#------------------------------------------------------------------------------ #$Date: 2021-10-20 02:22:01 +0300 (Wed, 20 Oct 2021) $ #$Revision: 270041 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/85/7708589.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708589 loop_ _publ_author_name 'Henry, Andrew Timothy' 'Cosby, Taylor P. L.' 'Boyle, Paul D.' 'Baines, Kim M.' _publ_section_title ; Assessing the Lewis Acidity and Catalytic Activity of Bis(catecholato)germanes ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT03180E _journal_year 2021 _chemical_formula_sum 'C28 H36 Br8 Cl Ge N O4' _chemical_formula_weight 1197.90 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2016/6 _audit_update_record ; 2021-06-15 deposited with the CCDC. 2021-10-18 downloaded from the CCDC. ; _cell_angle_alpha 84.984(10) _cell_angle_beta 88.202(8) _cell_angle_gamma 73.534(13) _cell_formula_units_Z 2 _cell_length_a 9.864(5) _cell_length_b 11.942(6) _cell_length_c 16.473(7) _cell_measurement_reflns_used 9198 _cell_measurement_temperature 223 _cell_measurement_theta_max 30.45 _cell_measurement_theta_min 2.38 _cell_volume 1853.7(15) _computing_cell_refinement SAINT _computing_data_collection Apex3 _computing_data_reduction SAINT _computing_molecular_graphics Mercury _computing_publication_material cif2tables.py _computing_structure_refinement SHELXL _computing_structure_solution SHELXT _diffrn_ambient_temperature 223 _diffrn_detector 'CCD plate' _diffrn_detector_type 'Bruker Apex2' _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device '\k-geometry diffractometer' _diffrn_measurement_device_type 'Bruker Kappa Axis Apex2' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0456 _diffrn_reflns_av_unetI/netI 0.0243 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 112781 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.556 _diffrn_reflns_theta_min 1.241 _diffrn_source 'sealed tube' _exptl_absorpt_coefficient_mu 9.554 _exptl_absorpt_correction_T_max 0.7461 _exptl_absorpt_correction_T_min 0.3819 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 2.146 _exptl_crystal_description prism _exptl_crystal_F_000 1144 _exptl_crystal_size_max 0.354 _exptl_crystal_size_mid 0.340 _exptl_crystal_size_min 0.144 _refine_diff_density_max 0.941 _refine_diff_density_min -0.928 _refine_diff_density_rms 0.099 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.033 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 392 _refine_ls_number_reflns 11316 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.033 _refine_ls_R_factor_all 0.0462 _refine_ls_R_factor_gt 0.0275 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0219P)^2^+1.5099P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0518 _refine_ls_wR_factor_ref 0.0571 _reflns_Friedel_coverage 0.000 _reflns_number_gt 8838 _reflns_number_total 11316 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt03180e3.cif _cod_data_source_block b21079 _cod_original_cell_volume 1853.6(16) _cod_database_code 7708589 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.133 _shelx_estimated_absorpt_t_max 0.340 _shelx_res_file ; TITL b21079 in P-1 b21079.res created by SHELXL-2016/6 at 10:24:13 on 11-Feb-2021 CELL 0.71073 9.86361 11.94167 16.47349 84.9840 88.2024 73.5336 ZERR 2 0.00548 0.00573 0.00708 0.0095 0.0083 0.0130 LATT 1 SFAC C H N O CL GE BR UNIT 56 72 2 8 2 2 16 TEMP -50.150 SIZE 0.144 0.34 0.354 ACTA REM omitted reflections chosen by beamstop_omit.py program: REM Please verify reflections are blocked on the images (verified by P. Boyle) OMIT 0 1 0 OMIT 0 1 1 OMIT 1 0 0 OMIT 0 -1 1 OMIT 1 1 0 OMIT 1 0 1 OMIT 0 0 2 OMIT -1 0 1 L.S. 12 4 FMAP 2 PLAN 20 BOND $H CONF REM Instructions for potential hydrogen bonds HTAB C13 O4 HTAB C13 Br9 HTAB C14 Br9 EQIV $1 x-1, y, z HTAB C17 Cl1_$1 HTAB C18 Br3 EQIV $2 -x+1, -y+1, -z HTAB C21 Br4_$2 EQIV $3 -x+1, -y+1, -z+1 HTAB C26 Br10_$3 WGHT 0.021900 1.509900 FVAR 0.24249 MOLE 1 GE1 6 0.952296 0.237073 0.249929 11.00000 0.01608 0.03326 = 0.01584 -0.00160 0.00150 -0.00718 CL1 5 0.921905 0.423955 0.246910 11.00000 0.03112 0.03354 = 0.04354 -0.00016 0.00236 -0.00930 O1 4 1.101123 0.179517 0.180891 11.00000 0.01841 0.04889 = 0.01888 -0.00738 0.00092 -0.00463 O2 4 0.833243 0.228505 0.167337 11.00000 0.01828 0.05188 = 0.01755 -0.00605 0.00264 -0.01045 O3 4 1.081071 0.187222 0.333888 11.00000 0.01704 0.04413 = 0.01751 0.00021 0.00098 -0.00820 O4 4 0.815777 0.213175 0.322319 11.00000 0.01768 0.04366 = 0.01679 0.00271 -0.00115 -0.01116 C1 1 1.054416 0.173538 0.105849 11.00000 0.02303 0.02998 = 0.01872 -0.00377 0.00159 -0.00458 C2 1 0.907511 0.201090 0.098238 11.00000 0.02224 0.02910 = 0.01870 -0.00149 0.00252 -0.00742 C3 1 0.848149 0.198215 0.023597 11.00000 0.02201 0.03117 = 0.02078 -0.00156 -0.00036 -0.00634 C4 1 0.936470 0.166232 -0.044000 11.00000 0.03374 0.02889 = 0.01773 -0.00249 -0.00124 -0.00598 C5 1 1.082008 0.138643 -0.036073 11.00000 0.02892 0.03178 = 0.02002 -0.00473 0.00840 -0.00293 C6 1 1.141760 0.141565 0.039386 11.00000 0.01948 0.03422 = 0.02384 -0.00249 0.00398 -0.00301 C7 1 1.013620 0.174618 0.404589 11.00000 0.01905 0.02627 = 0.01930 -0.00062 0.00156 -0.00687 C8 1 0.868423 0.188121 0.398467 11.00000 0.02079 0.02727 = 0.01787 0.00081 -0.00221 -0.00839 C9 1 0.788545 0.176267 0.467534 11.00000 0.01897 0.02996 = 0.02317 0.00090 0.00073 -0.00970 C10 1 0.853720 0.148999 0.543842 11.00000 0.02537 0.02733 = 0.01799 -0.00140 0.00268 -0.01054 C11 1 0.997618 0.135968 0.550302 11.00000 0.02597 0.02526 = 0.01668 -0.00168 -0.00387 -0.00762 C12 1 1.077793 0.150064 0.480223 11.00000 0.01906 0.02666 = 0.02374 -0.00432 -0.00099 -0.00737 BR3 7 0.650422 0.239029 0.016018 11.00000 0.02315 0.06893 = 0.02767 -0.00795 -0.00228 -0.01022 BR4 7 0.856892 0.159861 -0.145611 11.00000 0.04191 0.05088 = 0.02036 -0.00694 -0.00499 -0.00409 BR5 7 1.202101 0.096832 -0.126328 11.00000 0.03851 0.07690 = 0.02553 -0.01592 0.01039 -0.00044 BR6 7 1.338365 0.101981 0.054520 11.00000 0.02085 0.06808 = 0.03583 -0.01593 0.00521 -0.00344 BR9 7 0.592813 0.203054 0.455110 11.00000 0.01996 0.07267 = 0.02998 0.01026 -0.00050 -0.01750 BR10 7 0.744369 0.130022 0.636990 11.00000 0.03460 0.05105 = 0.02046 0.00034 0.00562 -0.02015 BR11 7 1.084842 0.101093 0.653072 11.00000 0.03631 0.04930 = 0.01926 -0.00048 -0.00699 -0.01714 BR12 7 1.271391 0.138506 0.484919 11.00000 0.02094 0.06379 = 0.02833 -0.00197 -0.00379 -0.01571 MOLE 2 N1 3 0.365568 0.444088 0.241304 11.00000 0.02058 0.02243 = 0.02234 0.00050 0.00051 -0.00544 C13 1 0.479493 0.327768 0.239155 11.00000 0.01947 0.02027 = 0.02372 -0.00047 -0.00051 -0.00362 AFIX 23 H13A 2 0.527021 0.325892 0.185942 11.00000 -1.20000 H13B 2 0.550091 0.324036 0.280620 11.00000 -1.20000 AFIX 0 C14 1 0.427403 0.219574 0.253497 11.00000 0.02316 0.02325 = 0.02789 -0.00243 0.00170 -0.00761 AFIX 23 H14A 2 0.350113 0.225403 0.215959 11.00000 -1.20000 H14B 2 0.391051 0.214321 0.309329 11.00000 -1.20000 AFIX 0 C15 1 0.547538 0.110326 0.240124 11.00000 0.02666 0.02270 = 0.03622 -0.00148 0.00703 -0.00611 AFIX 23 H15A 2 0.574544 0.110557 0.182364 11.00000 -1.20000 H15B 2 0.629907 0.110912 0.271663 11.00000 -1.20000 AFIX 0 C16 1 0.504421 0.000159 0.265848 11.00000 0.04902 0.02357 = 0.04849 0.00078 0.01256 -0.01042 AFIX 137 H16A 2 0.492594 -0.006601 0.324582 11.00000 -1.50000 H16B 2 0.577158 -0.067679 0.249420 11.00000 -1.50000 H16C 2 0.415930 0.004287 0.239996 11.00000 -1.50000 AFIX 0 C17 1 0.255165 0.457276 0.176088 11.00000 0.01968 0.02866 = 0.02940 0.00052 -0.00270 -0.00330 AFIX 23 H17A 2 0.201985 0.400393 0.190772 11.00000 -1.20000 H17B 2 0.188545 0.535643 0.176743 11.00000 -1.20000 AFIX 0 C18 1 0.310596 0.440774 0.090211 11.00000 0.02855 0.04999 = 0.02749 0.00040 -0.00350 -0.01069 AFIX 23 H18A 2 0.374664 0.361681 0.087573 11.00000 -1.20000 H18B 2 0.363679 0.497253 0.073981 11.00000 -1.20000 AFIX 0 C19 1 0.187694 0.458658 0.032581 11.00000 0.04124 0.05663 = 0.03331 0.00347 -0.01257 -0.01227 AFIX 23 H19A 2 0.131614 0.405310 0.051139 11.00000 -1.20000 H19B 2 0.126539 0.539101 0.033515 11.00000 -1.20000 AFIX 0 C20 1 0.238868 0.436330 -0.053847 11.00000 0.07543 0.10224 = 0.03044 0.00353 -0.01617 -0.01509 AFIX 137 H20A 2 0.288849 0.492621 -0.073667 11.00000 -1.50000 H20B 2 0.158476 0.444441 -0.088586 11.00000 -1.50000 H20C 2 0.302024 0.357641 -0.054590 11.00000 -1.50000 AFIX 0 C21 1 0.433378 0.543406 0.225738 11.00000 0.02823 0.02236 = 0.02928 0.00320 0.00007 -0.00734 AFIX 23 H21A 2 0.357810 0.616818 0.216571 11.00000 -1.20000 H21B 2 0.488863 0.531510 0.175216 11.00000 -1.20000 AFIX 0 C22 1 0.528845 0.558281 0.292176 11.00000 0.03276 0.02729 = 0.03340 -0.00089 -0.00186 -0.01094 AFIX 23 H22A 2 0.605004 0.485683 0.303129 11.00000 -1.20000 H22B 2 0.474388 0.575871 0.342572 11.00000 -1.20000 AFIX 0 C23 1 0.590936 0.658328 0.263813 11.00000 0.03846 0.02767 = 0.04008 -0.00087 -0.00149 -0.01433 AFIX 23 H23A 2 0.649322 0.637767 0.215131 11.00000 -1.20000 H23B 2 0.513783 0.728744 0.248748 11.00000 -1.20000 AFIX 0 C24 1 0.680216 0.685066 0.328781 11.00000 0.05337 0.03666 = 0.06081 -0.00431 -0.01447 -0.02067 AFIX 137 H24A 2 0.620928 0.712583 0.375171 11.00000 -1.50000 H24B 2 0.722978 0.745150 0.306747 11.00000 -1.50000 H24C 2 0.753830 0.614561 0.345968 11.00000 -1.50000 AFIX 0 C25 1 0.292038 0.446644 0.323863 11.00000 0.03042 0.02622 = 0.02394 -0.00294 0.00856 -0.00784 AFIX 23 H25A 2 0.246626 0.383213 0.329311 11.00000 -1.20000 H25B 2 0.364360 0.429656 0.366179 11.00000 -1.20000 AFIX 0 C26 1 0.181423 0.560053 0.340572 11.00000 0.03711 0.03054 = 0.04064 -0.00729 0.01052 -0.00663 AFIX 23 H26A 2 0.224690 0.624795 0.336097 11.00000 -1.20000 H26B 2 0.105978 0.577413 0.300116 11.00000 -1.20000 AFIX 0 C27 1 0.120034 0.548763 0.425102 11.00000 0.08537 0.03661 = 0.05888 -0.01484 0.04377 -0.01519 AFIX 23 H27A 2 0.042058 0.619147 0.432851 11.00000 -1.20000 H27B 2 0.081018 0.481566 0.429602 11.00000 -1.20000 AFIX 0 C28 1 0.226489 0.532948 0.491792 11.00000 0.15462 0.05768 = 0.03608 -0.00910 0.01475 0.00858 AFIX 137 H28A 2 0.290464 0.454346 0.493355 11.00000 -1.50000 H28B 2 0.177696 0.544703 0.543753 11.00000 -1.50000 H28C 2 0.279861 0.589609 0.481213 11.00000 -1.50000 MOLE 0 AFIX 0 HKLF 4 REM b21079 in P-1 REM R1 = 0.0275 for 8838 Fo > 4sig(Fo) and 0.0462 for all 11316 data REM 392 parameters refined using 0 restraints END WGHT 0.0219 1.5098 REM Highest difference peak 0.941, deepest hole -0.928, 1-sigma level 0.099 Q1 1 1.1711 0.1627 -0.1356 11.00000 0.05 0.94 Q2 1 1.2330 0.2035 0.4864 11.00000 0.05 0.69 Q3 1 0.9156 0.4148 0.2025 11.00000 0.05 0.53 Q4 1 0.6405 0.1357 0.4528 11.00000 0.05 0.51 Q5 1 1.1618 0.0871 0.6344 11.00000 0.05 0.50 Q6 1 0.9036 0.1002 -0.1308 11.00000 0.05 0.43 Q7 1 0.6891 0.1760 0.0275 11.00000 0.05 0.43 Q8 1 1.2917 0.1220 0.4498 11.00000 0.05 0.40 Q9 1 0.9573 0.3552 0.2533 11.00000 0.05 0.39 Q10 1 0.7973 0.0551 0.6544 11.00000 0.05 0.38 Q11 1 0.4784 0.5459 0.2683 11.00000 0.05 0.38 Q12 1 0.8983 0.2073 -0.1469 11.00000 0.05 0.37 Q13 1 0.8265 0.1248 0.6270 11.00000 0.05 0.37 Q14 1 0.9309 0.3054 0.2344 11.00000 0.05 0.36 Q15 1 0.1812 0.5445 0.4504 11.00000 0.05 0.36 Q16 1 0.3101 0.4454 0.2824 11.00000 0.05 0.35 Q17 1 1.0626 0.1496 0.3753 11.00000 0.05 0.35 Q18 1 0.9633 0.3206 0.2908 11.00000 0.05 0.35 Q19 1 0.9965 -0.0207 0.6357 11.00000 0.05 0.34 Q20 1 1.0281 0.2415 0.2420 11.00000 0.05 0.34 ; _shelx_res_checksum 23244 _shelx_hkl_file ; -1 0 0 -0.1495 0.12171 8 -1 0 0 0.17191 0.09938 11 -1 0 0 0.00401 0.09418 12 -1 0 0 -0.1252 0.13374 1 1 0 0 -0.0039 0.09618 1 1 0 0 -0.3277 0.12764 1 -2 0 0 625.639 18.0266 5 -2 0 0 639.854 18.1752 20 -2 0 0 622.283 18.0010 8 -2 0 0 554.366 18.1499 1 -2 0 0 636.120 17.8869 11 -2 0 0 596.461 17.9398 1 -2 0 0 628.503 18.0050 4 -2 0 0 558.571 18.9323 9 2 0 0 649.025 17.8437 15 2 0 0 656.534 17.9797 2 2 0 0 572.429 18.1483 1 2 0 0 629.390 18.0195 12 2 0 0 637.032 18.0423 18 -3 0 0 42.8032 3.68371 9 -3 0 0 43.1877 1.96996 11 -3 0 0 40.1410 1.95570 1 -3 0 0 45.8328 2.13958 12 -3 0 0 45.9654 2.15911 4 -3 0 0 44.6556 2.41255 20 -3 0 0 47.3839 2.16051 8 -3 0 0 42.7947 2.19537 5 -3 0 0 32.2207 2.48589 1 3 0 0 41.8765 2.18266 12 3 0 0 41.5608 2.08476 18 3 0 0 37.9478 2.43361 1 3 0 0 44.3902 1.87338 15 3 0 0 43.9238 2.05140 2 -4 0 0 378.957 11.3567 1 -4 0 0 383.955 11.5965 8 -4 0 0 338.191 13.5308 9 -4 0 0 379.377 11.3960 11 -4 0 0 347.259 11.9772 1 -4 0 0 359.431 11.6816 5 -4 0 0 376.222 11.6454 4 -4 0 0 372.057 11.9899 20 -4 0 0 384.332 11.6468 12 4 0 0 390.911 11.2922 15 4 0 0 380.566 11.7446 12 4 0 0 369.699 11.5580 2 4 0 0 381.079 11.4893 18 -5 0 0 77.0276 3.26165 1 -5 0 0 68.7152 4.12694 1 -5 0 0 70.0827 4.25366 20 -5 0 0 69.1978 6.20655 9 -5 0 0 78.5663 3.73635 8 -5 0 0 76.7565 3.78572 4 -5 0 0 75.9040 3.90990 5 -5 0 0 80.1778 3.39238 11 5 0 0 79.2291 3.49031 18 5 0 0 83.9829 3.32825 15 5 0 0 80.4903 3.90785 2 5 0 0 78.8286 3.46280 6 5 0 0 81.1103 4.15659 12 -6 0 0 178.103 6.99729 4 -6 0 0 176.976 6.61062 8 -6 0 0 166.989 9.79870 9 -6 0 0 173.726 6.05124 1 -6 0 0 168.207 6.88711 1 -6 0 0 168.081 7.40768 20 -6 0 0 162.122 6.93360 5 -6 0 0 176.217 6.27327 11 6 0 0 179.905 6.14155 15 6 0 0 173.943 7.07978 12 6 0 0 171.815 7.36047 16 6 0 0 181.897 6.87344 2 6 0 0 169.168 6.15753 6 6 0 0 180.405 6.22536 18 -7 0 0 156.034 5.76054 1 -7 0 0 163.934 7.13482 5 -7 0 0 167.040 10.5806 9 -7 0 0 161.523 6.20917 11 -7 0 0 146.563 6.59369 1 -7 0 0 160.902 7.66686 20 -7 0 0 168.729 7.21978 4 7 0 0 158.034 7.22727 12 7 0 0 158.870 5.95610 6 7 0 0 153.661 6.08257 15 7 0 0 159.309 6.90429 2 7 0 0 167.830 7.67177 16 7 0 0 163.146 5.98837 18 -8 0 0 19.4306 4.33067 20 -8 0 0 13.3843 3.74433 4 -8 0 0 18.5109 2.07192 1 -8 0 0 16.5730 6.39475 9 -8 0 0 17.7395 2.78379 1 -8 0 0 15.7139 2.97529 11 8 0 0 12.0201 3.90021 16 8 0 0 16.2876 2.34247 18 8 0 0 13.7793 2.43811 15 8 0 0 17.8565 3.84225 12 8 0 0 19.0540 3.23074 2 8 0 0 13.2529 2.27598 6 -9 0 0 33.6149 8.09634 9 -9 0 0 42.6374 3.46088 1 -9 0 0 30.8701 5.51283 20 -9 0 0 44.8211 2.92372 1 -9 0 0 45.4415 4.29928 11 -9 0 0 48.6390 5.31365 4 9 0 0 38.4362 4.66081 2 9 0 0 51.9549 3.36541 18 9 0 0 29.8973 5.27593 16 9 0 0 45.8282 5.12434 12 9 0 0 43.3532 3.74580 15 -10 0 0 117.746 8.32371 4 -10 0 0 104.914 6.90366 11 -10 0 0 99.5235 8.33576 20 -10 0 0 105.133 11.7589 9 -10 0 0 106.115 4.52113 1 -10 0 0 97.3030 4.95618 1 10 0 0 105.524 5.68195 15 10 0 0 100.724 8.05977 16 10 0 0 94.9033 9.95792 17 10 0 0 100.041 6.87094 2 10 0 0 106.388 7.35085 12 -11 0 0 5.40652 9.99758 9 -11 0 0 5.02912 1.57734 1 -11 0 0 0.54849 6.08351 20 -11 0 0 3.74739 4.83084 4 -11 0 0 2.05881 1.76517 1 -11 0 0 5.95850 4.18734 11 11 0 0 9.64560 6.96395 17 11 0 0 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6.59475 12 13 2 0 32.6134 6.50031 2 13 2 0 40.8180 8.66307 16 12 -3 0 -1.3402 7.79442 16 12 -3 0 5.08957 6.90355 12 12 -3 0 8.65446 6.66562 2 12 -3 0 -4.9549 8.06286 7 -12 3 0 -7.3554 4.90483 1 -12 3 0 20.5073 8.05537 4 -12 3 0 1.66981 9.99688 9 11 -3 0 9.07399 7.70379 7 11 -3 0 18.5444 8.31893 16 11 -3 0 21.1651 6.22688 2 11 -3 0 16.8809 8.15875 17 11 -3 0 14.6700 6.00785 12 -11 3 0 4.64723 6.95355 4 -11 3 0 16.4264 5.59839 1 -11 3 0 23.7808 10.0178 9 10 -3 0 28.5009 5.89803 2 10 -3 0 30.7876 7.71644 7 10 -3 0 39.2376 6.13565 12 10 -3 0 45.8216 8.54510 17 10 -3 0 22.4305 6.82296 16 -10 3 0 30.7085 6.08869 4 -10 3 0 27.9954 4.69954 11 -10 3 0 23.5584 5.89782 1 -10 3 0 28.2358 9.17121 9 9 -3 0 10.5745 4.18697 2 9 -3 0 8.19969 5.46002 16 9 -3 0 9.27332 5.28845 12 9 -3 0 17.0622 6.56988 17 -9 3 0 10.9920 4.90706 4 -9 3 0 6.71877 3.50663 11 -9 3 0 4.83746 5.06195 1 -9 3 0 6.78285 8.05496 9 8 -3 0 103.526 6.62830 2 8 -3 0 99.7056 7.73077 16 8 -3 0 92.3363 5.08347 15 8 -3 0 92.2957 7.07628 12 -8 3 0 99.4395 5.85321 11 -8 3 0 104.269 7.23031 4 -8 3 0 87.7722 7.57684 1 -8 3 0 108.501 10.1153 9 7 -3 0 18.7781 2.53996 15 7 -3 0 18.5789 4.56033 16 7 -3 0 28.4349 4.20625 12 7 -3 0 16.2727 3.59129 2 -7 3 0 10.2711 4.68902 1 -7 3 0 8.97913 3.58655 1 -7 3 0 20.2289 6.00583 9 -7 3 0 24.6932 4.26697 4 -7 3 0 18.9771 4.44636 20 -7 3 0 15.5578 2.98752 11 6 -3 0 944.685 29.8515 16 6 -3 0 940.311 28.8710 2 6 -3 0 907.985 29.1460 12 6 -3 0 969.528 31.1977 1 6 -3 0 944.411 27.8645 15 -6 3 0 919.234 28.2358 11 -6 3 0 995.282 31.8324 9 -6 3 0 928.100 29.5708 1 -6 3 0 938.340 29.4617 20 -6 3 0 915.273 30.4556 1 -6 3 0 942.841 29.2666 4 -6 3 0 953.276 28.8107 19 5 -3 0 19.0437 3.27726 12 5 -3 0 27.8252 2.25706 15 5 -3 0 26.7805 3.14744 2 5 -3 0 30.9986 3.80047 16 5 -3 0 33.3538 4.07676 1 -5 3 0 26.1936 3.37490 4 -5 3 0 26.8429 3.75891 1 -5 3 0 30.0812 2.09890 10 -5 3 0 29.8492 4.57600 1 -5 3 0 26.6495 2.78665 19 -5 3 0 38.0979 5.10413 9 -5 3 0 26.8946 3.52894 20 -5 3 0 30.0439 2.53652 11 4 -3 0 650.236 18.8088 15 4 -3 0 641.772 19.5924 2 4 -3 0 616.267 20.8215 1 4 -3 0 625.838 20.1498 16 4 -3 0 644.197 19.9490 12 -4 3 0 615.076 19.0374 11 -4 3 0 607.071 19.4807 19 -4 3 0 629.965 21.2158 1 -4 3 0 618.935 20.2566 3 -4 3 0 639.992 19.8792 4 -4 3 0 615.468 20.6081 1 -4 3 0 643.132 19.8182 20 -4 3 0 634.300 21.2091 9 -4 3 0 635.728 18.6973 10 3 -3 0 279.756 10.1298 16 3 -3 0 296.384 8.99689 15 3 -3 0 299.182 9.80242 2 3 -3 0 285.791 10.0426 12 3 -3 0 297.185 10.8722 1 -3 3 0 283.780 10.6889 9 -3 3 0 269.141 10.9349 1 -3 3 0 274.742 9.91653 4 -3 3 0 279.115 8.88611 10 -3 3 0 279.072 10.2271 3 -3 3 0 282.015 9.67408 19 -3 3 0 302.242 10.1198 13 2 -3 0 126.057 5.90882 1 2 -3 0 114.998 4.18926 15 2 -3 0 121.458 5.01325 2 2 -3 0 115.417 5.05381 12 2 -3 0 123.221 5.05784 13 2 -3 0 112.313 5.11213 16 -2 3 0 119.302 4.95599 12 -2 3 0 113.993 5.91401 1 -2 3 0 112.316 5.17359 13 -2 3 0 112.982 4.91307 19 -2 3 0 116.035 5.38150 9 -2 3 0 118.001 4.28893 10 -2 3 0 113.487 5.28795 3 -2 3 0 114.284 3.65742 18 1 -3 0 455.433 14.1770 7 1 -3 0 470.109 14.7230 13 1 -3 0 475.470 14.5000 2 1 -3 0 454.392 14.5374 16 1 -3 0 447.401 15.0601 1 1 -3 0 469.944 13.8985 15 1 -3 0 456.665 13.5637 8 1 -3 0 445.739 14.5628 12 -1 3 0 440.296 14.6009 3 -1 3 0 475.640 14.6407 12 -1 3 0 447.729 14.0992 9 -1 3 0 458.044 14.6251 19 -1 3 0 445.463 14.7519 13 -1 3 0 433.538 15.0511 1 -1 3 0 455.131 15.1673 1 -1 3 0 456.602 14.0985 10 0 -3 0 9854.51 263.580 7 0 -3 0 8560.76 263.768 1 0 -3 0 9980.29 268.133 12 0 -3 0 9724.16 265.450 15 0 -3 0 8805.10 266.921 1 0 -3 0 9478.49 265.436 13 0 -3 0 9813.91 267.279 16 0 -3 0 9236.12 262.904 8 0 3 0 8958.30 265.143 10 0 3 0 9999.99 263.739 12 0 3 0 8713.16 265.042 3 0 3 0 8457.84 264.334 13 0 3 0 8493.81 265.726 1 0 3 0 8961.49 262.417 9 0 3 0 8331.68 263.943 19 -1 -3 0 6231.57 177.706 12 -1 -3 0 6231.90 179.987 13 -1 -3 0 6330.42 179.812 8 -1 -3 0 6465.58 179.761 16 -1 -3 0 6375.94 180.745 2 -1 -3 0 6280.76 178.529 7 -1 -3 0 5706.50 177.946 1 1 3 0 6248.92 177.891 19 1 3 0 6138.43 178.856 10 1 3 0 6536.52 180.382 12 1 3 0 6238.56 178.092 14 1 3 0 5795.32 177.956 1 1 3 0 6244.10 180.840 3 1 3 0 6168.77 180.763 13 -2 -3 0 1004.06 29.9008 16 -2 -3 0 1012.99 30.1546 1 -2 -3 0 1000.53 29.9690 5 -2 -3 0 1030.39 29.9851 13 -2 -3 0 1013.84 30.4395 8 -2 -3 0 1002.98 30.0826 9 -2 -3 0 999.740 29.7998 20 2 3 0 1075.10 29.7830 3 2 3 0 1032.01 30.1304 1 2 3 0 1067.56 29.4832 14 2 3 0 1053.23 30.1173 19 2 3 0 1020.45 30.4769 10 2 3 0 1024.14 30.0319 13 -3 -3 0 152.245 5.29394 5 -3 -3 0 157.081 6.09532 9 -3 -3 0 156.437 5.94319 8 -3 -3 0 146.749 5.22634 20 -3 -3 0 153.927 5.16460 13 -3 -3 0 146.138 5.13970 4 -3 -3 0 153.274 5.45871 1 -3 -3 0 151.302 5.37863 11 -3 -3 0 146.907 4.92409 1 3 3 0 159.877 5.03535 3 3 3 0 159.891 5.30816 13 3 3 0 151.292 5.24890 19 -4 -3 0 68.1450 3.23002 11 -4 -3 0 67.7638 2.58560 1 -4 -3 0 67.8096 4.50867 9 -4 -3 0 63.7940 3.82826 8 -4 -3 0 65.7061 3.17774 5 -4 -3 0 67.1260 2.20510 1 -4 -3 0 67.9166 3.02292 4 -4 -3 0 64.3710 3.44691 20 4 3 0 55.8947 4.19377 18 4 3 0 64.8421 2.95773 13 -5 -3 0 204.418 7.05591 4 -5 -3 0 192.057 9.06899 9 -5 -3 0 196.116 7.21503 11 -5 -3 0 206.905 8.02245 8 -5 -3 0 216.075 7.29796 5 -5 -3 0 213.751 7.64965 20 5 3 0 207.339 7.04747 13 5 3 0 199.008 8.30994 18 -6 -3 0 30.1520 4.77794 9 -6 -3 0 32.7090 3.42346 8 -6 -3 0 38.0223 2.87481 5 -6 -3 0 38.7710 3.45432 20 -6 -3 0 33.0761 2.96360 11 -6 -3 0 31.5531 2.73119 4 6 3 0 37.7909 3.83197 18 -7 -3 0 541.554 17.7281 4 -7 -3 0 572.067 18.4981 20 -7 -3 0 566.193 18.4196 8 -7 -3 0 560.093 17.9662 5 -7 -3 0 551.447 21.0026 9 -7 -3 0 569.006 17.7979 11 7 3 0 587.005 18.7670 18 7 3 0 561.315 17.9220 12 -8 -3 0 2.54718 3.30231 8 -8 -3 0 6.20968 3.14575 5 -8 -3 0 0.91812 3.40794 20 -8 -3 0 3.42101 5.32540 9 -8 -3 0 2.95557 2.52172 11 -8 -3 0 5.22478 2.99808 4 8 3 0 4.89197 2.62555 15 8 3 0 5.80651 3.26654 18 8 3 0 1.86681 3.03100 12 -9 -3 0 129.391 7.00638 11 -9 -3 0 140.702 11.3575 9 -9 -3 0 147.590 8.27828 20 -9 -3 0 127.429 7.13041 4 -9 -3 0 133.076 7.80573 8 -9 -3 0 122.598 7.21093 5 9 3 0 129.973 6.84196 12 9 3 0 140.542 7.31130 18 9 3 0 121.576 7.10571 6 9 3 0 134.881 6.41110 15 9 3 0 136.658 7.16483 2 -10 -3 0 33.7825 5.52641 5 -10 -3 0 42.0729 8.85608 9 -10 -3 0 31.0197 4.47316 11 -10 -3 0 27.7271 4.33338 4 -10 -3 0 31.4714 5.11498 8 -10 -3 0 27.8518 5.60606 20 10 3 0 37.1052 4.43538 18 10 3 0 47.9515 5.15878 12 10 3 0 30.1753 6.66098 17 10 3 0 23.9717 4.54768 2 10 3 0 32.1801 4.29844 6 10 3 0 30.3978 3.61907 15 -11 -3 0 2.61236 4.65028 4 -11 -3 0 1.98150 4.13072 11 -11 -3 0 3.65607 6.29283 20 -11 -3 0 9.99482 9.20022 9 -11 -3 0 0.26361 4.89233 5 11 3 0 4.65769 4.60365 10 11 3 0 0.48554 3.45177 15 11 3 0 0.37287 3.81783 2 11 3 0 2.60601 3.91889 18 11 3 0 1.83439 5.50167 16 11 3 0 3.42390 3.86463 6 11 3 0 7.46734 7.03686 17 11 3 0 4.02794 4.11480 12 -12 -3 0 122.776 8.98780 5 -12 -3 0 78.9662 12.4205 9 -12 -3 0 90.1520 7.36123 4 -12 -3 0 90.3477 7.30033 11 -12 -3 0 94.1414 9.38779 20 12 3 0 120.899 7.60206 13 12 3 0 87.7775 7.05882 2 12 3 0 110.556 6.73751 15 12 3 0 120.539 8.23912 12 12 3 0 95.2562 9.23239 16 12 3 0 95.5465 11.0311 17 -13 -3 0 24.6849 11.2345 9 -13 -3 0 14.3776 8.71510 20 -13 -3 0 14.8783 5.53853 11 -13 -3 0 10.9825 6.39998 4 13 3 0 21.8155 6.48403 12 13 3 0 15.1255 7.02032 16 13 3 0 14.1856 7.32839 17 13 3 0 6.31233 4.92352 2 -14 -3 0 58.6978 10.9051 20 -14 -3 0 57.2472 8.27075 4 14 3 0 56.2420 7.27842 12 14 3 0 60.7075 10.1054 16 14 3 0 40.4175 9.90358 7 12 -4 0 40.3159 9.45002 16 12 -4 0 62.5177 8.64221 2 12 -4 0 42.3686 11.1957 7 12 -4 0 50.9259 8.27506 12 -12 4 0 48.3793 7.46696 1 -12 4 0 62.9444 12.3326 9 -12 4 0 48.3392 8.89995 4 11 -4 0 83.2323 10.8074 16 11 -4 0 103.450 11.5402 17 11 -4 0 60.6295 10.9026 7 11 -4 0 98.0981 9.08439 12 11 -4 0 69.6154 8.40606 2 -11 4 0 94.0977 10.1458 4 -11 4 0 84.1908 8.74866 1 -11 4 0 84.4846 13.1037 9 10 -4 0 -2.8764 6.78840 7 10 -4 0 2.85221 5.47651 12 10 -4 0 5.55856 5.72181 2 10 -4 0 -1.6350 6.57304 16 10 -4 0 7.74323 8.02582 17 -10 4 0 0.83315 7.99250 9 -10 4 0 1.04971 4.17560 11 -10 4 0 3.58873 6.10135 1 -10 4 0 7.59205 5.74893 4 9 -4 0 50.8448 8.54468 7 9 -4 0 53.1106 6.52932 2 9 -4 0 46.5988 7.20369 16 9 -4 0 47.1038 6.45567 12 9 -4 0 57.0728 8.49740 17 -9 4 0 47.5469 8.89483 9 -9 4 0 52.3509 7.22287 1 -9 4 0 51.4499 6.63228 4 -9 4 0 52.7279 5.23977 11 8 -4 0 40.6368 6.51017 16 8 -4 0 44.8609 3.63854 15 8 -4 0 33.4284 5.42419 12 8 -4 0 41.1255 6.94318 17 8 -4 0 40.0753 5.10023 2 -8 4 0 38.4821 7.75765 9 -8 4 0 27.2359 4.00797 11 -8 4 0 29.2496 6.25214 1 -8 4 0 35.9434 5.69207 4 7 -4 0 3.65377 4.39815 12 7 -4 0 -0.5893 3.43361 2 7 -4 0 9.43556 4.72880 16 7 -4 0 4.07161 2.38330 15 -7 4 0 3.57565 4.52379 4 -7 4 0 4.22233 4.84440 1 -7 4 0 -7.6620 5.84673 9 -7 4 0 2.99679 3.02943 19 -7 4 0 3.31551 2.93730 11 6 -4 0 261.166 10.6713 12 6 -4 0 249.297 8.82668 15 6 -4 0 257.807 11.3347 16 6 -4 0 266.935 10.2527 2 -6 4 0 266.372 11.3742 1 -6 4 0 258.211 10.2403 19 -6 4 0 250.534 12.2265 1 -6 4 0 248.735 9.37733 11 -6 4 0 246.774 10.6103 4 -6 4 0 271.446 12.6535 9 5 -4 0 17.5098 3.57205 12 5 -4 0 16.4861 3.84337 16 5 -4 0 15.8246 3.50787 2 5 -4 0 15.1278 3.81367 1 5 -4 0 19.2289 2.29168 15 -5 4 0 18.0787 4.56203 1 -5 4 0 13.8520 3.84805 1 -5 4 0 14.1228 3.13392 19 -5 4 0 16.2994 2.67302 11 -5 4 0 16.4504 1.93404 10 -5 4 0 5.48980 4.09678 9 -5 4 0 19.0117 3.64113 4 4 -4 0 237.867 9.62523 12 4 -4 0 246.428 10.7003 1 4 -4 0 246.529 10.0438 16 4 -4 0 256.899 9.62699 2 4 -4 0 252.017 8.33436 15 -4 4 0 241.266 9.70843 4 -4 4 0 263.949 10.7230 9 -4 4 0 248.906 8.80587 11 -4 4 0 244.192 10.2703 3 -4 4 0 249.264 8.21987 10 -4 4 0 251.287 9.58219 19 -4 4 0 261.199 10.0384 13 -4 4 0 264.360 11.3794 1 3 -4 0 943.537 27.4103 15 3 -4 0 927.153 29.4448 1 3 -4 0 912.585 28.4718 12 3 -4 0 900.360 28.6139 16 3 -4 0 933.772 28.3046 2 -3 4 0 918.475 29.6684 1 -3 4 0 955.408 28.7812 4 -3 4 0 921.363 28.6442 13 -3 4 0 909.885 28.4181 19 -3 4 0 894.712 30.3335 1 -3 4 0 928.463 28.9356 9 -3 4 0 936.507 27.3950 10 -3 4 0 948.791 29.0676 3 2 -4 0 1596.07 47.0190 16 2 -4 0 1591.53 46.9565 12 2 -4 0 1571.82 46.6640 7 2 -4 0 1587.46 45.9308 15 2 -4 0 1567.06 46.6663 2 2 -4 0 1566.24 47.6790 1 2 -4 0 1636.71 45.5142 8 -2 4 0 1565.68 47.1901 13 -2 4 0 1533.48 46.9066 19 -2 4 0 1468.34 45.4250 18 -2 4 0 1595.77 47.8943 1 -2 4 0 1628.47 47.8308 1 -2 4 0 1617.73 46.7924 9 -2 4 0 1567.97 46.1272 10 -2 4 0 1573.01 47.1868 3 1 -4 0 287.786 10.5877 16 1 -4 0 287.983 10.7090 12 1 -4 0 274.601 10.4828 2 1 -4 0 309.460 9.36554 8 1 -4 0 292.016 9.72860 15 1 -4 0 293.119 11.1658 1 1 -4 0 291.878 9.90831 7 1 -4 0 332.069 11.6287 13 -1 4 0 290.486 11.2711 1 -1 4 0 280.848 10.5541 3 -1 4 0 317.793 11.4216 12 -1 4 0 289.197 10.0692 10 -1 4 0 297.383 9.69114 9 -1 4 0 293.746 10.7488 19 -1 4 0 285.315 10.8668 13 0 -4 0 1357.47 40.1713 15 0 -4 0 1334.46 39.7301 17 0 -4 0 1372.95 39.8442 7 0 -4 0 1332.62 41.1117 1 0 -4 0 1346.85 40.7349 2 0 -4 0 1389.09 41.2622 1 0 -4 0 1349.48 39.9147 8 0 -4 0 1362.85 40.8326 16 0 -4 0 1313.61 40.9213 12 0 -4 0 1492.48 41.5759 13 0 4 0 1381.82 41.3189 13 0 4 0 1352.65 41.1853 1 0 4 0 1454.16 41.1714 12 0 4 0 1294.38 39.3562 9 0 4 0 1353.99 40.6927 10 0 4 0 1397.49 40.9173 3 -1 -4 0 2873.46 80.0237 2 -1 -4 0 2651.52 79.6789 8 -1 -4 0 2766.93 80.0717 12 -1 -4 0 2796.70 79.0109 7 -1 -4 0 2745.76 80.3293 13 -1 -4 0 2778.17 79.8852 16 -1 -4 0 2821.95 79.1213 17 -1 -4 0 2638.29 80.3049 1 1 4 0 2768.68 79.8926 3 1 4 0 2722.14 80.3089 10 1 4 0 2706.25 80.3463 1 1 4 0 2811.53 79.9609 12 1 4 0 2665.09 80.2590 13 1 4 0 2719.76 80.2784 19 1 4 0 2880.03 79.0289 14 -2 -4 0 261.679 8.63613 16 -2 -4 0 256.166 8.77207 13 -2 -4 0 268.974 9.46630 1 -2 -4 0 253.862 8.69571 5 -2 -4 0 258.258 8.13348 9 -2 -4 0 256.916 8.37811 20 -2 -4 0 273.334 9.26407 8 -2 -4 0 263.064 8.71741 2 -2 -4 0 262.260 7.99740 7 -2 -4 0 250.160 9.14217 1 2 4 0 255.540 8.44884 3 2 4 0 268.864 7.75944 14 2 4 0 264.804 7.65472 17 2 4 0 289.351 9.15374 19 2 4 0 254.084 8.66193 12 2 4 0 269.709 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20.0905 5.91680 17 -10 -5 2 13.5274 4.43977 11 -10 -5 2 22.7184 4.69680 5 -10 -5 2 26.8324 5.49291 20 -10 -5 2 24.1507 5.61562 8 -10 -5 2 35.3981 7.46155 9 -10 -5 2 29.8776 5.15600 4 9 5 -2 91.9353 6.39809 13 9 5 -2 90.6525 5.66648 12 9 5 -2 91.2822 7.77748 18 9 5 -2 97.1813 7.60903 17 -9 -5 2 109.489 7.28017 20 -9 -5 2 84.4191 6.91073 8 -9 -5 2 96.0684 6.84300 5 -9 -5 2 83.2910 5.99297 4 -9 -5 2 107.641 9.14923 9 -9 -5 2 92.9541 6.30754 11 8 5 -2 127.395 7.47355 17 8 5 -2 126.437 6.35893 13 8 5 -2 110.862 8.41707 18 -8 -5 2 117.863 7.43511 20 -8 -5 2 143.039 8.06856 8 -8 -5 2 122.670 6.60475 4 -8 -5 2 143.756 9.86843 9 -8 -5 2 140.473 6.87942 11 -8 -5 2 139.463 6.95507 5 7 5 -2 44.2282 4.45115 17 7 5 -2 50.3242 3.80341 3 7 5 -2 46.8498 3.82502 13 -7 -5 2 59.6221 4.54744 4 -7 -5 2 54.1977 5.67089 8 -7 -5 2 54.2260 4.42498 20 -7 -5 2 50.8958 4.33501 11 -7 -5 2 55.3585 4.06175 5 -7 -5 2 54.1181 5.94656 9 6 5 -2 30.5765 2.93787 3 6 5 -2 31.7093 3.06185 19 6 5 -2 37.4455 3.05567 14 6 5 -2 34.9751 3.35658 13 6 5 -2 36.5803 3.43456 17 -6 -5 2 39.2227 4.51273 8 -6 -5 2 35.8563 1.60861 1 -6 -5 2 30.7381 3.34011 5 -6 -5 2 34.6382 4.47866 9 -6 -5 2 31.5237 1.74325 1 -6 -5 2 31.5779 3.40428 20 -6 -5 2 35.8934 3.36396 4 -6 -5 2 35.2904 3.45910 11 5 5 -2 16.3342 2.11343 14 5 5 -2 14.0003 2.35632 19 5 5 -2 15.6508 2.24082 17 5 5 -2 11.6756 2.35794 13 5 5 -2 14.8963 2.09101 3 -5 -5 2 13.9443 3.51028 8 -5 -5 2 15.4781 2.14889 1 -5 -5 2 11.4417 2.24158 20 -5 -5 2 15.1435 2.62353 11 -5 -5 2 16.8870 2.53030 4 -5 -5 2 19.1149 2.40286 5 -5 -5 2 17.8517 1.62314 1 -5 -5 2 11.6511 2.84865 9 4 5 -2 1916.51 55.1534 19 4 5 -2 1930.58 54.8552 3 4 5 -2 1880.73 55.0923 13 4 5 -2 1935.13 54.4749 14 4 5 -2 1883.69 54.3923 17 -4 -5 2 1861.03 54.6188 20 -4 -5 2 1922.11 54.9061 5 -4 -5 2 1806.05 56.1388 8 -4 -5 2 1832.08 55.3036 1 -4 -5 2 1906.73 55.0610 9 -4 -5 2 1850.92 54.6902 1 -4 -5 2 1859.24 55.0579 11 3 5 -2 1943.55 56.6743 13 3 5 -2 1896.18 56.9986 1 3 5 -2 1976.86 56.7034 19 3 5 -2 2015.94 56.4446 3 3 5 -2 2011.84 55.8425 14 3 5 -2 1973.30 55.4866 17 -3 -5 2 1917.28 56.0372 16 -3 -5 2 1879.03 57.1444 1 -3 -5 2 1932.94 56.3833 5 -3 -5 2 1885.32 57.4610 8 -3 -5 2 1882.58 56.6473 1 -3 -5 2 1960.58 56.5981 2 -3 -5 2 1869.89 55.8053 20 -3 -5 2 1946.93 56.5535 11 2 5 -2 149.536 6.33188 19 2 5 -2 141.721 6.10487 3 2 5 -2 155.727 5.28399 14 2 5 -2 152.572 6.43145 13 2 5 -2 145.009 6.71391 1 -2 -5 2 162.376 6.23287 5 -2 -5 2 143.865 6.61648 8 -2 -5 2 143.505 5.64187 16 -2 -5 2 153.415 6.94361 1 -2 -5 2 146.473 5.01839 20 -2 -5 2 146.695 6.54719 1 -2 -5 2 154.924 6.64968 2 -2 -5 2 155.836 6.44580 12 1 5 -2 436.766 14.3585 13 1 5 -2 424.415 12.2208 9 1 5 -2 423.400 14.3270 1 1 5 -2 424.560 13.0252 14 1 5 -2 406.216 13.7069 10 1 5 -2 425.171 14.1505 3 1 5 -2 418.505 14.1466 19 -1 -5 2 425.007 13.8392 8 -1 -5 2 417.238 14.4096 1 -1 -5 2 434.607 14.4614 1 -1 -5 2 403.736 12.2660 7 -1 -5 2 390.147 14.4217 12 -1 -5 2 378.420 13.6431 16 -1 -5 2 427.983 13.9813 15 -1 -5 2 401.526 14.2368 2 -1 -5 2 429.539 12.5801 17 0 5 -2 1.33278 1.21455 9 0 5 -2 2.97038 2.77460 1 0 5 -2 2.53380 2.51469 19 0 5 -2 1.52248 1.81697 14 0 5 -2 0.31463 2.85286 3 0 5 -2 6.25786 2.04927 10 0 5 -2 1.28711 2.88413 13 0 -5 2 -1.7156 2.93356 12 0 -5 2 4.00509 2.17918 15 0 -5 2 -0.8143 2.26060 16 0 -5 2 0.39530 2.45435 2 0 -5 2 2.01290 2.68281 1 0 -5 2 -0.9266 1.95092 8 0 -5 2 2.55839 1.30536 7 -1 5 -2 699.507 22.7418 13 -1 5 -2 706.586 22.7049 3 -1 5 -2 664.400 21.5477 14 -1 5 -2 667.324 22.2134 1 -1 5 -2 702.388 21.3187 10 -1 5 -2 652.550 20.6205 9 -1 5 -2 704.692 22.4523 19 1 -5 2 681.962 21.8283 2 1 -5 2 668.571 21.0262 15 1 -5 2 653.440 21.8837 12 1 -5 2 664.225 22.1961 1 1 -5 2 669.727 21.5544 16 1 -5 2 660.286 20.5943 8 -2 5 -2 525.254 16.7983 9 -2 5 -2 529.724 18.3530 3 -2 5 -2 502.951 18.0421 1 -2 5 -2 493.262 18.1495 13 -2 5 -2 498.955 17.9171 19 -2 5 -2 516.330 15.5802 18 -2 5 -2 502.932 16.4942 10 2 -5 2 534.031 15.9822 8 2 -5 2 518.187 17.3639 12 2 -5 2 530.511 17.2457 16 2 -5 2 525.219 17.1587 2 2 -5 2 502.673 16.2602 15 2 -5 2 499.486 17.9054 1 -3 5 -2 175.825 5.73192 18 -3 5 -2 174.685 9.26158 13 -3 5 -2 147.446 8.89222 3 -3 5 -2 169.575 6.56434 10 -3 5 -2 175.227 8.06093 9 -3 5 -2 162.355 8.11855 19 3 -5 2 185.401 7.85895 2 3 -5 2 173.491 6.95062 15 3 -5 2 169.101 8.03423 12 3 -5 2 183.252 9.15857 1 3 -5 2 170.281 8.19257 16 -4 5 -2 14.2489 1.84377 10 -4 5 -2 9.09418 4.24305 3 -4 5 -2 12.7955 4.26328 13 -4 5 -2 20.0802 4.41648 9 -4 5 -2 14.4801 3.64307 19 -4 5 -2 24.3835 4.99263 1 -4 5 -2 7.02227 4.20200 4 -4 5 -2 12.0556 3.95331 1 4 -5 2 17.3357 4.05389 12 4 -5 2 14.5156 4.13212 1 4 -5 2 14.9077 2.51860 15 4 -5 2 11.8297 3.60960 16 4 -5 2 5.47580 3.29696 2 -5 5 -2 94.8908 4.15034 10 -5 5 -2 114.714 8.51547 1 -5 5 -2 113.262 7.24750 13 -5 5 -2 109.845 7.72616 9 -5 5 -2 120.149 8.78955 3 -5 5 -2 100.785 5.20988 11 -5 5 -2 102.795 7.32930 4 -5 5 -2 110.348 6.96027 19 5 -5 2 105.746 7.22724 16 5 -5 2 104.615 7.48306 12 5 -5 2 102.729 6.60487 2 5 -5 2 121.247 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1 1 -3 -2 1372.79 40.9346 7 1 -3 -2 1387.93 40.6687 13 1 -3 -2 1401.92 41.5722 16 1 -3 -2 1381.24 41.2863 12 1 -3 -2 1424.37 39.9816 18 -1 3 2 1407.71 39.9914 18 -1 3 2 1413.76 40.5292 3 -1 3 2 1388.03 40.7043 13 -1 3 2 1399.61 40.6928 19 -1 3 2 1470.23 40.7680 17 -1 3 2 1372.27 40.9144 1 -1 3 2 1234.52 40.5141 9 -1 3 2 1396.38 40.9893 1 -1 3 2 1419.69 39.9633 6 -1 3 2 1375.53 40.5038 10 -1 3 2 1374.15 41.2336 12 0 -3 -2 2645.01 76.0676 17 0 -3 -2 2652.56 76.5008 13 0 -3 -2 2677.64 76.3474 2 0 -3 -2 2587.92 76.3753 1 0 -3 -2 2558.43 76.8001 16 0 -3 -2 2720.13 75.9388 18 0 -3 -2 2701.03 75.7216 8 0 -3 -2 2651.46 76.2907 7 0 -3 -2 2674.76 76.6127 12 0 -3 -2 2583.64 76.3479 1 0 3 2 2611.93 76.3884 1 0 3 2 2647.47 75.9405 6 0 3 2 2617.34 76.8000 1 0 3 2 2591.23 76.4412 10 0 3 2 2642.49 76.4970 19 0 3 2 2568.63 75.9483 18 0 3 2 2730.21 75.9778 17 0 3 2 2672.98 76.4865 13 0 3 2 2704.62 76.0107 3 0 3 2 2655.91 76.6525 12 -1 -3 -2 301.793 9.37236 17 -1 -3 -2 314.636 9.64452 18 -1 -3 -2 304.762 9.83026 16 -1 -3 -2 303.326 9.61838 1 -1 -3 -2 311.403 9.48194 8 -1 -3 -2 305.127 9.51405 2 -1 -3 -2 309.488 10.3019 13 -1 -3 -2 314.922 9.00472 14 -1 -3 -2 300.092 9.52709 7 -1 -3 -2 309.820 9.75842 5 1 3 2 307.927 9.67474 6 1 3 2 309.067 9.33055 3 1 3 2 302.151 9.69492 18 1 3 2 299.388 9.62435 12 1 3 2 299.155 9.62626 1 1 3 2 290.353 10.1196 19 1 3 2 311.385 9.20965 17 1 3 2 281.204 10.0642 13 -2 -3 -2 1788.56 54.5880 9 -2 -3 -2 1907.89 54.1149 1 -2 -3 -2 1818.56 54.2487 17 -2 -3 -2 1910.17 54.2680 5 -2 -3 -2 1870.76 54.3529 16 -2 -3 -2 1830.79 54.0337 14 -2 -3 -2 1981.32 54.6873 18 -2 -3 -2 1897.94 54.1581 13 -2 -3 -2 1949.01 54.1860 1 -2 -3 -2 1834.27 54.3325 20 -2 -3 -2 1881.98 54.2181 7 -2 -3 -2 1887.90 54.3941 8 2 3 2 1892.69 54.0223 17 2 3 2 1850.54 54.3718 13 2 3 2 1923.29 54.6427 6 2 3 2 1772.23 55.1342 10 2 3 2 1923.51 54.1021 1 2 3 2 1850.08 54.5579 19 2 3 2 1889.52 53.8342 3 2 3 2 1876.85 54.6476 18 -3 -3 -2 13.1621 1.59126 5 -3 -3 -2 10.1473 1.12368 4 -3 -3 -2 14.3275 1.84101 8 -3 -3 -2 11.1711 1.61730 20 -3 -3 -2 11.1368 2.25504 9 -3 -3 -2 10.5412 1.23779 1 -3 -3 -2 10.4957 1.86221 18 -3 -3 -2 8.57185 1.09863 1 -3 -3 -2 12.1624 1.12110 13 3 3 2 11.6607 1.26003 13 3 3 2 22.7628 1.78210 17 3 3 2 11.3738 1.14329 1 3 3 2 7.91729 1.26588 19 3 3 2 8.83900 1.96245 18 3 3 2 12.0351 2.28747 10 3 3 2 9.66754 1.90640 6 -4 -3 -2 22.5678 1.62372 1 -4 -3 -2 24.3937 2.42493 8 -4 -3 -2 23.7048 3.48885 9 -4 -3 -2 19.2018 1.59032 4 -4 -3 -2 20.3081 2.19649 20 -4 -3 -2 22.7841 1.72392 1 -4 -3 -2 21.2939 2.09341 11 -4 -3 -2 22.9033 2.14836 5 4 3 2 23.3422 1.74898 19 4 3 2 20.9915 1.56426 13 4 3 2 24.3422 2.96325 10 4 3 2 21.0208 2.54447 18 4 3 2 23.6523 2.73040 6 -5 -3 -2 163.256 6.17209 11 -5 -3 -2 168.204 6.91162 8 -5 -3 -2 175.050 5.43617 1 -5 -3 -2 169.319 6.36975 5 -5 -3 -2 171.118 6.60819 20 -5 -3 -2 167.122 8.49592 9 -5 -3 -2 165.719 5.85019 4 -5 -3 -2 164.983 5.37980 1 5 3 2 165.889 7.25273 10 5 3 2 154.332 6.70575 6 5 3 2 165.847 5.75200 13 5 3 2 180.409 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7.25957 5 -6 -2 3 193.592 7.48065 4 -6 -2 3 201.383 7.88128 8 5 2 -3 4.92301 2.87509 17 5 2 -3 7.36455 1.60184 12 -5 -2 3 6.88824 2.35046 20 -5 -2 3 4.87229 0.94937 1 -5 -2 3 8.32034 2.46579 8 -5 -2 3 5.69628 1.92226 4 -5 -2 3 5.67597 3.10212 9 -5 -2 3 5.59416 1.57439 5 -5 -2 3 5.75646 1.82865 11 -5 -2 3 5.20058 0.71193 1 4 2 -3 575.150 18.9927 7 4 2 -3 604.942 18.8897 17 -4 -2 3 575.384 18.0235 11 -4 -2 3 622.414 19.5226 9 -4 -2 3 602.351 18.9174 8 -4 -2 3 605.876 17.3856 1 -4 -2 3 588.001 18.2843 20 -4 -2 3 610.774 17.3772 1 -4 -2 3 606.679 18.1652 4 -4 -2 3 586.685 17.8413 5 3 2 -3 1157.81 33.5280 14 3 2 -3 1161.08 33.4082 13 3 2 -3 1137.78 33.8801 7 3 2 -3 1171.76 33.6959 17 -3 -2 3 1142.93 33.3703 4 -3 -2 3 1101.28 34.1302 8 -3 -2 3 1133.09 34.0816 9 -3 -2 3 1131.11 32.9068 1 -3 -2 3 1120.73 33.3147 20 -3 -2 3 1142.81 34.0383 17 -3 -2 3 1127.70 33.2748 11 -3 -2 3 1151.30 33.0296 5 -3 -2 3 1149.06 32.8651 1 2 2 -3 352.062 11.0388 3 2 2 -3 369.235 10.9855 7 2 2 -3 359.512 11.0657 17 2 2 -3 369.390 10.8048 1 2 2 -3 375.357 11.1273 14 2 2 -3 365.982 11.0731 13 2 2 -3 356.822 10.7435 12 -2 -2 3 361.004 10.8138 1 -2 -2 3 333.945 11.8508 8 -2 -2 3 348.665 10.7750 20 -2 -2 3 365.217 10.9361 11 -2 -2 3 354.800 11.2660 17 -2 -2 3 365.255 10.7733 2 -2 -2 3 354.656 10.7646 1 -2 -2 3 357.677 11.0184 4 -2 -2 3 355.473 10.6364 5 -2 -2 3 352.824 11.4436 15 1 2 -3 186.903 6.31939 13 1 2 -3 198.727 6.32071 19 1 2 -3 197.697 6.23680 17 1 2 -3 203.433 6.46433 3 1 2 -3 198.365 5.90498 7 1 2 -3 201.537 6.42766 14 1 2 -3 195.786 6.27569 1 1 2 -3 181.879 6.45256 12 -1 -2 3 190.641 6.32641 17 -1 -2 3 193.230 5.64554 16 -1 -2 3 199.789 6.32107 13 -1 -2 3 191.532 6.07922 11 -1 -2 3 172.883 6.47977 2 -1 -2 3 193.291 6.02427 5 -1 -2 3 196.307 6.86927 8 -1 -2 3 200.706 6.81343 15 -1 -2 3 194.362 6.29318 1 -1 -2 3 183.974 6.39906 12 0 2 -3 16.1251 1.33774 18 0 2 -3 15.6113 1.05024 7 0 2 -3 15.0804 1.39753 12 0 2 -3 17.6668 1.67655 14 0 2 -3 19.1027 1.85162 3 0 2 -3 15.9543 1.42683 17 0 2 -3 16.2750 0.76908 20 0 2 -3 14.7511 1.45409 1 0 2 -3 15.2563 1.63983 13 0 2 -3 15.2858 1.38344 19 0 -2 3 15.4589 1.53448 17 0 -2 3 16.4037 1.11003 16 0 -2 3 13.1201 1.41122 1 0 -2 3 15.2258 1.32529 6 0 -2 3 12.2160 1.42694 12 0 -2 3 14.0553 1.50522 2 0 -2 3 14.6445 1.42939 1 0 -2 3 14.8742 1.58014 15 0 -2 3 16.2850 1.45608 13 0 -2 3 17.3146 1.23802 11 -1 2 -3 515.370 16.5577 14 -1 2 -3 536.451 16.1461 1 -1 2 -3 509.113 16.0285 1 -1 2 -3 543.794 15.5129 20 -1 2 -3 521.172 16.4442 19 -1 2 -3 520.775 16.2249 9 -1 2 -3 512.894 16.7155 13 -1 2 -3 524.716 15.9075 12 -1 2 -3 523.013 17.2001 3 -1 2 -3 520.319 15.6564 18 1 -2 3 540.984 15.7805 16 1 -2 3 554.665 16.5364 13 1 -2 3 529.393 16.0045 12 1 -2 3 537.157 15.9975 2 1 -2 3 533.853 16.1282 1 1 -2 3 528.769 16.3490 17 1 -2 3 533.110 15.6035 6 1 -2 3 524.506 15.8748 15 1 -2 3 527.002 15.6372 18 -2 2 -3 1998.64 56.8948 18 -2 2 -3 1847.80 57.8113 1 -2 2 -3 1812.17 58.5276 3 -2 2 -3 1973.69 57.6233 1 -2 2 -3 2031.08 56.8076 10 -2 2 -3 1978.55 57.3300 12 -2 2 -3 1938.27 57.9771 9 -2 2 -3 1976.61 58.5719 14 -2 2 -3 2047.63 57.0809 20 -2 2 -3 1852.33 57.9866 13 -2 2 -3 1891.55 57.6956 19 2 -2 3 2059.43 57.3964 2 2 -2 3 2005.82 58.2650 13 2 -2 3 2003.86 57.4059 12 2 -2 3 1996.13 57.3309 16 2 -2 3 2065.74 56.8487 18 2 -2 3 2034.29 57.1761 15 2 -2 3 2003.16 57.6066 1 2 -2 3 2066.87 56.8216 6 -3 2 -3 1799.88 54.1992 14 -3 2 -3 1793.53 52.8197 1 -3 2 -3 1734.39 53.4593 9 -3 2 -3 1767.80 53.5488 3 -3 2 -3 1837.94 51.6032 11 -3 2 -3 1765.28 52.1878 20 -3 2 -3 1797.56 51.8024 18 -3 2 -3 1779.24 52.2561 19 -3 2 -3 1777.40 52.6588 13 3 -2 3 1774.00 52.4542 12 3 -2 3 1767.88 52.4656 16 3 -2 3 1821.51 52.3836 2 3 -2 3 1863.10 51.6518 6 3 -2 3 1847.51 51.6801 18 3 -2 3 1785.73 52.7410 1 3 -2 3 1816.42 52.1006 15 3 -2 3 1833.26 53.0901 13 -4 2 -3 3.75516 1.94997 20 -4 2 -3 6.30180 1.56182 19 -4 2 -3 8.75543 2.02102 13 -4 2 -3 4.51722 2.52241 3 -4 2 -3 7.02422 1.41389 18 -4 2 -3 7.36067 2.07837 4 -4 2 -3 3.87634 1.89160 1 -4 2 -3 5.01984 1.17755 11 -4 2 -3 9.64774 2.44040 1 -4 2 -3 7.21985 3.24347 9 4 -2 3 4.71675 1.05222 18 4 -2 3 10.6674 2.23763 16 4 -2 3 5.95479 1.08146 6 4 -2 3 5.98074 2.21787 1 4 -2 3 6.18758 2.01414 2 4 -2 3 9.14977 1.88754 15 4 -2 3 8.91898 2.47224 12 -5 2 -3 242.416 10.0947 3 -5 2 -3 240.130 9.05482 4 -5 2 -3 246.469 11.2145 9 -5 2 -3 253.875 8.27219 18 -5 2 -3 225.588 8.76464 1 -5 2 -3 240.530 7.77111 11 -5 2 -3 242.078 8.98584 20 -5 2 -3 252.791 9.93729 1 -5 2 -3 241.179 8.29980 19 5 -2 3 249.199 8.96504 2 5 -2 3 231.383 9.05047 12 5 -2 3 248.773 9.63307 1 5 -2 3 243.867 7.57167 6 5 -2 3 249.214 7.62432 18 5 -2 3 248.261 9.37575 16 5 -2 3 246.448 8.41020 15 -6 2 -3 1.04302 2.16110 1 -6 2 -3 -1.1363 1.58839 11 -6 2 -3 -1.7074 3.23906 1 -6 2 -3 -2.5889 4.26660 9 -6 2 -3 2.10220 1.94666 19 -6 2 -3 2.65482 2.93033 20 -6 2 -3 0.92109 2.41615 4 6 -2 3 0.29718 1.19986 18 6 -2 3 2.32153 1.20704 6 6 -2 3 1.86827 2.99345 16 6 -2 3 0.72268 2.82028 12 6 -2 3 3.14789 2.78842 1 6 -2 3 1.29099 2.13395 15 6 -2 3 2.20490 2.80429 2 -7 2 -3 380.165 13.3812 20 -7 2 -3 359.154 12.4268 1 -7 2 -3 348.318 12.9552 4 -7 2 -3 360.530 16.2176 9 -7 2 -3 340.552 11.4702 11 7 -2 3 346.449 13.1198 2 7 -2 3 354.345 13.1228 12 7 -2 3 361.620 10.9198 6 7 -2 3 371.028 12.0694 15 7 -2 3 355.385 13.8897 16 7 -2 3 366.030 10.9595 18 -8 2 -3 1.84353 2.34361 11 -8 2 -3 5.48579 4.82632 1 -8 2 -3 0.11502 4.62277 1 -8 2 -3 5.54418 4.33369 20 -8 2 -3 -1.4039 3.29529 4 -8 2 -3 -1.4182 5.84169 9 8 -2 3 -0.0103 4.19251 12 8 -2 3 5.99778 4.33509 16 8 -2 3 -0.1211 2.75065 15 8 -2 3 7.48791 3.78022 2 -9 2 -3 5.44390 5.58443 20 -9 2 -3 8.34454 4.73390 4 -9 2 -3 4.22660 7.28944 9 -9 2 -3 3.54174 5.18336 1 -9 2 -3 9.30575 2.89988 11 9 -2 3 3.39691 3.45483 15 9 -2 3 10.5525 4.38971 2 9 -2 3 13.2390 4.62931 12 9 -2 3 4.63322 4.95362 16 -10 2 -3 102.392 7.73829 4 -10 2 -3 96.1303 8.54793 1 -10 2 -3 86.2450 11.1041 9 -10 2 -3 86.6489 8.31066 20 10 -2 3 83.7952 7.26913 2 10 -2 3 94.2068 7.78443 12 10 -2 3 113.599 7.04277 15 10 -2 3 81.3265 8.85960 16 -11 2 -3 28.0949 6.71320 1 -11 2 -3 39.8948 10.3857 9 -11 2 -3 40.1672 6.46154 4 -11 2 -3 42.5621 7.97882 20 11 -2 3 45.7017 6.86520 12 11 -2 3 49.2379 8.22263 15 11 -2 3 34.7299 7.45299 16 11 -2 3 31.9456 6.20352 2 -12 2 -3 1.37053 5.59315 1 -12 2 -3 6.06229 6.77259 4 -12 2 -3 2.09369 10.0361 9 -12 2 -3 9.47288 7.55698 20 12 -2 3 6.47411 6.88164 2 12 -2 3 9.76642 8.29668 16 12 -2 3 16.5214 7.25311 12 13 1 -3 0.31077 7.76925 16 13 1 -3 -5.1441 7.52147 17 13 1 -3 -7.7986 9.48996 7 -13 -1 3 1.89607 10.8728 9 -13 -1 3 3.49789 5.88661 11 -13 -1 3 1.70373 7.15935 4 12 1 -3 664.455 25.2274 16 12 1 -3 645.772 28.2073 7 12 1 -3 572.888 26.3071 17 12 1 -3 649.879 22.1434 2 12 1 -3 669.957 22.8884 12 -12 -1 3 691.363 30.2403 9 -12 -1 3 660.760 22.7456 11 -12 -1 3 638.132 23.2188 4 11 1 -3 46.1452 6.76270 16 11 1 -3 46.0284 5.22328 2 11 1 -3 26.8842 7.81798 17 11 1 -3 48.6260 5.86712 12 11 1 -3 48.0561 9.05877 7 -11 -1 3 32.5742 9.82517 9 -11 -1 3 38.3153 7.24719 20 -11 -1 3 55.9209 6.10611 11 -11 -1 3 39.9454 6.68842 4 10 1 -3 10.2860 4.15513 12 10 1 -3 13.4717 2.91344 15 10 1 -3 11.3213 6.74263 7 10 1 -3 16.5888 4.03025 2 10 1 -3 12.2809 6.62766 17 10 1 -3 9.25195 5.36245 16 -10 -1 3 14.3092 4.62675 4 -10 -1 3 20.1658 5.90584 20 -10 -1 3 5.33459 3.90808 8 -10 -1 3 10.6707 7.81355 9 -10 -1 3 13.2760 4.02004 11 9 1 -3 1229.89 35.9201 15 9 1 -3 1173.31 40.2662 7 9 1 -3 1187.28 40.4993 17 9 1 -3 1248.55 37.0898 12 9 1 -3 1225.05 36.8788 18 9 1 -3 1231.63 38.1235 16 9 1 -3 1246.19 36.6846 2 -9 -1 3 1118.57 41.5407 9 -9 -1 3 1200.21 38.4776 20 -9 -1 3 1217.85 37.0163 11 -9 -1 3 1278.50 37.0349 8 -9 -1 3 1190.21 37.3248 4 8 1 -3 13.5781 5.26406 7 8 1 -3 9.24137 3.03990 12 8 1 -3 8.78727 2.74779 2 8 1 -3 5.87028 2.92686 18 8 1 -3 8.75314 3.51087 16 8 1 -3 13.1911 5.25970 17 8 1 -3 8.87523 2.16727 15 -8 -1 3 15.9671 3.39484 5 -8 -1 3 14.0763 3.43636 11 -8 -1 3 9.43904 3.35036 4 -8 -1 3 10.2398 1.04022 1 -8 -1 3 9.86497 3.00138 8 -8 -1 3 9.68389 1.05206 1 -8 -1 3 8.78225 5.88404 9 -8 -1 3 7.98377 4.00884 20 7 1 -3 3.63349 3.15218 16 7 1 -3 5.25406 1.71064 15 7 1 -3 3.57256 2.15597 2 7 1 -3 5.66269 2.38515 12 7 1 -3 17.2499 4.74247 17 -7 -1 3 3.33418 2.56063 8 -7 -1 3 1.91298 3.28882 20 -7 -1 3 3.96829 1.19774 1 -7 -1 3 1.19203 4.66627 9 -7 -1 3 5.07154 2.75618 4 -7 -1 3 3.45882 1.03853 1 -7 -1 3 5.86297 2.88966 5 -7 -1 3 1.55091 2.43439 11 6 1 -3 4.97251 1.68652 2 6 1 -3 4.49190 1.95940 12 6 1 -3 2.61107 3.62144 17 6 1 -3 7.75005 2.61241 16 -6 -1 3 2.82405 1.95595 8 -6 -1 3 6.70425 2.13081 5 -6 -1 3 3.50490 2.10099 11 -6 -1 3 4.80933 1.04503 1 -6 -1 3 5.47473 2.25437 4 -6 -1 3 5.94490 2.72449 20 -6 -1 3 5.53446 4.08928 9 -6 -1 3 6.66211 1.56227 1 5 1 -3 18.7323 3.47622 7 5 1 -3 28.2597 3.75822 17 5 1 -3 23.1996 2.41749 16 5 1 -3 25.8277 1.95098 2 5 1 -3 23.5928 2.14581 12 -5 -1 3 25.3352 2.34678 11 -5 -1 3 29.1667 2.78260 8 -5 -1 3 28.1183 2.34386 5 -5 -1 3 24.6925 1.59648 1 -5 -1 3 27.1148 2.54067 4 -5 -1 3 23.6012 2.98486 20 -5 -1 3 30.6393 4.36252 9 -5 -1 3 23.8117 2.04631 1 4 1 -3 16.9161 1.90444 16 4 1 -3 14.3826 2.96690 7 4 1 -3 28.2203 3.04309 17 4 1 -3 17.2382 1.54078 12 -4 -1 3 15.6393 2.99183 9 -4 -1 3 16.1744 1.80676 11 -4 -1 3 16.6092 1.15511 1 -4 -1 3 16.8637 2.08889 8 -4 -1 3 14.7190 1.27134 1 -4 -1 3 18.5072 1.97909 4 -4 -1 3 16.8108 2.16917 20 -4 -1 3 15.1506 1.69675 5 3 1 -3 332.794 9.71545 12 3 1 -3 305.870 10.9064 7 3 1 -3 326.223 10.0302 16 3 1 -3 340.072 10.8759 17 -3 -1 3 324.189 10.0562 11 -3 -1 3 316.522 10.7001 8 -3 -1 3 328.607 9.67602 1 -3 -1 3 317.853 10.1089 4 -3 -1 3 320.058 11.1472 9 -3 -1 3 318.370 9.63179 1 -3 -1 3 340.603 11.1051 17 -3 -1 3 315.920 10.2774 20 -3 -1 3 321.888 9.82238 5 2 1 -3 924.829 27.3375 17 2 1 -3 944.253 26.8138 16 2 1 -3 946.085 27.2315 14 2 1 -3 923.774 27.3815 7 2 1 -3 941.495 26.7574 1 -2 -1 3 855.146 27.6514 8 -2 -1 3 926.138 26.7647 1 -2 -1 3 920.454 26.7655 1 -2 -1 3 919.365 26.6670 5 -2 -1 3 929.488 27.1301 15 -2 -1 3 926.430 26.9296 11 -2 -1 3 934.033 27.5000 17 -2 -1 3 943.226 27.0100 4 1 1 -3 230.027 7.09573 7 1 1 -3 232.317 6.64714 16 1 1 -3 230.414 7.08766 13 1 1 -3 229.326 7.15039 3 1 1 -3 191.867 7.08261 18 1 1 -3 236.628 7.27629 17 1 1 -3 232.133 7.28492 14 1 1 -3 233.812 7.01704 1 1 1 -3 220.945 6.84773 12 -1 -1 3 223.332 7.16567 6 -1 -1 3 227.394 6.76103 12 -1 -1 3 230.148 6.97433 2 -1 -1 3 230.449 7.38830 15 -1 -1 3 223.048 7.64231 1 -1 -1 3 237.310 7.59526 8 -1 -1 3 233.130 7.03362 1 -1 -1 3 233.538 6.95064 11 -1 -1 3 228.623 7.07315 4 -1 -1 3 235.446 6.63519 5 0 1 -3 189.639 6.06553 17 0 1 -3 186.960 6.05648 3 0 1 -3 186.395 5.63674 12 0 1 -3 190.086 5.77068 7 0 1 -3 179.843 5.85852 1 0 1 -3 185.532 5.81736 13 0 1 -3 190.499 6.19917 14 0 1 -3 189.382 5.52992 20 0 -1 3 188.548 5.88249 18 0 -1 3 177.558 5.85374 1 0 -1 3 180.305 5.74994 2 0 -1 3 186.923 5.55365 11 0 -1 3 185.486 5.83784 6 0 -1 3 182.273 5.69482 12 0 -1 3 178.927 5.75608 13 0 -1 3 180.142 5.89091 15 -1 1 -3 1974.37 55.9767 19 -1 1 -3 1973.23 55.8295 12 -1 1 -3 1904.98 56.4237 9 -1 1 -3 1898.97 56.5419 14 -1 1 -3 1949.68 55.9734 1 -1 1 -3 1923.06 55.7865 18 -1 1 -3 1971.32 56.0057 1 -1 1 -3 1831.09 56.6619 3 -1 1 -3 2009.14 55.6811 20 -1 1 -3 1904.87 56.2424 17 -1 1 -3 1877.53 56.2243 13 1 -1 3 1873.24 56.2778 17 1 -1 3 2033.73 55.7954 18 1 -1 3 1964.06 55.8523 2 1 -1 3 1960.76 55.9856 1 1 -1 3 1971.63 55.8613 12 1 -1 3 1912.00 55.9665 13 1 -1 3 1961.88 55.8718 15 1 -1 3 2008.27 55.7527 6 -2 1 -3 1245.32 36.2891 19 -2 1 -3 1211.72 37.1244 9 -2 1 -3 1122.60 37.2145 3 -2 1 -3 1222.69 37.4835 14 -2 1 -3 1300.65 35.6691 11 -2 1 -3 1237.10 36.4558 1 -2 1 -3 1202.99 36.5776 13 -2 1 -3 1265.59 36.2198 20 -2 1 -3 1252.04 36.2385 5 -2 1 -3 1286.67 36.3398 12 -2 1 -3 1277.09 36.1167 18 2 -1 3 1288.48 36.4710 1 2 -1 3 1256.43 36.3139 2 2 -1 3 1184.42 36.8306 13 2 -1 3 1265.03 36.2225 15 2 -1 3 1303.81 36.0366 6 2 -1 3 1288.93 36.0495 18 2 -1 3 1247.84 36.3587 12 -3 1 -3 4582.52 130.224 19 -3 1 -3 4535.99 129.225 20 -3 1 -3 4473.75 129.412 1 -3 1 -3 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5.17479 9 -5 -6 -3 60.8596 4.06169 1 -5 -6 -3 57.6669 4.48359 20 -5 -6 -3 53.2970 4.71477 8 5 6 3 57.4319 2.92617 3 5 6 3 51.3235 5.64409 10 5 6 3 64.4866 4.22852 13 5 6 3 58.9453 3.54788 17 5 6 3 55.5085 5.16271 6 5 6 3 53.4675 4.14913 19 5 6 3 56.8971 4.83568 18 -6 -6 -3 201.274 8.93021 8 -6 -6 -3 192.121 8.06483 5 -6 -6 -3 187.088 6.81434 1 -6 -6 -3 199.204 9.53033 9 -6 -6 -3 188.096 8.14336 20 -6 -6 -3 182.415 7.33611 1 6 6 3 178.828 9.94807 10 6 6 3 192.510 7.81399 19 6 6 3 186.980 6.47005 3 6 6 3 191.534 9.27150 6 6 6 3 196.701 7.60845 13 6 6 3 201.585 9.41670 18 -7 -6 -3 440.443 15.2153 5 -7 -6 -3 449.015 14.3817 1 -7 -6 -3 445.531 14.3748 4 -7 -6 -3 439.067 13.6734 1 -7 -6 -3 422.569 15.9466 8 -7 -6 -3 467.884 17.6336 9 -7 -6 -3 422.595 15.4647 20 7 6 3 442.217 16.3533 6 7 6 3 460.210 14.9157 19 7 6 3 445.018 16.3937 18 7 6 3 440.704 13.8099 3 7 6 3 463.859 17.5121 10 7 6 3 453.883 14.4817 13 -8 -6 -3 699.414 24.1019 20 -8 -6 -3 739.675 21.7321 1 -8 -6 -3 696.721 24.4141 8 -8 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23.9902 8.23292 1 -9 7 3 25.9557 9.04495 4 -9 7 3 10.2549 8.84858 9 8 -7 -3 32.2693 7.00851 2 8 -7 -3 19.1839 7.94077 17 8 -7 -3 32.5106 7.66082 7 8 -7 -3 26.7194 7.02220 12 8 -7 -3 27.4844 8.11975 16 -8 7 3 37.9103 8.07440 4 -8 7 3 46.2769 8.12643 9 -8 7 3 37.2485 6.32271 11 -8 7 3 32.8617 8.12949 1 7 -7 -3 34.7448 6.91707 17 7 -7 -3 45.6912 6.87029 2 7 -7 -3 26.7755 7.52940 16 7 -7 -3 33.1280 6.92775 7 7 -7 -3 44.4824 7.73995 12 -7 7 3 40.7969 5.97892 11 -7 7 3 37.4809 7.76908 1 -7 7 3 29.1309 6.97261 4 -7 7 3 40.5647 7.13991 9 -7 7 3 40.4852 6.47627 19 6 -7 -3 11.2702 6.97411 16 6 -7 -3 14.9490 5.73120 2 6 -7 -3 7.88465 5.48613 12 6 -7 -3 16.4765 5.59947 17 6 -7 -3 12.1036 5.50451 7 -6 7 3 12.7431 5.79389 4 -6 7 3 6.82259 3.78859 10 -6 7 3 6.45797 6.68344 1 -6 7 3 3.19432 5.57840 9 -6 7 3 14.0797 5.84056 19 -6 7 3 11.3852 4.86555 11 5 -7 -3 4.10069 5.04815 12 5 -7 -3 -1.3110 5.46795 16 5 -7 -3 -0.6083 5.12848 7 5 -7 -3 5.31151 4.66273 17 5 -7 -3 8.77340 5.03710 2 -5 7 3 4.45119 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7 3 58.9616 3.76719 6 -2 7 3 60.3522 6.75334 1 -2 7 3 59.3940 5.94895 13 -2 7 3 59.7378 3.77121 18 1 -7 -3 37.6153 2.61998 8 1 -7 -3 37.9251 5.51040 1 1 -7 -3 51.5524 5.37756 12 1 -7 -3 44.8318 3.90686 17 1 -7 -3 48.3568 5.54214 16 1 -7 -3 39.9075 4.66810 2 1 -7 -3 38.5251 4.21908 7 -1 7 3 44.0000 3.40473 18 -1 7 3 26.6741 4.16804 10 -1 7 3 40.7702 5.71834 1 -1 7 3 42.3316 5.05580 19 -1 7 3 41.0278 5.07204 13 -1 7 3 43.3420 3.47729 6 -1 7 3 42.2423 4.26110 3 0 -7 -3 333.061 13.3286 12 0 -7 -3 313.475 11.0215 17 0 -7 -3 308.180 12.4165 2 0 -7 -3 329.180 13.4366 16 0 -7 -3 318.251 12.7858 1 0 -7 -3 311.579 10.4626 8 0 -7 -3 324.383 11.5959 7 0 7 3 304.951 12.3503 10 0 7 3 316.597 12.7152 1 0 7 3 316.548 11.1397 18 0 7 3 316.993 11.7041 3 0 7 3 297.727 11.0861 6 0 7 3 311.031 12.7485 13 0 7 3 326.476 13.1982 19 -1 -7 -3 2017.80 56.9119 14 -1 -7 -3 2018.87 59.3029 1 -1 -7 -3 1997.68 59.2247 12 -1 -7 -3 1864.28 57.4912 17 -1 -7 -3 1883.94 59.3835 16 -1 -7 -3 1961.71 57.8305 8 -1 -7 -3 1887.97 58.1395 7 -1 -7 -3 1977.02 58.7789 2 1 7 3 2004.16 59.4377 10 1 7 3 1945.38 58.2054 3 1 7 3 1951.87 58.4433 18 1 7 3 1983.22 59.4784 13 1 7 3 1970.30 59.1132 1 1 7 3 2070.10 59.7006 19 1 7 3 1935.04 58.3181 6 1 7 3 2091.25 57.3002 17 -2 -7 -3 5.87213 3.15417 16 -2 -7 -3 4.31958 1.77342 17 -2 -7 -3 6.64271 2.59962 8 -2 -7 -3 5.72294 2.49550 7 -2 -7 -3 6.93169 2.90378 2 -2 -7 -3 3.21482 3.35962 5 -2 -7 -3 8.86860 1.93445 9 -2 -7 -3 7.31349 3.35049 1 -2 -7 -3 3.75779 2.62105 1 2 7 3 7.30000 3.02089 1 2 7 3 8.73126 3.42824 6 2 7 3 8.04148 1.45199 17 2 7 3 5.09163 3.49733 10 2 7 3 10.2733 3.11728 18 2 7 3 3.47976 3.23109 19 2 7 3 10.3031 3.46043 13 2 7 3 8.22173 2.38082 3 -3 -7 -3 119.946 6.37140 5 -3 -7 -3 130.714 5.32182 9 -3 -7 -3 110.207 6.47098 8 -3 -7 -3 104.638 6.44637 20 -3 -7 -3 117.928 5.67989 7 -3 -7 -3 119.931 6.39416 16 -3 -7 -3 113.817 6.03370 1 3 7 3 115.522 6.81609 13 3 7 3 116.228 4.21601 17 3 7 3 117.894 7.60750 10 3 7 3 119.317 7.50990 19 3 7 3 106.352 6.80279 18 3 7 3 118.279 6.01137 1 3 7 3 105.820 6.69516 6 3 7 3 124.421 5.54058 3 -4 -7 -3 162.371 7.53835 5 -4 -7 -3 180.146 7.16660 7 -4 -7 -3 165.284 8.04045 8 -4 -7 -3 170.749 7.64768 1 -4 -7 -3 183.276 7.41389 9 -4 -7 -3 175.376 7.69902 16 -4 -7 -3 170.976 7.57014 20 -4 -7 -3 159.978 7.22846 1 4 7 3 180.874 5.98481 17 4 7 3 165.870 6.57525 3 4 7 3 175.795 8.27181 13 4 7 3 169.464 8.75901 18 4 7 3 183.506 9.51269 10 4 7 3 174.566 8.58272 19 4 7 3 174.808 8.61958 6 4 7 3 161.647 6.93547 1 -5 -7 -3 14.4490 3.29249 5 -5 -7 -3 10.5036 3.29110 9 -5 -7 -3 8.25927 2.73152 1 -5 -7 -3 11.5580 3.07691 20 -5 -7 -3 6.50446 2.45818 1 -5 -7 -3 8.63614 3.86373 8 5 7 3 7.98218 4.04940 6 5 7 3 12.0995 1.83883 17 5 7 3 4.81525 4.35605 10 5 7 3 9.02255 3.08915 13 5 7 3 8.38961 4.03275 18 5 7 3 12.5066 1.92563 3 5 7 3 13.5778 3.47688 19 -6 -7 -3 161.781 7.78002 20 -6 -7 -3 164.186 7.42471 1 -6 -7 -3 161.933 6.55107 1 -6 -7 -3 160.092 7.64066 5 -6 -7 -3 169.316 8.74975 9 -6 -7 -3 179.841 9.34466 8 6 7 3 168.596 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3.99545 8 -7 -3 4 23.8335 3.81219 20 6 3 -4 4.28937 2.52500 14 6 3 -4 3.70114 3.41817 7 6 3 -4 -1.3823 1.76065 12 6 3 -4 -0.8831 2.61733 17 -6 -3 4 14.8134 2.20871 5 -6 -3 4 -1.4391 2.40833 4 -6 -3 4 4.52214 3.54335 9 -6 -3 4 -0.3352 2.69571 8 -6 -3 4 -1.1625 2.67623 20 -6 -3 4 2.77193 2.33612 11 -6 -3 4 4.21336 0.92042 1 -6 -3 4 0.65231 0.85041 1 5 3 -4 3.22472 2.03491 13 5 3 -4 2.63449 2.55319 7 5 3 -4 4.12169 2.17980 17 5 3 -4 2.20292 1.98124 14 -5 -3 4 3.12252 1.92902 11 -5 -3 4 5.48830 1.01604 1 -5 -3 4 4.88477 2.95780 8 -5 -3 4 1.27468 2.07803 4 -5 -3 4 3.34715 2.78163 9 -5 -3 4 2.33633 1.64375 5 -5 -3 4 5.14205 2.29054 20 -5 -3 4 2.75967 1.10859 1 4 3 -4 643.198 19.7989 13 4 3 -4 658.154 20.1939 7 4 3 -4 645.954 19.9690 17 4 3 -4 665.790 19.7771 3 4 3 -4 638.660 19.8089 14 -4 -3 4 625.505 20.9903 8 -4 -3 4 677.613 20.7486 9 -4 -3 4 607.718 20.4046 17 -4 -3 4 649.847 19.2648 5 -4 -3 4 652.657 19.7872 4 -4 -3 4 636.373 19.6799 20 -4 -3 4 655.560 19.6864 11 -4 -3 4 653.205 19.0385 1 -4 -3 4 648.619 19.1837 1 3 3 -4 75.5236 3.58635 14 3 3 -4 77.6480 3.64940 17 3 3 -4 75.5699 3.30043 1 3 3 -4 80.7875 3.85008 13 3 3 -4 79.2496 3.88618 3 3 3 -4 83.6072 3.27274 12 3 3 -4 81.9215 3.50446 7 -3 -3 4 74.3275 3.32932 20 -3 -3 4 75.8113 3.68514 4 -3 -3 4 80.0273 3.08435 5 -3 -3 4 78.4806 3.23204 1 -3 -3 4 76.2759 5.25283 8 -3 -3 4 77.7586 3.53271 11 -3 -3 4 81.1559 4.13799 17 -3 -3 4 75.9317 3.36366 1 2 3 -4 1858.28 54.7428 13 2 3 -4 1870.12 54.4878 17 2 3 -4 1919.31 54.5891 1 2 3 -4 1899.22 54.7061 14 2 3 -4 1874.24 54.7723 12 2 3 -4 1904.79 54.1378 7 2 3 -4 1870.18 54.7773 3 -2 -3 4 1844.67 54.4981 1 -2 -3 4 1884.31 54.6632 2 -2 -3 4 1929.16 54.8158 17 -2 -3 4 2045.35 55.2356 13 -2 -3 4 1797.76 55.3349 15 -2 -3 4 1803.64 55.6835 8 -2 -3 4 1850.54 54.4845 11 -2 -3 4 1916.89 54.6338 1 -2 -3 4 1893.15 54.2197 5 1 3 -4 182.755 6.33855 12 1 3 -4 172.944 6.33763 3 1 3 -4 174.657 6.12277 14 1 3 -4 172.934 5.87220 17 1 3 -4 176.781 5.30918 7 1 3 -4 179.191 6.08705 1 1 3 -4 169.385 6.05678 19 1 3 -4 174.900 6.25121 13 -1 -3 4 161.692 6.59781 15 -1 -3 4 161.323 6.58484 2 -1 -3 4 165.881 6.07662 1 -1 -3 4 172.964 6.72472 8 -1 -3 4 178.304 6.10700 13 -1 -3 4 154.424 6.44093 12 -1 -3 4 156.201 5.47602 16 -1 -3 4 166.951 5.70212 11 -1 -3 4 172.663 6.08548 17 0 3 -4 54.2532 3.48527 14 0 3 -4 51.7966 3.00374 12 0 3 -4 44.1187 3.25257 13 0 3 -4 55.8269 2.94095 17 0 3 -4 49.6848 3.23440 19 0 3 -4 49.3832 3.08060 1 0 3 -4 56.2469 1.91554 20 0 3 -4 55.6317 2.80931 18 0 -3 4 56.5118 3.08370 1 0 -3 4 56.8624 3.26966 15 0 -3 4 55.2823 2.98526 17 0 -3 4 57.4763 3.18098 1 0 -3 4 57.1833 3.12338 13 0 -3 4 43.5600 3.14278 2 0 -3 4 54.8586 2.74910 6 0 -3 4 48.5273 3.21007 12 0 -3 4 52.7157 2.60256 16 -1 3 -4 101.649 4.49782 9 -1 3 -4 102.164 5.14240 19 -1 3 -4 115.799 5.20446 14 -1 3 -4 107.672 3.64533 20 -1 3 -4 98.7049 4.05434 18 -1 3 -4 97.7152 4.26705 12 -1 3 -4 102.506 4.69953 1 -1 3 -4 104.361 5.86614 3 1 -3 4 95.4957 4.49539 2 1 -3 4 106.492 4.94283 13 1 -3 4 107.561 4.70925 1 1 -3 4 109.458 4.46334 15 1 -3 4 99.2725 4.54700 12 1 -3 4 101.706 3.99619 6 1 -3 4 104.520 4.16386 16 -2 3 -4 1745.07 53.0098 19 -2 3 -4 1729.35 53.3868 13 -2 3 -4 1731.78 52.6303 9 -2 3 -4 1794.96 52.6288 1 -2 3 -4 1799.85 54.0411 3 -2 3 -4 1746.13 52.4270 1 -2 3 -4 1777.92 53.3843 14 -2 3 -4 1794.67 51.6305 20 -2 3 -4 1783.31 51.6520 18 -2 3 -4 1831.04 51.6001 10 2 -3 4 1822.71 52.0920 16 2 -3 4 1768.64 52.2295 2 2 -3 4 1807.73 52.0176 15 2 -3 4 1796.56 52.3015 12 2 -3 4 1783.63 53.1951 13 2 -3 4 1807.27 51.5274 6 2 -3 4 1821.73 51.5801 18 -3 3 -4 67.7680 5.84684 14 -3 3 -4 84.8882 2.86033 10 -3 3 -4 84.0871 5.17942 1 -3 3 -4 81.8305 5.21225 9 -3 3 -4 86.7007 4.91218 19 -3 3 -4 76.2440 3.91701 20 -3 3 -4 77.2040 5.98634 3 -3 3 -4 82.0821 3.40993 18 -3 3 -4 84.8100 5.50165 13 -3 3 -4 85.2727 4.46536 1 3 -3 4 84.8931 4.86178 12 3 -3 4 76.1710 4.27026 16 3 -3 4 84.7894 4.99081 1 3 -3 4 85.3334 3.31647 18 3 -3 4 76.3723 4.37909 2 3 -3 4 73.4249 3.92983 15 3 -3 4 77.2693 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11 -6 3 -4 528.754 18.3529 1 -6 3 -4 559.535 17.7350 19 -6 3 -4 578.683 17.3907 18 6 -3 4 547.256 18.9531 16 6 -3 4 558.111 17.6828 15 6 -3 4 563.670 18.5481 2 6 -3 4 573.358 16.6172 6 6 -3 4 578.963 16.6514 18 6 -3 4 556.716 18.7883 12 -7 3 -4 70.1885 5.72513 20 -7 3 -4 68.1270 5.45059 4 -7 3 -4 60.8398 3.72943 11 -7 3 -4 60.8151 6.84061 1 -7 3 -4 66.3357 7.92077 9 -7 3 -4 64.6916 4.65034 19 7 -3 4 68.2862 5.73091 12 7 -3 4 73.5185 5.61765 2 7 -3 4 47.7237 5.50135 16 7 -3 4 56.3086 4.42725 15 7 -3 4 64.2927 2.92261 18 -8 3 -4 138.061 8.58729 20 -8 3 -4 139.683 11.2486 9 -8 3 -4 154.965 8.73349 4 -8 3 -4 151.745 10.3869 1 8 -3 4 160.292 8.84898 12 8 -3 4 140.274 9.17382 16 8 -3 4 126.933 8.23256 2 8 -3 4 132.357 7.06929 15 -9 3 -4 244.270 12.0739 20 -9 3 -4 238.213 15.3657 9 -9 3 -4 251.713 11.7960 4 -9 3 -4 250.320 14.0217 1 9 -3 4 249.899 10.1351 15 9 -3 4 239.033 12.1050 2 9 -3 4 252.897 12.5500 12 9 -3 4 245.672 12.5644 16 -10 3 -4 26.1803 7.02639 1 -10 3 -4 14.0203 8.57232 9 -10 3 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13.6821 4 -7 -4 -5 441.231 13.6962 1 -7 -4 -5 442.693 13.8324 1 -7 -4 -5 434.396 15.2795 20 -7 -4 -5 402.529 18.2036 9 7 4 5 438.950 13.7452 19 7 4 5 452.316 13.5097 13 7 4 5 431.178 14.8948 6 7 4 5 440.394 15.0436 18 7 4 5 450.366 14.6070 15 7 4 5 454.777 15.9572 10 -8 -4 -5 23.1208 2.33525 1 -8 -4 -5 19.8038 4.25942 20 -8 -4 -5 11.7667 6.31396 9 -8 -4 -5 23.3158 2.65672 1 -8 -4 -5 24.5337 2.73912 4 -8 -4 -5 28.2436 4.19235 5 8 4 5 22.2552 2.35642 13 8 4 5 24.6812 2.52640 19 8 4 5 25.8699 3.65113 15 8 4 5 22.0283 4.38092 10 8 4 5 19.8911 3.89896 6 8 4 5 24.6332 4.10611 18 8 4 5 20.8067 3.92694 12 -9 -4 -5 433.764 16.4678 20 -9 -4 -5 437.402 13.7323 1 -9 -4 -5 416.310 14.3193 4 -9 -4 -5 439.386 20.8875 9 -9 -4 -5 425.975 15.7201 5 -9 -4 -5 428.207 14.2479 1 9 4 5 473.638 16.6413 10 9 4 5 445.613 15.6638 18 9 4 5 449.649 14.0514 13 9 4 5 443.919 16.1321 12 9 4 5 454.382 15.5894 6 9 4 5 438.757 15.4140 15 -10 -4 -5 15.5579 5.02190 5 -10 -4 -5 8.54700 1.98801 1 -10 -4 -5 8.98210 3.03979 1 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29.8822 7.62386 12 10 -5 -5 25.6063 9.55942 16 10 -5 -5 20.0306 9.24026 7 10 -5 -5 24.3082 8.60429 17 10 -5 -5 28.9359 6.77914 2 -10 5 5 20.1255 9.93420 9 -10 5 5 19.0542 6.26298 1 -10 5 5 31.1858 7.87290 4 -10 5 5 22.7481 5.95889 11 9 -5 -5 59.5047 9.58925 7 9 -5 -5 51.0692 8.82494 16 9 -5 -5 61.3922 9.33226 17 9 -5 -5 59.1414 7.66109 12 9 -5 -5 68.1980 7.28947 2 -9 5 5 69.8214 8.01010 4 -9 5 5 69.4712 10.1162 9 -9 5 5 51.1891 6.78756 1 -9 5 5 70.2099 7.23294 11 8 -5 -5 429.135 16.2200 2 8 -5 -5 441.634 19.2989 17 8 -5 -5 435.942 17.3374 12 8 -5 -5 399.735 18.4711 16 8 -5 -5 396.793 18.3220 7 -8 5 5 395.361 15.4952 11 -8 5 5 415.861 16.5656 1 -8 5 5 406.506 19.2779 9 -8 5 5 419.372 17.3991 4 7 -5 -5 6.98923 5.79262 7 7 -5 -5 7.35027 5.77377 16 7 -5 -5 6.55629 4.96014 12 7 -5 -5 -9.5932 5.26873 17 7 -5 -5 6.11942 4.30308 2 -7 5 5 4.84638 6.92430 9 -7 5 5 -6.8231 4.48894 1 -7 5 5 3.29884 3.85962 11 -7 5 5 1.02523 4.69282 4 -7 5 5 -2.1068 3.26978 10 6 -5 -5 49.7999 5.30544 2 6 -5 -5 55.6469 6.08956 12 6 -5 -5 44.5772 6.79953 17 6 -5 -5 36.7719 6.20292 7 6 -5 -5 37.4668 6.35485 16 -6 5 5 46.6126 7.03309 9 -6 5 5 42.4697 4.52783 10 -6 5 5 49.1234 5.18818 19 -6 5 5 53.2977 6.07809 1 -6 5 5 51.0495 5.66412 4 -6 5 5 47.2321 4.91224 11 5 -5 -5 158.952 8.29920 2 5 -5 -5 171.716 5.18194 18 5 -5 -5 156.826 8.61200 12 5 -5 -5 159.338 9.56487 7 5 -5 -5 164.067 10.0463 16 5 -5 -5 174.023 10.1336 17 -5 5 5 167.974 8.36839 19 -5 5 5 157.004 7.75554 11 -5 5 5 165.724 7.61240 10 -5 5 5 159.073 9.09759 1 -5 5 5 165.897 9.80189 9 -5 5 5 154.571 8.21309 4 4 -5 -5 28.0709 4.03733 2 4 -5 -5 23.7226 1.74998 18 4 -5 -5 15.3648 4.47714 17 4 -5 -5 26.1886 4.53392 12 4 -5 -5 17.3654 4.77708 16 4 -5 -5 33.0024 4.34597 1 4 -5 -5 15.4530 4.32654 7 -4 5 5 25.0758 3.79049 19 -4 5 5 29.2597 4.00959 4 -4 5 5 23.6852 2.10078 18 -4 5 5 21.2098 3.56903 11 -4 5 5 31.8051 2.22473 6 -4 5 5 23.0594 3.16795 10 -4 5 5 24.6663 4.56014 1 3 -5 -5 2017.12 56.5273 18 3 -5 -5 1956.69 58.9391 7 3 -5 -5 2015.23 58.2472 2 3 -5 -5 2017.40 58.4481 1 3 -5 -5 1886.03 58.8333 17 3 -5 -5 2013.75 58.9337 12 3 -5 -5 1979.23 59.7130 16 -3 5 5 1964.53 58.5500 1 -3 5 5 1886.15 57.9737 19 -3 5 5 2005.17 58.7487 1 -3 5 5 1913.39 56.6481 6 -3 5 5 1925.54 56.7130 18 -3 5 5 1952.27 57.7676 10 -3 5 5 1902.91 57.8345 4 2 -5 -5 953.773 27.4087 18 2 -5 -5 922.781 29.3563 7 2 -5 -5 904.008 28.8289 1 2 -5 -5 962.894 30.1820 16 2 -5 -5 871.824 29.0759 17 2 -5 -5 971.603 28.8912 2 2 -5 -5 953.542 29.3691 12 -2 5 5 909.685 28.5924 19 -2 5 5 922.185 28.9611 1 -2 5 5 920.934 27.5416 6 -2 5 5 936.916 27.6271 18 -2 5 5 946.835 28.4443 4 -2 5 5 912.017 28.5010 10 1 -5 -5 744.837 23.2950 2 1 -5 -5 761.246 23.6510 17 1 -5 -5 730.310 24.6352 16 1 -5 -5 699.288 23.8522 7 1 -5 -5 743.580 23.8682 12 1 -5 -5 749.483 22.3578 18 1 -5 -5 748.842 23.5029 1 1 -5 -5 762.642 23.0362 14 -1 5 5 763.371 23.0163 4 -1 5 5 763.475 22.5646 6 -1 5 5 771.598 23.3780 19 -1 5 5 750.803 22.6221 18 -1 5 5 743.000 23.2138 13 -1 5 5 733.763 23.3483 10 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1074.25 31.9560 13 2 5 5 1032.20 32.1508 18 2 5 5 1056.18 32.8212 10 2 5 5 1104.78 31.5748 17 2 5 5 1083.44 32.2546 19 2 5 5 1060.68 31.8535 1 2 5 5 1065.06 32.0996 6 -3 -5 -5 508.570 18.2898 9 -3 -5 -5 530.068 17.4169 8 -3 -5 -5 565.090 17.3268 13 -3 -5 -5 551.423 17.3170 5 -3 -5 -5 571.830 17.3203 14 -3 -5 -5 553.259 17.8442 17 -3 -5 -5 549.831 17.6464 7 -3 -5 -5 553.673 17.6769 16 -3 -5 -5 561.862 17.2018 1 -3 -5 -5 529.167 17.7868 20 3 5 5 544.524 17.7649 18 3 5 5 535.441 18.3419 10 3 5 5 557.812 17.7008 6 3 5 5 543.884 17.3338 13 3 5 5 573.523 17.0410 17 3 5 5 544.031 17.7014 19 3 5 5 558.936 17.1221 1 -4 -5 -5 255.422 8.69387 1 -4 -5 -5 249.049 9.34725 8 -4 -5 -5 246.545 8.62317 1 -4 -5 -5 251.390 9.43677 20 -4 -5 -5 231.821 10.3966 9 -4 -5 -5 243.597 9.46165 7 -4 -5 -5 245.555 8.03981 13 -4 -5 -5 268.136 9.33038 14 -4 -5 -5 250.345 8.98209 5 4 5 5 247.151 9.03139 13 4 5 5 236.718 10.0764 10 4 5 5 246.235 9.59562 18 4 5 5 248.439 9.42400 19 4 5 5 245.947 9.47266 6 4 5 5 257.137 8.54742 1 -5 -5 -5 682.758 21.9359 20 -5 -5 -5 694.530 21.0544 1 -5 -5 -5 667.358 21.9629 8 -5 -5 -5 656.712 23.4830 9 -5 -5 -5 698.090 21.5717 5 -5 -5 -5 689.067 20.9464 1 5 5 5 720.823 19.9344 3 5 5 5 712.415 22.0923 6 5 5 5 697.762 22.1926 18 5 5 5 695.110 21.7190 19 5 5 5 653.595 22.7691 10 5 5 5 696.754 21.2008 13 -6 -5 -5 302.961 11.6795 20 -6 -5 -5 311.826 10.4112 1 -6 -5 -5 304.548 11.1798 5 -6 -5 -5 317.149 10.4005 1 -6 -5 -5 321.257 11.8167 8 -6 -5 -5 298.452 13.5564 9 6 5 5 326.155 10.3917 13 6 5 5 324.412 11.9058 18 6 5 5 293.941 12.4175 10 6 5 5 320.798 11.7391 6 6 5 5 315.026 10.9079 19 -7 -5 -5 616.951 21.4358 20 -7 -5 -5 643.824 19.9578 1 -7 -5 -5 656.589 19.9161 4 -7 -5 -5 623.960 24.2317 9 -7 -5 -5 685.238 20.0829 1 -7 -5 -5 674.269 21.1671 5 7 5 5 660.781 21.7429 18 7 5 5 611.357 22.5100 10 7 5 5 673.666 20.4254 19 7 5 5 661.353 20.8522 15 7 5 5 666.741 19.9410 13 7 5 5 678.795 21.6545 6 -8 -5 -5 22.1757 2.57408 1 -8 -5 -5 25.1750 4.16519 5 -8 -5 -5 25.0815 2.58116 1 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128.867 8.51052 7 -4 1 13 105.576 8.48522 8 -4 1 13 118.782 7.46907 6 -4 1 13 129.052 6.52510 15 -4 1 13 117.171 7.24516 1 -4 1 13 114.809 6.77546 11 -4 1 13 121.792 6.60741 4 3 -1 -13 136.166 8.49772 14 3 -1 -13 132.710 8.26448 7 3 -1 -13 142.530 7.76290 3 3 -1 -13 143.079 6.54029 16 3 -1 -13 133.065 8.82089 17 -3 1 13 139.115 7.33699 15 -3 1 13 125.203 7.38118 1 -3 1 13 133.602 9.12166 8 -3 1 13 143.737 6.76044 11 -3 1 13 144.310 7.70190 6 -3 1 13 140.560 6.83677 4 -3 1 13 132.945 7.68048 18 2 -1 -13 64.9561 6.46854 14 2 -1 -13 64.2794 5.07936 3 2 -1 -13 61.3138 6.19536 17 2 -1 -13 65.5749 4.99949 1 2 -1 -13 75.9447 5.84177 7 2 -1 -13 68.9480 4.50313 16 -2 1 13 55.5792 5.13886 18 -2 1 13 67.5401 5.52709 6 -2 1 13 60.2378 4.52478 11 -2 1 13 58.5392 4.21802 4 -2 1 13 75.0198 5.15828 15 -2 1 13 59.5515 5.10628 1 -2 1 13 70.9879 5.10826 10 1 -1 -13 1915.79 58.1408 7 1 -1 -13 1971.29 57.5242 1 1 -1 -13 2011.81 56.6958 16 1 -1 -13 1880.32 57.3060 3 1 -1 -13 1863.51 58.7144 17 1 -1 -13 1885.51 58.6073 14 -1 1 13 1934.12 55.8001 2 -1 1 13 1970.82 57.8499 18 -1 1 13 1956.28 56.6715 11 -1 1 13 1945.97 57.7124 6 -1 1 13 1985.10 56.7069 4 -1 1 13 1925.34 57.2048 15 -1 1 13 1933.70 57.3127 10 -1 1 13 1952.23 55.6959 12 -1 1 13 1961.19 57.6064 1 -1 1 13 1911.64 56.1507 12 0 -1 -13 2242.40 66.4673 1 0 -1 -13 2269.62 67.9204 14 0 -1 -13 2232.69 65.6616 13 0 -1 -13 2331.49 64.6385 5 0 -1 -13 2205.36 67.7866 17 0 -1 -13 2248.28 66.9698 7 0 -1 -13 2194.25 66.3258 3 0 1 13 2289.13 66.2073 10 0 1 13 2248.12 66.2239 15 0 1 13 2244.89 65.0235 12 0 1 13 2221.80 66.5075 1 0 1 13 2294.36 65.1380 2 0 1 13 2283.80 66.7853 18 0 1 13 2239.07 66.6056 6 0 1 13 2280.80 65.4474 11 -1 -1 -13 6.82628 2.25269 13 -1 -1 -13 8.68113 3.23067 20 -1 -1 -13 6.43840 4.17325 17 -1 -1 -13 3.40851 4.14360 14 -1 -1 -13 8.98804 3.39952 3 -1 -1 -13 8.84993 1.65458 5 -1 -1 -13 8.00629 4.01514 7 -1 -1 -13 12.9757 3.39099 1 1 1 13 12.3005 2.99149 15 1 1 13 8.86109 3.36992 18 1 1 13 6.26107 3.16908 1 1 1 13 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-22 16.8054 8.57076 7 -4 -5 -22 26.1350 11.3505 9 -4 -5 -22 36.8479 12.2748 14 4 5 22 6.22732 7.30043 15 4 5 22 20.7440 7.82849 6 4 5 22 6.04215 6.59235 10 -5 -5 -22 10.2277 11.7668 14 -5 -5 -22 18.4360 11.3372 9 -5 -5 -22 0.84957 7.96291 1 -5 -5 -22 -10.679 7.12988 20 -5 -5 -22 10.9253 8.56807 7 5 5 22 -1.2119 6.53387 15 5 5 22 -5.6980 7.34116 6 1 -6 -22 48.0079 11.5113 14 1 -6 -22 41.5174 9.99246 7 -1 6 22 35.2936 8.55943 10 -1 6 22 27.5005 9.87076 6 -1 6 22 44.1645 7.56691 11 0 -6 -22 68.8590 10.5323 7 0 -6 -22 58.3865 10.5217 20 0 -6 -22 69.8743 12.4029 14 0 6 22 78.4518 7.88637 11 0 6 22 66.4588 9.90361 10 0 6 22 85.6332 10.9813 6 -1 -6 -22 11.9072 8.55406 20 -1 -6 -22 1.71723 10.4475 14 -1 -6 -22 19.8980 9.70746 7 1 6 22 -0.9315 8.48685 6 1 6 22 9.60574 8.20357 10 -2 -6 -22 4.11374 7.17037 20 -2 -6 -22 15.6409 8.67660 7 -2 -6 -22 20.0892 10.7763 14 2 6 22 1.57795 8.59449 6 2 6 22 14.8012 7.80654 10 -3 -6 -22 -3.1349 8.21913 7 -3 -6 -22 -6.5035 7.68538 20 -3 -6 -22 -2.2294 10.5354 14 3 6 22 0.62717 6.66259 15 3 6 22 6.37595 7.57753 6 3 6 22 6.81774 7.38365 10 -4 -6 -22 32.0581 11.4926 9 -4 -6 -22 24.3598 9.30929 7 -4 -6 -22 19.8242 11.7721 14 -4 -6 -22 29.7083 7.69327 20 4 6 22 32.6603 7.73898 10 4 6 22 26.1166 7.49023 15 4 6 22 22.8643 8.17973 6 0 -7 -22 124.198 14.0765 14 0 -7 -22 119.145 14.0297 7 0 -7 -22 126.820 13.5037 20 0 7 22 129.131 11.8598 6 0 7 22 123.071 9.51317 11 0 7 22 148.261 12.1107 10 -1 -7 -22 35.1237 10.9844 14 -1 -7 -22 23.9170 8.95836 20 -1 -7 -22 37.3813 11.1143 7 1 7 22 35.9046 8.45355 10 1 7 22 34.0529 8.81137 6 -2 -7 -22 20.1043 10.6756 14 -2 -7 -22 7.21300 7.90741 20 -2 -7 -22 21.8403 9.56833 7 2 7 22 23.6194 7.89497 10 2 7 22 24.2777 9.52684 6 -3 -7 -22 -0.9057 9.92143 7 -3 -7 -22 -7.1957 9.99973 14 -3 -7 -22 -0.0278 7.46899 20 3 7 22 -8.0094 7.80108 6 3 7 22 3.79040 6.95088 10 1 2 -23 103.036 9.44457 7 1 2 -23 123.206 13.0609 14 1 2 -23 125.077 12.5164 3 -1 -2 23 100.834 10.8520 1 -1 -2 23 125.956 14.3582 8 -1 -2 23 104.767 11.2469 6 -1 -2 23 137.553 13.0751 15 0 2 -23 31.7993 11.3154 14 0 2 -23 30.8125 7.44734 7 0 2 -23 50.6394 10.4963 3 0 -2 23 35.7946 8.83361 6 0 -2 23 43.4829 9.96352 15 0 -2 23 27.6766 10.9219 8 2 1 -23 9.00581 6.96662 7 2 1 -23 12.0757 10.4069 14 2 1 -23 7.23875 8.12766 3 -2 -1 23 7.43257 10.7849 8 -2 -1 23 4.55629 8.03550 6 -2 -1 23 -5.2221 7.48094 1 1 1 -23 44.5579 9.46744 3 1 1 -23 30.6584 10.0291 14 1 1 -23 32.1520 7.83321 7 -1 -1 23 22.3047 9.51217 6 -1 -1 23 16.1011 8.28388 1 -1 -1 23 23.1876 9.08897 15 -1 -1 23 22.7828 9.84735 8 0 1 -23 6.38068 10.2351 14 0 1 -23 7.07544 8.82146 3 0 1 -23 2.82108 6.93051 7 0 -1 23 -7.2031 7.68876 6 0 -1 23 6.78539 8.19399 15 -1 1 -23 8.30248 9.32108 14 -1 1 -23 4.88926 7.22106 7 -1 1 -23 11.7182 9.03734 3 1 -1 23 12.3389 8.68125 15 1 -1 23 -4.8739 7.28047 6 2 0 -23 26.7540 8.48678 3 2 0 -23 38.6742 11.2370 14 2 0 -23 33.4373 7.39369 7 -2 0 23 28.8901 7.46319 1 -2 0 23 12.3817 8.50470 6 -2 0 23 31.5011 10.5167 8 1 0 -23 197.343 13.6565 7 1 0 -23 195.412 16.2285 14 1 0 -23 180.415 13.3233 3 -1 0 23 203.029 14.4388 6 -1 0 23 162.216 12.4545 1 -1 0 23 158.259 15.6585 8 0 0 -23 7.26710 9.20599 14 0 0 -23 -1.5014 7.87694 3 0 0 -23 14.3401 6.80901 7 0 0 23 8.65082 7.97762 15 0 0 23 1.72284 7.77387 6 -1 0 -23 6.26475 10.7111 14 -1 0 -23 18.8785 6.85451 7 1 0 23 12.4577 7.83770 6 1 0 23 11.5312 8.13868 15 -2 0 -23 28.8319 10.6944 14 -2 0 -23 19.6548 7.31344 7 2 0 23 26.5257 8.53938 6 2 0 23 26.9087 8.78307 15 2 -1 -23 25.9810 8.28690 3 2 -1 -23 32.7141 11.2507 14 2 -1 -23 24.4384 7.54607 7 -2 1 23 27.1073 8.35235 1 -2 1 23 31.1234 8.74344 6 -2 1 23 19.8332 9.68664 8 1 -1 -23 528.663 24.6352 14 1 -1 -23 518.175 22.0890 3 1 -1 -23 517.470 21.2925 7 -1 1 23 512.696 22.2992 6 -1 1 23 495.546 21.0271 1 0 -1 -23 20.8605 10.9834 14 0 -1 -23 14.1413 7.99771 7 0 1 23 22.1836 8.46220 6 0 1 23 21.2158 9.47815 15 -1 -1 -23 45.3804 8.89003 7 -1 -1 -23 46.1766 12.1089 14 1 1 23 54.0952 9.12473 6 1 1 23 57.9807 9.30889 15 -2 -1 -23 -2.8559 7.42450 7 -2 -1 -23 12.9274 11.1478 14 2 1 23 12.5540 8.85948 6 2 1 23 -12.072 7.50760 15 -3 -1 -23 24.5585 10.9165 14 -3 -1 -23 19.5132 10.5690 9 -3 -1 -23 0.64612 8.17642 7 3 1 23 7.79340 8.13970 15 3 1 23 10.9188 8.85814 6 2 -2 -23 -0.3496 10.2939 14 2 -2 -23 17.6229 7.69324 3 2 -2 -23 1.33641 8.18925 7 -2 2 23 -13.013 7.57040 6 -2 2 23 -2.4079 9.92507 8 -2 2 23 0.13944 6.73703 1 1 -2 -23 116.900 11.3435 7 1 -2 -23 130.068 13.5746 14 -1 2 23 140.129 12.6521 6 -1 2 23 116.819 12.2804 1 0 -2 -23 19.1453 11.0371 14 0 -2 -23 15.7467 8.10299 7 0 2 23 14.5532 8.24522 6 -1 -2 -23 71.5265 10.0359 7 -1 -2 -23 85.1263 13.4274 14 1 2 23 78.3055 9.80684 15 1 2 23 103.588 11.3460 6 -2 -2 -23 7.73732 10.0015 14 -2 -2 -23 6.56708 7.15041 7 2 2 23 6.22352 7.57169 15 2 2 23 8.07627 8.88753 6 -3 -2 -23 24.2236 12.2760 14 -3 -2 -23 16.6198 7.60828 7 3 2 23 16.2610 8.19419 15 3 2 23 7.67426 7.88686 6 1 -3 -23 33.3232 9.46178 7 1 -3 -23 57.8334 12.2584 14 1 -3 -23 54.8821 8.04934 20 -1 3 23 34.1169 10.0135 6 0 -3 -23 18.4979 8.66982 7 0 -3 -23 0.67810 5.69049 20 0 -3 -23 -0.8072 9.20179 14 0 3 23 -2.2325 7.94331 6 -1 -3 -23 -9.8175 9.09400 14 -1 -3 -23 -7.9956 5.98865 20 -1 -3 -23 0.55711 7.24029 7 1 3 23 -1.4716 7.82892 6 -2 -3 -23 43.9036 8.38640 7 -2 -3 -23 39.6378 7.47122 20 -2 -3 -23 36.2720 12.1386 14 2 3 23 41.4607 8.42028 15 2 3 23 36.2505 8.69030 6 -3 -3 -23 4.80079 11.5395 14 -3 -3 -23 2.12520 6.41540 20 -3 -3 -23 13.8346 8.57192 7 3 3 23 4.51535 7.63784 6 3 3 23 6.01345 7.94030 15 1 -4 -23 135.836 15.1414 14 1 -4 -23 130.435 10.8952 20 -1 4 23 164.516 12.9410 6 0 -4 -23 83.1657 10.3278 7 0 -4 -23 67.9396 8.88096 20 0 -4 -23 57.6397 11.7836 14 0 4 23 61.1533 10.1640 6 -1 -4 -23 45.1647 8.12870 20 -1 -4 -23 47.7115 11.1924 14 -1 -4 -23 27.6833 8.57525 7 1 4 23 39.7253 9.24696 6 1 4 23 43.1641 7.65687 10 -2 -4 -23 20.2964 8.39905 7 -2 -4 -23 31.4407 11.7109 14 -2 -4 -23 9.54776 7.14141 20 2 4 23 21.5035 7.84106 6 2 4 23 10.9669 7.57707 15 2 4 23 7.55507 7.27038 10 -3 -4 -23 26.6169 8.51720 7 -3 -4 -23 4.12348 11.2399 14 -3 -4 -23 3.98477 7.02648 20 3 4 23 19.2761 7.86395 15 3 4 23 17.1492 6.93354 10 3 4 23 10.0802 8.78840 6 -1 -5 -23 37.7622 8.80084 20 -1 -5 -23 51.7763 12.8397 14 -1 -5 -23 43.8050 9.52286 7 1 5 23 53.9143 9.25142 6 1 5 23 47.8502 8.95843 10 -2 -5 -23 6.89658 6.78514 20 0 0 0 0.00 0.00 0 _exptl_absorpt_process_details ) SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ) _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_max 0.7461 _exptl_absorpt_correction_T_min 0.3819 _exptl_special_details ) The following wavelength and cell were deduced by SADABS from the direction cosines etc. They are given here for emergency use only: CELL 0.71095 9.862 11.945 16.480 84.980 88.199 73.577 ) ; _shelx_hkl_checksum 44983 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ge1 Ge 0.95230(2) 0.23707(2) 0.24993(2) 0.02174(5) Uani 1 1 d . . . . . Cl1 Cl 0.92190(7) 0.42396(6) 0.24691(4) 0.03627(14) Uani 1 1 d . . . . . O1 O 1.10112(16) 0.17952(16) 0.18089(9) 0.0295(4) Uani 1 1 d . . . . . O2 O 0.83324(16) 0.22850(16) 0.16734(9) 0.0290(4) Uani 1 1 d . . . . . O3 O 1.08107(15) 0.18722(15) 0.33389(9) 0.0265(3) Uani 1 1 d . . . . . O4 O 0.81578(15) 0.21317(15) 0.32232(9) 0.0258(3) Uani 1 1 d . . . . . C1 C 1.0544(2) 0.1735(2) 0.10585(13) 0.0244(5) Uani 1 1 d . . . . . C2 C 0.9075(2) 0.2011(2) 0.09824(13) 0.0234(4) Uani 1 1 d . . . . . C3 C 0.8481(2) 0.1982(2) 0.02360(13) 0.0249(5) Uani 1 1 d . . . . . C4 C 0.9365(3) 0.1662(2) -0.04400(13) 0.0273(5) Uani 1 1 d . . . . . C5 C 1.0820(2) 0.1386(2) -0.03607(13) 0.0281(5) Uani 1 1 d . . . . . C6 C 1.1418(2) 0.1416(2) 0.03939(13) 0.0269(5) Uani 1 1 d . . . . . C7 C 1.0136(2) 0.1746(2) 0.40459(12) 0.0216(4) Uani 1 1 d . . . . . C8 C 0.8684(2) 0.1881(2) 0.39847(12) 0.0218(4) Uani 1 1 d . . . . . C9 C 0.7885(2) 0.1763(2) 0.46753(13) 0.0237(4) Uani 1 1 d . . . . . C10 C 0.8537(2) 0.1490(2) 0.54384(12) 0.0230(4) Uani 1 1 d . . . . . C11 C 0.9976(2) 0.1360(2) 0.55030(12) 0.0225(4) Uani 1 1 d . . . . . C12 C 1.0778(2) 0.1501(2) 0.48022(13) 0.0228(4) Uani 1 1 d . . . . . Br3 Br 0.65042(3) 0.23903(3) 0.01602(2) 0.04020(7) Uani 1 1 d . . . . . Br4 Br 0.85689(3) 0.15986(3) -0.14561(2) 0.03922(7) Uani 1 1 d . . . . . Br5 Br 1.20210(3) 0.09683(3) -0.12633(2) 0.04976(8) Uani 1 1 d . . . . . Br6 Br 1.33837(3) 0.10198(3) 0.05452(2) 0.04287(7) Uani 1 1 d . . . . . Br9 Br 0.59281(2) 0.20305(3) 0.45511(2) 0.04084(7) Uani 1 1 d . . . . . Br10 Br 0.74437(3) 0.13002(3) 0.63699(2) 0.03403(6) Uani 1 1 d . . . . . Br11 Br 1.08484(3) 0.10109(2) 0.65307(2) 0.03391(6) Uani 1 1 d . . . . . Br12 Br 1.27139(2) 0.13851(3) 0.48492(2) 0.03694(7) Uani 1 1 d . . . . . N1 N 0.36557(19) 0.44409(16) 0.24130(11) 0.0221(4) Uani 1 1 d . . . . . C13 C 0.4795(2) 0.32777(19) 0.23916(13) 0.0216(4) Uani 1 1 d . . . . . H13A H 0.527021 0.325892 0.185942 0.026 Uiso 1 1 calc R U . . . H13B H 0.550091 0.324036 0.280620 0.026 Uiso 1 1 calc R U . . . C14 C 0.4274(2) 0.2196(2) 0.25350(14) 0.0246(4) Uani 1 1 d . . . . . H14A H 0.350113 0.225403 0.215959 0.029 Uiso 1 1 calc R U . . . H14B H 0.391051 0.214321 0.309329 0.029 Uiso 1 1 calc R U . . . C15 C 0.5475(2) 0.1103(2) 0.24012(15) 0.0289(5) Uani 1 1 d . . . . . H15A H 0.574544 0.110557 0.182364 0.035 Uiso 1 1 calc R U . . . H15B H 0.629907 0.110912 0.271663 0.035 Uiso 1 1 calc R U . . . C16 C 0.5044(3) 0.0002(2) 0.26585(18) 0.0408(6) Uani 1 1 d . . . . . H16A H 0.492594 -0.006601 0.324582 0.061 Uiso 1 1 calc R U . . . H16B H 0.577158 -0.067679 0.249420 0.061 Uiso 1 1 calc R U . . . H16C H 0.415930 0.004287 0.239996 0.061 Uiso 1 1 calc R U . . . C17 C 0.2552(2) 0.4573(2) 0.17609(14) 0.0268(5) Uani 1 1 d . . . . . H17A H 0.201985 0.400393 0.190772 0.032 Uiso 1 1 calc R U . . . H17B H 0.188545 0.535643 0.176743 0.032 Uiso 1 1 calc R U . . . C18 C 0.3106(3) 0.4408(3) 0.09021(15) 0.0356(6) Uani 1 1 d . . . . . H18A H 0.374664 0.361681 0.087573 0.043 Uiso 1 1 calc R U . . . H18B H 0.363679 0.497253 0.073981 0.043 Uiso 1 1 calc R U . . . C19 C 0.1877(3) 0.4587(3) 0.03258(16) 0.0442(7) Uani 1 1 d . . . . . H19A H 0.131614 0.405310 0.051139 0.053 Uiso 1 1 calc R U . . . H19B H 0.126539 0.539101 0.033515 0.053 Uiso 1 1 calc R U . . . C20 C 0.2389(4) 0.4363(4) -0.05385(19) 0.0716(11) Uani 1 1 d . . . . . H20A H 0.288849 0.492621 -0.073667 0.107 Uiso 1 1 calc R U . . . H20B H 0.158476 0.444441 -0.088586 0.107 Uiso 1 1 calc R U . . . H20C H 0.302024 0.357641 -0.054590 0.107 Uiso 1 1 calc R U . . . C21 C 0.4334(2) 0.5434(2) 0.22574(14) 0.0269(5) Uani 1 1 d . . . . . H21A H 0.357810 0.616818 0.216571 0.032 Uiso 1 1 calc R U . . . H21B H 0.488863 0.531510 0.175216 0.032 Uiso 1 1 calc R U . . . C22 C 0.5288(3) 0.5583(2) 0.29218(15) 0.0307(5) Uani 1 1 d . . . . . H22A H 0.605004 0.485683 0.303129 0.037 Uiso 1 1 calc R U . . . H22B H 0.474388 0.575871 0.342572 0.037 Uiso 1 1 calc R U . . . C23 C 0.5909(3) 0.6583(2) 0.26381(16) 0.0345(6) Uani 1 1 d . . . . . H23A H 0.649322 0.637767 0.215131 0.041 Uiso 1 1 calc R U . . . H23B H 0.513783 0.728744 0.248748 0.041 Uiso 1 1 calc R U . . . C24 C 0.6802(3) 0.6851(3) 0.3288(2) 0.0483(7) Uani 1 1 d . . . . . H24A H 0.620928 0.712583 0.375171 0.072 Uiso 1 1 calc R U . . . H24B H 0.722978 0.745150 0.306747 0.072 Uiso 1 1 calc R U . . . H24C H 0.753830 0.614561 0.345968 0.072 Uiso 1 1 calc R U . . . C25 C 0.2920(2) 0.4466(2) 0.32386(13) 0.0270(5) Uani 1 1 d . . . . . H25A H 0.246626 0.383213 0.329311 0.032 Uiso 1 1 calc R U . . . H25B H 0.364360 0.429656 0.366179 0.032 Uiso 1 1 calc R U . . . C26 C 0.1814(3) 0.5601(2) 0.34057(16) 0.0367(6) Uani 1 1 d . . . . . H26A H 0.224690 0.624795 0.336097 0.044 Uiso 1 1 calc R U . . . H26B H 0.105978 0.577413 0.300116 0.044 Uiso 1 1 calc R U . . . C27 C 0.1200(4) 0.5488(3) 0.4251(2) 0.0610(10) Uani 1 1 d . . . . . H27A H 0.042058 0.619147 0.432851 0.073 Uiso 1 1 calc R U . . . H27B H 0.081018 0.481566 0.429602 0.073 Uiso 1 1 calc R U . . . C28 C 0.2265(6) 0.5329(4) 0.4918(2) 0.0907(16) Uani 1 1 d . . . . . H28A H 0.290464 0.454346 0.493355 0.136 Uiso 1 1 calc R U . . . H28B H 0.177696 0.544703 0.543753 0.136 Uiso 1 1 calc R U . . . H28C H 0.279861 0.589609 0.481213 0.136 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ge1 0.01608(10) 0.03326(13) 0.01584(10) -0.00160(9) 0.00150(8) -0.00718(9) Cl1 0.0311(3) 0.0335(3) 0.0435(3) -0.0002(3) 0.0024(2) -0.0093(3) O1 0.0184(7) 0.0489(11) 0.0189(7) -0.0074(7) 0.0009(6) -0.0046(7) O2 0.0183(7) 0.0519(11) 0.0176(7) -0.0061(7) 0.0026(6) -0.0104(7) O3 0.0170(7) 0.0441(10) 0.0175(7) 0.0002(7) 0.0010(5) -0.0082(7) O4 0.0177(7) 0.0437(10) 0.0168(7) 0.0027(7) -0.0012(5) -0.0112(7) C1 0.0230(10) 0.0300(13) 0.0187(9) -0.0038(9) 0.0016(8) -0.0046(9) C2 0.0222(10) 0.0291(12) 0.0187(9) -0.0015(9) 0.0025(8) -0.0074(9) C3 0.0220(10) 0.0312(13) 0.0208(10) -0.0016(9) -0.0004(8) -0.0063(9) C4 0.0337(12) 0.0289(13) 0.0177(10) -0.0025(9) -0.0012(9) -0.0060(10) C5 0.0289(11) 0.0318(13) 0.0200(10) -0.0047(9) 0.0084(9) -0.0029(10) C6 0.0195(10) 0.0342(13) 0.0238(10) -0.0025(9) 0.0040(8) -0.0030(9) C7 0.0191(9) 0.0263(12) 0.0193(9) -0.0006(8) 0.0016(7) -0.0069(8) C8 0.0208(10) 0.0273(12) 0.0179(9) 0.0008(8) -0.0022(7) -0.0084(9) C9 0.0190(10) 0.0300(12) 0.0232(10) 0.0009(9) 0.0007(8) -0.0097(9) C10 0.0254(10) 0.0273(12) 0.0180(9) -0.0014(8) 0.0027(8) -0.0105(9) C11 0.0260(10) 0.0253(12) 0.0167(9) -0.0017(8) -0.0039(8) -0.0076(9) C12 0.0191(10) 0.0267(12) 0.0237(10) -0.0043(9) -0.0010(8) -0.0074(9) Br3 0.02315(11) 0.0689(2) 0.02767(12) -0.00795(12) -0.00228(9) -0.01022(12) Br4 0.04191(14) 0.05088(17) 0.02036(11) -0.00694(10) -0.00499(10) -0.00409(12) Br5 0.03851(15) 0.0769(2) 0.02553(12) -0.01592(13) 0.01039(11) -0.00044(14) Br6 0.02085(11) 0.0681(2) 0.03583(13) -0.01593(13) 0.00521(10) -0.00344(12) Br9 0.01996(11) 0.0727(2) 0.02998(12) 0.01026(12) -0.00050(9) -0.01750(12) Br10 0.03460(13) 0.05105(17) 0.02046(10) 0.00034(10) 0.00562(9) -0.02015(12) Br11 0.03631(13) 0.04930(16) 0.01926(10) -0.00048(10) -0.00699(9) -0.01714(11) Br12 0.02094(11) 0.06379(19) 0.02833(12) -0.00197(11) -0.00379(9) -0.01571(11) N1 0.0206(8) 0.0224(10) 0.0223(8) 0.0005(7) 0.0005(7) -0.0054(7) C13 0.0195(10) 0.0203(11) 0.0237(10) -0.0005(8) -0.0005(8) -0.0036(8) C14 0.0232(10) 0.0232(12) 0.0279(11) -0.0024(9) 0.0017(8) -0.0076(9) C15 0.0267(11) 0.0227(12) 0.0362(12) -0.0015(10) 0.0070(9) -0.0061(9) C16 0.0490(16) 0.0236(14) 0.0485(16) 0.0008(12) 0.0126(13) -0.0104(12) C17 0.0197(10) 0.0287(13) 0.0294(11) 0.0005(9) -0.0027(8) -0.0033(9) C18 0.0286(12) 0.0500(17) 0.0275(12) 0.0004(11) -0.0035(9) -0.0107(12) C19 0.0412(15) 0.0566(19) 0.0333(13) 0.0035(13) -0.0126(11) -0.0123(14) C20 0.075(3) 0.102(3) 0.0304(15) 0.0035(18) -0.0162(16) -0.015(2) C21 0.0282(11) 0.0224(12) 0.0293(11) 0.0032(9) 0.0001(9) -0.0073(9) C22 0.0328(12) 0.0273(13) 0.0334(12) -0.0009(10) -0.0019(10) -0.0109(10) C23 0.0385(14) 0.0277(14) 0.0401(14) -0.0009(11) -0.0015(11) -0.0143(11) C24 0.0534(18) 0.0367(17) 0.0608(19) -0.0043(14) -0.0145(15) -0.0207(14) C25 0.0304(12) 0.0262(12) 0.0239(10) -0.0029(9) 0.0086(9) -0.0078(10) C26 0.0371(14) 0.0305(14) 0.0406(14) -0.0073(11) 0.0105(11) -0.0066(11) C27 0.085(3) 0.0366(17) 0.059(2) -0.0148(15) 0.0438(19) -0.0152(17) C28 0.155(5) 0.058(2) 0.0361(18) -0.0091(17) 0.015(2) 0.009(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O4 Ge1 O1 150.29(8) . . ? O4 Ge1 O3 87.88(7) . . ? O1 Ge1 O3 86.63(8) . . ? O4 Ge1 O2 87.33(8) . . ? O1 Ge1 O2 87.46(8) . . ? O3 Ge1 O2 158.98(8) . . ? O4 Ge1 Cl1 103.03(6) . . ? O1 Ge1 Cl1 106.68(6) . . ? O3 Ge1 Cl1 99.60(6) . . ? O2 Ge1 Cl1 101.42(6) . . ? C1 O1 Ge1 110.80(13) . . ? C2 O2 Ge1 110.38(13) . . ? C7 O3 Ge1 110.10(13) . . ? C8 O4 Ge1 110.26(13) . . ? O1 C1 C6 124.2(2) . . ? O1 C1 C2 115.40(18) . . ? C6 C1 C2 120.4(2) . . ? O2 C2 C3 124.6(2) . . ? O2 C2 C1 115.24(18) . . ? C3 C2 C1 120.16(19) . . ? C2 C3 C4 119.5(2) . . ? C2 C3 Br3 118.54(16) . . ? C4 C3 Br3 121.93(17) . . ? C5 C4 C3 120.1(2) . . ? C5 C4 Br4 120.02(17) . . ? C3 C4 Br4 119.90(18) . . ? C4 C5 C6 120.3(2) . . ? C4 C5 Br5 120.67(17) . . ? C6 C5 Br5 119.03(17) . . ? C1 C6 C5 119.5(2) . . ? C1 C6 Br6 118.21(17) . . ? C5 C6 Br6 122.29(16) . . ? O3 C7 C12 124.53(19) . . ? O3 C7 C8 115.51(18) . . ? C12 C7 C8 119.96(19) . . ? O4 C8 C9 124.19(19) . . ? O4 C8 C7 115.41(18) . . ? C9 C8 C7 120.40(19) . . ? C8 C9 C10 119.74(19) . . ? C8 C9 Br9 117.96(16) . . ? C10 C9 Br9 122.27(16) . . ? C11 C10 C9 120.09(19) . . ? C11 C10 Br10 120.66(16) . . ? C9 C10 Br10 119.24(16) . . ? C10 C11 C12 119.98(19) . . ? C10 C11 Br11 120.09(16) . . ? C12 C11 Br11 119.93(16) . . ? C7 C12 C11 119.81(19) . . ? C7 C12 Br12 117.98(16) . . ? C11 C12 Br12 122.21(16) . . ? C21 N1 C25 111.91(17) . . ? C21 N1 C17 108.46(17) . . ? C25 N1 C17 108.01(17) . . ? C21 N1 C13 109.07(17) . . ? C25 N1 C13 108.32(16) . . ? C17 N1 C13 111.09(17) . . ? C14 C13 N1 115.22(17) . . ? C14 C13 H13A 108.5 . . ? N1 C13 H13A 108.5 . . ? C14 C13 H13B 108.5 . . ? N1 C13 H13B 108.5 . . ? H13A C13 H13B 107.5 . . ? C13 C14 C15 110.04(18) . . ? C13 C14 H14A 109.7 . . ? C15 C14 H14A 109.7 . . ? C13 C14 H14B 109.7 . . ? C15 C14 H14B 109.7 . . ? H14A C14 H14B 108.2 . . ? C16 C15 C14 111.1(2) . . ? C16 C15 H15A 109.4 . . ? C14 C15 H15A 109.4 . . ? C16 C15 H15B 109.4 . . ? C14 C15 H15B 109.4 . . ? H15A C15 H15B 108.0 . . ? C15 C16 H16A 109.5 . . ? C15 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C15 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C18 C17 N1 116.04(18) . . ? C18 C17 H17A 108.3 . . ? N1 C17 H17A 108.3 . . ? C18 C17 H17B 108.3 . . ? N1 C17 H17B 108.3 . . ? H17A C17 H17B 107.4 . . ? C17 C18 C19 109.5(2) . . ? C17 C18 H18A 109.8 . . ? C19 C18 H18A 109.8 . . ? C17 C18 H18B 109.8 . . ? C19 C18 H18B 109.8 . . ? H18A C18 H18B 108.2 . . ? C20 C19 C18 111.4(3) . . ? C20 C19 H19A 109.3 . . ? C18 C19 H19A 109.3 . . ? C20 C19 H19B 109.3 . . ? C18 C19 H19B 109.3 . . ? H19A C19 H19B 108.0 . . ? C19 C20 H20A 109.5 . . ? C19 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C19 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? N1 C21 C22 116.65(19) . . ? N1 C21 H21A 108.1 . . ? C22 C21 H21A 108.1 . . ? N1 C21 H21B 108.1 . . ? C22 C21 H21B 108.1 . . ? H21A C21 H21B 107.3 . . ? C21 C22 C23 108.7(2) . . ? C21 C22 H22A 110.0 . . ? C23 C22 H22A 110.0 . . ? C21 C22 H22B 110.0 . . ? C23 C22 H22B 110.0 . . ? H22A C22 H22B 108.3 . . ? C24 C23 C22 112.4(2) . . ? C24 C23 H23A 109.1 . . ? C22 C23 H23A 109.1 . . ? C24 C23 H23B 109.1 . . ? C22 C23 H23B 109.1 . . ? H23A C23 H23B 107.9 . . ? C23 C24 H24A 109.5 . . ? C23 C24 H24B 109.5 . . ? H24A C24 H24B 109.5 . . ? C23 C24 H24C 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C26 C25 N1 116.44(19) . . ? C26 C25 H25A 108.2 . . ? N1 C25 H25A 108.2 . . ? C26 C25 H25B 108.2 . . ? N1 C25 H25B 108.2 . . ? H25A C25 H25B 107.3 . . ? C27 C26 C25 109.8(2) . . ? C27 C26 H26A 109.7 . . ? C25 C26 H26A 109.7 . . ? C27 C26 H26B 109.7 . . ? C25 C26 H26B 109.7 . . ? H26A C26 H26B 108.2 . . ? C28 C27 C26 113.3(3) . . ? C28 C27 H27A 108.9 . . ? C26 C27 H27A 108.9 . . ? C28 C27 H27B 108.9 . . ? C26 C27 H27B 108.9 . . ? H27A C27 H27B 107.7 . . ? C27 C28 H28A 109.5 . . ? C27 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C27 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ge1 O4 1.8369(16) . ? Ge1 O1 1.8387(16) . ? Ge1 O3 1.8489(16) . ? Ge1 O2 1.8529(16) . ? Ge1 Cl1 2.1622(13) . ? O1 C1 1.347(3) . ? O2 C2 1.348(3) . ? O3 C7 1.341(2) . ? O4 C8 1.349(2) . ? C1 C6 1.384(3) . ? C1 C2 1.399(3) . ? C2 C3 1.386(3) . ? C3 C4 1.403(3) . ? C3 Br3 1.877(2) . ? C4 C5 1.387(3) . ? C4 Br4 1.887(2) . ? C5 C6 1.400(3) . ? C5 Br5 1.883(2) . ? C6 Br6 1.881(2) . ? C7 C12 1.385(3) . ? C7 C8 1.401(3) . ? C8 C9 1.384(3) . ? C9 C10 1.400(3) . ? C9 Br9 1.880(2) . ? C10 C11 1.390(3) . ? C10 Br10 1.882(2) . ? C11 C12 1.404(3) . ? C11 Br11 1.883(2) . ? C12 Br12 1.879(2) . ? N1 C21 1.518(3) . ? N1 C25 1.520(3) . ? N1 C17 1.520(3) . ? N1 C13 1.521(3) . ? C13 C14 1.518(3) . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C14 C15 1.521(3) . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C15 C16 1.516(3) . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C16 H16A 0.9700 . ? C16 H16B 0.9700 . ? C16 H16C 0.9700 . ? C17 C18 1.509(3) . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C18 C19 1.519(4) . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C19 C20 1.516(4) . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C20 H20A 0.9700 . ? C20 H20B 0.9700 . ? C20 H20C 0.9700 . ? C21 C22 1.520(3) . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C22 C23 1.523(3) . ? C22 H22A 0.9800 . ? C22 H22B 0.9800 . ? C23 C24 1.517(4) . ? C23 H23A 0.9800 . ? C23 H23B 0.9800 . ? C24 H24A 0.9700 . ? C24 H24B 0.9700 . ? C24 H24C 0.9700 . ? C25 C26 1.520(3) . ? C25 H25A 0.9800 . ? C25 H25B 0.9800 . ? C26 C27 1.511(4) . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C27 C28 1.506(6) . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C28 H28A 0.9700 . ? C28 H28B 0.9700 . ? C28 H28C 0.9700 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A C13 H13B O4 0.98 2.66 3.484(3) 141.8 . C13 H13B Br9 0.98 3.09 3.808(3) 131.5 . C14 H14B Br9 0.98 3.14 3.711(3) 119.0 . C17 H17A Cl1 0.98 2.83 3.570(3) 132.9 1_455 C18 H18A Br3 0.98 2.96 3.770(3) 140.5 . C21 H21A Br4 0.98 3.06 4.020(3) 166.4 2_665 C26 H26A Br10 0.98 3.10 4.020(3) 157.1 2_666 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O4 Ge1 O1 C1 87.4(2) . . . . ? O3 Ge1 O1 C1 167.10(16) . . . . ? O2 Ge1 O1 C1 7.27(16) . . . . ? Cl1 Ge1 O1 C1 -93.89(15) . . . . ? O4 Ge1 O2 C2 -158.38(16) . . . . ? O1 Ge1 O2 C2 -7.64(16) . . . . ? O3 Ge1 O2 C2 -81.4(2) . . . . ? Cl1 Ge1 O2 C2 98.86(15) . . . . ? O4 Ge1 O3 C7 -8.19(15) . . . . ? O1 Ge1 O3 C7 -158.98(16) . . . . ? O2 Ge1 O3 C7 -85.1(2) . . . . ? Cl1 Ge1 O3 C7 94.66(14) . . . . ? O1 Ge1 O4 C8 87.25(19) . . . . ? O3 Ge1 O4 C8 7.84(15) . . . . ? O2 Ge1 O4 C8 167.37(16) . . . . ? Cl1 Ge1 O4 C8 -91.52(15) . . . . ? Ge1 O1 C1 C6 175.2(2) . . . . ? Ge1 O1 C1 C2 -5.5(3) . . . . ? Ge1 O2 C2 C3 -174.0(2) . . . . ? Ge1 O2 C2 C1 6.5(3) . . . . ? O1 C1 C2 O2 -0.7(3) . . . . ? C6 C1 C2 O2 178.6(2) . . . . ? O1 C1 C2 C3 179.7(2) . . . . ? C6 C1 C2 C3 -0.9(4) . . . . ? O2 C2 C3 C4 -178.8(2) . . . . ? C1 C2 C3 C4 0.7(4) . . . . ? O2 C2 C3 Br3 1.8(3) . . . . ? C1 C2 C3 Br3 -178.70(18) . . . . ? C2 C3 C4 C5 -0.5(4) . . . . ? Br3 C3 C4 C5 178.89(19) . . . . ? C2 C3 C4 Br4 179.10(18) . . . . ? Br3 C3 C4 Br4 -1.5(3) . . . . ? C3 C4 C5 C6 0.5(4) . . . . ? Br4 C4 C5 C6 -179.08(19) . . . . ? C3 C4 C5 Br5 -179.45(18) . . . . ? Br4 C4 C5 Br5 0.9(3) . . . . ? O1 C1 C6 C5 -179.8(2) . . . . ? C2 C1 C6 C5 1.0(4) . . . . ? O1 C1 C6 Br6 0.8(3) . . . . ? C2 C1 C6 Br6 -178.48(18) . . . . ? C4 C5 C6 C1 -0.8(4) . . . . ? Br5 C5 C6 C1 179.22(19) . . . . ? C4 C5 C6 Br6 178.66(19) . . . . ? Br5 C5 C6 Br6 -1.4(3) . . . . ? Ge1 O3 C7 C12 -173.08(19) . . . . ? Ge1 O3 C7 C8 6.8(2) . . . . ? Ge1 O4 C8 C9 173.79(19) . . . . ? Ge1 O4 C8 C7 -5.9(2) . . . . ? O3 C7 C8 O4 -0.6(3) . . . . ? C12 C7 C8 O4 179.3(2) . . . . ? O3 C7 C8 C9 179.6(2) . . . . ? C12 C7 C8 C9 -0.5(4) . . . . ? O4 C8 C9 C10 179.4(2) . . . . ? C7 C8 C9 C10 -0.9(4) . . . . ? O4 C8 C9 Br9 -2.7(3) . . . . ? C7 C8 C9 Br9 176.99(17) . . . . ? C8 C9 C10 C11 1.1(4) . . . . ? Br9 C9 C10 C11 -176.64(18) . . . . ? C8 C9 C10 Br10 -178.72(18) . . . . ? Br9 C9 C10 Br10 3.5(3) . . . . ? C9 C10 C11 C12 -0.1(3) . . . . ? Br10 C10 C11 C12 179.81(17) . . . . ? C9 C10 C11 Br11 179.26(18) . . . . ? Br10 C10 C11 Br11 -0.9(3) . . . . ? O3 C7 C12 C11 -178.5(2) . . . . ? C8 C7 C12 C11 1.6(3) . . . . ? O3 C7 C12 Br12 2.2(3) . . . . ? C8 C7 C12 Br12 -177.76(17) . . . . ? C10 C11 C12 C7 -1.3(3) . . . . ? Br11 C11 C12 C7 179.39(17) . . . . ? C10 C11 C12 Br12 177.98(17) . . . . ? Br11 C11 C12 Br12 -1.3(3) . . . . ? C21 N1 C13 C14 -179.78(18) . . . . ? C25 N1 C13 C14 58.2(2) . . . . ? C17 N1 C13 C14 -60.3(2) . . . . ? N1 C13 C14 C15 173.45(18) . . . . ? C13 C14 C15 C16 171.7(2) . . . . ? C21 N1 C17 C18 66.4(3) . . . . ? C25 N1 C17 C18 -172.2(2) . . . . ? C13 N1 C17 C18 -53.5(3) . . . . ? N1 C17 C18 C19 -179.1(2) . . . . ? C17 C18 C19 C20 -176.9(3) . . . . ? C25 N1 C21 C22 50.9(3) . . . . ? C17 N1 C21 C22 169.9(2) . . . . ? C13 N1 C21 C22 -69.0(2) . . . . ? N1 C21 C22 C23 177.7(2) . . . . ? C21 C22 C23 C24 176.1(2) . . . . ? C21 N1 C25 C26 55.3(3) . . . . ? C17 N1 C25 C26 -64.0(3) . . . . ? C13 N1 C25 C26 175.5(2) . . . . ? N1 C25 C26 C27 -179.3(2) . . . . ? C25 C26 C27 C28 64.6(3) . . . . ?