? Ru1 C24 2.191(2) . ? Ru1 C25 2.212(2) . ? Ru1 C26 2.202(2) . ? Ru1 C27 2.178(2) . ? S1 C2 1.698(2) . ? O1 C13 1.216(3) . ? N1 H1 0.8800 . ? N1 C2 1.332(3) . ? N1 C3 1.426(3) . ? N2 H2 0.8800 . ? N2 C2 1.369(3) . ? N2 C13 1.382(3) . ? C3 C4 1.364(3) . ? C3 C8 1.423(3) . ? C4 H4 0.9500 . ? C4 C5 1.408(3) . ? C5 H5 0.9500 . ? C5 C6 1.367(3) . ? C6 H6 0.9500 . ? C6 C7 1.411(3) . ? C7 C8 1.428(3) . ? C7 C9 1.423(3) . ? C8 C12 1.418(3) . ? C9 H9 0.9500 . ? C9 C10 1.359(4) . ? C10 H10 0.9500 . ? C10 C11 1.409(4) . ? C11 H11 0.9500 . ? C11 C12 1.369(4) . ? C12 H12 0.9500 . ? C13 C14 1.510(3) . ? C14 H14E 0.9900 . ? C14 H14F 0.9900 . ? C14 H14G 0.9900 . ? C14 H14H 0.9900 . ? C14 C15 1.482(5) . ? C14 C15A 1.424(8) . ? C15 H15E 0.9900 . ? C15 H15F 0.9900 . ? C15 C16 1.500(3) . ? C16 H16E 0.9900 . ? C16 H16F 0.9900 . ? C16 C17 1.496(3) . ? C17 H17E 0.9900 . ? C17 H17F 0.9900 . ? C17 C18 1.489(3) . ? C18 H18E 0.9900 . ? C18 H18F 0.9900 . ? C18 C19 1.495(4) . ? C19 H19E 0.9900 . ? C19 H19F 0.9900 . ? C19 C20 1.489(3) . ? C20 H20E 0.9900 . ? C20 H20F 0.9900 . ? C20 C21 1.490(4) . ? C21 H21G 0.9800 . ? C21 H21H 0.9800 . ? C21 H21I 0.9800 . ? C15A H15G 0.9900 . ? C15A H15H 0.9900 . ? C15A C16A 1.492(4) . ? C16A H16G 0.9900 . ? C16A H16H 0.9900 . ? C16A C17A 1.489(4) . ? C17A H17G 0.9900 . ? C17A H17H 0.9900 . ? C17A C18A 1.491(4) . ? C18A H18G 0.9900 . ? C18A H18H 0.9900 . ? C18A C19A 1.496(4) . ? C19A H19G 0.9900 . ? C19A H19H 0.9900 . ? C19A C20A 1.495(4) . ? C20A H20G 0.9900 . ? C20A H20H 0.9900 . ? C20A C21A 1.496(4) . ? C21A H21J 0.9800 . ? C21A H21K 0.9800 . ? C21A H21L 0.9800 . ? C22 C23 1.416(3) . ? C22 C27 1.426(3) . ? C22 C28 1.518(3) . ? C23 H23 0.9500 . ? C23 C24 1.426(3) . ? C24 H24 0.9500 . ? C24 C25 1.409(3) . ? C25 C26 1.427(3) . ? C25 C31 1.504(3) . ? C26 H26 0.9500 . ? C26 C27 1.404(3) . ? C27 H27 0.9500 . ? C28 H28 1.0000 . ? C28 C29 1.519(3) . ? C28 C30 1.544(3) . ? C29 H29D 0.9800 . ? C29 H29E 0.9800 . ? C29 H29F 0.9800 . ? C30 H30D 0.9800 . ? C30 H30E 0.9800 . ? C30 H30F 0.9800 . ? C31 H31D 0.9800 . ? C31 H31E 0.9800 . ? C31 H31F 0.9800 . ? Ru1B Cl1B 2.4178(6) . ? Ru1B Cl2B 2.4481(6) . ? Ru1B S1B 2.4159(6) . ? Ru1B C22B 2.192(2) . ? Ru1B C23B 2.175(2) . ? Ru1B C24B 2.175(2) . ? Ru1B C25B 2.210(2) . ? Ru1B C26B 2.184(2) . ? Ru1B C27B 2.171(3) . ? S1B C2B 1.698(3) . ? N1B H1B 0.8800 . ? N1B C2B 1.330(3) . ? N1B C3B 1.438(3) . ? N2B H2B 0.8800 . ? N2B H2BA 0.8800 . ? N2B C2B 1.360(3) . ? N2B C13B 1.317(14) . ? N2B C13C 1.452(15) . ? C3B C4B 1.345(4) . ? C3B C8B 1.406(4) . ? C4B H4B 0.9500 . ? C4B C5B 1.410(5) . ? C5B H5B 0.9500 . ? C5B C6B 1.389(5) . ? C6B H6B 0.9500 . ? C6B C7B 1.389(5) . ? C7B C8B 1.429(3) . ? C7B C9B 1.433(5) . ? C8B C12B 1.443(4) . ? C9B H9B 0.9500 . ? C9B C10B 1.349(6) . ? C10B H10B 0.9500 . ? C10B C11B 1.352(6) . ? C11B H11B 0.9500 . ? C11B C12B 1.352(4) . ? C12B H12B 0.9500 . ? O1B C13B 1.251(7) . ? C13B C14B 1.481(4) . ? C14B H14A 0.9900 . ? C14B H14B 0.9900 . ? C14B C15B 1.459(4) . ? C15B H15A 0.9900 . ? C15B H15B 0.9900 . ? C15B C16B 1.469(4) . ? C16B H16A 0.9900 . ? C16B H16B 0.9900 . ? C16B C17B 1.476(4) . ? C17B H17A 0.9900 . ? C17B H17B 0.9900 . ? C17B C18B 1.472(4) . ? C18B H18A 0.9900 . ? C18B H18B 0.9900 . ? C18B C19B 1.482(4) . ? C19B H19A 0.9900 . ? C19B H19B 0.9900 . ? C19B C20B 1.470(4) . ? C20B H20A 0.9900 . ? C20B H20B 0.9900 . ? C20B C21B 1.472(4) . ? C21B H21A 0.9800 . ? C21B H21B 0.9800 . ? C21B H21C 0.9800 . ? O1C C13C 1.253(7) . ? C13C C14C 1.483(4) . ? C14C H14C 0.9900 . ? C14C H14D 0.9900 . ? C14C C15C 1.480(4) . ? C15C H15C 0.9900 . ? C15C H15D 0.9900 . ? C15C C16C 1.477(4) . ? C16C H16C 0.9900 . ? C16C H16D 0.9900 . ? C16C C17C 1.474(4) . ? C17C H17C 0.9900 . ? C17C H17D 0.9900 . ? C17C C18C 1.468(4) . ? C18C H18C 0.9900 . ? C18C H18D 0.9900 . ? C18C C19C 1.483(4) . ? C19C H19C 0.9900 . ? C19C H19D 0.9900 . ? C19C C20C 1.475(4) . ? C20C H20C 0.9900 . ? C20C H20D 0.9900 . ? C20C C21C 1.471(4) . ? C21C H21D 0.9800 . ? C21C H21E 0.9800 . ? C21C H21F 0.9800 . ? C22B C23B 1.431(3) . ? C22B C27B 1.404(3) . ? C22B C28B 1.513(3) . ? C23B H23B 0.9500 . ? C23B C24B 1.402(3) . ? C24B H24B 0.9500 . ? C24B C25B 1.430(3) . ? C25B C26B 1.402(3) . ? C25B C31B 1.499(3) . ? C26B H26B 0.9500 . ? C26B C27B 1.426(3) . ? C27B H27B 0.9500 . ? C28B H28B 1.0000 . ? C28B C29B 1.526(4) . ? C28B C30B 1.530(5) . ? C29B H29A 0.9800 . ? C29B H29B 0.9800 . ? C29B H29C 0.9800 . ? C30B H30A 0.9800 . ? C30B H30B 0.9800 . ? C30B H30C 0.9800 . ? C31B H31A 0.9800 . ? C31B H31B 0.9800 . ? C31B H31C 0.9800 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag N1 H1 O1 0.88 1.92 2.609(3) 134.1 . yes N2 H2 Cl2 0.88 2.34 3.189(2) 161.1 . yes N1B H1B O1B 0.88 1.92 2.587(10) 131.9 . yes N1B H1B O1B 0.88 2.37 3.082(9) 138.1 2_756 yes N1B H1B O1C 0.88 2.04 2.750(11) 136.8 . yes N1B H1B O1C 0.88 2.11 2.820(11) 137.6 2_756 yes N2B H2B Cl1B 0.88 2.54 3.117(3) 123.9 . yes N2B H2BA Cl2B 0.88 2.33 3.099(2) 146.5 . yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Ru1 S1 C2 N1 -160.76(16) . . . . ? Ru1 S1 C2 N2 18.9(2) . . . . ? Ru1 C22 C23 C24 -54.80(19) . . . . ? Ru1 C22 C27 C26 54.14(19) . . . . ? Ru1 C22 C28 C29 -36.8(3) . . . . ? Ru1 C22 C28 C30 -160.28(17) . . . . ? Ru1 C23 C24 C25 -53.60(18) . . . . ? Ru1 C24 C25 C26 -53.68(18) . . . . ? Ru1 C24 C25 C31 126.1(2) . . . . ? Ru1 C25 C26 C27 -52.81(18) . . . . ? Ru1 C26 C27 C22 -53.97(19) . . . . ? O1 C13 C14 C15 -120.5(4) . . . . ? O1 C13 C14 C15A -56.6(5) . . . . ? N1 C3 C4 C5 179.7(2) . . . . ? N1 C3 C8 C7 179.49(19) . . . . ? N1 C3 C8 C12 -0.5(3) . . . . ? N2 C13 C14 C15 60.3(4) . . . . ? N2 C13 C14 C15A 124.2(4) . . . . ? C2 N1 C3 C4 -54.7(3) . . . . ? C2 N1 C3 C8 128.1(2) . . . . ? C2 N2 C13 O1 -9.1(4) . . . . ? C2 N2 C13 C14 170.1(2) . . . . ? C3 N1 C2 S1 1.0(3) . . . . ? C3 N1 C2 N2 -178.8(2) . . . . ? C3 C4 C5 C6 1.6(3) . . . . ? C3 C8 C12 C11 179.7(3) . . . . ? C4 C3 C8 C7 2.3(3) . . . . ? C4 C3 C8 C12 -177.6(2) . . . . ? C4 C5 C6 C7 0.8(3) . . . . ? C5 C6 C7 C8 -1.6(3) . . . . ? C5 C6 C7 C9 179.0(2) . . . . ? C6 C7 C8 C3 0.1(3) . . . . ? C6 C7 C8 C12 -180.0(2) . . . . ? C6 C7 C9 C10 -179.5(3) . . . . ? C7 C8 C12 C11 -0.2(4) . . . . ? C7 C9 C10 C11 -0.8(5) . . . . ? C8 C3 C4 C5 -3.2(3) . . . . ? C8 C7 C9 C10 1.1(4) . . . . ? C9 C7 C8 C3 179.5(2) . . . . ? C9 C7 C8 C12 -0.5(3) . . . . ? C9 C10 C11 C12 0.0(5) . . . . ? C10 C11 C12 C8 0.5(5) . . . . ? C13 N2 C2 S1 -164.7(2) . . . . ? C13 N2 C2 N1 15.0(3) . . . . ? C13 C14 C15 C16 53.1(5) . . . . ? C13 C14 C15A C16A -50.8(7) . . . . ? C14 C15 C16 C17 -165.8(3) . . . . ? C14 C15A C16A C17A -74.3(9) . . . . ? C15 C16 C17 C18 -65.2(6) . . . . ? C16 C17 C18 C19 177.7(4) . . . . ? C17 C18 C19 C20 176.3(5) . . . . ? C18 C19 C20 C21 67.2(7) . . . . ? C15A C16A C17A C18A -72.0(11) . . . . ? C16A C17A C18A C19A -178.2(9) . . . . ? C17A C18A C19A C20A 178.5(11) . . . . ? C18A C19A C20A C21A 177.4(12) . . . . ? C22 C23 C24 Ru1 55.05(19) . . . . ? C22 C23 C24 C25 1.4(3) . . . . ? C23 C22 C27 Ru1 -53.29(17) . . . . ? C23 C22 C27 C26 0.8(3) . . . . ? C23 C22 C28 C29 53.7(3) . . . . ? C23 C22 C28 C30 -69.9(3) . . . . ? C23 C24 C25 Ru1 52.53(18) . . . . ? C23 C24 C25 C26 -1.2(3) . . . . ? C23 C24 C25 C31 178.6(2) . . . . ? C24 C25 C26 Ru1 53.58(18) . . . . ? C24 C25 C26 C27 0.8(3) . . . . ? C25 C26 C27 Ru1 53.34(18) . . . . ? C25 C26 C27 C22 -0.6(3) . . . . ? C27 C22 C23 Ru1 53.55(17) . . . . ? C27 C22 C23 C24 -1.2(3) . . . . ? C27 C22 C28 C29 -126.8(2) . . . . ? C27 C22 C28 C30 109.7(2) . . . . ? C28 C22 C23 Ru1 -126.9(2) . . . . ? C28 C22 C23 C24 178.3(2) . . . . ? C28 C22 C27 Ru1 127.1(2) . . . . ? C28 C22 C27 C26 -178.7(2) . . . . ? C31 C25 C26 Ru1 -126.2(2) . . . . ? C31 C25 C26 C27 -179.0(2) . . . . ? Ru1B S1B C2B N1B -173.0(2) . . . . ? Ru1B S1B C2B N2B 6.3(3) . . . . ? Ru1B C22B C23B C24B 53.37(19) . . . . ? Ru1B C22B C27B C26B -53.9(2) . . . . ? Ru1B C22B C28B C29B -59.6(3) . . . . ? Ru1B C22B C28B C30B 176.13(18) . . . . ? Ru1B C23B C24B C25B 54.54(19) . . . . ? Ru1B C24B C25B C26B 52.99(19) . . . . ? Ru1B C24B C25B C31B -123.3(2) . . . . ? Ru1B C25B C26B C27B 53.0(2) . . . . ? Ru1B C26B C27B C22B 54.2(2) . . . . ? N1B C3B C4B C5B 172.8(3) . . . . ? N1B C3B C8B C7B -172.5(2) . . . . ? N1B C3B C8B C12B 6.8(4) . . . . ? N2B C13B C14B C15B -87.8(14) . . . . ? N2B C13C C14C C15C -120.9(12) . . . . ? C2B N1B C3B C4B 106.3(3) . . . . ? C2B N1B C3B C8B -80.9(4) . . . . ? C2B N2B C13B O1B 19(2) . . . . ? C2B N2B C13B C14B -176.4(6) . . . . ? C2B N2B C13C O1C -21(2) . . . . ? C2B N2B C13C C14C 171.6(6) . . . . ? C3B N1B C2B S1B 1.5(5) . . . . ? C3B N1B C2B N2B -177.8(3) . . . . ? C3B C4B C5B C6B -1.3(4) . . . . ? C3B C8B C12B C11B 179.6(3) . . . . ? C4B C3B C8B C7B 0.1(4) . . . . ? C4B C3B C8B C12B 179.5(3) . . . . ? C4B C5B C6B C7B 2.1(4) . . . . ? C5B C6B C7B C8B -1.8(4) . . . . ? C5B C6B C7B C9B 178.1(3) . . . . ? C6B C7B C8B C3B 0.7(4) . . . . ? C6B C7B C8B C12B -178.7(2) . . . . ? C6B C7B C9B C10B 179.1(3) . . . . ? C7B C8B C12B C11B -1.0(4) . . . . ? C7B C9B C10B C11B 0.3(5) . . . . ? C8B C3B C4B C5B 0.2(4) . . . . ? C8B C7B C9B C10B -1.0(4) . . . . ? C9B C7B C8B C3B -179.3(2) . . . . ? C9B C7B C8B C12B 1.3(4) . . . . ? C9B C10B C11B C12B 0.2(5) . . . . ? C10B C11B C12B C8B 0.2(5) . . . . ? O1B C13B C14B C15B 76.9(17) . . . . ? C13B N2B C2B S1B -178.9(10) . . . . ? C13B N2B C2B N1B 0.4(11) . . . . ? C13B C14B C15B C16B -48.0(13) . . . . ? C14B C15B C16B C17B -166.4(9) . . . . ? C15B C16B C17B C18B -169.9(9) . . . . ? C16B C17B C18B C19B -169.6(9) . . . . ? C17B C18B C19B C20B 168.9(10) . . . . ? C18B C19B C20B C21B -173.1(11) . . . . ? O1C C13C C14C C15C 72(2) . . . . ? C13C N2B C2B S1B -173.2(11) . . . . ? C13C N2B C2B N1B 6.1(12) . . . . ? C13C C14C C15C C16C 66.3(14) . . . . ? C14C C15C C16C C17C 159.1(8) . . . . ? C15C C16C C17C C18C 59.3(11) . . . . ? C16C C17C C18C C19C 169.3(10) . . . . ? C17C C18C C19C C20C 178.6(11) . . . . ? C18C C19C C20C C21C -176.9(13) . . . . ? C22B C23B C24B Ru1B -53.5(2) . . . . ? C22B C23B C24B C25B 1.0(3) . . . . ? C23B C22B C27B Ru1B 53.6(2) . . . . ? C23B C22B C27B C26B -0.4(4) . . . . ? C23B C22B C28B C29B -148.5(3) . . . . ? C23B C22B C28B C30B 87.2(3) . . . . ? C23B C24B C25B Ru1B -54.04(19) . . . . ? C23B C24B C25B C26B -1.0(3) . . . . ? C23B C24B C25B C31B -177.3(2) . . . . ? C24B C25B C26B Ru1B -52.62(18) . . . . ? C24B C25B C26B C27B 0.4(4) . . . . ? C25B C26B C27B Ru1B -53.9(2) . . . . ? C25B C26B C27B C22B 0.3(4) . . . . ? C27B C22B C23B Ru1B -53.7(2) . . . . ? C27B C22B C23B C24B -0.3(4) . . . . ? C27B C22B C28B C29B 33.0(4) . . . . ? C27B C22B C28B C30B -91.2(3) . . . . ? C28B C22B C23B Ru1B 127.8(2) . . . . ? C28B C22B C23B C24B -178.8(2) . . . . ? C28B C22B C27B Ru1B -127.9(3) . . . . ? C28B C22B C27B C26B 178.1(3) . . . . ? C31B C25B C26B Ru1B 123.6(2) . . . . ? C31B C25B C26B C27B 176.6(2) . . . . ?