#------------------------------------------------------------------------------ #$Date: 2021-10-16 01:59:07 +0300 (Sat, 16 Oct 2021) $ #$Revision: 269973 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/85/7708577.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708577 loop_ _publ_author_name 'Swaminathan, Srividya' 'Haribabu, Jebiti' 'Mohamed Kasim, Mohamed Subarkhan' 'dasararaju, gayathri' 'Balakrishnan, Nithya' 'Bhuvanesh, Nattamai' 'Echeverria, Cesar' 'Karvembu, R.' _publ_section_title ; Impact of aliphatic acyl and aromatic thioamide substituents on the anticancer activity of Ru(II)-p-cymene complexes carrying acylthiourea ligands -- In vitro and in vivo studies ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT02611A _journal_year 2021 _chemical_formula_moiety 'C26 H38 Cl2 N2 O Ru S' _chemical_formula_sum 'C26 H38 Cl2 N2 O Ru S' _chemical_formula_weight 598.61 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _audit_creation_date 2020-01-10 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-09-18 deposited with the CCDC. 2021-10-15 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 109.562(5) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 17.5533(13) _cell_length_b 13.3945(13) _cell_length_c 24.754(2) _cell_measurement_reflns_used 9468 _cell_measurement_temperature 110.0 _cell_measurement_theta_max 27.576 _cell_measurement_theta_min 2.884 _cell_volume 5484.2(8) _computing_cell_refinement 'SAINT V8.38 Bruker AXS Inc., Madison, WI, USA.' _computing_data_collection 'APEX 3 (Bruker AXS)' _computing_data_reduction 'SAINT V8.38 Bruker AXS Inc., Madison, WI, USA.' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 110.0 _diffrn_detector 'Bruker APEX2 area detector' _diffrn_detector_area_resol_mean 7.9 _diffrn_detector_type 'CCD area detector' _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker PHOTON-II' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator 'mirror optics' _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0637 _diffrn_reflns_av_unetI/netI 0.0240 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 32 _diffrn_reflns_limit_l_min -32 _diffrn_reflns_number 83206 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.610 _diffrn_reflns_theta_min 2.463 _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_type 'Incoatec I\ms' _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.864 _exptl_absorpt_correction_T_max 0.4305 _exptl_absorpt_correction_T_min 0.3082 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1436 before and 0.0889 after correction. The Ratio of minimum to maximum transmission is 0.7159. The \l/2 correction factor is Not present.' _exptl_crystal_colour brown _exptl_crystal_colour_primary brown _exptl_crystal_density_diffrn 1.450 _exptl_crystal_description plate _exptl_crystal_F_000 2480 _exptl_crystal_size_max 0.41 _exptl_crystal_size_mid 0.405 _exptl_crystal_size_min 0.107 _refine_diff_density_max 1.111 _refine_diff_density_min -0.909 _refine_diff_density_rms 0.077 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.088 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 370 _refine_ls_number_reflns 6343 _refine_ls_number_restraints 538 _refine_ls_restrained_S_all 1.081 _refine_ls_R_factor_all 0.0362 _refine_ls_R_factor_gt 0.0318 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0257P)^2^+19.3902P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0761 _refine_ls_wR_factor_ref 0.0790 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5792 _reflns_number_total 6343 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt02611a2.cif _cod_data_source_block svpncana _cod_original_cell_volume 5484.1(8) _cod_database_code 7708577 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.913 _shelx_estimated_absorpt_t_min 0.718 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All C(H,H,H,H) groups, All N(H) groups, All N(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances C11A-C10 = C11-C10 = C12A-C11A = C12-C11 = C13A-C12A = C13-C12 = C14A-C13A = C14-C13 = C15A-C14A = C15-C14 = C16A-C15A = C16-C15 1.54 with sigma of 0.01 N1-C2 \\sim N1-C2A with sigma of 0.02 C11A-C10 \\sim C11-C10 \\sim C12A-C11A \\sim C12-C11 \\sim C13A-C12A \\sim C13-C12 \\sim C14A-C13A ~ C14-C13 \\sim C15A-C14A \\sim C15-C14 \\sim C16A-C15A \\sim C16-C15 with sigma of 0.05 3. Uiso/Uaniso restraints and constraints C2 \\sim C7 \\sim C6 \\sim C5 \\sim C4 \\sim C3 \\sim C2A \\sim C7A \\sim C6A \\sim C5A \\sim C4A \\sim C3A: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 C11 \\sim C12 \\sim C13 \\sim C14 \\sim C15 \\sim C16 \\sim C11A \\sim C12A \\sim C13A \\sim C14A \\sim C15A \\sim C16A: within 2A with sigma of 0.005 and sigma for terminal atoms of 0.01 Uanis(C2) = Uanis(C2A) Uanis(C16) = Uanis(C16A) Uanis(C11) = Uanis(C11A) 4. Rigid body (RIGU) restrains C2, C7, C6, C5, C4, C3, C2A, C7A, C6A, C5A, C4A, C3A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C11, C12, C13, C14, C15, C16, C11A, C12A, C13A, C14A, C15A, C16A with sigma for 1-2 distances of 0.005 and sigma for 1-3 distances of 0.005 5. Same fragment restrains {C11, C12, C13, C14, C15, C16} sigma for 1-2: 0.02, 1-3: 0.04 as {C11A, C12A, C13A, C14A, C15A, C16A} 6. Others Sof(H1B)=Sof(H10C)=Sof(H10D)=Sof(C2A)=Sof(C7A)=Sof(H7A)=Sof(C6A)=Sof(H6A)= Sof(C5A)=Sof(H5A)=Sof(C4A)=Sof(H4A)=Sof(C3A)=Sof(H3A)=Sof(C11A)=Sof(H11C)= Sof(H11D)=Sof(C12A)=Sof(H12C)=Sof(H12D)=Sof(C13A)=Sof(H13C)=Sof(H13D)= Sof(C14A)=Sof(H14C)=Sof(H14D)=Sof(C15A)=Sof(H15C)=Sof(H15D)=Sof(C16A)= Sof(H16D)=Sof(H16E)=Sof(H16F)=1-FVAR(1) Sof(H1A)=Sof(H10A)=Sof(H10B)=Sof(C2)=Sof(C7)=Sof(H7)=Sof(C6)=Sof(H6)=Sof(C5)= Sof(H5)=Sof(C4)=Sof(H4)=Sof(C3)=Sof(H3)=Sof(C11)=Sof(H11A)=Sof(H11B)=Sof(C12)= Sof(H12A)=Sof(H12B)=Sof(C13)=Sof(H13A)=Sof(H13B)=Sof(C14)=Sof(H14A)=Sof(H14B)= Sof(C15)=Sof(H15A)=Sof(H15B)=Sof(C16)=Sof(H16A)=Sof(H16B)=Sof(H16C)=FVAR(1) 7.a Ternary CH refined with riding coordinates: C23(H23) 7.b Secondary CH2 refined with riding coordinates: C9(H9A,H9B), C10(H10A,H10B), C10(H10C,H10D), C11(H11A,H11B), C12(H12A,H12B), C13(H13A,H13B), C14(H14A,H14B), C15(H15A,H15B), C11A(H11C,H11D), C12A(H12C, H12D), C13A(H13C,H13D), C14A(H14C,H14D), C15A(H15C,H15D) 7.c Aromatic/amide H refined with riding coordinates: N1(H1A), N1(H1B), N2(H2), C18(H18), C19(H19), C21(H21), C22(H22), C7(H7), C6(H6), C5(H5), C4(H4), C3(H3), C7A(H7A), C6A(H6A), C5A(H5A), C4A(H4A), C3A(H3A) 7.d Fitted hexagon refined as free rotating group: C2(C7,C6,C5,C4,C3), C2A(C7A,C6A,C5A,C4A,C3A) 7.e Idealised Me refined as rotating group: C24(H24A,H24B,H24C), C25(H25A,H25B,H25C), C26(H26A,H26B,H26C), C16(H16A,H16B, H16C), C16A(H16D,H16E,H16F) ; _shelx_res_file ; TITL svpncana_a.res in C2/c svpncana.res created by SHELXL-2018/3 at 10:13:36 on 10-Jan-2020 REM Old TITL SVPNCANa in C2/c #15 REM SHELXT solution in C2/c REM R1 0.101, Rweak 0.004, Alpha 0.089, Orientation as input REM Formula found by SHELXT: C25 N O3 Cl3 Ru CELL 0.71073 17.5533 13.3945 24.7537 90 109.562 90 ZERR 8 0.0013 0.0013 0.0022 0 0.005 0 LATT 7 SYMM -X,+Y,0.5-Z SFAC C H Cl N O Ru S UNIT 208 304 16 16 8 8 8 EQIV $1 0.5-X,0.5-Y,1-Z DFIX 1.54 0.01 C11A C10 C11 C10 C12A C11A C12 C11 C13A C12A C13 C12 C14A = C13A C14 C13 C15A C14A C15 C14 C16A C15A C16 C15 SADI N1 C2 N1 C2A SADI 0.05 C11A C10 C11 C10 C12A C11A C12 C11 C13A C12A C13 C12 C14A C13A = C14 C13 C15A C14A C15 C14 C16A C15A C16 C15 SIMU C2 > C3A SIMU 0.005 0.01 2 C11 > C16A RIGU C2 > C3A RIGU 0.005 0.005 C11 > C16A EADP C2 C2A EADP C16 C16A EADP C11 C11A L.S. 10 PLAN 20 SIZE 0.41 0.405 0.107 TEMP -163.15 HTAB N1 O1 HTAB N1 O1_$1 HTAB N2 Cl1 HTAB N2 Cl2 BOND $H wpdb -1 htab conf MORE -1 CONF fmap 2 acta OMIT -2 0 2 OMIT 1 1 0 OMIT 1 1 1 OMIT -1 1 1 OMIT -1 3 3 OMIT 1 1 4 OMIT -6 4 1 OMIT 1 1 6 REM REM REM WGHT 0.025700 19.390200 FVAR 0.16339 0.75597 RU1 6 0.290186 0.354912 0.251015 11.00000 0.01800 0.01699 = 0.01951 -0.00159 0.00411 -0.00468 CL1 3 0.422787 0.313983 0.319650 11.00000 0.01687 0.03052 = 0.02748 -0.00372 0.00571 -0.00201 CL2 3 0.282074 0.489790 0.313987 11.00000 0.02655 0.01903 = 0.02628 -0.00406 0.00551 -0.00210 S1 7 0.218576 0.252168 0.297335 11.00000 0.01779 0.02485 = 0.01784 -0.00164 0.00187 -0.00840 O1 5 0.320126 0.293271 0.490556 11.00000 0.02327 0.08538 = 0.01973 0.00008 0.00223 -0.02019 N1 4 0.201019 0.233083 0.398820 11.00000 0.01580 0.02647 = 0.01847 -0.00163 0.00157 -0.00588 PART 1 AFIX 43 H1A 2 0.220911 0.234361 0.436507 21.00000 -1.20000 AFIX 43 PART 0 PART 2 H1B 2 0.218422 0.245406 0.435878 -21.00000 -1.20000 AFIX 0 PART 0 N2 4 0.320934 0.305642 0.399557 11.00000 0.01605 0.03122 = 0.01984 0.00071 0.00240 -0.00603 AFIX 43 H2 2 0.349836 0.326943 0.378887 11.00000 -1.20000 AFIX 0 C1 1 0.247140 0.265306 0.369819 11.00000 0.01628 0.02044 = 0.01856 0.00063 0.00074 -0.00245 C8 1 0.355022 0.316726 0.457612 11.00000 0.01705 0.04582 = 0.02254 0.00125 -0.00037 -0.00586 C9 1 0.440607 0.356921 0.477665 11.00000 0.01847 0.06117 = 0.02386 -0.00133 -0.00030 -0.01211 AFIX 23 H9A 2 0.445599 0.411748 0.505463 11.00000 -1.20000 H9B 2 0.453740 0.383889 0.444595 11.00000 -1.20000 AFIX 0 C10 1 0.499141 0.273260 0.505818 11.00000 0.01869 0.06607 = 0.06392 0.00703 0.00279 -0.00157 PART 1 AFIX 23 H10A 2 0.500805 0.224207 0.476317 21.00000 -1.20000 H10B 2 0.479893 0.238403 0.534086 21.00000 -1.20000 AFIX 23 PART 0 PART 2 H10C 2 0.481442 0.250662 0.537811 -21.00000 -1.20000 H10D 2 0.484662 0.218466 0.477343 -21.00000 -1.20000 AFIX 0 PART 0 C17 1 0.209896 0.437724 0.178052 11.00000 0.03389 0.02457 = 0.01917 0.00116 0.00215 -0.00325 C18 1 0.187593 0.336534 0.172759 11.00000 0.02632 0.02567 = 0.01836 -0.00127 0.00000 -0.00396 AFIX 43 H18 2 0.133070 0.319048 0.167303 11.00000 -1.20000 AFIX 0 C19 1 0.244514 0.259631 0.175358 11.00000 0.03014 0.02079 = 0.02086 -0.00436 0.00549 -0.00587 AFIX 43 H19 2 0.227476 0.191910 0.171995 11.00000 -1.20000 AFIX 0 C20 1 0.325633 0.282204 0.182828 11.00000 0.03178 0.02869 = 0.02211 -0.00447 0.01136 -0.00672 C21 1 0.348622 0.385678 0.187905 11.00000 0.03362 0.03090 = 0.02550 -0.00144 0.01343 -0.01143 AFIX 43 H21 2 0.403065 0.403014 0.192987 11.00000 -1.20000 AFIX 0 C22 1 0.292801 0.461460 0.185547 11.00000 0.03726 0.02900 = 0.02216 0.00130 0.00935 -0.00909 AFIX 43 H22 2 0.309742 0.529219 0.188922 11.00000 -1.20000 AFIX 0 C23 1 0.150508 0.520488 0.176414 11.00000 0.03722 0.02426 = 0.03039 -0.00151 -0.00349 0.00204 AFIX 13 H23 2 0.181489 0.576608 0.200542 11.00000 -1.20000 AFIX 0 C24 1 0.083770 0.491192 0.199583 11.00000 0.03048 0.03803 = 0.04463 -0.00954 -0.00062 0.00674 AFIX 137 H24A 2 0.048868 0.441034 0.174359 11.00000 -1.50000 H24B 2 0.051633 0.550266 0.201144 11.00000 -1.50000 H24C 2 0.107731 0.463367 0.238202 11.00000 -1.50000 AFIX 0 C25 1 0.115115 0.558807 0.114215 11.00000 0.06531 0.03283 = 0.03529 0.00661 -0.00696 0.00654 AFIX 137 H25A 2 0.159222 0.579926 0.100849 11.00000 -1.50000 H25B 2 0.079314 0.615618 0.112792 11.00000 -1.50000 H25C 2 0.084326 0.505223 0.089486 11.00000 -1.50000 AFIX 0 C26 1 0.386053 0.201637 0.187212 11.00000 0.03294 0.03582 = 0.03653 -0.01033 0.01536 -0.00320 AFIX 137 H26A 2 0.434673 0.214437 0.220296 11.00000 -1.50000 H26B 2 0.400312 0.200463 0.152177 11.00000 -1.50000 H26C 2 0.362877 0.137067 0.192045 11.00000 -1.50000 AFIX 66 PART 1 C2 1 0.120507 0.196205 0.372383 21.00000 0.01615 0.02954 = 0.02125 -0.00572 0.00639 -0.00610 C7 1 0.061308 0.255658 0.334800 21.00000 0.01734 0.03572 = 0.02420 -0.00132 0.00410 -0.00174 AFIX 43 H7 2 0.073997 0.321641 0.326580 21.00000 -1.20000 AFIX 65 C6 1 -0.016458 0.218567 0.309244 21.00000 0.01895 0.05850 = 0.02553 -0.00059 0.00567 0.00016 AFIX 43 H6 2 -0.056917 0.259200 0.283558 21.00000 -1.20000 AFIX 65 C5 1 -0.035025 0.122023 0.321271 21.00000 0.02375 0.06194 = 0.03069 -0.02037 0.01067 -0.01958 AFIX 43 H5 2 -0.088174 0.096673 0.303804 21.00000 -1.20000 AFIX 65 C4 1 0.024173 0.062569 0.358854 21.00000 0.03632 0.03618 = 0.04155 -0.01701 0.02332 -0.01839 AFIX 43 H4 2 0.011483 -0.003414 0.367074 21.00000 -1.20000 AFIX 65 C3 1 0.101939 0.099659 0.384411 21.00000 0.02624 0.02703 = 0.03092 -0.00618 0.01223 -0.00293 AFIX 43 H3 2 0.142399 0.059025 0.410097 21.00000 -1.20000 AFIX 66 PART 0 PART 2 C2A 1 0.127147 0.181238 0.377162 -21.00000 0.01615 0.02954 = 0.02125 -0.00572 0.00639 -0.00610 C7A 1 0.059549 0.225607 0.337948 -21.00000 0.02243 0.03442 = 0.02798 0.00108 0.01060 -0.00956 AFIX 43 H7A 2 0.062839 0.291713 0.325000 -21.00000 -1.20000 AFIX 65 C6A 1 -0.012864 0.173253 0.317679 -21.00000 0.01106 0.03283 = 0.02168 -0.00611 0.00034 -0.00395 AFIX 43 H6A 2 -0.059065 0.203578 0.290879 -21.00000 -1.20000 AFIX 65 C5A 1 -0.017679 0.076530 0.336624 -21.00000 0.02019 0.02800 = 0.03654 -0.01319 0.01476 -0.00895 AFIX 43 H5A 2 -0.067171 0.040749 0.322771 -21.00000 -1.20000 AFIX 65 C4A 1 0.049918 0.032160 0.375838 -21.00000 0.02620 0.02827 = 0.03369 -0.00863 0.01345 -0.00819 AFIX 43 H4A 2 0.046627 -0.033946 0.388786 -21.00000 -1.20000 AFIX 65 C3A 1 0.122332 0.084513 0.396107 -21.00000 0.01928 0.02387 = 0.03787 -0.00579 0.01542 -0.00991 AFIX 43 H3A 2 0.168532 0.054188 0.422908 -21.00000 -1.20000 AFIX 0 PART 0 PART 1 C11 1 0.585358 0.314845 0.536365 21.00000 0.02406 0.05591 = 0.05145 0.00537 0.00526 0.00524 AFIX 23 H11A 2 0.581043 0.370028 0.561790 21.00000 -1.20000 H11B 2 0.617845 0.261417 0.561181 21.00000 -1.20000 AFIX 0 C12 1 0.632053 0.353300 0.498697 21.00000 0.02548 0.05079 = 0.05010 -0.00002 0.00799 0.00213 AFIX 23 H12A 2 0.602615 0.410449 0.475699 21.00000 -1.20000 H12B 2 0.635187 0.299951 0.471841 21.00000 -1.20000 AFIX 0 C13 1 0.717598 0.386334 0.534130 21.00000 0.02764 0.04711 = 0.06166 0.00366 0.00408 0.00421 AFIX 23 H13A 2 0.744898 0.331624 0.560369 21.00000 -1.20000 H13B 2 0.714407 0.444722 0.557801 21.00000 -1.20000 AFIX 0 C14 1 0.768328 0.414269 0.495982 21.00000 0.03562 0.04896 = 0.06293 0.01110 0.00625 -0.00173 AFIX 23 H14A 2 0.767508 0.357565 0.470140 21.00000 -1.20000 H14B 2 0.742790 0.472104 0.471782 21.00000 -1.20000 AFIX 0 C15 1 0.853686 0.439541 0.528829 21.00000 0.04030 0.04440 = 0.06264 0.00626 0.00566 -0.00178 AFIX 23 H15A 2 0.875884 0.385463 0.556974 21.00000 -1.20000 H15B 2 0.884385 0.438939 0.501787 21.00000 -1.20000 AFIX 0 C16 1 0.870193 0.535661 0.560154 21.00000 0.06604 0.05540 = 0.11716 -0.02892 -0.03447 0.01309 AFIX 137 H16A 2 0.888689 0.584778 0.537932 21.00000 -1.50000 H16B 2 0.912183 0.525995 0.597561 21.00000 -1.50000 H16C 2 0.820634 0.559828 0.565700 21.00000 -1.50000 AFIX 0 SAME 0.02 0.04 C11 > C16 PART 0 PART 2 C11A 1 0.590516 0.269899 0.530176 -21.00000 0.02406 0.05591 = 0.05145 0.00537 0.00526 0.00524 AFIX 23 H11C 2 0.610392 0.207483 0.518088 -21.00000 -1.20000 H11D 2 0.608331 0.270828 0.572584 -21.00000 -1.20000 AFIX 0 C12A 1 0.625364 0.359750 0.508725 -21.00000 0.02749 0.05153 = 0.05798 0.00132 0.00372 0.00281 AFIX 23 H12C 2 0.604850 0.422277 0.520192 -21.00000 -1.20000 H12D 2 0.608672 0.358174 0.466364 -21.00000 -1.20000 AFIX 0 C13A 1 0.717965 0.356140 0.534837 -21.00000 0.02936 0.04876 = 0.05968 0.00483 0.00777 0.00070 AFIX 23 H13C 2 0.732773 0.339584 0.576054 -21.00000 -1.20000 H13D 2 0.737880 0.301314 0.516277 -21.00000 -1.20000 AFIX 0 C14A 1 0.761543 0.452082 0.529185 -21.00000 0.02987 0.04200 = 0.06320 0.00253 0.00691 0.00245 AFIX 23 H14C 2 0.757696 0.455826 0.488412 -21.00000 -1.20000 H14D 2 0.727820 0.507271 0.535318 -21.00000 -1.20000 AFIX 0 C15A 1 0.847969 0.479611 0.563376 -21.00000 0.03726 0.04483 = 0.06913 0.00515 0.00166 0.00309 AFIX 23 H15C 2 0.882374 0.419431 0.574800 -21.00000 -1.20000 H15D 2 0.871322 0.524664 0.541321 -21.00000 -1.20000 AFIX 0 C16A 1 0.839063 0.531980 0.614983 -21.00000 0.06604 0.05540 = 0.11716 -0.02892 -0.03447 0.01309 AFIX 137 H16D 2 0.855677 0.601870 0.615200 -21.00000 -1.50000 H16E 2 0.873259 0.498962 0.650048 -21.00000 -1.50000 H16F 2 0.782477 0.529079 0.613178 -21.00000 -1.50000 AFIX 0 HKLF 4 REM svpncana_a.res in C2/c REM wR2 = 0.079022, GooF = S = 1.08806, Restrained GooF = 1.08105 for all data REM R1 = 0.031850 for 5792 Fo > 4sig(Fo) and 0.036205 for all 6343 data REM 370 parameters refined using 538 restraints END WGHT 0.0257 19.3916 REM Instructions for potential hydrogen bonds HTAB N1 O1 HTAB N1 O1_$1 HTAB N1 O1 HTAB N1 O1_$1 HTAB N2 Cl1 HTAB N2 Cl2 REM Highest difference peak 1.111, deepest hole -0.909, 1-sigma level 0.077 Q1 1 0.8944 0.5438 0.5320 11.00000 0.05 1.11 Q2 1 0.8696 0.5263 0.5778 11.00000 0.05 0.69 Q3 1 0.6275 0.3532 0.5407 11.00000 0.05 0.69 Q4 1 0.7654 0.4447 0.5510 11.00000 0.05 0.65 Q5 1 0.8551 0.3252 0.5208 11.00000 0.05 0.60 Q6 1 0.7650 0.4562 0.5167 11.00000 0.05 0.52 Q7 1 0.6399 0.2339 0.5328 11.00000 0.05 0.49 Q8 1 0.1183 0.1796 0.3601 11.00000 0.05 0.40 Q9 1 0.4944 0.2165 0.5205 11.00000 0.05 0.35 Q10 1 0.9322 0.5595 0.5714 11.00000 0.05 0.35 Q11 1 0.8291 0.4989 0.5894 11.00000 0.05 0.35 Q12 1 0.5724 0.2474 0.5090 11.00000 0.05 0.34 Q13 1 0.4200 0.2634 0.3029 11.00000 0.05 0.34 Q14 1 0.3614 0.2467 0.1877 11.00000 0.05 0.34 Q15 1 0.2975 0.3628 0.2887 11.00000 0.05 0.33 Q16 1 0.3298 0.2386 0.4871 11.00000 0.05 0.33 Q17 1 0.4624 0.2958 0.4771 11.00000 0.05 0.33 Q18 1 0.5861 0.3658 0.5438 11.00000 0.05 0.32 Q19 1 0.2121 0.4790 0.2519 11.00000 0.05 0.32 Q20 1 0.8421 0.4818 0.6004 11.00000 0.05 0.32 ; _shelx_res_checksum 83985 _shelx_hkl_file ; 1 1 -1 0.10 0.30 1 1 -1 -0.10 0.30 2 2 -2 2.20 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11.20 14 -8 -3 146.99 15.00 14 -8 -3 131.99 19.20 14 -8 -3 120.19 18.10 14 -8 -3 110.19 9.80 -13 9 2 19.00 10.60 -13 9 2 26.50 6.60 -13 9 2 11.80 9.30 -13 9 2 25.30 7.30 -13 9 2 26.50 4.80 13 -9 -2 25.60 11.00 13 -9 -2 21.30 6.40 13 -9 -2 23.50 12.70 13 -9 -2 23.80 4.10 -12 10 1 173.28 22.30 -12 10 1 172.68 12.50 -12 10 1 134.69 21.10 -12 10 1 152.38 16.50 -12 10 1 159.08 13.40 12 -10 -1 157.58 16.80 12 -10 -1 149.99 11.20 12 -10 -1 99.99 19.80 12 -10 -1 170.18 22.00 -11 11 0 9.90 11.10 -11 11 0 22.20 5.30 -11 11 0 14.10 4.00 -11 11 0 25.00 11.90 -11 11 0 11.90 6.00 11 -11 0 -1.80 10.70 11 -11 0 30.40 12.30 11 -11 0 20.40 3.80 11 -11 0 17.70 7.00 -10 12 -1 116.59 19.10 -10 12 -1 161.48 13.20 -10 12 -1 151.28 17.80 -10 12 -1 172.88 13.90 -10 12 -1 131.19 19.40 10 -12 1 130.29 21.20 10 -12 1 186.48 18.60 10 -12 1 122.29 20.50 10 -12 1 159.88 11.30 -9 13 -2 283.47 25.10 -9 13 -2 266.37 30.00 -9 13 -2 287.57 19.30 -9 13 -2 264.97 30.10 -9 13 -2 286.07 18.90 9 -13 2 264.17 30.10 9 -13 2 264.37 16.90 9 -13 2 226.08 23.30 9 -13 2 241.88 28.50 -8 14 -3 49.90 17.30 -8 14 -3 51.79 17.50 -8 14 -3 83.59 13.60 -8 14 -3 86.69 9.20 -8 14 -3 81.89 9.20 8 -14 3 83.09 8.80 8 -14 3 71.29 12.30 8 -14 3 66.99 19.80 8 -14 3 98.39 21.00 -7 15 -4 116.49 16.30 -7 15 -4 138.59 11.90 -7 15 -4 133.69 12.10 7 -15 4 126.19 11.70 7 -15 4 114.99 15.40 7 -15 4 116.69 11.20 -6 16 -5 11.20 5.30 -6 16 -5 11.80 7.60 -6 16 -5 17.90 4.80 -6 16 -5 0.60 19.80 -6 16 -5 18.40 20.10 6 -16 5 3.20 15.20 6 -16 5 24.20 17.10 6 -16 5 14.10 5.40 6 -16 5 16.80 4.90 6 -16 5 -3.80 5.60 -22 2 10 19.90 6.10 -22 2 10 27.50 6.50 22 -2 -10 25.20 11.20 22 -2 -10 15.60 10.60 22 -2 -10 15.80 4.80 -21 3 9 17.40 5.00 -21 3 9 16.80 5.90 21 -3 -9 27.00 10.50 21 -3 -9 20.30 10.10 21 -3 -9 14.50 4.40 -20 4 8 33.70 6.40 -20 4 8 12.00 5.30 20 -4 -8 33.10 11.60 20 -4 -8 24.20 9.50 20 -4 -8 15.90 11.30 20 -4 -8 11.30 4.20 -19 5 7 383.16 24.60 -19 5 7 380.06 26.60 -19 5 7 361.46 26.90 19 -5 -7 365.46 30.70 19 -5 -7 369.56 27.20 19 -5 -7 340.37 30.60 19 -5 -7 374.66 24.10 -18 6 6 40.60 6.20 -18 6 6 32.80 7.60 -18 6 6 35.50 8.90 18 -6 -6 41.70 6.20 18 -6 -6 39.40 12.20 18 -6 -6 31.20 11.70 18 -6 -6 39.30 8.50 -17 7 5 73.49 7.70 -17 7 5 62.69 9.40 17 -7 -5 70.39 15.90 17 -7 -5 63.39 7.00 17 -7 -5 33.10 12.90 -16 8 4 5.10 4.00 -16 8 4 -1.10 4.00 -16 8 4 3.20 2.70 16 -8 -4 -2.40 9.80 16 -8 -4 11.30 10.50 16 -8 -4 4.70 4.60 -15 9 3 37.30 9.50 -15 9 3 62.09 8.20 -15 9 3 44.50 6.50 15 -9 -3 49.40 15.00 15 -9 -3 45.30 6.00 15 -9 -3 50.59 9.60 15 -9 -3 45.10 14.40 -14 10 2 266.67 25.50 -14 10 2 383.76 23.90 -14 10 2 314.87 31.70 -14 10 2 314.87 32.50 -14 10 2 386.86 22.00 14 -10 -2 293.37 29.30 14 -10 -2 299.87 20.20 14 -10 -2 302.37 30.10 14 -10 -2 300.87 26.10 -13 11 1 69.69 8.60 -13 11 1 52.29 11.10 -13 11 1 41.80 15.80 -13 11 1 80.09 18.80 -13 11 1 68.39 7.90 13 -11 -1 52.19 16.10 13 -11 -1 67.89 17.70 13 -11 -1 52.99 6.70 13 -11 -1 57.99 10.90 -12 12 0 7.00 3.40 -12 12 0 8.40 6.00 -12 12 0 15.80 14.00 -12 12 0 1.90 3.20 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11.20 3.80 18 -8 -5 24.30 14.00 18 -8 -5 3.40 3.10 18 -8 -5 13.30 12.50 18 -8 -5 5.00 5.50 -17 9 4 124.79 12.60 -17 9 4 137.79 11.30 -17 9 4 108.99 14.70 17 -9 -4 95.69 14.00 17 -9 -4 90.09 21.10 17 -9 -4 125.89 22.20 17 -9 -4 117.49 10.40 -16 10 3 9.80 3.70 -16 10 3 3.70 4.20 -16 10 3 11.60 5.60 16 -10 -3 7.60 3.80 16 -10 -3 6.90 13.20 16 -10 -3 11.60 5.50 16 -10 -3 6.80 13.30 -15 11 2 110.99 10.60 -15 11 2 79.59 13.50 -15 11 2 87.29 10.70 15 -11 -2 64.49 16.90 15 -11 -2 86.09 19.30 15 -11 -2 66.89 12.40 -14 12 1 21.60 16.20 -14 12 1 30.80 16.80 14 -12 -1 38.60 11.60 14 -12 -1 30.90 5.40 14 -12 -1 44.30 17.00 14 -12 -1 47.70 16.30 -13 13 0 27.20 6.40 -13 13 0 9.70 17.70 -13 13 0 18.40 7.90 -13 13 0 14.10 18.30 -13 13 0 27.00 6.20 13 -13 0 24.30 14.40 13 -13 0 44.40 15.90 13 -13 0 19.00 8.70 -12 14 -1 62.69 8.70 -12 14 -1 74.39 13.40 -12 14 -1 43.30 7.70 12 -14 1 48.50 11.20 -20 8 6 4.60 3.90 -20 8 6 1.10 5.20 -20 8 6 1.10 4.40 20 -8 -6 -3.80 6.20 -19 9 5 0.10 3.90 -19 9 5 -4.70 5.10 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14 -12 -2 8.80 3.50 14 -12 -2 10.10 13.20 -14 12 2 13.00 4.50 -14 12 2 14.40 7.40 -14 12 2 19.30 5.00 -14 12 2 17.70 12.10 -14 12 2 -7.70 10.10 15 -11 -3 44.60 13.50 15 -11 -3 52.89 6.50 15 -11 -3 42.00 10.40 15 -11 -3 41.60 12.30 -15 11 3 44.10 11.00 -15 11 3 46.90 8.20 -15 11 3 37.60 6.80 -15 11 3 27.60 15.40 -15 11 3 53.99 16.90 16 -10 -4 26.80 8.30 16 -10 -4 26.20 11.50 16 -10 -4 34.50 5.60 16 -10 -4 20.20 11.30 -16 10 4 29.70 9.10 -16 10 4 22.50 6.20 -16 10 4 38.40 6.60 17 -9 -5 3.70 2.80 17 -9 -5 27.90 15.20 17 -9 -5 3.00 14.30 17 -9 -5 6.30 5.60 -17 9 5 4.90 4.20 -17 9 5 1.10 5.10 -17 9 5 8.50 3.90 18 -8 -6 9.90 3.80 18 -8 -6 6.60 5.40 -18 8 6 24.10 5.30 -18 8 6 14.10 4.90 -18 8 6 3.50 5.90 19 -7 -7 26.00 7.60 19 -7 -7 38.50 6.20 -19 7 7 43.00 6.60 -19 7 7 32.50 9.10 -19 7 7 34.30 7.80 20 -6 -8 2.50 3.00 20 -6 -8 2.90 6.10 -20 6 8 5.20 4.30 -20 6 8 3.20 4.10 -21 5 9 60.39 9.80 22 -4 -10 24.80 12.00 22 -4 -10 27.50 12.70 22 -4 -10 22.20 5.40 -22 4 10 20.80 5.40 -22 4 10 19.00 7.70 9 -15 2 16.70 7.50 9 -15 2 13.10 14.70 9 -15 2 30.50 16.30 -9 15 -2 37.40 11.00 -9 15 -2 5.90 16.60 -9 15 -2 21.40 16.20 10 -14 1 64.09 12.20 10 -14 1 28.70 16.10 10 -14 1 51.89 17.50 -10 14 -1 76.69 15.30 -10 14 -1 79.39 9.00 -10 14 -1 66.59 20.00 -10 14 -1 41.80 18.00 -10 14 -1 79.59 9.30 11 -13 0 47.70 6.20 11 -13 0 48.80 10.70 -11 13 0 53.29 7.50 -11 13 0 51.79 11.40 -11 13 0 57.79 7.80 12 -12 -1 267.57 30.40 12 -12 -1 302.97 26.70 12 -12 -1 294.57 31.60 12 -12 -1 321.07 19.80 -12 12 1 342.67 22.40 -12 12 1 335.37 33.20 -12 12 1 313.37 20.80 -12 12 1 261.97 31.30 -12 12 1 301.87 26.90 13 -11 -2 49.90 9.80 13 -11 -2 50.59 14.50 13 -11 -2 50.39 14.60 13 -11 -2 73.79 7.30 -13 11 2 67.69 8.20 -13 11 2 64.49 11.30 -13 11 2 66.29 8.80 -13 11 2 87.29 18.90 -13 11 2 61.49 16.90 14 -10 -3 110.89 13.50 14 -10 -3 84.69 19.00 14 -10 -3 86.69 17.90 14 -10 -3 85.79 8.40 -14 10 3 118.19 11.30 -14 10 3 87.99 10.40 -14 10 3 74.39 17.90 -14 10 3 72.59 18.50 -14 10 3 92.99 13.00 15 -9 -4 60.49 10.20 15 -9 -4 78.59 18.00 15 -9 -4 70.89 16.50 15 -9 -4 69.99 7.10 -15 9 4 78.09 7.90 -15 9 4 68.39 9.00 -15 9 4 54.19 13.60 -15 9 4 70.09 14.60 -15 9 4 62.99 10.60 16 -8 -5 59.39 14.30 16 -8 -5 87.59 12.20 16 -8 -5 92.59 15.50 -16 8 5 94.99 10.90 -16 8 5 92.19 8.60 -16 8 5 75.59 11.50 17 -7 -6 77.69 14.60 17 -7 -6 55.49 14.10 17 -7 -6 80.59 13.30 17 -7 -6 77.79 8.20 -17 7 6 100.99 9.00 -17 7 6 91.19 10.40 18 -6 -7 11.10 9.90 18 -6 -7 -2.50 10.10 18 -6 -7 -0.60 5.00 18 -6 -7 3.10 2.70 -18 6 7 0.90 2.90 -18 6 7 1.50 3.90 -18 6 7 1.30 4.10 19 -5 -8 5.30 9.30 19 -5 -8 12.50 6.50 19 -5 -8 9.20 3.70 19 -5 -8 3.40 9.80 -19 5 8 11.40 4.40 -19 5 8 15.10 4.20 -19 5 8 9.50 5.20 20 -4 -9 43.30 12.00 20 -4 -9 49.99 12.50 20 -4 -9 22.00 5.30 -20 4 9 34.00 7.20 -20 4 9 38.60 6.70 21 -3 -10 167.88 19.60 21 -3 -10 160.68 19.10 21 -3 -10 174.08 14.10 -21 3 10 186.48 16.00 -21 3 10 155.98 14.10 22 -2 -11 157.48 14.10 22 -2 -11 181.58 21.20 22 -2 -11 177.78 21.00 -22 2 11 172.68 14.80 -22 2 11 164.68 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54.59 0 -10 4 947.51 54.79 0 -10 4 877.21 46.10 0 -10 4 829.82 46.10 0 -10 4 763.92 49.10 0 -10 4 822.52 50.39 0 -10 4 875.21 46.70 0 10 -4 860.81 46.30 0 10 -4 841.32 45.80 0 10 -4 844.52 49.70 0 10 -4 835.72 50.29 0 10 -4 854.11 53.89 0 10 -4 887.41 46.80 0 10 -4 845.72 53.79 1 -9 3 186.38 19.20 1 -9 3 208.28 19.70 1 -9 3 212.78 13.10 1 -9 3 200.58 15.00 1 -9 3 237.08 12.80 1 -9 3 200.68 12.80 1 -9 3 200.88 16.20 -1 9 -3 166.38 14.40 -1 9 -3 190.58 16.00 -1 9 -3 219.08 13.20 -1 9 -3 212.98 12.50 -1 9 -3 194.78 18.60 -1 9 -3 208.68 12.90 2 -8 2 1804.92 104.39 2 -8 2 2120.79 105.49 2 -8 2 1760.72 101.29 2 -8 2 1708.43 98.69 2 -8 2 2001.80 96.99 -2 8 -2 2014.80 97.59 -2 8 -2 1687.63 100.99 -2 8 -2 1779.12 103.79 -2 8 -2 1921.51 104.69 -2 8 -2 1689.93 98.79 -2 8 -2 1911.01 97.49 -2 8 -2 1948.01 96.69 3 -7 1 16.70 2.00 3 -7 1 12.20 2.60 3 -7 1 15.90 5.90 3 -7 1 25.40 7.00 -3 7 -1 16.50 3.00 -3 7 -1 18.50 2.40 -3 7 -1 12.80 1.90 -3 7 -1 13.40 5.80 -3 7 -1 16.10 2.40 -3 7 -1 19.00 4.70 -3 7 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60.09 -9 1 5 1073.19 61.69 -9 1 5 1148.79 60.59 10 0 -6 793.12 47.30 10 0 -6 880.01 49.50 10 0 -6 881.51 49.40 10 0 -6 872.91 47.10 10 0 -6 926.11 49.50 -10 0 6 914.21 48.00 -10 0 6 820.32 47.40 -10 0 6 899.91 49.20 11 1 -7 510.35 28.80 11 1 -7 431.06 26.80 11 1 -7 479.25 27.10 11 1 -7 504.35 30.10 11 1 -7 484.35 28.80 -11 -1 7 493.55 27.90 -11 -1 7 432.56 26.30 -11 -1 7 460.65 27.70 12 2 -8 309.97 21.60 12 2 -8 279.27 18.90 -12 -2 8 279.67 18.70 -12 -2 8 309.57 20.60 13 3 -9 4.40 3.30 13 3 -9 0.40 3.10 13 3 -9 2.20 2.90 -13 -3 9 2.60 2.10 14 4 -10 739.33 40.10 14 4 -10 704.93 40.10 14 4 -10 769.22 40.00 14 4 -10 606.34 46.60 -14 -4 10 695.93 41.50 -14 -4 10 691.83 40.70 15 5 -11 102.79 9.50 15 5 -11 108.79 14.10 -15 -5 11 109.79 10.80 -15 -5 11 129.59 11.00 16 6 -12 79.39 11.90 -16 -6 12 64.89 8.60 -16 -6 12 65.39 7.90 17 7 -13 8.30 3.50 17 7 -13 3.60 6.00 -17 -7 13 4.50 4.30 -17 -7 13 4.30 3.20 18 8 -14 78.29 13.00 18 8 -14 80.89 9.40 -18 -8 14 68.29 9.80 -18 -8 14 62.59 13.50 -18 -8 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0.10 3.00 -10 -12 12 -1.50 2.70 -10 -12 12 0.60 2.10 -10 -12 12 2.90 5.20 11 13 -13 19.30 5.50 11 13 -13 20.40 8.40 11 13 -13 26.40 5.80 11 13 -13 9.40 4.10 -11 -13 13 10.40 4.60 -11 -13 13 15.90 4.20 -11 -13 13 14.40 6.00 12 14 -14 429.66 27.30 12 14 -14 399.56 29.10 12 14 -14 466.95 27.60 -12 -14 14 389.16 28.20 -12 -14 14 383.96 33.90 -16 -12 13 87.79 11.10 -16 -12 13 89.99 11.10 -16 -12 13 87.79 16.10 16 12 -13 107.09 13.30 16 12 -13 92.19 16.90 -15 -11 12 0.60 3.50 -15 -11 12 -9.40 6.10 -15 -11 12 1.10 3.80 15 11 -12 1.90 3.60 15 11 -12 -1.70 4.10 15 11 -12 4.50 6.90 -14 -10 11 6.90 6.10 -14 -10 11 6.00 2.90 -14 -10 11 8.50 4.00 14 10 -11 8.90 7.00 14 10 -11 3.80 3.20 14 10 -11 4.20 3.50 -13 -9 10 26.70 5.90 -13 -9 10 30.90 5.20 13 9 -10 33.10 5.10 13 9 -10 32.60 6.30 -12 -8 9 125.39 10.80 -12 -8 9 100.59 9.80 -12 -8 9 101.99 13.40 12 8 -9 125.49 9.40 12 8 -9 97.79 13.50 12 8 -9 104.99 10.40 -11 -7 8 10.30 3.00 -11 -7 8 9.30 3.00 11 7 -8 15.50 5.60 11 7 -8 9.10 3.40 11 7 -8 17.10 6.00 11 7 -8 11.90 5.20 -10 -6 7 385.56 24.00 10 6 -7 443.36 25.50 10 6 -7 402.86 31.30 10 6 -7 440.06 25.40 10 6 -7 394.76 23.90 -9 -5 6 82.39 6.70 -9 -5 6 79.09 7.40 9 5 -6 82.89 9.80 9 5 -6 84.39 6.60 9 5 -6 98.99 7.80 9 5 -6 85.19 7.50 9 5 -6 97.19 7.70 -8 -4 5 -0.50 0.90 -8 -4 5 -0.40 1.00 8 4 -5 0.40 2.00 8 4 -5 -1.20 1.70 8 4 -5 0.80 1.30 8 4 -5 0.10 0.90 8 4 -5 1.10 1.70 -7 -3 4 850.71 44.80 -7 -3 4 842.22 44.00 7 3 -4 782.62 43.70 7 3 -4 819.52 44.70 7 3 -4 791.72 46.80 7 3 -4 826.92 44.70 7 3 -4 831.32 44.90 -6 -2 3 88.99 6.00 -6 -2 3 89.79 6.50 6 2 -3 77.09 5.70 6 2 -3 88.19 6.10 6 2 -3 84.59 6.00 -5 -1 2 713.63 37.00 -5 -1 2 715.83 37.20 5 1 -2 675.53 37.30 5 1 -2 693.33 37.20 5 1 -2 670.83 36.60 4 0 -1 1.00 1.10 4 0 -1 0.20 1.10 -3 1 0 177.08 11.50 -3 1 0 170.58 11.40 3 -1 0 186.28 11.80 3 -1 0 182.28 11.60 -2 2 -1 2251.17 116.09 -2 2 -1 2277.57 116.19 2 -2 1 2117.09 115.99 -1 3 -2 29.40 3.90 -1 3 -2 28.00 2.60 -1 3 -2 30.80 3.90 1 -3 2 29.70 4.10 1 -3 2 45.10 4.70 0 4 -3 30.90 2.60 0 4 -3 35.30 4.30 0 4 -3 33.90 4.70 0 4 -3 33.50 3.60 0 4 -3 29.20 4.40 0 4 -3 33.80 2.80 0 -4 3 35.50 5.20 0 -4 3 33.40 2.70 0 -4 3 28.10 3.40 0 -4 3 35.60 5.00 1 5 -4 141.99 8.90 1 5 -4 139.19 11.40 1 5 -4 139.99 8.40 1 5 -4 133.59 9.80 1 5 -4 142.99 10.70 1 5 -4 147.89 8.70 1 5 -4 141.29 11.30 -1 -5 4 172.78 12.00 -1 -5 4 142.99 8.60 -1 -5 4 145.89 8.90 -1 -5 4 138.49 11.40 2 6 -5 235.18 13.30 2 6 -5 228.78 14.00 2 6 -5 242.28 16.80 2 6 -5 236.28 16.50 2 6 -5 231.28 13.50 2 6 -5 209.28 14.60 2 6 -5 223.28 16.30 -2 -6 5 230.18 14.80 -2 -6 5 224.38 16.70 -2 -6 5 224.08 13.90 -2 -6 5 255.37 13.60 -2 -6 5 273.47 17.60 3 7 -6 22.60 3.20 3 7 -6 15.00 4.40 3 7 -6 21.60 2.40 3 7 -6 19.00 3.00 3 7 -6 21.30 5.00 3 7 -6 26.70 5.80 3 7 -6 13.70 2.20 -3 -7 6 19.90 2.40 -3 -7 6 20.40 5.30 -3 -7 6 22.80 5.50 -3 -7 6 23.80 3.30 -3 -7 6 22.50 3.20 4 8 -7 86.49 7.60 4 8 -7 91.29 6.80 4 8 -7 93.79 6.80 4 8 -7 86.99 7.40 4 8 -7 97.79 10.20 4 8 -7 87.59 10.60 4 8 -7 102.69 10.70 -4 -8 7 98.69 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126.89 12.90 21 -5 -7 126.19 19.50 -20 6 6 18.00 4.80 -20 6 6 10.40 6.00 20 -6 -6 12.80 4.40 20 -6 -6 4.60 5.70 20 -6 -6 29.50 12.30 20 -6 -6 5.80 10.60 -19 7 5 93.99 9.70 -19 7 5 98.39 13.70 -19 7 5 96.89 11.90 19 -7 -5 102.79 9.40 19 -7 -5 50.99 15.60 19 -7 -5 88.69 13.10 19 -7 -5 104.89 19.10 -18 8 4 121.69 12.70 -18 8 4 100.29 9.90 -18 8 4 96.99 13.00 18 -8 -4 70.09 13.10 18 -8 -4 72.69 15.30 18 -8 -4 90.19 9.00 18 -8 -4 79.49 15.70 -17 9 3 18.30 5.20 -17 9 3 5.40 5.20 -17 9 3 19.40 4.80 17 -9 -3 25.70 8.30 17 -9 -3 7.00 12.90 17 -9 -3 18.20 13.40 17 -9 -3 16.70 5.00 -16 10 2 24.90 6.00 -16 10 2 17.30 6.60 -16 10 2 25.80 5.70 16 -10 -2 22.50 7.40 16 -10 -2 -5.70 13.50 16 -10 -2 27.50 14.60 16 -10 -2 19.60 4.40 -15 11 1 36.20 9.70 -15 11 1 27.70 6.10 -15 11 1 22.20 6.90 15 -11 -1 34.90 15.20 15 -11 -1 21.20 4.80 15 -11 -1 31.10 13.80 15 -11 -1 22.80 7.70 -14 12 0 42.00 7.00 14 -12 0 24.00 12.20 14 -12 0 26.00 5.40 14 -12 0 45.00 13.40 -13 13 -1 4.90 4.20 -13 13 -1 -0.80 5.60 -13 13 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110.89 19.80 -15 7 6 137.89 13.80 -15 7 6 109.29 19.80 -15 7 6 104.49 13.40 16 -6 -7 140.89 11.60 16 -6 -7 148.19 15.00 -16 6 7 143.49 14.70 -16 6 7 174.98 12.40 -16 6 7 149.49 15.20 17 -5 -8 96.69 11.60 -17 5 8 107.49 11.00 -17 5 8 96.89 9.00 -17 5 8 93.29 11.70 18 -4 -9 18.60 5.90 18 -4 -9 19.00 4.70 -18 4 9 21.80 5.90 -18 4 9 16.20 5.00 -18 4 9 26.70 5.20 19 -3 -10 479.15 29.90 -19 3 10 486.45 32.10 -19 3 10 483.05 30.40 20 -2 -11 8.40 3.80 20 -2 -11 3.50 8.50 20 -2 -11 7.10 8.70 -20 2 11 2.70 3.40 -20 2 11 2.70 3.80 21 -1 -12 190.98 15.80 21 -1 -12 207.08 21.50 21 -1 -12 188.08 21.20 -21 1 12 215.88 16.80 -21 1 12 199.88 17.40 22 0 -13 -1.10 3.30 -22 0 13 4.10 4.50 4 -16 4 0.30 5.60 4 -16 4 1.80 3.40 4 -16 4 -10.20 14.20 4 -16 4 16.60 15.00 4 -16 4 3.90 2.50 -4 16 -4 3.60 16.70 -4 16 -4 -1.90 2.90 -4 16 -4 -13.00 15.20 -4 16 -4 1.20 7.00 -4 16 -4 2.70 3.70 5 -15 3 205.88 21.30 5 -15 3 199.48 15.70 5 -15 3 234.78 15.90 5 -15 3 240.88 27.10 5 -15 3 204.08 27.10 -5 15 -3 218.68 21.90 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606.64 36.50 -16 4 8 622.84 34.80 -16 4 8 566.44 38.90 17 -3 -9 -1.30 6.70 17 -3 -9 7.20 2.60 17 -3 -9 4.20 6.90 17 -3 -9 4.30 4.10 -17 3 9 0.10 3.40 -17 3 9 0.10 2.30 -17 3 9 2.70 3.20 18 -2 -10 6.90 8.00 18 -2 -10 17.80 4.30 18 -2 -10 8.00 8.70 -18 2 10 19.50 5.00 19 -1 -11 369.76 28.70 19 -1 -11 377.96 24.40 19 -1 -11 392.06 28.90 -19 1 11 375.96 26.10 -19 1 11 357.96 24.80 20 0 -12 8.40 8.40 20 0 -12 5.00 3.40 20 0 -12 3.70 7.90 -20 0 12 4.40 3.90 -20 0 12 -0.80 3.10 21 1 -13 506.65 30.30 -21 -1 13 427.26 30.60 -21 -1 13 465.55 30.90 22 2 -14 7.00 4.30 -22 -2 14 2.70 4.40 -22 -2 14 11.00 5.90 1 -17 6 5.10 5.40 1 -17 6 6.40 3.00 1 -17 6 12.10 4.60 -1 17 -6 0.50 23.40 -1 17 -6 10.80 7.30 -1 17 -6 4.70 3.60 -1 17 -6 4.50 23.70 2 -16 5 126.39 24.40 2 -16 5 85.49 13.10 2 -16 5 109.39 10.90 2 -16 5 95.89 23.80 2 -16 5 99.09 9.10 -2 16 -5 120.79 25.60 -2 16 -5 104.49 10.40 -2 16 -5 108.69 9.90 -2 16 -5 88.69 22.30 -2 16 -5 107.09 16.20 3 -15 4 75.49 6.80 3 -15 4 52.59 10.60 3 -15 4 54.49 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81.59 4 4 -6 1558.04 84.99 -4 -4 6 1731.53 82.49 -4 -4 6 1567.44 82.29 -4 -4 6 1632.44 82.39 -4 -4 6 1573.84 81.59 5 5 -7 2971.60 149.99 5 5 -7 2778.02 149.88 5 5 -7 2960.90 150.08 5 5 -7 2716.43 148.79 5 5 -7 2791.62 153.18 5 5 -7 2783.02 149.09 -5 -5 7 2983.80 150.18 -5 -5 7 3270.57 150.28 -5 -5 7 2859.91 149.88 -5 -5 7 2770.92 148.99 6 6 -8 0.60 2.50 6 6 -8 0.50 0.90 6 6 -8 -0.90 2.80 6 6 -8 0.80 2.80 6 6 -8 0.90 1.00 6 6 -8 0.80 1.20 -6 -6 8 0.00 1.00 -6 -6 8 1.10 1.20 -6 -6 8 -0.30 2.70 -6 -6 8 0.50 2.50 7 7 -9 91.89 7.10 7 7 -9 102.39 7.00 7 7 -9 100.09 9.10 7 7 -9 88.29 10.70 7 7 -9 99.69 9.20 7 7 -9 97.79 8.10 -7 -7 9 109.79 9.40 -7 -7 9 78.79 8.90 -7 -7 9 86.89 5.80 -7 -7 9 87.99 7.90 -7 -7 9 88.69 6.90 8 8 -10 132.29 9.30 8 8 -10 140.69 11.50 8 8 -10 126.49 9.10 8 8 -10 132.19 11.70 8 8 -10 109.29 13.10 8 8 -10 119.19 11.20 -8 -8 10 119.19 11.20 -8 -8 10 123.79 11.30 -8 -8 10 127.99 11.40 -8 -8 10 117.79 8.80 9 9 -11 804.32 43.20 9 9 -11 801.42 43.50 9 9 -11 759.52 44.90 9 9 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644.04 34.30 4 2 -1 605.94 33.60 4 2 -1 660.43 34.30 4 2 -1 620.94 34.20 4 2 -1 641.94 35.60 3 1 0 191.48 10.80 3 1 0 184.68 10.80 2 0 1 2.20 0.70 2 0 1 0.90 0.60 1 -1 2 34.50 3.00 1 -1 2 28.50 2.70 0 2 -3 4565.64 236.78 0 2 -3 4512.35 236.78 0 -2 3 4887.21 236.98 0 -2 3 4456.55 236.78 1 3 -4 793.32 43.80 1 3 -4 787.62 42.80 1 3 -4 793.52 42.60 1 3 -4 835.12 44.00 -1 -3 4 788.12 42.50 -1 -3 4 837.52 44.10 -1 -3 4 948.61 44.40 -1 -3 4 754.12 42.70 2 4 -5 1561.74 79.29 2 4 -5 1569.84 79.29 2 4 -5 1574.34 81.69 2 4 -5 1406.66 77.49 2 4 -5 1465.45 77.89 -2 -4 5 1447.06 77.79 -2 -4 5 1402.96 77.39 -2 -4 5 1520.85 79.39 -2 -4 5 1522.45 79.29 3 5 -6 8.80 1.30 3 5 -6 7.10 2.50 3 5 -6 10.70 1.90 3 5 -6 8.90 2.80 3 5 -6 11.80 2.00 3 5 -6 11.50 1.50 3 5 -6 9.80 3.00 -3 -5 6 11.00 1.90 -3 -5 6 11.40 1.60 -3 -5 6 5.40 2.80 -3 -5 6 11.70 3.20 -3 -5 6 6.90 1.70 4 6 -7 586.54 32.80 4 6 -7 554.84 30.20 4 6 -7 521.85 30.60 4 6 -7 580.24 32.20 4 6 -7 556.64 30.40 4 6 -7 568.74 32.50 4 6 -7 545.45 34.30 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1019.60 56.49 7 9 -5 942.91 50.79 7 9 -5 986.40 56.59 -6 -8 4 11.50 4.10 -6 -8 4 9.60 1.90 -6 -8 4 8.10 2.40 -6 -8 4 7.40 2.30 6 8 -4 12.40 6.10 6 8 -4 14.10 2.10 6 8 -4 11.50 3.80 6 8 -4 13.80 2.80 6 8 -4 10.80 2.90 6 8 -4 6.90 2.10 6 8 -4 11.40 5.30 -5 -7 3 21.60 3.00 -5 -7 3 14.70 1.90 -5 -7 3 18.60 4.70 -5 -7 3 12.50 2.80 5 7 -3 25.20 3.10 5 7 -3 21.10 5.30 5 7 -3 15.00 3.20 5 7 -3 16.10 2.00 5 7 -3 11.00 4.70 5 7 -3 16.60 4.40 -4 -6 2 354.36 20.60 -4 -6 2 377.06 23.90 -4 -6 2 337.07 21.10 -4 -6 2 362.16 19.70 4 6 -2 362.86 23.70 4 6 -2 358.76 19.70 4 6 -2 381.46 23.40 4 6 -2 335.07 21.10 4 6 -2 366.76 20.70 4 6 -2 355.56 20.30 4 6 -2 420.26 24.00 -3 -5 1 695.73 37.00 -3 -5 1 718.53 40.60 3 5 -1 698.43 40.50 3 5 -1 728.33 40.40 3 5 -1 683.13 37.60 3 5 -1 700.53 37.10 3 5 -1 740.03 40.60 -2 -4 0 14.10 2.60 2 4 0 14.50 2.80 2 4 0 19.60 3.30 2 4 0 13.80 1.60 2 4 0 12.90 3.10 1 3 1 677.23 38.30 1 3 1 710.03 38.30 0 2 2 109.29 7.70 0 2 2 116.49 7.90 -1 1 3 7.60 1.60 -1 1 3 9.30 1.60 -2 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238.08 14.00 9 7 -11 219.78 14.10 -9 -7 11 202.38 16.00 -9 -7 11 200.68 13.70 10 8 -12 116.99 13.90 10 8 -12 127.29 11.10 10 8 -12 138.89 10.20 10 8 -12 124.09 9.50 -10 -8 12 130.59 11.30 -10 -8 12 125.19 9.90 11 9 -13 173.48 12.90 11 9 -13 162.38 12.20 11 9 -13 189.68 18.60 11 9 -13 153.98 13.60 -11 -9 13 169.28 14.00 -11 -9 13 183.18 12.90 12 10 -14 66.59 9.50 12 10 -14 110.89 9.20 12 10 -14 105.09 14.80 -12 -10 14 108.39 9.60 -12 -10 14 80.39 9.60 13 11 -15 23.90 5.80 13 11 -15 8.30 7.40 13 11 -15 17.60 5.90 -13 -11 15 20.20 4.70 -13 -11 15 16.30 5.10 14 12 -16 8.80 4.40 14 12 -16 3.50 4.30 14 12 -16 0.20 7.00 -14 -12 16 -1.80 3.80 -14 -12 16 7.20 4.00 -13 -13 10 15.40 5.60 -13 -13 10 11.10 4.60 13 13 -10 17.80 6.40 13 13 -10 16.30 4.70 -12 -12 9 108.99 15.80 -12 -12 9 126.29 10.60 -12 -12 9 124.99 12.40 12 12 -9 131.99 16.90 12 12 -9 131.89 11.20 12 12 -9 141.09 13.30 -11 -11 8 78.99 12.30 -11 -11 8 93.69 10.00 -11 -11 8 88.09 8.30 11 11 -8 111.69 9.20 11 11 -8 95.19 9.90 11 11 -8 71.89 12.50 -10 -10 7 17.00 7.80 -10 -10 7 6.90 7.70 -10 -10 7 4.80 2.10 -10 -10 7 4.20 2.90 -10 -10 7 1.70 3.20 10 10 -7 9.40 8.30 10 10 -7 2.90 2.20 10 10 -7 1.90 7.60 10 10 -7 14.50 3.50 10 10 -7 6.20 2.80 10 10 -7 6.10 4.30 -9 -9 6 -3.20 1.80 -9 -9 6 1.90 1.50 -9 -9 6 -2.50 3.40 9 9 -6 2.80 2.50 9 9 -6 1.90 1.80 9 9 -6 2.40 4.00 9 9 -6 9.00 7.30 9 9 -6 2.20 6.70 9 9 -6 1.90 2.00 -8 -8 5 6.20 4.00 -8 -8 5 11.40 3.00 -8 -8 5 7.90 1.80 8 8 -5 4.30 1.80 8 8 -5 7.70 5.10 8 8 -5 9.20 4.20 8 8 -5 10.10 5.50 8 8 -5 5.00 2.40 -7 -7 4 1257.37 71.39 -7 -7 4 1185.78 67.09 -7 -7 4 1304.37 65.79 7 7 -4 1311.77 69.69 7 7 -4 1332.17 69.59 7 7 -4 1198.08 71.19 7 7 -4 1272.87 65.79 7 7 -4 1166.08 65.99 7 7 -4 1210.48 67.19 -6 -6 3 70.19 4.80 -6 -6 3 61.69 5.60 -6 -6 3 55.09 7.50 6 6 -3 75.79 5.30 6 6 -3 67.29 7.60 6 6 -3 62.89 7.80 6 6 -3 61.89 4.70 6 6 -3 56.29 7.10 6 6 -3 60.69 5.60 -5 -5 2 49.40 6.60 -5 -5 2 65.49 4.80 -5 -5 2 68.09 5.50 5 5 -2 74.29 5.70 5 5 -2 59.69 7.20 5 5 -2 70.19 6.70 5 5 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2.50 -5 -5 8 5.60 1.40 -5 -5 8 0.90 2.00 -5 -5 8 4.60 2.20 -5 -5 8 2.40 1.10 -5 -5 8 2.50 1.40 6 6 -9 145.39 9.80 6 6 -9 125.09 9.50 6 6 -9 116.79 8.40 6 6 -9 123.59 8.80 6 6 -9 129.59 12.20 6 6 -9 142.19 9.90 -6 -6 9 155.08 10.10 -6 -6 9 124.39 7.80 -6 -6 9 163.78 10.10 -6 -6 9 125.39 8.70 -6 -6 9 128.79 9.50 7 7 -10 580.04 32.30 7 7 -10 538.95 31.10 7 7 -10 580.74 32.20 7 7 -10 535.75 31.50 -7 -7 10 541.45 31.40 -7 -7 10 609.54 32.50 -7 -7 10 525.35 30.00 -7 -7 10 635.44 32.50 8 8 -11 113.89 9.70 8 8 -11 107.19 8.10 8 8 -11 101.59 8.40 8 8 -11 115.99 10.30 8 8 -11 99.69 12.40 8 8 -11 124.19 10.10 -8 -8 11 114.69 9.60 -8 -8 11 104.99 8.40 9 9 -12 93.19 12.30 9 9 -12 79.29 6.60 9 9 -12 76.59 8.20 9 9 -12 65.59 6.50 -9 -9 12 71.69 7.60 -9 -9 12 70.39 6.80 10 10 -13 15.00 6.90 10 10 -13 23.30 4.90 10 10 -13 20.40 4.40 10 10 -13 21.60 4.40 -10 -10 13 26.90 5.20 -10 -10 13 18.00 4.20 11 11 -14 22.50 8.20 11 11 -14 36.70 6.30 11 11 -14 32.20 5.40 11 11 -14 41.90 6.80 -11 -11 14 32.90 6.10 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1.80 9 7 -5 5.10 2.80 9 7 -5 7.30 2.00 -8 -6 4 142.59 13.00 -8 -6 4 125.19 8.70 -8 -6 4 137.49 10.00 8 6 -4 123.39 12.40 8 6 -4 131.29 8.90 8 6 -4 132.69 11.10 8 6 -4 126.39 9.70 8 6 -4 144.19 11.30 -7 -5 3 1044.30 56.79 -7 -5 3 1074.79 55.59 -7 -5 3 1083.59 61.89 7 5 -3 994.90 55.79 7 5 -3 1005.50 61.59 7 5 -3 1076.19 57.39 7 5 -3 1083.39 57.49 7 5 -3 1057.69 56.89 -6 -4 2 28.60 2.50 -6 -4 2 18.50 3.90 -6 -4 2 26.60 3.20 6 4 -2 27.00 3.50 6 4 -2 25.30 3.00 6 4 -2 20.90 3.20 6 4 -2 18.40 2.30 6 4 -2 22.10 4.10 -5 -3 1 1394.76 75.09 5 3 -1 1439.56 75.29 5 3 -1 1346.37 72.39 -4 -2 0 252.27 15.80 -4 -2 0 274.57 14.80 4 2 0 268.77 16.10 4 2 0 250.37 14.90 4 2 0 258.07 14.90 4 2 0 242.38 14.10 3 1 1 859.91 45.40 3 1 1 863.11 45.40 2 0 2 2639.04 139.49 2 0 2 2775.72 139.49 1 -1 3 1003.10 49.00 1 -1 3 854.51 48.80 0 -2 4 344.07 20.00 0 -2 4 374.86 20.30 1 3 -5 1100.59 58.69 1 3 -5 1057.29 56.99 1 3 -5 1041.80 57.99 1 3 -5 1084.09 57.29 1 3 -5 1130.99 58.19 -1 -3 5 1164.38 58.29 -1 -3 5 1142.29 58.19 -1 -3 5 1085.29 56.99 -1 -3 5 1062.69 57.19 2 4 -6 2061.29 107.69 2 4 -6 2161.58 108.69 2 4 -6 1895.61 107.59 2 4 -6 2120.59 107.39 2 4 -6 2006.70 109.69 2 4 -6 2162.88 108.59 -2 -4 6 2072.99 107.59 -2 -4 6 2135.39 108.79 -2 -4 6 2009.20 107.69 -2 -4 6 2007.40 107.19 -2 -4 6 2205.88 108.69 3 5 -7 2293.67 117.99 3 5 -7 2125.09 116.69 3 5 -7 2124.29 116.29 3 5 -7 2303.47 117.19 3 5 -7 2317.57 117.89 3 5 -7 2227.58 119.99 3 5 -7 2055.59 115.79 -3 -5 7 2221.68 116.29 -3 -5 7 2525.15 118.39 -3 -5 7 2454.45 118.19 -3 -5 7 1990.50 116.49 -3 -5 7 2386.16 117.29 4 6 -8 693.63 39.50 4 6 -8 814.02 41.20 4 6 -8 666.63 38.40 4 6 -8 766.22 40.90 4 6 -8 760.32 40.20 -4 -6 8 603.64 40.30 -4 -6 8 743.93 39.50 -4 -6 8 747.23 40.80 -4 -6 8 750.92 40.10 5 7 -9 26.90 5.30 5 7 -9 19.30 3.10 5 7 -9 23.60 2.80 5 7 -9 24.60 5.70 5 7 -9 13.90 2.30 5 7 -9 22.30 5.20 5 7 -9 18.70 2.60 -5 -7 9 20.00 5.00 -5 -7 9 20.30 3.10 -5 -7 9 19.10 4.90 -5 -7 9 21.00 2.60 -5 -7 9 15.70 2.50 6 8 -10 1.30 1.30 6 8 -10 2.30 2.70 6 8 -10 -0.40 6.10 6 8 -10 0.90 1.60 6 8 -10 0.70 1.40 6 8 -10 6.60 6.80 6 8 -10 4.30 2.10 -6 -8 10 0.30 1.00 -6 -8 10 -0.20 4.30 -6 -8 10 5.20 4.60 -6 -8 10 3.30 1.80 7 9 -11 663.43 39.20 7 9 -11 749.13 37.30 7 9 -11 676.83 37.60 7 9 -11 679.23 44.50 7 9 -11 634.34 39.10 -7 -9 11 692.63 39.50 -7 -9 11 686.03 36.90 -7 -9 11 667.93 37.90 8 10 -12 27.10 4.40 8 10 -12 20.50 4.50 8 10 -12 16.30 6.60 8 10 -12 16.70 4.20 -8 -10 12 19.60 4.60 -8 -10 12 24.50 3.80 9 11 -13 153.78 11.80 9 11 -13 131.49 16.30 9 11 -13 155.18 13.10 9 11 -13 143.89 11.30 -9 -11 13 158.98 13.10 -9 -11 13 161.38 11.60 10 12 -14 7.40 3.20 10 12 -14 14.20 7.80 10 12 -14 9.80 3.60 10 12 -14 6.20 4.10 -10 -12 14 5.90 2.90 -10 -12 14 12.60 4.50 11 13 -15 10.40 3.80 11 13 -15 27.50 14.50 11 13 -15 4.50 4.40 11 13 -15 11.40 5.00 -11 -13 15 14.20 5.80 -11 -13 15 10.90 3.80 -16 -12 11 153.58 15.20 -16 -12 11 171.18 19.70 16 12 -11 142.09 20.00 16 12 -11 149.19 15.00 -15 -11 10 -8.30 5.20 -15 -11 10 -5.70 3.00 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24.90 14 -8 0 281.07 28.10 14 -8 0 316.27 20.00 14 -8 0 300.57 29.00 -13 9 -1 125.19 11.50 -13 9 -1 128.59 13.90 13 -9 1 86.29 17.60 13 -9 1 88.49 18.00 13 -9 1 106.09 13.10 13 -9 1 107.79 9.20 -12 10 -2 185.68 14.00 -12 10 -2 153.68 12.50 -12 10 -2 162.98 16.90 12 -10 2 165.08 11.50 12 -10 2 160.68 16.90 12 -10 2 136.19 19.30 12 -10 2 103.29 19.10 -11 11 -3 37.60 5.70 -11 11 -3 42.40 9.30 -11 11 -3 30.40 6.10 11 -11 3 28.60 5.10 11 -11 3 30.00 11.60 11 -11 3 28.30 8.00 11 -11 3 37.10 12.30 -10 12 -4 11.60 5.40 -10 12 -4 -1.70 13.10 -10 12 -4 4.60 12.70 10 -12 4 5.70 5.00 10 -12 4 15.60 10.70 10 -12 4 6.70 9.50 -9 13 -5 128.59 24.40 -9 13 -5 164.48 25.20 -9 13 -5 146.59 17.00 -9 13 -5 130.09 12.20 -9 13 -5 152.38 12.90 9 -13 5 141.89 12.30 9 -13 5 124.29 16.00 9 -13 5 185.78 23.80 9 -13 5 139.29 23.90 -8 14 -6 205.98 28.40 -8 14 -6 201.48 15.50 -8 14 -6 209.28 15.80 -8 14 -6 214.78 29.10 -8 14 -6 192.48 20.30 8 -14 6 126.89 26.90 8 -14 6 198.58 15.60 8 -14 6 193.58 20.00 8 -14 6 265.27 29.10 -7 15 -7 86.09 9.70 -7 15 -7 144.79 31.80 -7 15 -7 57.59 12.80 -7 15 -7 85.09 10.20 -7 15 -7 58.29 25.10 7 -15 7 54.19 8.20 7 -15 7 101.49 14.80 7 -15 7 69.99 21.40 7 -15 7 64.69 9.00 7 -15 7 55.09 23.00 -22 2 7 17.90 5.10 22 -2 -7 35.20 6.40 -21 3 6 109.39 13.10 21 -3 -6 106.89 16.70 21 -3 -6 111.49 10.80 21 -3 -6 106.39 16.90 -20 4 5 75.49 10.30 -20 4 5 68.09 8.70 20 -4 -5 95.69 16.50 20 -4 -5 87.89 15.40 20 -4 -5 77.19 8.30 20 -4 -5 76.89 11.20 -19 5 4 121.09 12.20 -19 5 4 101.89 10.30 -19 5 4 114.19 12.10 19 -5 -4 100.89 10.00 19 -5 -4 88.99 16.70 19 -5 -4 93.59 13.10 19 -5 -4 74.39 16.80 -18 6 3 24.40 6.50 -18 6 3 7.70 5.70 -18 6 3 12.20 3.70 18 -6 -3 25.50 11.40 18 -6 -3 19.20 10.80 18 -6 -3 12.70 4.00 -17 7 2 107.59 10.00 -17 7 2 102.79 11.60 -17 7 2 97.29 12.10 17 -7 -2 82.79 17.50 17 -7 -2 83.89 17.90 17 -7 -2 102.69 13.10 -16 8 1 108.89 11.50 -16 8 1 101.59 13.10 -16 8 1 110.69 10.40 16 -8 -1 85.09 18.60 16 -8 -1 104.79 9.50 16 -8 -1 109.79 14.40 16 -8 -1 105.39 18.60 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6.10 5.20 19 -7 -3 2.20 3.70 19 -7 -3 14.40 11.40 19 -7 -3 9.20 6.30 19 -7 -3 6.30 10.70 -18 8 2 79.69 9.50 -18 8 2 80.89 12.30 -18 8 2 80.19 12.00 18 -8 -2 94.49 12.80 18 -8 -2 72.99 18.10 18 -8 -2 87.59 18.30 18 -8 -2 78.19 8.70 -17 9 1 82.89 12.30 -17 9 1 80.89 11.80 -17 9 1 87.09 9.50 17 -9 -1 84.99 8.90 17 -9 -1 77.29 12.40 17 -9 -1 77.69 19.10 17 -9 -1 65.49 16.50 -16 10 0 32.00 6.80 -16 10 0 41.50 10.00 16 -10 0 19.40 14.00 16 -10 0 51.39 10.50 16 -10 0 55.29 15.30 16 -10 0 35.80 6.20 -15 11 -1 40.40 9.20 -15 11 -1 45.90 7.70 15 -11 1 40.60 13.30 15 -11 1 45.40 13.80 -14 12 -2 8.50 4.10 -14 12 -2 10.10 6.20 -14 12 -2 20.70 5.60 14 -12 2 3.90 6.20 -13 13 -3 49.40 8.20 -13 13 -3 50.59 11.90 13 -13 3 45.40 11.90 15 -13 -5 139.49 18.30 15 -13 -5 138.49 12.30 -15 13 5 159.18 13.90 -15 13 5 169.28 19.40 -15 13 5 193.38 16.00 16 -12 -6 1.40 5.90 16 -12 -6 6.20 3.40 -16 12 6 4.00 6.40 -16 12 6 3.40 4.10 -16 12 6 8.60 5.30 17 -11 -7 27.60 5.40 17 -11 -7 20.40 8.70 -17 11 7 24.70 6.50 -17 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119.79 21.90 -15 11 6 115.79 12.10 -15 11 6 140.49 11.10 -15 11 6 104.59 22.00 16 -10 -7 2.70 5.20 16 -10 -7 0.20 2.80 -16 10 7 0.40 4.40 -16 10 7 3.50 3.30 -16 10 7 -1.00 4.00 17 -9 -8 21.60 7.60 17 -9 -8 29.00 5.20 -17 9 8 14.30 6.70 -17 9 8 47.20 8.30 -17 9 8 22.70 5.40 18 -8 -9 20.20 7.80 18 -8 -9 24.80 12.80 18 -8 -9 7.00 11.60 18 -8 -9 23.70 5.30 -18 8 9 42.40 8.00 -18 8 9 28.80 8.00 -18 8 9 39.70 6.20 19 -7 -10 78.09 13.40 19 -7 -10 94.79 9.80 19 -7 -10 88.99 19.10 19 -7 -10 80.19 18.20 -19 7 10 121.99 10.70 -19 7 10 106.09 13.50 -19 7 10 118.09 12.10 20 -6 -11 2.90 6.20 20 -6 -11 23.10 12.20 20 -6 -11 7.90 4.00 20 -6 -11 29.40 12.10 -20 6 11 8.00 3.80 -20 6 11 4.50 4.70 21 -5 -12 15.20 12.80 21 -5 -12 -7.80 11.90 21 -5 -12 11.30 4.10 -21 5 12 9.30 4.20 -21 5 12 8.30 5.40 22 -4 -13 12.80 4.50 22 -4 -13 5.60 13.40 22 -4 -13 12.70 14.50 -22 4 13 22.90 5.90 -22 4 13 19.50 5.80 8 -16 0 4.70 6.90 8 -16 0 6.70 4.10 -8 16 0 -0.60 3.90 -8 16 0 4.40 5.00 -8 16 0 14.90 8.20 9 -15 -1 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155.38 12.20 5 -13 8 159.18 16.70 5 -13 8 171.08 22.50 -4 14 -9 -2.40 15.60 -4 14 -9 26.00 5.80 -4 14 -9 10.20 3.70 -4 14 -9 15.10 6.10 -4 14 -9 2.80 16.50 4 -14 9 14.50 6.00 4 -14 9 28.60 13.90 4 -14 9 10.20 3.50 4 -14 9 18.50 12.90 4 -14 9 6.00 3.40 -3 15 -10 1.20 3.50 -3 15 -10 3.30 18.70 -3 15 -10 4.30 2.80 -3 15 -10 -1.60 19.00 -3 15 -10 -0.40 5.10 3 -15 10 0.20 3.50 3 -15 10 3.80 12.90 3 -15 10 0.80 4.50 3 -15 10 1.70 2.70 3 -15 10 0.40 13.80 -22 -2 8 8.30 4.90 -22 -2 8 11.40 4.70 22 2 -8 18.50 5.10 -21 -1 7 12.70 4.60 -21 -1 7 3.80 5.10 21 1 -7 5.00 7.90 21 1 -7 9.00 3.60 21 1 -7 2.90 7.60 -20 0 6 245.28 18.40 -20 0 6 234.68 18.70 20 0 -6 247.98 21.40 20 0 -6 245.68 17.60 20 0 -6 228.58 21.20 -19 1 5 64.39 8.90 -19 1 5 75.29 8.70 19 -1 -5 65.79 7.90 19 -1 -5 65.59 12.40 19 -1 -5 56.49 11.70 -18 2 4 3.30 3.20 -18 2 4 3.30 3.00 18 -2 -4 2.60 6.70 18 -2 -4 4.80 7.00 18 -2 -4 2.70 3.60 -17 3 3 59.79 8.10 -17 3 3 73.19 8.70 17 -3 -3 66.09 7.10 17 -3 -3 47.20 7.50 -16 4 2 6.80 3.80 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3.80 -8 12 -6 17.50 11.60 -8 12 -6 1.10 2.50 -8 12 -6 3.10 2.50 8 -12 6 5.40 10.50 8 -12 6 1.30 2.80 8 -12 6 2.60 2.40 8 -12 6 0.00 11.20 -7 13 -7 179.08 13.90 -7 13 -7 170.38 25.70 -7 13 -7 178.28 18.40 -7 13 -7 174.18 13.80 -7 13 -7 199.38 25.90 7 -13 7 159.08 13.30 7 -13 7 137.99 22.90 7 -13 7 202.38 19.00 7 -13 7 176.18 22.30 -6 14 -8 -6.20 4.90 -6 14 -8 -3.00 3.00 -6 14 -8 9.40 14.90 -6 14 -8 0.00 2.90 -6 14 -8 2.60 15.80 6 -14 8 4.50 4.80 6 -14 8 20.20 13.70 6 -14 8 -5.90 2.80 6 -14 8 -3.30 2.70 6 -14 8 -5.90 13.50 -5 15 -9 9.90 6.90 -5 15 -9 39.10 17.00 -5 15 -9 16.70 4.70 -5 15 -9 0.10 15.90 5 -15 9 7.10 4.10 5 -15 9 6.20 14.30 5 -15 9 -11.80 15.10 5 -15 9 13.30 7.20 5 -15 9 12.00 4.70 -22 0 7 1.00 3.90 -22 0 7 0.50 3.80 22 0 -7 10.20 9.60 22 0 -7 -3.30 9.30 22 0 -7 -1.90 3.00 -21 1 6 -3.20 3.70 -21 1 6 -2.70 3.50 21 -1 -6 3.90 9.20 21 -1 -6 5.60 8.80 21 -1 -6 0.00 3.50 -20 2 5 60.79 9.30 -20 2 5 61.39 7.90 20 -2 -5 56.49 7.20 20 -2 -5 62.89 14.70 20 -2 -5 34.10 11.30 -19 3 4 321.97 21.70 -19 3 4 307.77 21.70 -19 3 4 339.17 23.30 19 -3 -4 306.17 20.80 19 -3 -4 282.67 21.90 19 -3 -4 287.17 25.70 19 -3 -4 300.17 25.80 -18 4 3 36.70 7.50 -18 4 3 44.60 8.10 -18 4 3 48.90 6.70 18 -4 -3 39.30 10.80 18 -4 -3 42.90 7.30 18 -4 -3 43.70 8.50 18 -4 -3 33.60 10.70 -17 5 2 2.90 3.20 -17 5 2 -0.50 2.30 -17 5 2 -1.50 3.20 17 -5 -2 5.10 2.70 17 -5 -2 4.40 8.10 17 -5 -2 -6.40 7.90 17 -5 -2 4.50 4.30 -16 6 1 21.40 5.50 -16 6 1 28.70 4.90 -16 6 1 30.40 7.10 16 -6 -1 41.30 11.10 16 -6 -1 31.00 7.30 16 -6 -1 29.00 10.70 16 -6 -1 32.00 4.80 -15 7 0 113.49 9.80 -15 7 0 106.49 12.80 -15 7 0 121.69 11.50 15 -7 0 122.59 15.90 15 -7 0 79.79 11.70 15 -7 0 90.69 14.60 15 -7 0 103.29 9.40 -14 8 -1 389.56 25.20 -14 8 -1 363.86 23.50 14 -8 1 352.46 32.10 14 -8 1 369.56 22.70 14 -8 1 350.36 31.50 -13 9 -2 7.40 4.20 -13 9 -2 11.50 5.50 -13 9 -2 6.40 3.30 13 -9 2 11.10 3.10 13 -9 2 14.40 10.30 13 -9 2 7.30 4.30 13 -9 2 3.70 10.20 -12 10 -3 108.29 10.80 -12 10 -3 109.79 13.40 -12 10 -3 107.79 9.90 12 -10 3 107.19 18.60 12 -10 3 88.29 12.60 12 -10 3 103.99 8.80 12 -10 3 104.39 18.70 -11 11 -4 10.30 3.00 -11 11 -4 16.90 4.70 -11 11 -4 9.40 5.10 11 -11 4 8.70 5.90 11 -11 4 7.30 11.50 11 -11 4 13.80 11.70 -10 12 -5 366.96 28.40 -10 12 -5 353.36 22.70 -10 12 -5 341.27 23.00 10 -12 5 301.07 26.80 10 -12 5 338.57 33.90 10 -12 5 323.27 32.10 -9 13 -6 12.40 6.60 -9 13 -6 35.30 6.00 -9 13 -6 16.10 4.30 9 -13 6 17.70 7.00 9 -13 6 20.00 14.40 9 -13 6 25.00 5.60 9 -13 6 34.20 14.80 -8 14 -7 5.60 4.00 -7 15 -8 4.60 3.90 -7 15 -8 4.80 7.10 -7 15 -8 10.60 5.50 7 -15 8 7.70 4.30 7 -15 8 9.20 4.10 7 -15 8 2.40 14.10 7 -15 8 28.40 16.00 7 -15 8 3.20 5.80 -22 2 6 82.19 9.90 22 -2 -6 92.79 16.40 22 -2 -6 77.59 15.80 -21 3 5 131.69 13.80 21 -3 -5 124.39 11.60 -20 4 4 47.70 8.00 -20 4 4 26.00 7.50 -20 4 4 28.90 6.40 20 -4 -4 21.20 5.80 20 -4 -4 18.40 6.40 20 -4 -4 34.00 13.90 20 -4 -4 32.30 13.00 -19 5 3 291.97 20.20 -19 5 3 331.47 22.70 19 -5 -3 240.48 25.80 19 -5 -3 289.57 19.50 19 -5 -3 268.27 25.80 19 -5 -3 262.37 23.80 -18 6 2 3.60 2.80 -18 6 2 -7.50 3.20 -18 6 2 1.00 4.30 18 -6 -2 4.40 4.60 18 -6 -2 -5.30 8.70 18 -6 -2 -0.40 9.50 18 -6 -2 -0.50 2.70 -17 7 1 50.59 8.90 -17 7 1 40.20 7.80 -17 7 1 51.99 6.70 17 -7 -1 30.10 6.80 17 -7 -1 55.09 14.60 17 -7 -1 63.69 10.00 17 -7 -1 29.80 11.80 -16 8 0 317.77 20.70 -16 8 0 271.57 24.20 -16 8 0 313.87 22.30 16 -8 0 302.97 24.80 16 -8 0 318.17 30.30 16 -8 0 285.07 29.20 16 -8 0 280.67 19.50 -15 9 -1 120.49 12.10 -15 9 -1 122.59 14.30 -15 9 -1 121.29 10.80 15 -9 1 88.99 18.70 15 -9 1 120.89 19.30 15 -9 1 97.39 9.30 15 -9 1 107.49 14.30 -14 10 -2 57.09 7.60 -14 10 -2 57.99 10.60 -14 10 -2 65.59 8.20 14 -10 2 47.10 6.40 14 -10 2 55.19 17.80 14 -10 2 53.79 18.60 14 -10 2 55.29 10.50 -13 11 -3 20.70 6.70 -13 11 -3 31.10 6.30 -13 11 -3 35.30 5.90 13 -11 3 15.30 5.70 -12 12 -4 16.80 4.70 -12 12 -4 4.90 5.70 -12 12 -4 2.60 3.70 12 -12 4 -17.70 12.00 12 -12 4 19.00 13.50 12 -12 4 6.20 5.80 -11 13 -5 134.69 16.90 -11 13 -5 128.09 11.70 11 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7.40 -14 12 -3 108.89 12.20 -14 12 -3 134.49 16.00 14 -12 3 102.69 15.10 -13 13 -4 78.99 10.30 -13 13 -4 79.49 9.90 -13 13 -4 84.59 14.50 13 -13 4 110.69 15.20 15 -13 -6 62.29 7.40 15 -13 -6 47.40 12.20 -15 13 6 59.09 12.10 -15 13 6 45.00 8.50 -15 13 6 54.29 9.50 16 -12 -7 94.39 15.40 16 -12 -7 114.59 10.10 -16 12 7 78.69 11.50 -16 12 7 106.79 15.70 -16 12 7 116.29 11.40 17 -11 -8 171.28 22.30 17 -11 -8 156.58 13.10 -17 11 8 211.78 15.40 -17 11 8 130.49 19.70 -17 11 8 185.38 16.10 18 -10 -9 -3.30 5.50 -18 10 9 6.90 4.30 -18 10 9 -1.90 4.00 -18 10 9 0.00 5.70 19 -9 -10 36.80 7.30 19 -9 -10 41.70 18.10 19 -9 -10 25.20 17.70 19 -9 -10 37.10 11.30 -19 9 10 38.30 8.20 -19 9 10 54.89 11.20 -19 9 10 55.39 7.30 20 -8 -11 -21.60 13.40 20 -8 -11 8.80 7.00 20 -8 -11 11.80 13.80 20 -8 -11 5.60 3.80 -20 8 11 8.00 4.90 -20 8 11 19.10 5.40 -20 8 11 12.60 7.40 11 -15 -3 96.89 14.80 11 -15 -3 107.09 9.70 -11 15 3 95.89 11.30 -11 15 3 101.79 16.20 -11 15 3 82.49 12.50 12 -14 -4 37.00 11.20 12 -14 -4 54.39 6.40 -12 14 4 45.70 11.80 -12 14 4 42.60 7.60 -12 14 4 39.00 7.60 13 -13 -5 -8.10 13.80 13 -13 -5 17.40 14.40 13 -13 -5 11.70 4.00 -13 13 5 20.40 16.40 -13 13 5 20.10 15.70 -13 13 5 14.90 4.90 -13 13 5 12.20 5.10 14 -12 -6 15.20 14.00 14 -12 -6 30.80 4.90 14 -12 -6 30.40 15.70 14 -12 -6 25.50 7.80 -14 12 6 30.10 7.00 -14 12 6 21.70 14.00 -14 12 6 23.00 14.20 -14 12 6 11.70 6.50 -14 12 6 34.50 7.20 15 -11 -7 13.50 3.60 15 -11 -7 6.50 13.30 15 -11 -7 17.50 6.70 15 -11 -7 15.60 13.40 -15 11 7 2.90 12.50 -15 11 7 15.40 5.10 -15 11 7 16.40 4.60 -15 11 7 9.40 12.60 -15 11 7 15.00 7.40 16 -10 -8 145.09 16.40 16 -10 -8 122.29 11.40 -16 10 8 168.58 14.60 -16 10 8 169.38 12.90 -16 10 8 120.29 16.60 17 -9 -9 116.09 10.30 17 -9 -9 82.49 13.50 -17 9 9 112.09 14.50 -17 9 9 142.29 13.20 -17 9 9 122.99 10.50 -17 9 9 106.79 23.80 18 -8 -10 30.00 8.80 18 -8 -10 35.20 5.50 18 -8 -10 28.70 13.70 18 -8 -10 31.00 14.60 -18 8 10 32.90 7.60 -18 8 10 38.50 9.40 -18 8 10 38.00 6.90 19 -7 -11 -2.00 5.00 19 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66.39 21.90 11 -13 -4 97.29 8.80 11 -13 -4 85.29 13.00 -11 13 4 108.59 9.90 -11 13 4 117.79 15.30 -11 13 4 91.59 23.10 -11 13 4 81.99 21.60 -11 13 4 105.99 10.60 12 -12 -5 286.87 26.00 12 -12 -5 244.88 30.20 12 -12 -5 306.57 19.60 12 -12 -5 285.37 32.00 -12 12 5 298.77 31.60 -12 12 5 341.97 20.50 -12 12 5 334.97 22.10 -12 12 5 301.87 31.80 -12 12 5 281.37 26.00 13 -11 -6 17.90 12.80 13 -11 -6 24.30 4.50 13 -11 -6 26.40 8.00 13 -11 -6 30.90 13.40 -13 11 6 14.20 12.60 -13 11 6 32.30 5.80 -13 11 6 26.60 5.80 -13 11 6 45.40 14.20 -13 11 6 21.50 8.00 14 -10 -7 37.20 8.40 14 -10 -7 32.90 5.00 14 -10 -7 14.50 11.90 14 -10 -7 25.80 13.10 -14 10 7 29.40 5.70 -14 10 7 9.40 11.30 -14 10 7 22.80 11.80 -14 10 7 32.30 6.50 -14 10 7 19.50 6.90 15 -9 -8 0.50 2.60 15 -9 -8 0.30 10.60 15 -9 -8 2.60 4.10 15 -9 -8 -5.40 9.70 -15 9 8 -0.20 10.50 -15 9 8 1.60 3.40 -15 9 8 0.80 2.70 -15 9 8 2.20 4.70 -15 9 8 0.30 10.10 16 -8 -9 91.09 17.70 16 -8 -9 73.89 8.00 16 -8 -9 61.79 15.20 -16 8 9 75.79 16.20 -16 8 9 102.59 17.10 -16 8 9 86.79 8.20 -16 8 9 84.09 9.70 -16 8 9 87.99 13.90 17 -7 -10 272.07 18.80 17 -7 -10 254.07 22.50 17 -7 -10 262.77 27.20 17 -7 -10 258.87 26.50 -17 7 10 259.57 22.90 -17 7 10 310.87 28.50 -17 7 10 318.17 22.00 -17 7 10 322.07 28.40 -17 7 10 285.17 20.10 18 -6 -11 5.20 5.30 18 -6 -11 29.20 11.90 18 -6 -11 1.40 10.10 18 -6 -11 3.50 3.00 -18 6 11 6.50 5.10 -18 6 11 3.00 3.10 -18 6 11 1.90 3.40 19 -5 -12 11.10 3.50 19 -5 -12 6.50 6.30 19 -5 -12 12.70 10.50 19 -5 -12 19.20 10.20 -19 5 12 12.20 5.30 -19 5 12 16.50 4.50 -19 5 12 35.80 6.60 20 -4 -13 32.30 11.20 20 -4 -13 32.30 6.00 20 -4 -13 33.60 11.20 -20 4 13 31.60 6.30 -20 4 13 38.40 8.30 21 -3 -14 92.19 18.40 21 -3 -14 92.49 18.60 -21 3 14 93.49 10.80 22 -2 -15 117.89 11.20 -22 2 15 121.49 12.60 -22 2 15 116.69 13.20 6 -16 0 59.99 18.60 6 -16 0 83.39 8.30 6 -16 0 73.39 8.40 6 -16 0 58.79 7.00 6 -16 0 53.19 14.70 6 -16 0 57.29 17.50 -6 16 0 65.99 7.40 -6 16 0 49.10 14.00 -6 16 0 73.69 20.60 -6 16 0 69.19 9.30 -6 16 0 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5 -8 5.50 2.50 -1 -5 8 9.50 1.70 -1 -5 8 8.20 1.50 -1 -5 8 5.30 1.70 2 6 -9 364.86 21.50 2 6 -9 363.86 19.90 2 6 -9 376.46 21.80 2 6 -9 372.96 24.60 2 6 -9 365.66 24.40 2 6 -9 380.76 21.00 2 6 -9 352.56 23.90 -2 -6 9 383.06 24.30 -2 -6 9 358.16 23.90 -2 -6 9 357.26 21.70 -2 -6 9 376.56 20.90 -2 -6 9 371.46 21.50 3 7 -10 1317.77 69.69 3 7 -10 1311.07 70.69 3 7 -10 1409.46 72.69 3 7 -10 1334.57 71.59 3 7 -10 1415.46 71.59 3 7 -10 1278.67 72.39 3 7 -10 1291.07 74.79 -3 -7 10 1315.57 72.49 -3 -7 10 1334.07 72.69 -3 -7 10 1327.67 71.49 -3 -7 10 1366.66 70.59 4 8 -11 215.78 15.30 4 8 -11 198.38 17.10 4 8 -11 192.98 12.10 4 8 -11 198.58 12.90 4 8 -11 198.28 13.90 4 8 -11 215.98 15.30 4 8 -11 211.38 13.50 -4 -8 11 198.28 14.70 -4 -8 11 204.98 13.20 -4 -8 11 199.38 13.80 -4 -8 11 200.28 12.80 -4 -8 11 204.48 14.90 5 9 -12 14.30 5.00 5 9 -12 1.60 4.70 5 9 -12 12.60 2.60 5 9 -12 14.50 2.90 5 9 -12 10.30 3.00 5 9 -12 8.90 4.10 -5 -9 12 17.20 3.80 -5 -9 12 15.40 4.40 -5 -9 12 3.80 4.10 -5 -9 12 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162.78 13.90 13 7 -5 126.09 14.70 13 7 -5 139.09 10.70 -12 -6 4 19.70 3.90 12 6 -4 25.70 4.00 12 6 -4 22.40 5.90 12 6 -4 19.60 5.60 -11 -5 3 122.89 10.20 -11 -5 3 127.49 10.50 -11 -5 3 136.79 13.10 11 5 -3 132.09 9.50 11 5 -3 131.39 13.00 11 5 -3 124.29 11.00 11 5 -3 143.19 11.30 -10 -4 2 427.86 25.50 -10 -4 2 431.76 24.50 -10 -4 2 416.76 27.90 10 4 -2 410.56 24.30 10 4 -2 431.36 28.30 -9 -3 1 383.66 25.10 -9 -3 1 381.36 22.30 9 3 -1 414.66 25.60 9 3 -1 392.86 23.50 9 3 -1 368.66 22.00 9 3 -1 383.66 23.30 -8 -2 0 180.98 11.80 -8 -2 0 195.58 11.50 -8 -2 0 172.28 13.00 8 2 0 163.78 10.90 8 2 0 176.38 13.20 -7 -1 -1 38.90 3.90 -7 -1 -1 45.50 3.90 -7 -1 -1 45.00 4.60 7 1 1 41.70 4.60 7 1 1 43.20 3.40 7 1 1 45.40 4.60 7 1 1 40.10 3.60 7 1 1 39.70 4.40 -6 0 -2 56.99 4.60 -6 0 -2 55.79 4.50 -6 0 -2 63.59 4.80 6 0 2 56.29 4.60 6 0 2 63.29 5.70 6 0 2 71.69 6.10 6 0 2 60.89 4.60 -5 1 -3 1601.94 87.69 -5 1 -3 1617.64 87.89 5 -1 3 1762.62 87.49 5 -1 3 1701.73 90.19 5 -1 3 1777.02 90.19 -4 2 -4 1022.60 54.79 -4 2 -4 990.20 53.49 -4 2 -4 1008.70 53.69 4 -2 4 1089.59 56.59 4 -2 4 1104.99 56.39 4 -2 4 931.51 54.59 -3 3 -5 36.50 3.40 -3 3 -5 40.90 3.40 -3 3 -5 46.00 4.50 3 -3 5 38.50 5.40 3 -3 5 40.60 4.30 3 -3 5 46.90 5.50 -2 4 -6 1543.15 81.39 -2 4 -6 1569.74 81.39 -2 4 -6 1543.85 82.79 -2 4 -6 1529.85 81.99 2 -4 6 1565.54 84.39 2 -4 6 1732.43 84.69 2 -4 6 1496.15 82.69 2 -4 6 1502.55 81.19 -1 5 -7 8.60 2.30 -1 5 -7 6.80 3.70 -1 5 -7 13.70 2.00 -1 5 -7 13.70 3.90 -1 5 -7 8.20 2.30 -1 5 -7 14.90 2.20 1 -5 7 14.40 4.20 1 -5 7 8.80 2.60 1 -5 7 17.90 4.20 1 -5 7 11.80 1.70 0 6 -8 38.70 4.10 0 6 -8 41.80 5.70 0 6 -8 37.40 6.60 0 6 -8 44.10 4.90 0 6 -8 42.00 6.80 0 6 -8 45.30 4.00 0 -6 8 49.99 5.10 0 -6 8 45.80 6.20 0 -6 8 39.20 3.70 0 -6 8 41.20 6.10 0 -6 8 37.20 4.00 1 7 -9 3.00 4.10 1 7 -9 6.20 4.00 1 7 -9 3.60 2.50 1 7 -9 4.30 1.60 1 7 -9 2.10 1.10 1 7 -9 2.30 0.90 1 7 -9 4.10 1.80 -1 -7 9 2.40 1.40 -1 -7 9 1.60 1.00 -1 -7 9 4.20 2.00 -1 -7 9 9.60 4.10 -1 -7 9 3.60 1.00 -1 -7 9 4.20 3.50 2 8 -10 92.69 10.80 2 8 -10 92.09 6.10 2 8 -10 99.19 8.40 2 8 -10 93.09 10.80 2 8 -10 77.59 9.30 -2 -8 10 70.69 7.30 -2 -8 10 80.49 10.10 -2 -8 10 101.29 6.20 -2 -8 10 95.19 10.50 3 9 -11 755.32 53.99 3 9 -11 891.01 50.39 3 9 -11 854.31 50.29 3 9 -11 893.31 45.80 3 9 -11 889.31 48.30 3 9 -11 803.82 47.80 -3 -9 11 864.21 47.90 -3 -9 11 915.11 50.39 -3 -9 11 863.31 50.29 -3 -9 11 818.42 47.50 -3 -9 11 871.01 48.10 -3 -9 11 879.11 45.90 4 10 -12 194.18 13.40 4 10 -12 165.88 17.30 4 10 -12 190.28 16.60 4 10 -12 168.68 12.10 4 10 -12 163.88 13.20 4 10 -12 171.38 16.60 -4 -10 12 181.28 12.10 -4 -10 12 192.78 12.40 -4 -10 12 176.08 15.90 -4 -10 12 195.38 16.30 -4 -10 12 183.88 13.50 -4 -10 12 179.98 13.00 5 11 -13 71.99 8.30 5 11 -13 92.39 8.80 5 11 -13 97.09 7.20 5 11 -13 90.69 7.80 5 11 -13 82.39 12.00 -5 -11 13 89.59 8.00 -5 -11 13 91.39 7.80 -5 -11 13 79.59 7.40 -5 -11 13 83.69 8.30 6 12 -14 3.70 3.00 6 12 -14 7.50 2.60 -6 -12 14 4.40 3.10 -6 -12 14 3.50 2.20 7 13 -15 -3.90 3.00 7 13 -15 -1.20 2.70 7 13 -15 -2.40 6.20 -7 -13 15 8.10 3.50 -7 -13 15 0.60 2.60 8 14 -16 49.90 14.50 8 14 -16 47.70 7.20 8 14 -16 50.69 8.50 -8 -14 16 42.90 10.20 -8 -14 16 46.60 7.80 -8 -14 16 54.09 6.80 -18 -10 9 -2.90 6.70 -18 -10 9 1.20 4.80 18 10 -9 -4.50 3.80 18 10 -9 5.40 6.60 -17 -9 8 31.70 6.30 -17 -9 8 18.40 9.40 -17 -9 8 32.00 7.20 17 9 -8 16.90 8.00 17 9 -8 24.00 5.30 -16 -8 7 79.99 12.50 -16 -8 7 86.59 9.00 -16 -8 7 77.89 9.40 16 8 -7 67.29 12.40 16 8 -7 87.79 8.70 -15 -7 6 131.39 11.20 -15 -7 6 150.38 12.50 -15 -7 6 139.39 15.60 15 7 -6 143.39 14.40 15 7 -6 154.78 14.90 15 7 -6 127.79 15.40 15 7 -6 126.59 12.10 -14 -6 5 483.55 34.40 -14 -6 5 498.45 30.60 14 6 -5 474.15 31.00 14 6 -5 487.55 29.10 14 6 -5 453.65 34.20 14 6 -5 537.15 31.40 -13 -5 4 161.98 11.60 -13 -5 4 153.68 12.40 -13 -5 4 134.79 14.60 13 5 -4 158.38 13.40 13 5 -4 167.08 15.80 13 5 -4 157.68 11.50 13 5 -4 172.28 13.40 -12 -4 3 65.09 8.60 -12 -4 3 52.19 5.40 -12 -4 3 54.79 6.30 12 4 -3 54.29 5.60 12 4 -3 64.59 7.80 12 4 -3 64.19 7.60 12 4 -3 62.59 8.70 -11 -3 2 101.79 8.70 -11 -3 2 105.29 8.40 -11 -3 2 104.39 10.50 11 3 -2 107.29 10.70 11 3 -2 112.59 9.80 11 3 -2 111.19 9.50 11 3 -2 104.19 8.00 -10 -2 1 1100.29 57.89 -10 -2 1 1045.20 60.09 -10 -2 1 1031.80 58.19 10 2 -1 1104.19 58.89 10 2 -1 1034.30 58.79 10 2 -1 1118.89 60.49 10 2 -1 998.10 57.19 10 2 -1 1132.09 56.09 -9 -1 0 598.74 34.50 -9 -1 0 595.34 34.80 -9 -1 0 620.84 35.90 -9 -1 0 599.14 33.50 9 1 0 660.03 36.30 9 1 0 622.74 34.10 9 1 0 649.34 36.20 9 1 0 625.04 36.20 9 1 0 639.14 33.60 -8 0 -1 -0.20 1.30 -8 0 -1 -1.80 0.90 -8 0 -1 0.10 0.90 -8 0 -1 1.00 1.00 8 0 1 0.30 0.90 8 0 1 0.80 2.40 8 0 1 -0.30 0.80 8 0 1 0.80 1.30 8 0 1 1.50 2.30 -7 1 -2 755.82 41.90 -7 1 -2 769.92 42.10 -7 1 -2 791.22 42.60 7 -1 2 740.53 42.50 7 -1 2 810.72 44.80 7 -1 2 853.61 44.90 7 -1 2 758.92 41.40 -6 2 -3 225.08 13.30 -6 2 -3 217.18 14.40 -6 2 -3 225.88 13.60 6 -2 3 239.08 16.50 6 -2 3 222.38 12.90 6 -2 3 213.78 14.40 6 -2 3 251.87 16.90 -5 3 -4 1980.30 105.29 -5 3 -4 1983.30 106.69 -5 3 -4 2003.90 104.89 5 -3 4 2062.69 106.89 5 -3 4 2072.29 104.29 -4 4 -5 657.03 38.00 -4 4 -5 657.63 39.90 -4 4 -5 706.73 38.50 4 -4 5 825.92 40.80 -3 5 -6 51.09 4.90 -3 5 -6 55.39 5.90 -3 5 -6 57.59 4.70 -3 5 -6 55.59 4.60 3 -5 6 45.90 8.10 3 -5 6 49.10 5.60 3 -5 6 56.29 8.90 -2 6 -7 632.24 39.30 -2 6 -7 675.33 38.20 -2 6 -7 722.93 38.70 -2 6 -7 719.13 42.40 -2 6 -7 707.03 42.50 2 -6 7 725.73 42.90 2 -6 7 745.63 42.70 2 -6 7 729.43 38.50 -1 7 -8 136.99 8.00 -1 7 -8 130.89 11.20 -1 7 -8 136.19 9.40 -1 7 -8 165.38 14.30 -1 7 -8 141.39 9.90 -1 7 -8 135.19 11.10 -1 7 -8 152.78 14.00 1 -7 8 132.39 8.00 1 -7 8 148.79 11.40 1 -7 8 160.08 13.70 1 -7 8 139.09 13.10 1 -7 8 141.39 9.40 0 8 -9 352.16 22.00 0 8 -9 354.36 24.40 0 8 -9 338.57 24.30 0 8 -9 337.07 21.10 0 8 -9 327.47 22.00 0 -8 9 355.26 20.90 0 -8 9 358.16 19.20 0 -8 9 291.87 21.60 0 -8 9 352.86 24.80 0 -8 9 359.66 21.80 0 -8 9 354.36 24.60 1 9 -10 -0.60 2.30 1 9 -10 0.50 6.50 1 9 -10 1.20 1.60 1 9 -10 2.10 1.30 1 9 -10 6.90 6.60 1 9 -10 0.20 2.90 -1 -9 10 -5.20 4.80 -1 -9 10 -0.30 5.60 -1 -9 10 0.60 1.20 -1 -9 10 3.40 2.30 2 10 -11 111.39 9.40 2 10 -11 116.89 7.60 2 10 -11 98.89 11.40 2 10 -11 106.29 10.00 2 10 -11 115.39 8.70 2 10 -11 107.79 14.30 2 10 -11 110.69 14.10 -2 -10 11 106.29 13.10 -2 -10 11 109.09 11.00 -2 -10 11 126.99 7.80 -2 -10 11 117.99 9.60 -2 -10 11 98.89 13.20 -2 -10 11 113.89 8.60 3 11 -12 101.39 15.40 3 11 -12 106.89 13.10 3 11 -12 136.89 9.80 3 11 -12 129.39 15.50 3 11 -12 137.29 11.50 3 11 -12 128.29 9.40 3 11 -12 119.99 10.50 -3 -11 12 104.79 10.20 -3 -11 12 128.69 9.60 -3 -11 12 138.69 11.30 4 12 -13 96.59 9.00 4 12 -13 73.19 9.50 4 12 -13 70.69 12.70 -4 -12 13 91.79 9.00 5 13 -14 277.57 18.40 5 13 -14 280.67 25.10 5 13 -14 274.27 20.00 -5 -13 14 288.07 18.30 -5 -13 14 271.67 19.90 6 14 -15 5.30 4.40 6 14 -15 13.10 7.60 6 14 -15 0.70 2.50 -6 -14 15 5.70 3.90 -6 -14 15 -3.50 4.50 -6 -14 15 1.10 2.60 -19 -9 9 121.59 13.40 19 9 -9 141.49 12.70 -18 -8 8 62.59 13.30 -18 -8 8 58.89 8.80 -18 -8 8 66.19 8.60 18 8 -8 56.29 12.20 18 8 -8 63.09 7.90 -17 -7 7 17.10 5.00 -17 -7 7 16.50 4.50 -17 -7 7 24.30 8.20 17 7 -7 16.40 4.80 17 7 -7 12.60 6.50 -16 -6 6 93.89 9.60 -16 -6 6 89.09 10.70 -16 -6 6 108.79 13.80 16 6 -6 98.99 11.40 16 6 -6 102.49 10.50 16 6 -6 101.99 13.30 16 6 -6 74.69 11.00 -15 -5 5 393.86 28.80 -15 -5 5 365.46 24.50 -15 -5 5 342.47 23.30 15 5 -5 393.66 25.30 15 5 -5 380.16 23.50 15 5 -5 383.66 25.00 15 5 -5 373.46 28.10 -14 -4 4 501.55 31.20 -14 -4 4 473.75 30.20 -14 -4 4 503.35 34.40 14 4 -4 526.25 31.80 14 4 -4 537.45 34.80 14 4 -4 533.65 32.10 14 4 -4 520.55 30.20 -13 -3 3 65.69 7.20 -13 -3 3 80.89 9.90 13 3 -3 83.29 9.90 13 3 -3 92.39 9.10 13 3 -3 72.99 8.60 -12 -2 2 172.48 13.20 12 2 -2 200.18 14.90 12 2 -2 208.08 11.80 12 2 -2 210.18 14.80 -11 -1 1 122.99 10.50 -11 -1 1 119.29 8.10 -11 -1 1 124.59 9.60 11 1 -1 120.29 8.20 11 1 -1 123.89 10.50 11 1 -1 125.49 8.90 11 1 -1 122.29 10.40 11 1 -1 116.69 10.40 -10 0 0 1582.44 81.29 -10 0 0 1512.85 80.79 -10 0 0 1530.15 80.79 -10 0 0 1478.75 79.99 10 0 0 1562.44 82.89 10 0 0 1421.96 82.59 10 0 0 1591.54 81.49 10 0 0 1492.25 80.09 10 0 0 1476.85 79.99 -9 1 -1 92.29 7.10 -9 1 -1 88.09 7.50 -9 1 -1 95.59 7.40 -9 1 -1 103.49 7.70 9 -1 1 97.59 7.10 9 -1 1 93.19 7.70 9 -1 1 106.59 9.70 9 -1 1 103.09 7.00 9 -1 1 111.69 9.70 -8 2 -2 361.16 22.20 -8 2 -2 368.56 21.40 -8 2 -2 345.87 21.40 8 -2 2 359.56 22.20 8 -2 2 358.56 24.20 8 -2 2 378.26 24.70 8 -2 2 376.36 20.60 -7 3 -3 268.67 15.80 -7 3 -3 269.47 16.30 -7 3 -3 269.67 17.90 7 -3 3 269.77 19.70 7 -3 3 279.77 19.70 7 -3 3 262.57 17.50 7 -3 3 259.17 15.30 -6 4 -4 29.10 4.20 -6 4 -4 26.60 3.30 -6 4 -4 27.30 3.30 6 -4 4 30.60 6.40 6 -4 4 26.10 4.20 6 -4 4 28.10 2.70 6 -4 4 31.80 6.40 -5 5 -5 1483.05 77.89 -5 5 -5 1452.65 80.19 -5 5 -5 1493.55 77.59 5 -5 5 1366.26 81.99 5 -5 5 1400.06 79.99 5 -5 5 1441.26 82.69 5 -5 5 1637.74 76.49 -4 6 -6 270.17 20.20 -4 6 -6 287.97 20.40 -4 6 -6 246.88 15.20 -4 6 -6 246.38 15.20 -4 6 -6 236.18 17.20 -4 6 -6 218.18 15.10 4 -6 6 271.47 19.90 4 -6 6 197.58 16.50 4 -6 6 278.27 13.80 4 -6 6 250.57 19.80 -3 7 -7 21.60 6.80 -3 7 -7 27.50 3.40 -3 7 -7 23.30 4.30 -3 7 -7 27.60 2.30 -3 7 -7 29.30 4.80 -3 7 -7 29.50 3.50 -3 7 -7 33.30 7.60 3 -7 7 28.60 3.40 3 -7 7 30.90 4.80 3 -7 7 23.60 7.00 3 -7 7 26.30 2.40 3 -7 7 23.70 6.30 -2 8 -8 4.40 2.40 -2 8 -8 4.20 2.90 -2 8 -8 1.20 1.00 -2 8 -8 -3.40 5.50 -2 8 -8 -1.40 5.80 2 -8 8 3.40 5.00 2 -8 8 4.50 5.30 2 -8 8 0.10 1.50 2 -8 8 2.70 1.00 -1 9 -9 246.68 13.60 -1 9 -9 277.97 21.80 -1 9 -9 248.18 17.00 -1 9 -9 238.58 21.40 -1 9 -9 214.38 17.50 1 -9 9 236.48 13.70 1 -9 9 300.17 21.60 1 -9 9 217.78 20.00 0 10 -10 625.84 33.80 0 10 -10 544.45 38.50 0 10 -10 648.14 36.60 0 10 -10 697.23 42.50 0 10 -10 652.83 35.80 0 10 -10 701.23 42.60 0 10 -10 661.13 38.80 0 -10 10 609.34 41.40 0 -10 10 651.33 38.60 0 -10 10 588.64 33.90 0 -10 10 705.33 42.40 0 -10 10 622.44 36.30 0 -10 10 608.24 35.50 1 11 -11 74.79 6.80 1 11 -11 74.59 11.20 1 11 -11 76.89 14.50 1 11 -11 73.39 9.00 1 11 -11 61.39 7.10 1 11 -11 81.69 14.60 -1 -11 11 70.59 7.30 -1 -11 11 84.99 13.10 -1 -11 11 77.09 8.50 -1 -11 11 68.39 13.00 -1 -11 11 75.59 6.70 2 12 -12 67.69 8.60 2 12 -12 80.09 9.30 2 12 -12 69.99 7.10 2 12 -12 54.99 15.20 2 12 -12 63.69 10.10 2 12 -12 61.59 15.60 -2 -12 12 85.49 8.60 -2 -12 12 69.99 8.70 -2 -12 12 82.49 7.10 3 13 -13 -0.20 2.70 3 13 -13 4.30 4.30 3 13 -13 4.50 6.20 3 13 -13 5.20 2.40 -3 -13 13 2.40 2.90 -3 -13 13 1.40 2.70 -3 -13 13 5.20 2.60 4 14 -14 61.89 8.40 4 14 -14 47.50 13.70 4 14 -14 74.39 7.50 -4 -14 14 35.20 9.30 -4 -14 14 47.90 7.90 -4 -14 14 56.49 6.40 5 15 -15 196.98 16.30 5 15 -15 188.58 22.00 -5 -15 15 190.88 15.70 -5 -15 15 151.08 19.00 -20 -8 9 15.40 6.40 20 8 -9 34.00 6.80 -19 -7 8 82.29 15.80 -19 -7 8 92.79 11.40 19 7 -8 104.49 10.40 19 7 -8 102.99 15.20 -18 -6 7 6.10 3.20 -18 -6 7 4.00 3.50 -18 -6 7 -1.30 5.50 18 6 -7 -1.40 2.60 18 6 -7 -4.70 5.00 -17 -5 6 -4.30 5.00 -17 -5 6 4.40 3.10 -17 -5 6 5.30 3.00 17 5 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183.28 22.90 8 -12 9 178.38 14.40 8 -12 9 197.88 18.80 8 -12 9 175.18 22.10 -7 13 -10 181.48 14.40 -7 13 -10 202.88 19.70 -7 13 -10 181.48 14.40 7 -13 10 166.48 18.30 7 -13 10 185.08 27.00 7 -13 10 184.98 26.70 7 -13 10 169.48 14.00 -6 14 -11 -0.70 3.10 6 -14 11 -4.70 12.70 6 -14 11 1.90 2.50 6 -14 11 16.70 13.30 -22 0 4 -2.50 4.30 -22 0 4 -2.10 3.70 22 0 -4 -0.90 8.90 22 0 -4 6.40 9.20 22 0 -4 -3.10 3.40 -21 1 3 4.30 4.10 -21 1 3 3.40 4.20 21 -1 -3 4.90 3.50 -20 2 2 22.70 6.20 -20 2 2 34.90 6.10 20 -2 -2 23.80 9.60 20 -2 -2 18.90 10.00 20 -2 -2 19.10 4.80 -19 3 1 179.88 15.90 -19 3 1 168.38 14.30 -19 3 1 167.58 14.00 19 -3 -1 177.28 19.70 19 -3 -1 146.19 18.20 19 -3 -1 172.18 14.90 19 -3 -1 171.98 13.50 -18 4 0 21.50 5.90 -18 4 0 23.20 6.20 -18 4 0 30.60 5.60 18 -4 0 15.00 5.10 18 -4 0 31.50 10.20 18 -4 0 20.30 9.10 -17 5 -1 243.28 17.90 -17 5 -1 257.27 20.10 -17 5 -1 275.77 20.40 17 -5 1 206.08 23.40 17 -5 1 254.47 17.50 17 -5 1 272.97 24.60 17 -5 1 246.58 20.30 -16 6 -2 -2.60 2.40 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30.40 9.00 -14 10 -5 45.30 8.00 -14 10 -5 49.80 7.50 -14 10 -5 54.29 10.00 14 -10 5 40.90 15.00 14 -10 5 36.80 13.90 14 -10 5 61.09 10.60 -13 11 -6 9.90 3.90 13 -11 6 19.80 12.20 13 -11 6 14.40 12.00 -12 12 -7 134.49 12.50 -12 12 -7 103.09 14.60 12 -12 7 143.99 16.60 12 -12 7 108.39 22.60 -11 13 -8 -0.90 4.00 -11 13 -8 1.10 3.60 -11 13 -8 1.10 5.50 11 -13 8 9.50 15.50 11 -13 8 1.50 3.80 11 -13 8 -7.20 4.50 11 -13 8 -3.90 15.80 -20 6 0 2.40 4.40 -20 6 0 8.60 4.30 -20 6 0 7.70 5.10 20 -6 0 1.00 5.40 20 -6 0 4.70 3.60 -19 7 -1 12.20 5.90 -19 7 -1 9.30 4.90 19 -7 1 13.00 6.10 19 -7 1 25.20 6.10 -18 8 -2 24.20 5.80 -18 8 -2 35.40 8.10 -18 8 -2 32.50 8.30 18 -8 2 17.80 7.10 -17 9 -3 467.15 30.50 -17 9 -3 481.75 32.00 -16 10 -4 182.08 16.00 -16 10 -4 175.48 18.50 -16 10 -4 155.38 14.50 16 -10 4 164.28 18.50 -15 11 -5 88.79 10.10 -15 11 -5 75.89 13.30 -15 11 -5 67.39 10.20 15 -11 5 78.49 13.30 15 -13 -9 10.50 6.50 15 -13 -9 7.70 4.30 -15 13 9 7.10 5.00 -15 13 9 3.80 6.50 16 -12 -10 107.19 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5.00 -20 6 15 18.70 5.90 21 -5 -16 15.30 4.80 21 -5 -16 10.00 13.10 21 -5 -16 6.30 12.70 -21 5 16 4.20 4.30 -21 5 16 7.00 4.70 8 -16 -4 19.80 4.70 8 -16 -4 41.30 11.60 -8 16 4 23.50 4.60 -8 16 4 27.40 9.00 -8 16 4 31.30 7.70 9 -15 -5 23.00 5.10 9 -15 -5 37.80 14.30 9 -15 -5 12.00 14.60 -9 15 5 22.00 5.50 -9 15 5 31.40 17.30 -9 15 5 12.10 15.10 -9 15 5 26.20 5.90 10 -14 -6 4.10 2.90 10 -14 -6 7.70 14.10 10 -14 -6 2.20 4.70 10 -14 -6 13.10 14.00 -10 14 6 12.40 7.30 -10 14 6 5.60 3.20 -10 14 6 1.10 10.90 -10 14 6 5.30 3.70 -10 14 6 11.50 12.10 11 -13 -7 -0.50 4.90 11 -13 -7 6.20 2.70 -11 13 7 9.40 4.10 -11 13 7 9.10 3.40 -11 13 7 3.30 3.50 -11 13 7 9.70 6.40 12 -12 -8 6.60 5.70 12 -12 -8 26.70 14.80 12 -12 -8 6.50 2.90 12 -12 -8 18.70 14.10 -12 12 8 -4.40 11.70 -12 12 8 3.90 3.50 -12 12 8 3.40 12.40 -12 12 8 3.10 3.40 -12 12 8 11.00 6.30 13 -11 -9 38.00 5.50 13 -11 -9 50.29 15.40 13 -11 -9 79.19 18.90 13 -11 -9 44.80 9.30 -13 11 9 40.30 8.50 -13 11 9 47.90 6.40 -13 11 9 36.70 6.90 -13 11 9 26.60 13.40 -13 11 9 28.10 14.80 14 -10 -10 78.29 12.30 14 -10 -10 64.09 16.50 14 -10 -10 96.19 19.40 14 -10 -10 106.29 9.30 -14 10 10 99.79 16.70 -14 10 10 101.39 8.80 -14 10 10 107.19 10.90 -14 10 10 89.69 16.50 -14 10 10 81.69 12.70 15 -9 -11 71.79 7.70 15 -9 -11 56.49 15.70 15 -9 -11 63.79 10.50 15 -9 -11 68.09 16.80 -15 9 11 65.89 9.00 -15 9 11 56.39 15.20 -15 9 11 60.49 15.50 -15 9 11 89.09 7.70 -15 9 11 52.29 10.70 16 -8 -12 41.20 9.20 16 -8 -12 49.60 6.60 16 -8 -12 39.50 13.90 16 -8 -12 33.10 12.90 -16 8 12 59.39 14.40 -16 8 12 42.80 13.60 -16 8 12 67.39 7.10 -16 8 12 58.99 7.90 -16 8 12 41.30 9.50 17 -7 -13 6.30 3.00 17 -7 -13 -9.30 9.50 17 -7 -13 10.60 10.70 -17 7 13 0.80 9.70 -17 7 13 11.00 9.70 -17 7 13 -1.20 3.30 -17 7 13 4.30 2.90 18 -6 -14 0.90 10.40 18 -6 -14 -3.40 4.40 18 -6 -14 -8.40 10.40 18 -6 -14 2.10 2.70 -18 6 14 -6.30 9.30 -18 6 14 0.70 4.10 -18 6 14 4.90 9.20 -18 6 14 3.30 3.60 -18 6 14 5.70 3.80 19 -5 -15 57.69 14.20 19 -5 -15 100.49 17.20 19 -5 -15 76.69 11.00 19 -5 -15 58.99 7.70 -19 5 15 71.89 9.90 -19 5 15 65.09 10.80 -19 5 15 68.09 8.90 20 -4 -16 88.39 16.90 20 -4 -16 81.19 17.20 20 -4 -16 94.19 9.60 -20 4 16 98.89 10.40 -20 4 16 76.19 10.30 21 -3 -17 24.40 5.90 -21 3 17 18.80 5.60 -21 3 17 22.00 6.20 5 -17 -2 319.57 20.40 5 -17 -2 291.47 20.40 5 -17 -2 292.87 28.40 -5 17 2 309.87 20.10 6 -16 -3 21.10 4.90 6 -16 -3 18.00 9.70 6 -16 -3 1.30 15.40 6 -16 -3 27.10 6.40 6 -16 -3 16.90 15.80 -6 16 3 21.30 17.90 -6 16 3 26.90 5.40 -6 16 3 9.20 4.20 -6 16 3 21.50 8.20 -6 16 3 13.40 16.90 7 -15 -4 52.09 11.90 7 -15 -4 68.79 7.00 -7 15 4 67.59 7.10 -7 15 4 81.59 13.80 -7 15 4 67.09 8.00 8 -14 -5 20.20 13.50 8 -14 -5 7.50 6.70 8 -14 -5 25.90 4.60 8 -14 -5 27.40 13.50 -8 14 5 16.30 4.60 -8 14 5 34.80 5.00 -8 14 5 30.60 14.80 -8 14 5 35.80 15.60 -8 14 5 22.20 7.10 9 -13 -6 88.09 16.80 9 -13 -6 62.39 17.00 9 -13 -6 86.49 7.70 9 -13 -6 66.89 12.30 -9 13 6 90.29 20.60 -9 13 6 120.99 21.90 -9 13 6 76.79 7.50 -9 13 6 79.59 7.90 -9 13 6 84.89 13.00 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136.79 9.10 -1 9 4 145.29 15.50 -1 9 4 130.19 12.80 -1 9 4 138.39 11.40 -1 9 4 140.79 9.70 2 -8 -5 1024.80 49.50 2 -8 -5 1089.49 58.09 2 -8 -5 853.41 48.70 2 -8 -5 856.81 55.59 2 -8 -5 828.32 49.50 -2 8 5 889.71 53.09 -2 8 5 913.91 56.29 -2 8 5 840.62 48.10 -2 8 5 890.31 55.79 -2 8 5 878.11 48.50 -2 8 5 889.61 49.90 -2 8 5 973.80 47.70 3 -7 -6 7.70 6.00 3 -7 -6 18.50 2.40 3 -7 -6 12.80 6.30 3 -7 -6 21.70 3.00 -3 7 6 20.50 2.90 -3 7 6 16.40 2.30 -3 7 6 13.10 6.10 -3 7 6 20.50 6.80 -3 7 6 19.70 4.10 -3 7 6 19.30 2.00 -3 7 6 14.90 2.40 4 -6 -7 544.75 35.30 4 -6 -7 510.65 34.60 4 -6 -7 516.95 28.70 -4 6 7 547.25 35.10 -4 6 7 556.34 29.10 -4 6 7 484.75 28.80 -4 6 7 521.15 34.50 5 -5 -8 5.90 1.40 5 -5 -8 4.50 1.20 -5 5 8 1.70 2.00 -5 5 8 1.50 0.90 -5 5 8 2.20 1.30 -5 5 8 2.60 0.90 6 -4 -9 0.10 0.80 6 -4 -9 1.20 4.10 6 -4 -9 1.70 3.80 6 -4 -9 0.90 0.80 -6 4 9 -1.90 3.70 -6 4 9 0.50 1.00 -6 4 9 0.90 0.90 -6 4 9 1.10 3.60 -6 4 9 1.10 0.80 7 -3 -10 1863.01 99.59 7 -3 -10 1944.11 99.99 -7 3 10 1920.01 99.59 -7 3 10 1894.51 99.69 -7 3 10 1988.60 100.79 -7 3 10 1867.71 102.69 8 -2 -11 718.63 39.50 8 -2 -11 703.93 42.20 8 -2 -11 672.53 42.20 8 -2 -11 699.33 39.20 -8 2 11 715.73 42.20 -8 2 11 702.43 40.90 -8 2 11 694.63 42.20 -8 2 11 748.83 38.70 9 -1 -12 152.38 11.40 9 -1 -12 152.98 12.90 9 -1 -12 157.38 10.10 9 -1 -12 136.89 12.30 -9 1 12 142.99 10.70 -9 1 12 128.79 11.90 -9 1 12 148.49 11.50 -9 1 12 152.48 12.50 -9 1 12 162.88 10.50 10 0 -13 0.70 3.50 10 0 -13 2.20 1.40 10 0 -13 1.70 3.30 10 0 -13 -0.10 1.50 -10 0 13 1.10 1.70 -10 0 13 -2.00 2.90 -10 0 13 0.30 3.00 -10 0 13 -0.50 1.60 -10 0 13 -1.00 1.40 11 1 -14 66.99 7.50 11 1 -14 65.29 6.00 11 1 -14 69.39 8.20 11 1 -14 56.79 7.30 -11 -1 14 65.49 6.60 -11 -1 14 65.19 6.40 -11 -1 14 72.49 7.00 12 2 -15 217.08 13.60 12 2 -15 231.58 13.90 12 2 -15 223.48 15.70 12 2 -15 223.58 14.70 12 2 -15 241.88 18.40 -12 -2 15 191.68 14.20 -12 -2 15 217.68 15.40 -12 -2 15 213.88 15.40 13 3 -16 8.70 4.00 13 3 -16 14.30 3.50 13 3 -16 5.50 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-4 4 8 1869.31 102.69 -4 4 8 1855.01 100.99 -4 4 8 1851.01 97.79 -4 4 8 1941.61 98.29 5 -3 -9 230.08 17.40 5 -3 -9 249.28 17.90 5 -3 -9 235.48 13.80 5 -3 -9 238.08 13.90 -5 3 9 247.08 17.50 -5 3 9 255.27 16.50 -5 3 9 224.68 17.20 -5 3 9 238.98 13.70 -5 3 9 232.58 14.40 6 -2 -10 756.32 40.50 6 -2 -10 751.92 44.10 6 -2 -10 758.72 41.10 6 -2 -10 742.03 43.90 -6 2 10 739.63 43.70 -6 2 10 749.73 42.80 -6 2 10 732.63 41.20 -6 2 10 739.83 40.40 -6 2 10 743.33 44.00 -6 2 10 854.91 40.80 7 -1 -11 996.20 52.39 7 -1 -11 950.00 50.79 7 -1 -11 954.00 53.69 7 -1 -11 901.01 53.29 -7 1 11 936.41 51.69 -7 1 11 963.90 52.79 -7 1 11 930.11 53.49 -7 1 11 1037.60 51.39 -7 1 11 924.61 53.29 8 0 -12 1134.59 70.09 8 0 -12 1249.38 64.49 8 0 -12 1130.79 70.39 8 0 -12 1245.88 63.89 8 0 -12 1193.88 65.89 -8 0 12 1199.08 64.59 -8 0 12 1211.08 64.29 -8 0 12 1231.38 65.29 9 1 -13 232.08 16.30 9 1 -13 223.58 13.50 9 1 -13 204.28 14.00 9 1 -13 222.88 14.30 9 1 -13 204.08 13.90 -9 -1 13 198.38 13.90 -9 -1 13 214.18 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0 8 486.65 27.50 4 0 8 482.45 25.50 4 0 8 475.95 25.20 -3 1 -9 2131.39 106.99 -3 1 -9 2012.90 106.59 -3 1 -9 2015.60 106.79 3 -1 9 1975.00 106.49 3 -1 9 2168.38 107.49 -2 2 -10 5.50 1.40 -2 2 -10 9.00 1.90 -2 2 -10 4.40 1.30 2 -2 10 6.50 1.20 2 -2 10 6.70 2.30 2 -2 10 10.90 2.50 -1 3 -11 5.40 1.40 -1 3 -11 2.20 1.00 -1 3 -11 3.00 1.90 1 -3 11 11.60 2.60 1 -3 11 4.20 2.00 1 -3 11 3.40 1.10 1 -3 11 4.50 1.50 0 4 -12 1096.99 58.89 0 4 -12 1080.29 61.19 0 4 -12 1114.09 59.39 0 -4 12 1181.58 59.89 0 -4 12 1119.89 59.59 0 -4 12 1077.29 58.69 0 -4 12 1115.49 59.69 1 5 -13 1.60 1.10 1 5 -13 0.40 1.30 1 5 -13 -1.20 1.80 -1 -5 13 2.90 1.40 -1 -5 13 1.00 1.00 -1 -5 13 1.90 1.90 -1 -5 13 3.40 1.40 -1 -5 13 3.40 2.20 2 6 -14 378.66 25.40 2 6 -14 357.96 23.40 2 6 -14 373.86 21.90 -2 -6 14 383.46 21.80 -2 -6 14 360.26 23.40 -2 -6 14 378.86 22.10 -2 -6 14 381.56 22.00 -2 -6 14 377.96 21.70 3 7 -15 36.90 4.70 3 7 -15 31.30 6.30 3 7 -15 31.10 3.90 -3 -7 15 24.90 4.30 -3 -7 15 30.50 3.80 -3 -7 15 34.20 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23.90 15.70 -6 14 14 11.60 3.70 -6 14 14 4.90 6.10 -6 14 14 16.40 14.60 7 -13 -15 0.30 2.70 7 -13 -15 3.10 2.60 -7 13 15 3.50 2.70 -7 13 15 7.20 5.70 8 -12 -16 14.10 3.20 8 -12 -16 16.80 13.20 8 -12 -16 21.80 11.90 8 -12 -16 18.40 4.20 -8 12 16 -6.50 12.40 -8 12 16 13.00 3.30 -8 12 16 9.60 6.30 -8 12 16 15.00 4.90 -8 12 16 20.40 13.60 9 -11 -17 -1.10 2.30 9 -11 -17 10.50 12.90 9 -11 -17 9.00 11.90 9 -11 -17 2.70 2.40 -9 11 17 -0.60 4.70 -9 11 17 1.60 2.10 -9 11 17 4.10 13.10 -9 11 17 -0.70 3.30 -9 11 17 -6.70 11.20 10 -10 -18 38.00 16.30 10 -10 -18 65.59 6.80 10 -10 -18 38.10 15.30 10 -10 -18 68.69 7.40 -10 10 18 63.89 6.90 -10 10 18 67.39 8.50 -10 10 18 70.99 17.20 -10 10 18 46.20 9.70 -10 10 18 49.60 14.90 11 -9 -19 20.20 4.40 11 -9 -19 18.00 12.50 11 -9 -19 12.80 11.70 -11 9 19 19.10 11.40 -11 9 19 22.40 12.00 -11 9 19 13.60 6.10 -11 9 19 7.20 4.00 -11 9 19 18.50 4.20 12 -8 -20 140.69 11.50 12 -8 -20 119.09 20.70 12 -8 -20 144.89 12.10 12 -8 -20 143.99 21.60 -12 8 20 172.18 20.80 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-22 138.49 13.40 4 10 22 124.09 19.50 4 10 22 148.69 12.20 -3 -9 -23 45.00 7.80 -3 -9 -23 29.00 7.40 3 9 23 47.10 18.50 3 9 23 22.30 9.80 3 9 23 33.00 5.90 3 9 23 39.70 16.80 -2 -8 -24 5.70 3.70 2 8 24 10.80 6.10 2 8 24 8.10 3.10 2 8 24 33.40 13.70 2 8 24 2.90 12.10 -1 -7 -25 43.90 7.50 -1 -7 -25 28.20 6.30 1 7 25 34.90 5.00 1 7 25 22.90 7.40 0 -6 -26 72.59 8.90 0 -6 -26 45.20 7.60 0 6 26 66.59 16.80 0 6 26 47.40 10.70 0 6 26 56.09 5.80 0 6 26 67.29 16.50 1 -5 -27 60.39 8.30 1 -5 -27 28.00 6.70 -1 5 27 51.69 10.00 -1 5 27 45.20 14.20 -1 5 27 38.50 13.00 2 -4 -28 276.37 20.10 -2 4 28 243.98 25.90 -2 4 28 259.87 22.60 -2 4 28 230.98 25.20 3 -3 -29 5.90 4.50 -3 3 29 13.80 10.70 -3 3 29 31.90 11.40 -3 3 29 2.10 4.50 4 -2 -30 74.59 11.70 5 -1 -31 121.29 13.90 -5 1 31 152.88 17.00 6 0 -32 42.10 9.70 -6 0 32 35.40 8.30 -6 0 32 39.40 8.90 -5 -9 -22 136.59 12.60 -5 -9 -22 139.49 13.30 5 9 22 121.39 10.70 5 9 22 81.99 17.00 -4 -8 -23 -1.00 3.60 -4 -8 -23 3.40 4.20 4 8 23 5.00 12.00 4 8 23 1.40 5.80 4 8 23 21.00 13.20 4 8 23 0.40 3.00 -3 -7 -24 67.19 8.30 -3 -7 -24 79.29 10.50 3 7 24 50.29 14.50 3 7 24 42.70 13.50 3 7 24 64.59 6.80 3 7 24 54.69 11.30 -2 -6 -25 35.10 5.60 -2 -6 -25 35.60 7.30 2 6 25 40.00 4.90 2 6 25 31.20 8.70 -1 -5 -26 12.40 4.60 1 5 26 8.30 10.10 1 5 26 3.20 9.70 1 5 26 9.60 5.50 0 -4 -27 153.18 13.40 0 4 27 117.99 14.40 0 4 27 109.09 18.20 0 4 27 126.79 19.60 1 -3 -28 8.20 4.20 -1 3 28 5.10 5.00 -1 3 28 17.00 10.30 -1 3 28 21.10 10.10 2 -2 -29 267.47 19.90 -2 2 29 233.28 21.00 -2 2 29 192.28 24.90 -2 2 29 224.38 26.40 4 0 -31 6.00 4.90 -4 0 31 -5.50 3.50 -4 0 31 -8.70 4.10 7 9 21 134.89 12.00 -6 -8 -22 7.50 4.80 6 8 22 9.20 3.60 6 8 22 6.30 6.40 -5 -7 -23 1.50 4.00 5 7 23 3.60 5.70 5 7 23 2.90 10.30 5 7 23 -4.40 11.10 5 7 23 2.20 3.00 -4 -6 -24 43.20 7.10 4 6 24 34.70 8.80 4 6 24 31.80 6.00 4 6 24 28.10 12.70 4 6 24 35.60 11.80 3 5 25 106.39 22.00 3 5 25 132.29 22.30 3 5 25 103.99 13.00 -2 -4 -26 32.20 6.90 2 4 26 23.60 11.20 2 4 26 32.50 8.00 2 4 26 33.60 12.20 -1 -3 -27 53.39 8.20 1 3 27 51.99 9.20 1 3 27 52.89 13.40 1 3 27 33.50 12.10 0 -2 -28 6.00 4.10 0 2 28 8.60 9.60 0 2 28 7.30 4.10 0 2 28 -3.80 8.60 1 -1 -29 13.80 5.40 -2 0 30 218.18 19.10 3 1 -31 154.08 16.60 -3 -1 31 164.88 16.00 -3 -1 31 156.48 13.40 -8 -8 -21 34.80 8.50 8 8 21 26.20 5.80 -7 -7 -22 104.59 10.50 -7 -7 -22 121.99 12.60 7 7 22 90.99 14.20 7 7 22 114.79 9.80 -6 -6 -23 0.60 3.90 -6 -6 -23 3.30 4.00 6 6 23 -0.30 10.00 6 6 23 -2.90 5.30 6 6 23 5.00 10.70 -5 -5 -24 195.88 15.20 5 5 24 151.58 20.70 5 5 24 140.69 16.00 5 5 24 136.29 20.40 -4 -4 -25 -3.30 3.20 4 4 25 4.50 4.40 -3 -3 -26 370.96 23.60 3 3 26 313.87 28.10 3 3 26 321.57 24.80 3 3 26 238.68 26.40 -2 -2 -27 69.19 9.30 2 2 27 72.99 16.10 2 2 27 86.69 14.60 2 2 27 59.99 10.70 -1 -1 -28 9.20 5.00 1 1 28 3.30 9.90 1 1 28 27.50 10.90 0 0 29 21.60 6.30 1 1 -30 36.50 10.90 -1 -1 30 34.30 7.90 -8 -6 -22 60.59 11.50 -8 -6 -22 66.89 12.10 8 6 22 52.19 12.60 -7 -5 -23 240.18 17.60 7 5 23 134.89 21.20 7 5 23 190.88 23.00 7 5 23 180.78 18.50 -6 -4 -24 62.29 9.10 6 4 24 41.40 10.00 6 4 24 36.70 12.40 6 4 24 30.60 11.70 -5 -3 -25 6.30 4.60 5 3 25 4.80 4.90 -4 -2 -26 -7.40 3.80 4 2 26 1.20 8.30 4 2 26 -3.50 8.30 -3 -1 -27 129.59 13.50 3 1 27 110.09 16.50 3 1 27 101.49 14.20 3 1 27 121.39 16.90 -2 0 -28 258.27 19.90 2 0 28 178.28 21.60 2 0 28 225.78 22.20 2 0 28 224.88 19.10 -1 1 -29 167.28 16.50 1 -1 29 155.28 15.00 0 2 -30 23.80 8.00 0 -2 30 33.90 7.50 -8 -4 -23 2.60 4.20 -7 -3 -24 205.78 16.40 7 3 24 136.99 20.20 7 3 24 157.58 18.50 7 3 24 170.28 20.80 -6 -2 -25 3.70 4.10 6 2 25 9.20 9.20 6 2 25 4.60 4.20 6 2 25 0.90 8.60 -5 -1 -26 1.80 4.00 5 1 26 -4.00 2.90 -4 0 -27 -3.50 4.60 4 0 27 1.80 8.80 4 0 27 -5.30 8.30 4 0 27 -1.10 4.00 -3 1 -28 16.60 6.20 3 -1 28 19.50 10.70 3 -1 28 5.50 10.10 -2 2 -29 94.39 20.20 2 -2 29 146.49 13.90 -9 -3 -23 20.90 6.90 9 3 23 18.00 6.40 -8 -2 -24 26.20 7.80 8 2 24 26.00 7.00 -7 -1 -25 58.99 9.70 7 1 25 73.69 10.10 7 1 25 83.89 17.30 7 1 25 89.49 16.90 -6 0 -26 57.29 10.30 6 0 26 71.79 9.70 6 0 26 62.79 14.40 6 0 26 26.30 11.30 -5 1 -27 93.39 12.90 5 -1 27 109.69 18.20 5 -1 27 93.49 11.30 5 -1 27 61.69 15.60 3 -9 -27 40.90 7.10 3 -9 -27 59.99 8.40 -3 9 27 29.60 20.40 -3 9 27 60.69 6.50 -3 9 27 46.10 22.10 -3 9 27 25.70 9.10 4 -8 -28 1.20 16.30 4 -8 -28 4.50 4.00 4 -8 -28 -8.00 16.10 4 -8 -28 0.90 3.40 -4 8 28 9.90 14.40 -4 8 28 -5.80 14.50 -4 8 28 0.10 5.90 -4 8 28 3.80 3.00 5 -7 -29 11.10 4.40 5 -7 -29 18.60 4.90 -5 7 29 2.80 3.40 -5 7 29 4.40 6.20 6 -6 -30 47.10 6.90 6 -6 -30 5.00 19.90 6 -6 -30 46.40 23.50 6 -6 -30 33.40 7.80 -6 6 30 36.60 17.30 -6 6 30 47.50 18.50 -6 6 30 38.00 10.40 -6 6 30 37.90 5.30 1 -9 -26 -2.30 3.50 1 -9 -26 3.50 3.80 -1 9 26 -3.00 2.70 -1 9 26 -9.00 5.10 2 -8 -27 155.18 12.50 -2 8 27 156.18 11.40 -2 8 27 110.89 15.40 -2 8 27 112.89 23.00 -2 8 27 143.29 23.80 3 -7 -28 138.39 13.10 3 -7 -28 132.89 11.20 -3 7 28 128.99 38.00 -3 7 28 123.69 36.00 -3 7 28 128.59 10.30 4 -6 -29 43.00 6.20 4 -6 -29 62.99 8.80 -4 6 29 49.90 6.20 -4 6 29 35.70 16.40 -4 6 29 33.90 10.00 -4 6 29 28.70 15.20 5 -5 -30 23.60 17.70 5 -5 -30 -43.70 15.90 5 -5 -30 -1.70 3.50 -5 5 30 -1.20 4.90 -5 5 30 6.50 16.30 -5 5 30 10.80 16.70 6 -4 -31 29.70 7.50 -6 4 31 14.50 6.90 -1 -9 -25 49.50 8.30 -1 -9 -25 30.70 6.30 1 9 25 25.70 9.00 1 9 25 52.69 6.50 0 -8 -26 36.50 7.30 0 -8 -26 23.30 5.50 0 8 26 26.30 5.50 0 8 26 40.60 15.80 0 8 26 16.30 6.80 0 8 26 37.50 14.30 1 -7 -27 96.19 9.40 1 -7 -27 118.89 11.50 -1 7 27 80.89 8.30 -1 7 27 131.89 21.70 -1 7 27 122.19 22.40 -1 7 27 91.69 13.80 2 -6 -28 122.39 11.60 2 -6 -28 89.79 8.80 -2 6 28 80.19 21.50 -2 6 28 90.09 22.50 -2 6 28 81.49 12.80 3 -5 -29 42.60 7.50 -3 5 29 40.40 14.80 -3 5 29 31.50 14.30 -3 5 29 38.20 10.20 4 -4 -30 145.29 13.90 -4 4 30 136.09 16.30 5 -3 -31 12.80 5.10 -5 3 31 8.20 5.90 -3 -9 -24 98.69 10.20 -3 -9 -24 93.99 11.20 3 9 24 71.89 13.70 3 9 24 90.39 8.80 -2 -8 -25 49.10 8.30 -2 -8 -25 35.40 6.60 2 8 25 49.40 16.40 2 8 25 36.40 5.40 2 8 25 35.60 16.30 2 8 25 43.50 11.20 -1 -7 -26 -3.00 3.60 -1 -7 -26 -1.10 3.30 1 7 26 9.30 13.00 1 7 26 2.40 2.50 1 7 26 6.60 12.40 1 7 26 2.70 5.70 0 -6 -27 55.79 7.10 0 -6 -27 52.19 8.30 0 6 27 39.30 9.90 1 -5 -28 87.79 10.00 -1 5 28 49.00 15.20 -1 5 28 63.39 11.20 -1 5 28 57.79 15.60 -2 4 29 5.50 5.30 -2 4 29 16.10 12.10 -2 4 29 24.80 12.20 3 -3 -30 17.80 5.70 -3 3 30 17.50 6.40 4 -2 -31 66.59 9.80 -4 2 31 61.49 10.80 -4 -8 -24 62.79 9.00 -4 -8 -24 35.10 8.20 4 8 24 54.99 6.70 4 8 24 37.60 11.00 -3 -7 -25 -3.60 3.50 -3 -7 -25 4.90 3.90 3 7 25 1.00 2.70 3 7 25 9.10 11.70 3 7 25 -6.90 11.20 3 7 25 0.00 5.60 -2 -6 -26 26.50 6.70 -2 -6 -26 30.10 7.30 2 6 26 29.20 13.00 2 6 26 37.10 13.70 2 6 26 19.80 8.80 1 5 27 4.70 5.70 0 4 28 161.78 17.00 0 4 28 186.88 22.10 0 4 28 156.88 21.20 1 -3 -29 2.00 4.10 -1 3 29 3.10 10.80 -1 3 29 -3.50 4.20 -1 3 29 12.90 10.60 2 -2 -30 28.90 7.70 -2 2 30 27.60 7.90 3 -1 -31 181.58 17.10 -3 1 31 159.58 17.00 -5 -7 -24 123.09 11.30 -5 -7 -24 122.39 12.50 5 7 24 104.59 9.60 5 7 24 104.79 15.10 -4 -6 -25 37.60 7.50 4 6 25 29.00 8.80 4 6 25 9.80 12.50 4 6 25 36.50 14.60 3 5 26 -1.70 10.70 3 5 26 16.90 11.40 3 5 26 0.50 5.30 2 4 27 6.40 5.50 1 3 28 84.69 12.30 1 3 28 76.29 16.90 1 3 28 101.89 17.60 0 2 29 235.88 25.00 0 2 29 240.58 25.40 0 2 29 277.57 22.30 1 -1 -30 37.30 9.00 -1 1 30 50.59 9.10 2 0 -31 7.60 5.90 -2 0 31 5.40 4.50 -6 -6 -24 111.29 11.40 6 6 24 78.59 13.00 -5 -5 -25 132.69 14.60 5 5 25 102.39 13.70 5 5 25 108.09 18.70 5 5 25 54.79 15.40 -4 -4 -26 9.10 8.10 4 4 26 -6.40 9.00 4 4 26 2.00 4.10 4 4 26 0.60 10.70 -3 -3 -27 16.70 9.10 3 3 27 6.30 4.30 2 2 28 2.50 9.60 2 2 28 -0.30 3.50 2 2 28 -6.00 9.50 1 1 29 151.78 21.60 1 1 29 140.09 21.40 1 1 29 157.78 15.80 0 0 -30 200.08 18.60 0 0 30 205.08 18.30 -7 -5 -24 125.89 13.20 7 5 24 92.59 13.50 6 4 25 -12.20 10.00 6 4 25 -2.50 10.40 6 4 25 0.20 4.60 -5 -3 -26 158.48 15.40 5 3 26 105.49 17.80 5 3 26 138.39 14.70 5 3 26 118.69 18.30 -4 -2 -27 8.40 5.00 4 2 27 -5.10 9.70 4 2 27 17.50 10.80 4 2 27 5.90 4.30 3 1 28 10.30 5.00 -2 0 -29 5.80 6.40 2 0 29 3.10 4.30 2 0 29 3.80 9.60 2 0 29 3.50 9.60 7 3 25 32.60 8.40 -6 -2 -26 15.90 6.80 6 2 26 38.40 13.70 6 2 26 36.20 8.10 6 2 26 25.10 12.90 -5 -1 -27 93.39 12.60 5 1 27 96.49 16.70 5 1 27 76.79 16.40 5 1 27 83.49 11.30 4 0 28 19.40 15.00 4 0 28 24.00 14.40 -3 7 29 0.20 13.80 1 -7 -28 12.90 5.20 1 -7 -28 13.50 4.30 -1 7 28 6.50 4.30 -1 7 28 17.00 15.30 -1 7 28 4.10 6.00 -1 7 28 7.20 14.90 2 -6 -29 65.29 9.20 -2 6 29 52.09 16.40 -2 6 29 34.80 16.20 -2 6 29 65.69 11.70 3 -5 -30 5.20 4.50 -3 5 30 19.80 16.90 -3 5 30 14.40 6.90 -3 5 30 10.90 17.20 -1 -7 -27 22.40 6.30 -1 -7 -27 18.40 4.60 1 7 27 12.70 14.90 1 7 27 36.20 17.30 1 7 27 19.70 6.50 0 6 28 135.99 16.00 0 6 28 129.29 22.50 0 6 28 164.28 22.70 1 -5 -29 10.10 4.60 -1 5 29 5.40 5.50 2 -4 -30 147.49 14.10 -2 4 30 114.49 20.10 -2 4 30 86.79 19.50 -2 4 30 113.29 15.20 3 -3 -31 -1.40 4.20 -3 3 31 0.70 4.80 -3 -7 -26 -3.80 3.60 -3 -7 -26 6.70 4.40 3 7 26 1.00 5.90 -2 -6 -27 56.59 8.90 2 6 27 49.50 14.80 2 6 27 61.69 16.00 -1 -5 -28 32.80 7.10 1 5 28 10.50 6.20 1 5 28 25.70 12.80 1 5 28 4.90 11.70 0 -4 -29 114.29 11.90 0 4 29 88.19 11.90 1 -3 -30 -1.80 4.00 -1 3 30 -3.00 11.10 -1 3 30 -4.30 10.90 -1 3 30 -2.30 4.20 -4 -6 -26 10.80 5.20 4 6 26 5.00 5.70 -3 -5 -27 25.90 6.40 3 5 27 22.70 7.60 3 5 27 21.30 11.80 3 5 27 50.09 14.10 -2 -4 -28 15.50 5.60 2 4 28 12.60 11.30 2 4 28 8.90 5.90 2 4 28 15.10 11.90 -1 -3 -29 55.89 9.40 1 3 29 31.90 9.00 0 -2 -30 40.50 9.60 0 2 30 20.30 14.70 0 2 30 29.30 15.80 0 2 30 19.10 6.40 -4 -4 -27 0.50 4.20 4 4 27 -3.90 11.00 4 4 27 -18.00 12.00 4 4 27 -3.80 4.20 -3 -3 -28 204.38 17.10 3 3 28 153.48 24.10 3 3 28 148.19 23.50 3 3 28 178.78 17.50 -2 -2 -29 128.19 13.70 2 2 29 114.69 13.30 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 75311 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ru1 Ru 0.29019(2) 0.35491(2) 0.25101(2) 0.01871(6) Uani 1 1 d . . . . . Cl1 Cl 0.42279(3) 0.31398(5) 0.31965(3) 0.02539(12) Uani 1 1 d . . . . . Cl2 Cl 0.28207(4) 0.48979(4) 0.31399(2) 0.02479(12) Uani 1 1 d . . . . . S1 S 0.21858(3) 0.25217(4) 0.29734(2) 0.02119(12) Uani 1 1 d . . . . . O1 O 0.32013(12) 0.2933(2) 0.49056(8) 0.0440(6) Uani 1 1 d . . . . . N1 N 0.20102(11) 0.23308(15) 0.39882(8) 0.0213(4) Uani 1 1 d D . . . . H1A H 0.220911 0.234361 0.436507 0.026 Uiso 0.756(4) 1 calc R . P A 1 H1B H 0.218422 0.245406 0.435878 0.026 Uiso 0.244(4) 1 calc R . P A 2 N2 N 0.32093(12) 0.30564(16) 0.39956(8) 0.0233(4) Uani 1 1 d . . . . . H2 H 0.349836 0.326943 0.378887 0.028 Uiso 1 1 calc R . . . . C1 C 0.24714(13) 0.26531(17) 0.36982(10) 0.0197(4) Uani 1 1 d . . . . . C8 C 0.35502(15) 0.3167(2) 0.45761(11) 0.0302(6) Uani 1 1 d . . . . . C9 C 0.44061(16) 0.3569(2) 0.47767(12) 0.0364(7) Uani 1 1 d . . . . . H9A H 0.445599 0.411748 0.505463 0.044 Uiso 1 1 calc R . . . . H9B H 0.453740 0.383889 0.444595 0.044 Uiso 1 1 calc R . . . . C10 C 0.49914(17) 0.2733(3) 0.50582(17) 0.0523(9) Uani 1 1 d D . . . . H10A H 0.500805 0.224207 0.476317 0.063 Uiso 0.756(4) 1 calc R . P A 1 H10B H 0.479893 0.238403 0.534086 0.063 Uiso 0.756(4) 1 calc R . P A 1 H10C H 0.481442 0.250662 0.537811 0.063 Uiso 0.244(4) 1 calc R . P A 2 H10D H 0.484662 0.218466 0.477343 0.063 Uiso 0.244(4) 1 calc R . P A 2 C17 C 0.20990(16) 0.43772(19) 0.17805(10) 0.0276(5) Uani 1 1 d . . . . . C18 C 0.18759(16) 0.33653(18) 0.17276(10) 0.0253(5) Uani 1 1 d . . . . . H18 H 0.133070 0.319048 0.167303 0.030 Uiso 1 1 calc R . . . . C19 C 0.24451(15) 0.25963(18) 0.17536(10) 0.0247(5) Uani 1 1 d . . . . . H19 H 0.227476 0.191910 0.171995 0.030 Uiso 1 1 calc R . . . . C20 C 0.32563(16) 0.2822(2) 0.18283(10) 0.0269(5) Uani 1 1 d . . . . . C21 C 0.34862(17) 0.3857(2) 0.18791(11) 0.0291(5) Uani 1 1 d . . . . . H21 H 0.403065 0.403014 0.192987 0.035 Uiso 1 1 calc R . . . . C22 C 0.29280(17) 0.4615(2) 0.18555(11) 0.0296(5) Uani 1 1 d . . . . . H22 H 0.309742 0.529219 0.188922 0.036 Uiso 1 1 calc R . . . . C23 C 0.15051(18) 0.5205(2) 0.17641(12) 0.0343(6) Uani 1 1 d . . . . . H23 H 0.181489 0.576608 0.200542 0.041 Uiso 1 1 calc R . . . . C24 C 0.08377(18) 0.4912(2) 0.19958(14) 0.0410(7) Uani 1 1 d . . . . . H24A H 0.048868 0.441034 0.174359 0.062 Uiso 1 1 calc GR . . . . H24B H 0.051633 0.550266 0.201144 0.062 Uiso 1 1 calc GR . . . . H24C H 0.107731 0.463367 0.238202 0.062 Uiso 1 1 calc GR . . . . C25 C 0.1151(2) 0.5588(2) 0.11421(14) 0.0505(9) Uani 1 1 d . . . . . H25A H 0.159222 0.579926 0.100849 0.076 Uiso 1 1 calc GR . . . . H25B H 0.079314 0.615618 0.112792 0.076 Uiso 1 1 calc GR . . . . H25C H 0.084326 0.505223 0.089486 0.076 Uiso 1 1 calc GR . . . . C26 C 0.38605(17) 0.2016(2) 0.18721(12) 0.0342(6) Uani 1 1 d . . . . . H26A H 0.434673 0.214437 0.220296 0.051 Uiso 1 1 calc GR . . . . H26B H 0.400312 0.200463 0.152177 0.051 Uiso 1 1 calc GR . . . . H26C H 0.362877 0.137067 0.192045 0.051 Uiso 1 1 calc GR . . . . C2 C 0.12051(19) 0.1962(3) 0.3724(3) 0.0223(7) Uani 0.756(4) 1 d D U P A 1 C7 C 0.0613(2) 0.2557(3) 0.3348(2) 0.0265(9) Uani 0.756(4) 1 d G U P A 1 H7 H 0.073997 0.321641 0.326580 0.032 Uiso 0.756(4) 1 calc R . P A 1 C6 C -0.01646(19) 0.2186(3) 0.30924(15) 0.0348(10) Uani 0.756(4) 1 d G U P A 1 H6 H -0.056917 0.259200 0.283558 0.042 Uiso 0.756(4) 1 calc R . P A 1 C5 C -0.03502(17) 0.1220(3) 0.32127(14) 0.0384(11) Uani 0.756(4) 1 d G U P A 1 H5 H -0.088174 0.096673 0.303804 0.046 Uiso 0.756(4) 1 calc R . P A 1 C4 C 0.0242(2) 0.0626(2) 0.35885(17) 0.0354(11) Uani 0.756(4) 1 d G U P A 1 H4 H 0.011483 -0.003414 0.367074 0.043 Uiso 0.756(4) 1 calc R . P A 1 C3 C 0.1019(2) 0.0997(3) 0.3844(2) 0.0274(10) Uani 0.756(4) 1 d G U P A 1 H3 H 0.142399 0.059025 0.410097 0.033 Uiso 0.756(4) 1 calc R . P A 1 C2A C 0.1271(7) 0.1812(11) 0.3772(9) 0.0223(7) Uani 0.244(4) 1 d D U P A 2 C7A C 0.0595(8) 0.2256(8) 0.3379(8) 0.028(3) Uani 0.244(4) 1 d G U P A 2 H7A H 0.062839 0.291713 0.325000 0.033 Uiso 0.244(4) 1 calc R . P A 2 C6A C -0.0129(6) 0.1733(8) 0.3177(5) 0.023(2) Uani 0.244(4) 1 d G U P A 2 H6A H -0.059065 0.203578 0.290879 0.028 Uiso 0.244(4) 1 calc R . P A 2 C5A C -0.0177(5) 0.0765(7) 0.3366(5) 0.027(3) Uani 0.244(4) 1 d G U P A 2 H5A H -0.067171 0.040749 0.322771 0.032 Uiso 0.244(4) 1 calc R . P A 2 C4A C 0.0499(6) 0.0322(7) 0.3758(5) 0.029(3) Uani 0.244(4) 1 d G U P A 2 H4A H 0.046627 -0.033946 0.388786 0.034 Uiso 0.244(4) 1 calc R . P A 2 C3A C 0.1223(6) 0.0845(10) 0.3961(7) 0.026(3) Uani 0.244(4) 1 d G U P A 2 H3A H 0.168532 0.054188 0.422908 0.031 Uiso 0.244(4) 1 calc R . P A 2 C11 C 0.5854(2) 0.3148(4) 0.5364(2) 0.0457(9) Uani 0.756(4) 1 d D U P A 1 H11A H 0.581043 0.370028 0.561790 0.055 Uiso 0.756(4) 1 calc R . P A 1 H11B H 0.617845 0.261417 0.561181 0.055 Uiso 0.756(4) 1 calc R . P A 1 C12 C 0.6321(3) 0.3533(5) 0.4987(2) 0.0433(11) Uani 0.756(4) 1 d D U P A 1 H12A H 0.602615 0.410449 0.475699 0.052 Uiso 0.756(4) 1 calc R . P A 1 H12B H 0.635187 0.299951 0.471841 0.052 Uiso 0.756(4) 1 calc R . P A 1 C13 C 0.7176(3) 0.3863(4) 0.5341(3) 0.0482(10) Uani 0.756(4) 1 d D U P A 1 H13A H 0.744898 0.331624 0.560369 0.058 Uiso 0.756(4) 1 calc R . P A 1 H13B H 0.714407 0.444722 0.557801 0.058 Uiso 0.756(4) 1 calc R . P A 1 C14 C 0.7683(2) 0.4143(4) 0.4960(2) 0.0517(10) Uani 0.756(4) 1 d D U P A 1 H14A H 0.767508 0.357565 0.470140 0.062 Uiso 0.756(4) 1 calc R . P A 1 H14B H 0.742790 0.472104 0.471782 0.062 Uiso 0.756(4) 1 calc R . P A 1 C15 C 0.8537(3) 0.4395(3) 0.5288(2) 0.0520(11) Uani 0.756(4) 1 d D U P A 1 H15A H 0.875884 0.385463 0.556974 0.062 Uiso 0.756(4) 1 calc R . P A 1 H15B H 0.884385 0.438939 0.501787 0.062 Uiso 0.756(4) 1 calc R . P A 1 C16 C 0.8702(4) 0.5357(4) 0.5602(3) 0.096(2) Uani 0.756(4) 1 d D U P A 1 H16A H 0.888689 0.584778 0.537932 0.144 Uiso 0.756(4) 1 calc GR . P A 1 H16B H 0.912183 0.525995 0.597561 0.144 Uiso 0.756(4) 1 calc GR . P A 1 H16C H 0.820634 0.559828 0.565700 0.144 Uiso 0.756(4) 1 calc GR . P A 1 C11A C 0.5905(5) 0.2699(12) 0.5302(7) 0.0457(9) Uani 0.244(4) 1 d D U P A 2 H11C H 0.610392 0.207483 0.518088 0.055 Uiso 0.244(4) 1 calc R . P A 2 H11D H 0.608331 0.270828 0.572584 0.055 Uiso 0.244(4) 1 calc R . P A 2 C12A C 0.6254(9) 0.3598(16) 0.5087(10) 0.0483(16) Uani 0.244(4) 1 d D U P A 2 H12C H 0.604850 0.422277 0.520192 0.058 Uiso 0.244(4) 1 calc R . P A 2 H12D H 0.608672 0.358174 0.466364 0.058 Uiso 0.244(4) 1 calc R . P A 2 C13A C 0.7180(9) 0.3561(11) 0.5348(10) 0.0477(15) Uani 0.244(4) 1 d D U P A 2 H13C H 0.732773 0.339584 0.576054 0.057 Uiso 0.244(4) 1 calc R . P A 2 H13D H 0.737880 0.301314 0.516277 0.057 Uiso 0.244(4) 1 calc R . P A 2 C14A C 0.7615(6) 0.4521(9) 0.5292(6) 0.0472(15) Uani 0.244(4) 1 d D U P A 2 H14C H 0.757696 0.455826 0.488412 0.057 Uiso 0.244(4) 1 calc R . P A 2 H14D H 0.727820 0.507271 0.535318 0.057 Uiso 0.244(4) 1 calc R . P A 2 C15A C 0.8480(7) 0.4796(12) 0.5634(7) 0.0545(17) Uani 0.244(4) 1 d D U P A 2 H15C H 0.882374 0.419431 0.574800 0.065 Uiso 0.244(4) 1 calc R . P A 2 H15D H 0.871322 0.524664 0.541321 0.065 Uiso 0.244(4) 1 calc R . P A 2 C16A C 0.8391(12) 0.5320(14) 0.6150(8) 0.096(2) Uani 0.244(4) 1 d D U P A 2 H16D H 0.855677 0.601870 0.615200 0.144 Uiso 0.244(4) 1 calc GR . P A 2 H16E H 0.873259 0.498962 0.650048 0.144 Uiso 0.244(4) 1 calc GR . P A 2 H16F H 0.782477 0.529079 0.613178 0.144 Uiso 0.244(4) 1 calc GR . P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ru1 0.01800(10) 0.01699(9) 0.01951(10) -0.00159(7) 0.00411(7) -0.00468(7) Cl1 0.0169(3) 0.0305(3) 0.0275(3) -0.0037(2) 0.0057(2) -0.0020(2) Cl2 0.0266(3) 0.0190(3) 0.0263(3) -0.0041(2) 0.0055(2) -0.0021(2) S1 0.0178(3) 0.0248(3) 0.0178(3) -0.0016(2) 0.0019(2) -0.0084(2) O1 0.0233(9) 0.0854(17) 0.0197(9) 0.0001(10) 0.0022(7) -0.0202(10) N1 0.0158(9) 0.0265(10) 0.0185(9) -0.0016(8) 0.0016(7) -0.0059(8) N2 0.0160(9) 0.0312(11) 0.0198(9) 0.0007(8) 0.0024(7) -0.0060(8) C1 0.0163(10) 0.0204(11) 0.0186(10) 0.0006(8) 0.0007(8) -0.0025(8) C8 0.0171(11) 0.0458(16) 0.0225(12) 0.0012(11) -0.0004(9) -0.0059(11) C9 0.0185(12) 0.0612(19) 0.0239(13) -0.0013(12) -0.0003(10) -0.0121(12) C10 0.0187(13) 0.066(2) 0.064(2) 0.0070(18) 0.0028(14) -0.0016(14) C17 0.0339(13) 0.0246(12) 0.0192(11) 0.0012(9) 0.0022(10) -0.0032(10) C18 0.0263(12) 0.0257(12) 0.0184(11) -0.0013(9) 0.0000(9) -0.0040(10) C19 0.0301(13) 0.0208(11) 0.0209(11) -0.0044(9) 0.0055(10) -0.0059(10) C20 0.0318(13) 0.0287(13) 0.0221(11) -0.0045(10) 0.0114(10) -0.0067(10) C21 0.0336(14) 0.0309(13) 0.0255(12) -0.0014(10) 0.0134(11) -0.0114(11) C22 0.0373(14) 0.0290(13) 0.0222(12) 0.0013(10) 0.0093(10) -0.0091(11) C23 0.0372(15) 0.0243(13) 0.0304(14) -0.0015(10) -0.0035(11) 0.0020(11) C24 0.0305(14) 0.0380(16) 0.0446(17) -0.0095(13) -0.0006(12) 0.0067(12) C25 0.065(2) 0.0328(16) 0.0353(16) 0.0066(13) -0.0070(15) 0.0065(15) C26 0.0329(14) 0.0358(15) 0.0365(14) -0.0103(12) 0.0154(12) -0.0032(12) C2 0.0162(12) 0.0295(19) 0.0212(16) -0.0057(14) 0.0064(11) -0.0061(13) C7 0.0173(17) 0.036(2) 0.0242(19) -0.0013(19) 0.0041(14) -0.0017(15) C6 0.0190(17) 0.059(3) 0.0255(19) -0.001(2) 0.0057(14) 0.000(2) C5 0.024(2) 0.062(4) 0.031(2) -0.020(2) 0.0107(17) -0.020(2) C4 0.036(3) 0.036(3) 0.042(3) -0.017(2) 0.023(2) -0.018(2) C3 0.026(2) 0.027(2) 0.031(2) -0.0062(17) 0.0122(18) -0.0029(17) C2A 0.0162(12) 0.0295(19) 0.0212(16) -0.0057(14) 0.0064(11) -0.0061(13) C7A 0.022(5) 0.034(7) 0.028(6) 0.001(5) 0.011(4) -0.010(4) C6A 0.011(4) 0.033(6) 0.022(5) -0.006(5) 0.000(4) -0.004(5) C5A 0.020(6) 0.028(6) 0.037(7) -0.013(5) 0.015(5) -0.009(5) C4A 0.026(6) 0.028(6) 0.034(7) -0.009(5) 0.013(5) -0.008(4) C3A 0.019(5) 0.024(5) 0.038(7) -0.006(4) 0.015(5) -0.010(4) C11 0.0241(14) 0.056(2) 0.0514(18) 0.0054(19) 0.0053(13) 0.0052(16) C12 0.0255(16) 0.0508(19) 0.050(2) 0.0000(17) 0.0080(14) 0.0021(15) C13 0.0276(15) 0.047(2) 0.0617(19) 0.004(2) 0.0041(15) 0.0042(16) C14 0.0356(17) 0.049(2) 0.063(2) 0.0111(17) 0.0063(16) -0.0017(16) C15 0.0403(19) 0.044(2) 0.063(2) 0.0063(18) 0.0057(18) -0.0018(17) C16 0.066(3) 0.055(3) 0.117(4) -0.029(3) -0.034(3) 0.013(3) C11A 0.0241(14) 0.056(2) 0.0514(18) 0.0054(19) 0.0053(13) 0.0052(16) C12A 0.027(2) 0.052(3) 0.058(3) 0.001(2) 0.004(2) 0.003(2) C13A 0.029(2) 0.049(3) 0.060(3) 0.005(3) 0.008(2) 0.001(2) C14A 0.030(2) 0.042(3) 0.063(3) 0.003(2) 0.007(2) 0.002(2) C15A 0.037(3) 0.045(3) 0.069(3) 0.005(3) 0.002(3) 0.003(3) C16A 0.066(3) 0.055(3) 0.117(4) -0.029(3) -0.034(3) 0.013(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cl2 Ru1 Cl1 88.13(2) . . ? S1 Ru1 Cl1 93.94(2) . . ? S1 Ru1 Cl2 88.12(2) . . ? C17 Ru1 Cl1 152.91(7) . . ? C17 Ru1 Cl2 89.58(7) . . ? C17 Ru1 S1 112.96(7) . . ? C17 Ru1 C20 82.01(10) . . ? C18 Ru1 Cl1 155.21(7) . . ? C18 Ru1 Cl2 116.66(7) . . ? C18 Ru1 S1 87.17(7) . . ? C18 Ru1 C17 37.61(9) . . ? C18 Ru1 C19 38.08(9) . . ? C18 Ru1 C20 68.32(10) . . ? C18 Ru1 C21 80.25(10) . . ? C19 Ru1 Cl1 117.14(7) . . ? C19 Ru1 Cl2 154.67(7) . . ? C19 Ru1 S1 88.51(7) . . ? C19 Ru1 C17 68.78(9) . . ? C19 Ru1 C20 37.30(9) . . ? C20 Ru1 Cl1 89.19(7) . . ? C20 Ru1 Cl2 155.84(7) . . ? C20 Ru1 S1 116.02(7) . . ? C21 Ru1 Cl1 88.47(8) . . ? C21 Ru1 Cl2 117.67(7) . . ? C21 Ru1 S1 154.19(7) . . ? C21 Ru1 C17 68.84(11) . . ? C21 Ru1 C19 67.74(9) . . ? C21 Ru1 C20 38.24(9) . . ? C22 Ru1 Cl1 114.43(7) . . ? C22 Ru1 Cl2 90.60(7) . . ? C22 Ru1 S1 151.55(8) . . ? C22 Ru1 C17 38.59(10) . . ? C22 Ru1 C18 68.12(10) . . ? C22 Ru1 C19 80.65(10) . . ? C22 Ru1 C20 68.78(10) . . ? C22 Ru1 C21 37.53(10) . . ? C1 S1 Ru1 115.33(8) . . ? C1 N1 H1A 118.1 . . ? C1 N1 H1B 116.3 . . ? C1 N1 C2 123.7(3) . . ? C1 N1 C2A 127.4(10) . . ? C2 N1 H1A 118.1 . . ? C2A N1 H1B 116.3 . . ? C1 N2 H2 116.2 . . ? C8 N2 H2 116.2 . . ? C8 N2 C1 127.6(2) . . ? N1 C1 S1 121.39(17) . . ? N1 C1 N2 118.6(2) . . ? N2 C1 S1 119.95(18) . . ? O1 C8 N2 122.4(2) . . ? O1 C8 C9 122.7(2) . . ? N2 C8 C9 114.8(2) . . ? C8 C9 H9A 109.8 . . ? C8 C9 H9B 109.8 . . ? C8 C9 C10 109.4(3) . . ? H9A C9 H9B 108.2 . . ? C10 C9 H9A 109.8 . . ? C10 C9 H9B 109.8 . . ? C9 C10 H10A 109.4 . . ? C9 C10 H10B 109.4 . . ? C9 C10 H10C 104.3 . . ? C9 C10 H10D 104.3 . . ? C9 C10 C11 111.0(3) . . ? H10A C10 H10B 108.0 . . ? H10C C10 H10D 105.6 . . ? C11 C10 H10A 109.4 . . ? C11 C10 H10B 109.4 . . ? C11A C10 C9 131.8(7) . . ? C11A C10 H10C 104.3 . . ? C11A C10 H10D 104.3 . . ? C18 C17 Ru1 70.72(14) . . ? C18 C17 C22 117.6(2) . . ? C18 C17 C23 122.4(2) . . ? C22 C17 Ru1 70.19(14) . . ? C22 C17 C23 120.0(2) . . ? C23 C17 Ru1 129.95(18) . . ? Ru1 C18 H18 130.5 . . ? C17 C18 Ru1 71.67(14) . . ? C17 C18 H18 119.2 . . ? C17 C18 C19 121.7(2) . . ? C19 C18 Ru1 71.43(14) . . ? C19 C18 H18 119.2 . . ? Ru1 C19 H19 130.3 . . ? C18 C19 Ru1 70.49(13) . . ? C18 C19 H19 119.5 . . ? C20 C19 Ru1 72.35(14) . . ? C20 C19 C18 121.0(2) . . ? C20 C19 H19 119.5 . . ? C19 C20 Ru1 70.34(14) . . ? C19 C20 C21 117.5(2) . . ? C19 C20 C26 121.2(2) . . ? C21 C20 Ru1 69.57(14) . . ? C21 C20 C26 121.3(2) . . ? C26 C20 Ru1 129.66(18) . . ? Ru1 C21 H21 130.3 . . ? C20 C21 Ru1 72.19(14) . . ? C20 C21 H21 119.2 . . ? C22 C21 Ru1 71.05(15) . . ? C22 C21 C20 121.6(2) . . ? C22 C21 H21 119.2 . . ? Ru1 C22 H22 130.3 . . ? C17 C22 Ru1 71.21(14) . . ? C17 C22 H22 119.7 . . ? C21 C22 Ru1 71.42(15) . . ? C21 C22 C17 120.6(2) . . ? C21 C22 H22 119.7 . . ? C17 C23 H23 107.6 . . ? C17 C23 C24 114.4(2) . . ? C17 C23 C25 108.3(2) . . ? C24 C23 H23 107.6 . . ? C24 C23 C25 111.1(3) . . ? C25 C23 H23 107.6 . . ? C23 C24 H24A 109.5 . . ? C23 C24 H24B 109.5 . . ? C23 C24 H24C 109.5 . . ? H24A C24 H24B 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C23 C25 H25A 109.5 . . ? C23 C25 H25B 109.5 . . ? C23 C25 H25C 109.5 . . ? H25A C25 H25B 109.5 . . ? H25A C25 H25C 109.5 . . ? H25B C25 H25C 109.5 . . ? C20 C26 H26A 109.5 . . ? C20 C26 H26B 109.5 . . ? C20 C26 H26C 109.5 . . ? H26A C26 H26B 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C7 C2 N1 120.7(3) . . ? C7 C2 C3 120.0 . . ? C3 C2 N1 119.3(3) . . ? C2 C7 H7 120.0 . . ? C6 C7 C2 120.0 . . ? C6 C7 H7 120.0 . . ? C7 C6 H6 120.0 . . ? C5 C6 C7 120.0 . . ? C5 C6 H6 120.0 . . ? C6 C5 H5 120.0 . . ? C6 C5 C4 120.0 . . ? C4 C5 H5 120.0 . . ? C5 C4 H4 120.0 . . ? C3 C4 C5 120.0 . . ? C3 C4 H4 120.0 . . ? C2 C3 H3 120.0 . . ? C4 C3 C2 120.0 . . ? C4 C3 H3 120.0 . . ? C7A C2A N1 121.1(8) . . ? C7A C2A C3A 120.0 . . ? C3A C2A N1 118.9(8) . . ? C2A C7A H7A 120.0 . . ? C6A C7A C2A 120.0 . . ? C6A C7A H7A 120.0 . . ? C7A C6A H6A 120.0 . . ? C7A C6A C5A 120.0 . . ? C5A C6A H6A 120.0 . . ? C6A C5A H5A 120.0 . . ? C6A C5A C4A 120.0 . . ? C4A C5A H5A 120.0 . . ? C5A C4A H4A 120.0 . . ? C3A C4A C5A 120.0 . . ? C3A C4A H4A 120.0 . . ? C2A C3A H3A 120.0 . . ? C4A C3A C2A 120.0 . . ? C4A C3A H3A 120.0 . . ? C10 C11 H11A 107.9 . . ? C10 C11 H11B 107.9 . . ? H11A C11 H11B 107.2 . . ? C12 C11 C10 117.4(4) . . ? C12 C11 H11A 107.9 . . ? C12 C11 H11B 107.9 . . ? C11 C12 H12A 109.2 . . ? C11 C12 H12B 109.2 . . ? C11 C12 C13 111.9(4) . . ? H12A C12 H12B 107.9 . . ? C13 C12 H12A 109.2 . . ? C13 C12 H12B 109.2 . . ? C12 C13 H13A 109.2 . . ? C12 C13 H13B 109.2 . . ? C12 C13 C14 112.1(5) . . ? H13A C13 H13B 107.9 . . ? C14 C13 H13A 109.2 . . ? C14 C13 H13B 109.2 . . ? C13 C14 H14A 108.8 . . ? C13 C14 H14B 108.8 . . ? H14A C14 H14B 107.7 . . ? C15 C14 C13 113.8(4) . . ? C15 C14 H14A 108.8 . . ? C15 C14 H14B 108.8 . . ? C14 C15 H15A 107.8 . . ? C14 C15 H15B 107.8 . . ? H15A C15 H15B 107.1 . . ? C16 C15 C14 118.0(5) . . ? C16 C15 H15A 107.8 . . ? C16 C15 H15B 107.8 . . ? C15 C16 H16A 109.5 . . ? C15 C16 H16B 109.5 . . ? C15 C16 H16C 109.5 . . ? H16A C16 H16B 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C10 C11A H11C 109.8 . . ? C10 C11A H11D 109.8 . . ? C10 C11A C12A 109.5(10) . . ? H11C C11A H11D 108.2 . . ? C12A C11A H11C 109.8 . . ? C12A C11A H11D 109.8 . . ? C11A C12A H12C 110.0 . . ? C11A C12A H12D 110.0 . . ? C11A C12A C13A 108.7(11) . . ? H12C C12A H12D 108.3 . . ? C13A C12A H12C 110.0 . . ? C13A C12A H12D 110.0 . . ? C12A C13A H13C 108.5 . . ? C12A C13A H13D 108.4 . . ? H13C C13A H13D 107.5 . . ? C14A C13A C12A 115.3(11) . . ? C14A C13A H13C 108.4 . . ? C14A C13A H13D 108.4 . . ? C13A C14A H14C 105.7 . . ? C13A C14A H14D 105.7 . . ? H14C C14A H14D 106.2 . . ? C15A C14A C13A 126.4(12) . . ? C15A C14A H14C 105.7 . . ? C15A C14A H14D 105.7 . . ? C14A C15A H15C 111.3 . . ? C14A C15A H15D 111.3 . . ? H15C C15A H15D 109.2 . . ? C16A C15A C14A 102.6(11) . . ? C16A C15A H15C 111.3 . . ? C16A C15A H15D 111.3 . . ? C15A C16A H16D 109.5 . . ? C15A C16A H16E 109.5 . . ? C15A C16A H16F 109.5 . . ? H16D C16A H16E 109.5 . . ? H16D C16A H16F 109.5 . . ? H16E C16A H16F 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ru1 Cl1 2.4406(6) . ? Ru1 Cl2 2.4213(6) . ? Ru1 S1 2.3987(6) . ? Ru1 C17 2.185(2) . ? Ru1 C18 2.173(2) . ? Ru1 C19 2.185(2) . ? Ru1 C20 2.211(2) . ? Ru1 C21 2.176(3) . ? Ru1 C22 2.171(3) . ? S1 C1 1.703(2) . ? O1 C8 1.214(3) . ? N1 H1A 0.8800 . ? N1 H1B 0.8800 . ? N1 C1 1.321(3) . ? N1 C2 1.432(3) . ? N1 C2A 1.409(7) . ? N2 H2 0.8800 . ? N2 C1 1.369(3) . ? N2 C8 1.367(3) . ? C8 C9 1.515(3) . ? C9 H9A 0.9900 . ? C9 H9B 0.9900 . ? C9 C10 1.522(5) . ? C10 H10A 0.9900 . ? C10 H10B 0.9900 . ? C10 H10C 0.9900 . ? C10 H10D 0.9900 . ? C10 C11 1.551(5) . ? C10 C11A 1.513(8) . ? C17 C18 1.405(3) . ? C17 C22 1.440(4) . ? C17 C23 1.513(4) . ? C18 H18 0.9500 . ? C18 C19 1.421(4) . ? C19 H19 0.9500 . ? C19 C20 1.406(4) . ? C20 C21 1.437(4) . ? C20 C26 1.491(4) . ? C21 H21 0.9500 . ? C21 C22 1.398(4) . ? C22 H22 0.9500 . ? C23 H23 1.0000 . ? C23 C24 1.518(4) . ? C23 C25 1.543(4) . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? C25 H25A 0.9800 . ? C25 H25B 0.9800 . ? C25 H25C 0.9800 . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C2 C7 1.3900 . ? C2 C3 1.3900 . ? C7 H7 0.9500 . ? C7 C6 1.3900 . ? C6 H6 0.9500 . ? C6 C5 1.3900 . ? C5 H5 0.9500 . ? C5 C4 1.3900 . ? C4 H4 0.9500 . ? C4 C3 1.3900 . ? C3 H3 0.9500 . ? C2A C7A 1.3900 . ? C2A C3A 1.3900 . ? C7A H7A 0.9500 . ? C7A C6A 1.3900 . ? C6A H6A 0.9500 . ? C6A C5A 1.3900 . ? C5A H5A 0.9500 . ? C5A C4A 1.3900 . ? C4A H4A 0.9500 . ? C4A C3A 1.3900 . ? C3A H3A 0.9500 . ? C11 H11A 0.9900 . ? C11 H11B 0.9900 . ? C11 C12 1.523(5) . ? C12 H12A 0.9900 . ? C12 H12B 0.9900 . ? C12 C13 1.529(5) . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C13 C14 1.545(6) . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C14 C15 1.485(5) . ? C15 H15A 0.9900 . ? C15 H15B 0.9900 . ? C15 C16 1.481(6) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C11A H11C 0.9900 . ? C11A H11D 0.9900 . ? C11A C12A 1.524(9) . ? C12A H12C 0.9900 . ? C12A H12D 0.9900 . ? C12A C13A 1.536(8) . ? C13A H13C 0.9900 . ? C13A H13D 0.9900 . ? C13A C14A 1.526(8) . ? C14A H14C 0.9900 . ? C14A H14D 0.9900 . ? C14A C15A 1.515(8) . ? C15A H15C 0.9900 . ? C15A H15D 0.9900 . ? C15A C16A 1.511(9) . ? C16A H16D 0.9800 . ? C16A H16E 0.9800 . ? C16A H16F 0.9800 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag N1 H1A O1 0.88 2.19 2.905(3) 138.4 7_556 yes N1 H1B O1 0.88 1.95 2.645(3) 134.6 . yes N2 H2 Cl1 0.88 2.25 3.081(2) 156.5 . yes N2 H2 Cl2 0.88 2.73 3.173(2) 112.2 . yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Ru1 S1 C1 N1 163.20(17) . . . . ? Ru1 S1 C1 N2 -20.0(2) . . . . ? Ru1 C17 C18 C19 -53.2(2) . . . . ? Ru1 C17 C22 C21 53.7(2) . . . . ? Ru1 C17 C23 C24 -60.6(3) . . . . ? Ru1 C17 C23 C25 175.0(2) . . . . ? Ru1 C18 C19 C20 -53.9(2) . . . . ? Ru1 C19 C20 C21 -52.9(2) . . . . ? Ru1 C19 C20 C26 125.2(2) . . . . ? Ru1 C20 C21 C22 -53.3(2) . . . . ? Ru1 C21 C22 C17 -53.6(2) . . . . ? O1 C8 C9 C10 70.7(4) . . . . ? N1 C2 C7 C6 179.6(6) . . . . ? N1 C2 C3 C4 -179.7(6) . . . . ? N1 C2A C7A C6A -179(2) . . . . ? N1 C2A C3A C4A 179.3(19) . . . . ? N2 C8 C9 C10 -107.2(3) . . . . ? C1 N1 C2 C7 -58.2(5) . . . . ? C1 N1 C2 C3 121.5(3) . . . . ? C1 N1 C2A C7A -64.0(15) . . . . ? C1 N1 C2A C3A 116.6(9) . . . . ? C1 N2 C8 O1 -2.5(5) . . . . ? C1 N2 C8 C9 175.4(2) . . . . ? C8 N2 C1 S1 -176.3(2) . . . . ? C8 N2 C1 N1 0.7(4) . . . . ? C8 C9 C10 C11 -170.0(3) . . . . ? C8 C9 C10 C11A 176.3(10) . . . . ? C9 C10 C11 C12 -70.6(6) . . . . ? C9 C10 C11A C12A -16(2) . . . . ? C10 C11 C12 C13 -176.7(4) . . . . ? C10 C11A C12A C13A 178.9(16) . . . . ? C17 C18 C19 Ru1 53.3(2) . . . . ? C17 C18 C19 C20 -0.6(4) . . . . ? C18 C17 C22 Ru1 -54.2(2) . . . . ? C18 C17 C22 C21 -0.6(4) . . . . ? C18 C17 C23 C24 30.6(3) . . . . ? C18 C17 C23 C25 -93.8(3) . . . . ? C18 C19 C20 Ru1 53.1(2) . . . . ? C18 C19 C20 C21 0.2(4) . . . . ? C18 C19 C20 C26 178.3(2) . . . . ? C19 C20 C21 Ru1 53.3(2) . . . . ? C19 C20 C21 C22 0.0(4) . . . . ? C20 C21 C22 Ru1 53.8(2) . . . . ? C20 C21 C22 C17 0.2(4) . . . . ? C22 C17 C18 Ru1 54.0(2) . . . . ? C22 C17 C18 C19 0.8(4) . . . . ? C22 C17 C23 C24 -149.1(2) . . . . ? C22 C17 C23 C25 86.5(3) . . . . ? C23 C17 C18 Ru1 -125.7(2) . . . . ? C23 C17 C18 C19 -178.9(2) . . . . ? C23 C17 C22 Ru1 125.5(2) . . . . ? C23 C17 C22 C21 179.1(2) . . . . ? C26 C20 C21 Ru1 -124.8(2) . . . . ? C26 C20 C21 C22 -178.1(2) . . . . ? C2 N1 C1 S1 -7.8(4) . . . . ? C2 N1 C1 N2 175.3(3) . . . . ? C2 C7 C6 C5 0.0 . . . . ? C7 C2 C3 C4 0.0 . . . . ? C7 C6 C5 C4 0.0 . . . . ? C6 C5 C4 C3 0.0 . . . . ? C5 C4 C3 C2 0.0 . . . . ? C3 C2 C7 C6 0.0 . . . . ? C2A N1 C1 S1 3.3(9) . . . . ? C2A N1 C1 N2 -173.6(9) . . . . ? C2A C7A C6A C5A 0.0 . . . . ? C7A C2A C3A C4A 0.0 . . . . ? C7A C6A C5A C4A 0.0 . . . . ? C6A C5A C4A C3A 0.0 . . . . ? C5A C4A C3A C2A 0.0 . . . . ? C3A C2A C7A C6A 0.0 . . . . ? C11 C12 C13 C14 173.6(5) . . . . ? C12 C13 C14 C15 -175.7(5) . . . . ? C13 C14 C15 C16 -72.2(7) . . . . ? C11A C12A C13A C14A -166.4(18) . . . . ? C12A C13A C14A C15A 162.7(18) . . . . ? C13A C14A C15A C16A -89(2) . . . . ?