#------------------------------------------------------------------------------ #$Date: 2021-10-29 02:53:16 +0300 (Fri, 29 Oct 2021) $ #$Revision: 270128 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/86/7708643.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708643 loop_ _publ_author_name 'Suzuki, Noriyuki' 'Ban, Sayaka' 'Mochizuki, Ayari' 'Ito, Saki' _publ_section_title ; Reactions of Five-Membered Zirconacycloalkynes And Zirconacycloallenes with Cp2Zr(H)Cl; Formal Hydrogenation by Metal Hydrides ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT03313A _journal_year 2021 _chemical_formula_moiety 'C20 H32 Si2 Zr' _chemical_formula_sum 'C46 H78 Si4 Zr2' _chemical_formula_weight 453.38 _chemical_name_systematic 1,1-bis(\h5-cyclopentadienyl)-cis-2,5-bis(trimethylsilyl)-1-zirconacyclopent-3-ene _chemical_properties_physical Air-sensitive,Moisture-sensitive,Heat-sensitive,Oxygen-sensitive _space_group_crystal_system orthorhombic _space_group_IT_number 57 _space_group_name_Hall '-P 2c 2b' _space_group_name_H-M_alt 'P b c m' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_update_record ; 2021-10-19 deposited with the CCDC. 2021-10-26 downloaded from the CCDC. ; _cell_angle_alpha 90.0000 _cell_angle_beta 90.0000 _cell_angle_gamma 90.0000 _cell_formula_units_Z 8 _cell_length_a 13.37714(16) _cell_length_b 15.7203(2) _cell_length_c 23.1966(4) _cell_measurement_reflns_used 21619 _cell_measurement_temperature 123 _cell_measurement_theta_max 77.17 _cell_measurement_theta_min 3.80 _cell_volume 4878.07(12) _computing_cell_refinement 'CrysAlisPro 1.171.41.116a (Rigaku OD, 2021)' _computing_data_collection 'CrysAlisPro 1.171.41.116a (Rigaku OD, 2021)' _computing_data_reduction 'CrysAlisPro 1.171.41.116a (Rigaku OD, 2021)' _computing_molecular_graphics 'CrystalStructure 4.2.5' _computing_publication_material 'CrystalStructure 4.2.5 (Rigaku, 2017)' _computing_structure_refinement 'SHELXL97 (Sheldrick, 2008)' _computing_structure_solution 'Il Milione (Burla, et al., 2007)' _diffrn_ambient_temperature 123 _diffrn_detector_area_resol_mean 10.000 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Rigaku XtaLAB P100' _diffrn_measurement_method \w _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54187 _diffrn_reflns_av_R_equivalents 0.0563 _diffrn_reflns_Laue_measured_fraction_full 0.000 _diffrn_reflns_Laue_measured_fraction_max 0.000 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 59269 _diffrn_reflns_point_group_measured_fraction_full 0.000 _diffrn_reflns_point_group_measured_fraction_max 0.000 _diffrn_reflns_theta_full 64.990 _diffrn_reflns_theta_max 64.990 _diffrn_reflns_theta_min 3.304 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 4.769 _exptl_absorpt_correction_T_max 0.909 _exptl_absorpt_correction_T_min 0.601 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.116a (Rigaku Oxford Diffraction, 2021) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear light orange' _exptl_crystal_density_diffrn 1.235 _exptl_crystal_density_method 'not measured' _exptl_crystal_description plate _exptl_crystal_F_000 1884.00 _exptl_crystal_recrystallization_method 'Re-crystallisation from solvent: hexane' _exptl_crystal_size_max 0.070 _exptl_crystal_size_mid 0.030 _exptl_crystal_size_min 0.020 _refine_diff_density_max 2.21 _refine_diff_density_min -1.13 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.046 _refine_ls_hydrogen_treatment constr _refine_ls_number_parameters 260 _refine_ls_number_reflns 4279 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0766 _refine_ls_R_factor_gt 0.0707 _refine_ls_shift/su_max 0.003 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w = 1/[\s^2^(Fo^2^)+(0.0548P)^2^+32.7574P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1629 _refine_ls_wR_factor_ref 0.1669 _reflns_d_resolution_high 0.8507 _reflns_number_gt 3847 _reflns_number_total 4279 _reflns_threshold_expression F^2^>2.0\s(F^2^) _cod_data_source_file d1dt03313a2.cif _cod_data_source_block ns402ar _cod_database_code 7708643 _shelx_title ' ns402ar' _shelx_refln_list_code 4 _shelx_f_calc_maximum 622.75 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 +X,+Y,+Z 2 -X,-Y,1/2+Z 3 +X,1/2-Y,-Z 4 -X,1/2+Y,1/2-Z 5 -X,-Y,-Z 6 +X,+Y,-1/2-Z 7 -X,-1/2+Y,+Z 8 +X,-1/2-Y,-1/2+Z loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, y, -z-1/2' '-x, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Zr1 Zr 1.00193(4) 0.36288(4) 0.7500 0.0353(2) Uani 1 2 d S . . Zr2 Zr 0.51020(4) 0.59573(4) 0.7500 0.0345(2) Uani 1 2 d S . . Si1 Si 0.88904(18) 0.43547(13) 0.60292(8) 0.0621(6) Uani 1 1 d . . . Si18 Si 0.3825(3) 0.6495(2) 0.89440(17) 0.1269(14) Uani 1 1 d . . . C1 C 0.8902(5) 0.4171(4) 0.6822(3) 0.0445(14) Uani 1 1 d . . . H1 H 0.8245 0.3896 0.6912 0.053 Uiso 1 1 calc R . . C2 C 0.8976(4) 0.4855(4) 0.7200(3) 0.0433(13) Uani 1 1 d . . . H2 H 0.9385 0.5330 0.7037 0.052 Uiso 1 1 calc R . . C3 C 0.9741(14) 0.5234(7) 0.5840(4) 0.183(9) Uani 1 1 d . . . H3A H 0.9685 0.5357 0.5427 0.219 Uiso 1 1 calc R . . H3B H 1.0431 0.5071 0.5930 0.219 Uiso 1 1 calc R . . H3C H 0.9560 0.5742 0.6061 0.219 Uiso 1 1 calc R . . C4 C 0.7602(10) 0.4638(11) 0.5789(4) 0.194(9) Uani 1 1 d . . . H4A H 0.7150 0.4161 0.5867 0.233 Uiso 1 1 calc R . . H4B H 0.7607 0.4760 0.5375 0.233 Uiso 1 1 calc R . . H4C H 0.7373 0.5142 0.6000 0.233 Uiso 1 1 calc R . . C5 C 0.9308(6) 0.3406(5) 0.5622(3) 0.070(2) Uani 1 1 d . . . H5A H 0.9404 0.3558 0.5216 0.084 Uiso 1 1 calc R . . H5B H 0.8801 0.2958 0.5652 0.084 Uiso 1 1 calc R . . H5C H 0.9941 0.3199 0.5783 0.084 Uiso 1 1 calc R . . C6 C 0.8940(7) 0.2290(5) 0.7500 0.088(5) Uani 1 2 d S . . H6 H 0.8236 0.2368 0.7500 0.105 Uiso 1 2 calc SR . . C7 C 0.9574(9) 0.2219(4) 0.7020(4) 0.088(3) Uani 1 1 d . . . H7 H 0.9381 0.2238 0.6626 0.105 Uiso 1 1 calc R . . C8 C 1.0503(7) 0.2120(4) 0.7225(5) 0.103(5) Uani 1 1 d . . . H8 H 1.1083 0.2057 0.6993 0.123 Uiso 1 1 calc R . . C9 C 1.1824 0.3720 0.7785 0.094(4) Uani 1 1 d . . . H9 H 1.2079 0.3273 0.8018 0.113 Uiso 1 1 calc R . . C10 C 1.1395 0.4472 0.7998 0.152(7) Uani 1 1 d . . . H10 H 1.1283 0.4640 0.8387 0.183 Uiso 1 1 calc R . . C11 C 1.1180 0.4900 0.7500 0.176(15) Uani 1 2 d S . . H11 H 1.0901 0.5456 0.7500 0.211 Uiso 1 2 calc SR . . C12 C 0.3877(6) 0.6305(6) 0.8167(4) 0.081(3) Uani 1 1 d . . . H12 H 0.3283 0.5945 0.8072 0.097 Uiso 1 1 calc R . . C13 C 0.3825(5) 0.7028(6) 0.7800(5) 0.098(4) Uani 1 1 d . . . H13 H 0.4118 0.7555 0.7973 0.118 Uiso 1 1 calc R . . C14 C 0.432(3) 0.7587(14) 0.9121(9) 0.51(3) Uani 1 1 d . . . H14A H 0.5009 0.7636 0.8988 0.611 Uiso 1 1 calc R . . H14B H 0.4290 0.7676 0.9539 0.611 Uiso 1 1 calc R . . H14C H 0.3905 0.8017 0.8928 0.611 Uiso 1 1 calc R . . C15 C 0.2555(9) 0.6382(9) 0.9215(6) 0.160(7) Uani 1 1 d . . . H15A H 0.2525 0.6583 0.9614 0.191 Uiso 1 1 calc R . . H15B H 0.2358 0.5782 0.9200 0.191 Uiso 1 1 calc R . . H15C H 0.2099 0.6719 0.8976 0.191 Uiso 1 1 calc R . . C16 C 0.4612(11) 0.5803(15) 0.9346(6) 0.287(16) Uani 1 1 d . . . H16A H 0.5309 0.5894 0.9232 0.345 Uiso 1 1 calc R . . H16B H 0.4424 0.5211 0.9269 0.345 Uiso 1 1 calc R . . H16C H 0.4536 0.5923 0.9758 0.345 Uiso 1 1 calc R . . C17 C 0.4317(10) 0.4485(7) 0.7500 0.096(5) Uani 1 2 d S . . H17 H 0.3610 0.4430 0.7500 0.115 Uiso 1 2 calc SR . . C18 C 0.4879(11) 0.4530(5) 0.7026(4) 0.109(4) Uani 1 1 d . . . H18 H 0.4652 0.4547 0.6638 0.131 Uiso 1 1 calc R . . C19 C 0.5842(9) 0.4545(5) 0.7211(5) 0.102(4) Uani 1 1 d . . . H19 H 0.6418 0.4554 0.6971 0.123 Uiso 1 1 calc R . . C20 C 0.695(2) 0.6251(16) 0.7500 0.054(15) Uani 0.50 2 d SP . . C21 C 0.6867(14) 0.6312(15) 0.7197(10) 0.056(8) Uani 0.50 1 d P . . C22 C 0.646(6) 0.670(4) 0.689(2) 0.106(14) Uani 0.50 1 d P . . C23 C 0.6063(15) 0.7290(11) 0.7207(8) 0.043(7) Uani 0.50 1 d P . . C24 C 0.596(2) 0.7385(16) 0.7500 0.044(12) Uani 0.50 2 d SP . . C25 C 0.636(7) 0.699(5) 0.7012(19) 0.15(5) Uani 0.50 1 d P . . C26 C 0.6993(17) 0.8488(15) 0.5557(15) 0.293(15) Uani 1 1 d . . . C27 C 0.7725(15) 0.7628(16) 0.5638(11) 0.202(9) Uani 1 1 d . . . C28 C 0.774(2) 0.707(2) 0.5216(11) 0.35(2) Uani 1 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zr1 0.0263(3) 0.0193(3) 0.0603(5) 0.000 0.000 0.0012(2) Zr2 0.0262(3) 0.0222(3) 0.0551(4) 0.000 0.000 -0.0024(2) Si1 0.0956(15) 0.0532(11) 0.0376(9) -0.0059(8) 0.0008(10) 0.0145(10) Si18 0.107(2) 0.138(3) 0.136(3) -0.067(2) 0.069(2) -0.026(2) C1 0.051(3) 0.038(3) 0.044(3) -0.004(3) -0.002(3) 0.011(3) C2 0.046(3) 0.037(3) 0.047(3) 0.001(3) -0.002(3) 0.007(3) C3 0.40(2) 0.104(9) 0.041(5) -0.004(5) 0.041(9) -0.119(12) C4 0.196(14) 0.34(2) 0.045(5) -0.015(9) -0.021(7) 0.188(15) C5 0.086(6) 0.070(5) 0.053(4) -0.015(4) 0.006(4) -0.004(4) C6 0.033(5) 0.017(4) 0.213(17) 0.000 0.000 -0.003(4) C7 0.171(10) 0.017(3) 0.075(5) -0.009(3) -0.034(6) -0.005(5) C8 0.088(6) 0.027(3) 0.193(14) -0.009(4) 0.062(7) 0.006(4) C9 0.032(3) 0.094(6) 0.157(10) 0.025(6) -0.024(4) -0.014(4) C10 0.054(5) 0.185(13) 0.218(17) -0.129(13) 0.012(8) -0.046(7) C11 0.034(6) 0.023(5) 0.47(5) 0.000 0.000 -0.015(5) C12 0.048(4) 0.088(6) 0.106(7) -0.026(5) 0.028(4) -0.001(4) C13 0.039(4) 0.063(5) 0.193(12) -0.025(6) 0.016(5) 0.006(3) C14 0.98(7) 0.26(2) 0.29(3) -0.22(2) 0.44(4) -0.38(4) C15 0.122(9) 0.206(14) 0.151(11) 0.109(11) 0.079(9) 0.081(9) C16 0.168(14) 0.61(4) 0.088(9) -0.066(16) -0.035(9) 0.25(2) C17 0.069(8) 0.036(6) 0.183(17) 0.000 0.000 -0.029(5) C18 0.217(15) 0.031(4) 0.079(6) -0.015(4) -0.043(8) -0.007(6) C19 0.128(8) 0.033(4) 0.146(10) -0.010(4) 0.070(7) 0.013(5) C20 0.023(11) 0.033(11) 0.11(5) 0.000 0.000 0.002(8) C21 0.026(8) 0.104(16) 0.037(19) -0.016(11) 0.002(9) -0.028(9) C22 0.084(19) 0.13(3) 0.10(4) -0.02(3) 0.01(3) -0.09(2) C23 0.069(10) 0.054(10) 0.01(2) 0.008(10) 0.015(10) -0.035(8) C24 0.039(12) 0.034(10) 0.06(4) 0.000 0.000 -0.024(8) C25 0.14(5) 0.30(10) 0.009(14) -0.03(3) 0.022(16) -0.18(7) C26 0.23(2) 0.21(2) 0.44(4) -0.02(2) -0.16(3) 0.016(19) C27 0.169(15) 0.21(2) 0.23(2) 0.081(18) 0.009(16) 0.026(16) C28 0.49(4) 0.37(5) 0.18(3) -0.09(2) -0.11(3) 0.31(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; H H 0.0000 0.0000 ; International Tables for Crystallography (Vol. C, Table 6.1.1.4) ; Si Si 0.2541 0.3302 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; Zr Zr -0.1862 2.2449 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 Zr1 C1 84.8(3) 6_557 . ? C1 Zr1 C2 62.9(2) 6_557 . ? C1 Zr1 C2 33.42(19) . . ? C1 Zr1 C2 33.42(19) 6_557 6_557 ? C1 Zr1 C2 62.9(2) . 6_557 ? C2 Zr1 C2 32.6(3) . 6_557 ? C1 Zr1 C9 114.77(16) 6_557 . ? C1 Zr1 C9 140.77(16) . . ? C2 Zr1 C9 124.88(14) . . ? C2 Zr1 C9 115.07(14) 6_557 . ? C1 Zr1 C9 140.77(16) 6_557 6_557 ? C1 Zr1 C9 114.77(16) . 6_557 ? C2 Zr1 C9 115.07(14) . 6_557 ? C2 Zr1 C9 124.88(14) 6_557 6_557 ? C9 Zr1 C9 30.568(7) . 6_557 ? C1 Zr1 C11 96.02(16) 6_557 . ? C1 Zr1 C11 96.02(16) . . ? C2 Zr1 C11 74.43(14) . . ? C2 Zr1 C11 74.43(14) 6_557 . ? C9 Zr1 C11 50.519(12) . . ? C9 Zr1 C11 50.518(12) 6_557 . ? C1 Zr1 C8 109.6(3) 6_557 6_557 ? C1 Zr1 C8 132.4(2) . 6_557 ? C2 Zr1 C8 160.0(3) . 6_557 ? C2 Zr1 C8 143.0(3) 6_557 6_557 ? C9 Zr1 C8 75.1(2) . 6_557 ? C9 Zr1 C8 82.8(2) 6_557 6_557 ? C11 Zr1 C8 125.6(2) . 6_557 ? C1 Zr1 C8 132.4(2) 6_557 . ? C1 Zr1 C8 109.6(3) . . ? C2 Zr1 C8 143.0(3) . . ? C2 Zr1 C8 160.0(3) 6_557 . ? C9 Zr1 C8 82.8(2) . . ? C9 Zr1 C8 75.1(2) 6_557 . ? C11 Zr1 C8 125.6(2) . . ? C8 Zr1 C8 29.0(5) 6_557 . ? C1 Zr1 C10 88.10(16) 6_557 . ? C1 Zr1 C10 125.42(16) . . ? C2 Zr1 C10 97.45(14) . . ? C2 Zr1 C10 82.79(14) 6_557 . ? C9 Zr1 C10 32.284(7) . . ? C9 Zr1 C10 52.703(12) 6_557 . ? C11 Zr1 C10 31.270(7) . . ? C8 Zr1 C10 100.87(19) 6_557 . ? C8 Zr1 C10 114.6(2) . . ? C1 Zr1 C10 125.42(16) 6_557 6_557 ? C1 Zr1 C10 88.09(16) . 6_557 ? C2 Zr1 C10 82.78(14) . 6_557 ? C2 Zr1 C10 97.45(14) 6_557 6_557 ? C9 Zr1 C10 52.705(12) . 6_557 ? C9 Zr1 C10 32.283(7) 6_557 6_557 ? C11 Zr1 C10 31.270(7) . 6_557 ? C8 Zr1 C10 114.6(2) 6_557 6_557 ? C8 Zr1 C10 100.87(19) . 6_557 ? C10 Zr1 C10 54.033(12) . 6_557 ? C1 Zr1 C7 117.5(3) 6_557 . ? C1 Zr1 C7 82.7(3) . . ? C2 Zr1 C7 114.9(3) . . ? C2 Zr1 C7 131.8(3) 6_557 . ? C9 Zr1 C7 112.9(3) . . ? C9 Zr1 C7 99.2(3) 6_557 . ? C11 Zr1 C7 146.0(3) . . ? C8 Zr1 C7 50.0(3) 6_557 . ? C8 Zr1 C7 30.5(3) . . ? C10 Zr1 C7 145.0(3) . . ? C10 Zr1 C7 115.0(3) 6_557 . ? C12 Zr2 C12 83.7(5) 6_557 . ? C12 Zr2 C13 62.9(4) 6_557 . ? C12 Zr2 C13 34.1(3) . . ? C12 Zr2 C13 34.1(3) 6_557 6_557 ? C12 Zr2 C13 62.9(4) . 6_557 ? C13 Zr2 C13 32.3(5) . 6_557 ? C12 Zr2 C20 130.6(4) 6_557 . ? C12 Zr2 C20 130.6(4) . . ? C13 Zr2 C20 123.3(6) . . ? C13 Zr2 C20 123.3(6) 6_557 . ? C12 Zr2 C19 107.9(4) 6_557 . ? C12 Zr2 C19 131.5(3) . . ? C13 Zr2 C19 159.4(3) . . ? C13 Zr2 C19 142.0(4) 6_557 . ? C20 Zr2 C19 77.1(6) . . ? C12 Zr2 C19 131.5(3) 6_557 6_557 ? C12 Zr2 C19 107.9(4) . 6_557 ? C13 Zr2 C19 142.0(4) . 6_557 ? C13 Zr2 C19 159.4(3) 6_557 6_557 ? C20 Zr2 C19 77.1(6) . 6_557 ? C19 Zr2 C19 30.8(5) . 6_557 ? C12 Zr2 C18 80.5(4) 6_557 . ? C12 Zr2 C18 114.7(4) . . ? C13 Zr2 C18 129.9(4) . . ? C13 Zr2 C18 113.5(4) 6_557 . ? C20 Zr2 C18 106.3(6) . . ? C19 Zr2 C18 31.3(3) . . ? C19 Zr2 C18 51.5(3) 6_557 . ? C12 Zr2 C18 114.7(4) 6_557 6_557 ? C12 Zr2 C18 80.5(4) . 6_557 ? C13 Zr2 C18 113.5(4) . 6_557 ? C13 Zr2 C18 129.9(4) 6_557 6_557 ? C20 Zr2 C18 106.3(6) . 6_557 ? C19 Zr2 C18 51.5(3) . 6_557 ? C19 Zr2 C18 31.3(3) 6_557 6_557 ? C18 Zr2 C18 51.8(5) . 6_557 ? C12 Zr2 C17 85.6(3) 6_557 . ? C12 Zr2 C17 85.6(3) . . ? C13 Zr2 C17 109.3(4) . . ? C13 Zr2 C17 109.3(4) 6_557 . ? C20 Zr2 C17 125.0(6) . . ? C19 Zr2 C17 50.2(4) . . ? C19 Zr2 C17 50.2(4) 6_557 . ? C18 Zr2 C17 30.6(3) . . ? C18 Zr2 C17 30.6(3) 6_557 . ? C12 Zr2 C24 96.4(6) 6_557 . ? C12 Zr2 C24 96.4(6) . . ? C13 Zr2 C24 73.2(7) . . ? C13 Zr2 C24 73.2(7) 6_557 . ? C20 Zr2 C24 52.3(9) . . ? C19 Zr2 C24 127.2(7) . . ? C19 Zr2 C24 127.2(7) 6_557 . ? C18 Zr2 C24 148.0(5) . . ? C18 Zr2 C24 148.0(5) 6_557 . ? C17 Zr2 C24 177.3(8) . . ? C12 Zr2 C21 115.0(5) 6_557 . ? C12 Zr2 C21 142.6(6) . . ? C13 Zr2 C21 124.6(6) . . ? C13 Zr2 C21 114.4(5) 6_557 . ? C20 Zr2 C21 16.4(5) . . ? C19 Zr2 C21 75.7(6) . . ? C19 Zr2 C21 84.3(6) 6_557 . ? C18 Zr2 C21 100.7(7) . . ? C18 Zr2 C21 115.4(6) 6_557 . ? C17 Zr2 C21 126.0(6) . . ? C24 Zr2 C21 51.5(9) . . ? C3 Si1 C5 107.2(5) . . ? C3 Si1 C1 110.3(4) . . ? C5 Si1 C1 112.1(3) . . ? C3 Si1 C4 108.7(8) . . ? C5 Si1 C4 108.6(5) . . ? C1 Si1 C4 109.8(4) . . ? C16 Si18 C12 113.2(5) . . ? C16 Si18 C15 108.2(7) . . ? C12 Si18 C15 111.1(6) . . ? C16 Si18 C14 103.7(13) . . ? C12 Si18 C14 110.5(7) . . ? C15 Si18 C14 109.9(10) . . ? C2 C1 Si1 120.2(5) . . ? C2 C1 Zr1 79.2(4) . . ? Si1 C1 Zr1 136.7(3) . . ? C2 C1 H1 105.4 . . ? Si1 C1 H1 105.4 . . ? Zr1 C1 H1 105.4 . . ? C2 C2 C1 129.0(4) 6_557 . ? C2 C2 Zr1 73.69(13) 6_557 . ? C1 C2 Zr1 67.4(3) . . ? C2 C2 H2 112.2 6_557 . ? C1 C2 H2 112.2 . . ? Zr1 C2 H2 112.2 . . ? Si1 C3 H3A 109.5 . . ? Si1 C3 H3B 109.5 . . ? H3A C3 H3B 109.5 . . ? Si1 C3 H3C 109.5 . . ? H3A C3 H3C 109.5 . . ? H3B C3 H3C 109.5 . . ? Si1 C4 H4A 109.5 . . ? Si1 C4 H4B 109.5 . . ? H4A C4 H4B 109.5 . . ? Si1 C4 H4C 109.5 . . ? H4A C4 H4C 109.5 . . ? H4B C4 H4C 109.5 . . ? Si1 C5 H5A 109.5 . . ? Si1 C5 H5B 109.5 . . ? H5A C5 H5B 109.5 . . ? Si1 C5 H5C 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? C7 C6 C7 104.9(10) 6_557 . ? C7 C6 Zr1 74.0(5) 6_557 . ? C7 C6 Zr1 74.0(5) . . ? C7 C6 H6 127.5 6_557 . ? C7 C6 H6 127.5 . . ? Zr1 C6 H6 117.0 . . ? C8 C7 C6 106.7(8) . . ? C8 C7 Zr1 74.3(4) . . ? C6 C7 Zr1 74.1(5) . . ? C8 C7 H7 126.6 . . ? C6 C7 H7 126.6 . . ? Zr1 C7 H7 117.1 . . ? C8 C8 C7 110.8(6) 6_557 . ? C8 C8 Zr1 75.5(2) 6_557 . ? C7 C8 Zr1 75.2(4) . . ? C8 C8 H8 124.6 6_557 . ? C7 C8 H8 124.6 . . ? Zr1 C8 H8 116.5 . . ? C9 C9 C10 110.647(1) 6_557 . ? C9 C9 Zr1 74.718(4) 6_557 . ? C10 C9 Zr1 75.374(13) . . ? C9 C9 H9 124.7 6_557 . ? C10 C9 H9 124.7 . . ? Zr1 C9 H9 117.0 . . ? C11 C10 C9 101.6 . . ? C11 C10 Zr1 73.763(9) . . ? C9 C10 Zr1 72.342(13) . . ? C11 C10 H10 129.2 . . ? C9 C10 H10 129.2 . . ? Zr1 C10 H10 117.5 . . ? C10 C11 C10 115.383(1) . 6_557 ? C10 C11 Zr1 74.968(7) . . ? C10 C11 Zr1 74.969(7) 6_557 . ? C10 C11 H11 122.3 . . ? C10 C11 H11 122.3 6_557 . ? Zr1 C11 H11 119.0 . . ? C13 C12 Si18 117.3(7) . . ? C13 C12 Zr2 79.8(5) . . ? Si18 C12 Zr2 136.3(5) . . ? C13 C12 H12 106.3 . . ? Si18 C12 H12 106.3 . . ? Zr2 C12 H12 106.3 . . ? C13 C13 C12 126.8(5) 6_557 . ? C13 C13 Zr2 73.8(3) 6_557 . ? C12 C13 Zr2 66.1(4) . . ? C13 C13 H13 113.7 6_557 . ? C12 C13 H13 113.7 . . ? Zr2 C13 H13 113.7 . . ? Si18 C14 H14A 109.5 . . ? Si18 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? Si18 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? Si18 C15 H15A 109.5 . . ? Si18 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? Si18 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? Si18 C16 H16A 109.5 . . ? Si18 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? Si18 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C18 C17 C18 111.1(14) . 6_557 ? C18 C17 Zr2 73.7(6) . . ? C18 C17 Zr2 73.7(6) 6_557 . ? C18 C17 H17 124.4 . . ? C18 C17 H17 124.4 6_557 . ? Zr2 C17 H17 119.7 . . ? C17 C18 C19 105.9(10) . . ? C17 C18 Zr2 75.7(6) . . ? C19 C18 Zr2 74.6(5) . . ? C17 C18 H18 127.0 . . ? C19 C18 H18 127.0 . . ? Zr2 C18 H18 115.2 . . ? C19 C19 C18 108.5(7) 6_557 . ? C19 C19 Zr2 74.6(3) 6_557 . ? C18 C19 Zr2 74.2(5) . . ? C19 C19 H19 125.8 6_557 . ? C18 C19 H19 125.8 . . ? Zr2 C19 H19 117.4 . . ? C21 C20 C21 156(7) . 6_557 ? C21 C20 C22 23(4) . . ? C21 C20 C22 134(5) 6_557 . ? C21 C20 C22 134(5) . 6_557 ? C21 C20 C22 23(4) 6_557 6_557 ? C22 C20 C22 111(5) . 6_557 ? C21 C20 C25 117(4) . 6_557 ? C21 C20 C25 40(4) 6_557 6_557 ? C22 C20 C25 95(2) . 6_557 ? C22 C20 C25 18(4) 6_557 6_557 ? C21 C20 C25 40(4) . . ? C21 C20 C25 117(4) 6_557 . ? C22 C20 C25 18(4) . . ? C22 C20 C25 95(2) 6_557 . ? C25 C20 C25 78(4) 6_557 . ? C21 C20 Zr2 82(3) . . ? C21 C20 Zr2 82(3) 6_557 . ? C22 C20 Zr2 72(2) . . ? C22 C20 Zr2 72(2) 6_557 . ? C25 C20 Zr2 72(2) 6_557 . ? C25 C20 Zr2 72(2) . . ? C20 C21 C22 143(6) . . ? C20 C21 C21 12(4) . 6_557 ? C22 C21 C21 131(4) . 6_557 ? C20 C21 C25 120(4) . . ? C22 C21 C25 24(4) . . ? C21 C21 C25 109(2) 6_557 . ? C20 C21 C23 101(4) . . ? C22 C21 C23 42(4) . . ? C21 C21 C23 89.3(9) 6_557 . ? C25 C21 C23 19.6(18) . . ? C20 C21 Zr2 81(4) . . ? C22 C21 Zr2 80(3) . . ? C21 C21 Zr2 73.9(5) 6_557 . ? C25 C21 Zr2 78(3) . . ? C23 C21 Zr2 69.0(9) . . ? C25 C22 C21 106(10) . . ? C25 C22 C23 12(9) . . ? C21 C22 C23 104(5) . . ? C25 C22 C20 92(10) . . ? C21 C22 C20 15(2) . . ? C23 C22 C20 90(3) . . ? C25 C22 C24 22(9) . . ? C21 C22 C24 91(4) . . ? C23 C22 C24 13.9(18) . . ? C20 C22 C24 76.0(19) . . ? C25 C22 Zr2 86(10) . . ? C21 C22 Zr2 75(3) . . ? C23 C22 Zr2 74(3) . . ? C20 C22 Zr2 68.8(17) . . ? C24 C22 Zr2 66.7(17) . . ? C24 C23 C25 143(7) . . ? C24 C23 C23 17(4) . 6_557 ? C25 C23 C23 126(6) . 6_557 ? C24 C23 C22 140(6) . . ? C25 C23 C22 9(6) . . ? C23 C23 C22 124(3) 6_557 . ? C24 C23 C25 35(6) . 6_557 ? C25 C23 C25 108(10) . 6_557 ? C23 C23 C25 19(3) 6_557 6_557 ? C22 C23 C25 106(2) . 6_557 ? C24 C23 C21 107(4) . . ? C25 C23 C21 36(6) . . ? C23 C23 C21 90.7(9) 6_557 . ? C22 C23 C21 34(4) . . ? C25 C23 C21 72(4) 6_557 . ? C24 C23 Zr2 80(2) . . ? C25 C23 Zr2 85(4) . . ? C23 C23 Zr2 74.5(4) 6_557 . ? C22 C23 Zr2 76(2) . . ? C25 C23 Zr2 69.4(16) 6_557 . ? C21 C23 Zr2 67.6(8) . . ? C23 C24 C23 147(7) 6_557 . ? C23 C24 C25 19(4) 6_557 6_557 ? C23 C24 C25 128(7) . 6_557 ? C23 C24 C25 128(7) 6_557 . ? C23 C24 C25 19(4) . . ? C25 C24 C25 109(10) 6_557 . ? C23 C24 C22 121(4) 6_557 . ? C23 C24 C22 26(4) . . ? C25 C24 C22 102(3) 6_557 . ? C25 C24 C22 9(5) . . ? C23 C24 C22 26(4) 6_557 6_557 ? C23 C24 C22 121(4) . 6_557 ? C25 C24 C22 8(5) 6_557 6_557 ? C25 C24 C22 102(3) . 6_557 ? C22 C24 C22 96(5) . 6_557 ? C23 C24 Zr2 84(2) 6_557 . ? C23 C24 Zr2 84(2) . . ? C25 C24 Zr2 77(3) 6_557 . ? C25 C24 Zr2 77(3) . . ? C22 C24 Zr2 69.6(14) . . ? C22 C24 Zr2 69.6(14) 6_557 . ? C23 C25 C22 159(10) . . ? C23 C25 C24 18(2) . . ? C22 C25 C24 150(10) . . ? C23 C25 C21 124(6) . . ? C22 C25 C21 51(10) . . ? C24 C25 C21 107(4) . . ? C23 C25 C23 35(3) . 6_557 ? C22 C25 C23 136(10) . 6_557 ? C24 C25 C23 17(2) . 6_557 ? C21 C25 C23 90(3) . 6_557 ? C23 C25 C20 105(5) . . ? C22 C25 C20 70(10) . . ? C24 C25 C20 87(4) . . ? C21 C25 C20 20.1(14) . . ? C23 C25 C20 70(2) 6_557 . ? C23 C25 Zr2 78(4) . . ? C22 C25 Zr2 81(10) . . ? C24 C25 Zr2 71(2) . . ? C21 C25 Zr2 72(2) . . ? C23 C25 Zr2 66.9(16) 6_557 . ? C20 C25 Zr2 67(2) . . ? C28 C27 C26 118(2) . . ? C28 C27 C28 56(2) . 3_566 ? C26 C27 C28 73.0(17) . 3_566 ? C27 C28 C28 84(3) . 3_566 ? C27 C28 C27 124(2) . 3_566 ? C28 C28 C27 40.0(12) 3_566 3_566 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zr1 C1 2.331(6) 6_557 ? Zr1 C1 2.331(6) . ? Zr1 C2 2.480(6) . ? Zr1 C2 2.480(6) 6_557 ? Zr1 C9 2.5069(6) . ? Zr1 C9 2.5070(6) 6_557 ? Zr1 C11 2.5307(6) . ? Zr1 C8 2.540(7) 6_557 ? Zr1 C8 2.540(7) . ? Zr1 C10 2.5456(5) . ? Zr1 C10 2.5457(5) 6_557 ? Zr1 C7 2.550(6) . ? Zr2 C12 2.320(7) 6_557 ? Zr2 C12 2.320(7) . ? Zr2 C13 2.498(7) . ? Zr2 C13 2.498(7) 6_557 ? Zr2 C20 2.52(3) . ? Zr2 C19 2.522(7) . ? Zr2 C19 2.522(7) 6_557 ? Zr2 C18 2.518(8) . ? Zr2 C18 2.518(8) 6_557 ? Zr2 C17 2.541(10) . ? Zr2 C24 2.52(2) . ? Zr2 C21 2.53(2) . ? Si1 C3 1.844(11) . ? Si1 C5 1.852(7) . ? Si1 C1 1.862(6) . ? Si1 C4 1.865(11) . ? Si18 C16 1.778(15) . ? Si18 C12 1.827(10) . ? Si18 C15 1.820(11) . ? Si18 C14 1.883(16) . ? C1 C2 1.391(8) . ? C1 H1 1.0000 . ? C2 C2 1.393(12) 6_557 ? C2 H2 1.0000 . ? C3 H3A 0.9800 . ? C3 H3B 0.9800 . ? C3 H3C 0.9800 . ? C4 H4A 0.9800 . ? C4 H4B 0.9800 . ? C4 H4C 0.9800 . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C6 C7 1.403(12) 6_557 ? C6 C7 1.403(12) . ? C6 H6 0.9500 . ? C7 C8 1.339(13) . ? C7 H7 0.9500 . ? C8 C8 1.27(2) 6_557 ? C8 H8 0.9500 . ? C9 C9 1.3217 6_557 ? C9 C10 1.4052 . ? C9 H9 0.9500 . ? C10 C11 1.3682 . ? C10 H10 0.9500 . ? C11 C10 1.3682 6_557 ? C11 H11 0.9500 . ? C12 C13 1.423(13) . ? C12 H12 1.0000 . ? C13 C13 1.39(2) 6_557 ? C13 H13 1.0000 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 C18 1.334(14) . ? C17 C18 1.334(14) 6_557 ? C17 H17 0.9500 . ? C18 C19 1.358(15) . ? C18 H18 0.9500 . ? C19 C19 1.34(2) 6_557 ? C19 H19 0.9500 . ? C20 C21 0.72(2) . ? C20 C21 0.72(2) 6_557 ? C20 C22 1.70(7) . ? C20 C22 1.70(7) 6_557 ? C20 C25 1.81(10) 6_557 ? C20 C25 1.81(10) . ? C21 C22 1.08(8) . ? C21 C21 1.40(5) 6_557 ? C21 C25 1.34(12) . ? C21 C23 1.88(3) . ? C22 C25 0.56(14) . ? C22 C23 1.30(8) . ? C22 C24 1.90(7) . ? C23 C24 0.709(16) . ? C23 C25 0.76(8) . ? C23 C23 1.36(4) 6_557 ? C23 C25 1.91(5) 6_557 ? C24 C23 0.709(16) 6_557 ? C24 C25 1.40(6) 6_557 ? C24 C25 1.40(6) . ? C24 C22 1.90(7) 6_557 ? C25 C23 1.91(5) 6_557 ? C26 C27 1.68(3) . ? C27 C28 1.32(3) . ? C27 C28 2.04(3) 3_566 ? C28 C28 1.69(6) 3_566 ? C28 C27 2.04(3) 3_566 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C3 Si1 C1 C2 36.9(8) . . . . ? C5 Si1 C1 C2 156.3(5) . . . . ? C4 Si1 C1 C2 -82.8(8) . . . . ? C3 Si1 C1 Zr1 -70.6(8) . . . . ? C5 Si1 C1 Zr1 48.8(6) . . . . ? C4 Si1 C1 Zr1 169.7(7) . . . . ? C1 Zr1 C1 C2 46.1(4) 6_557 . . . ? C2 Zr1 C1 C2 19.6(3) 6_557 . . . ? C9 Zr1 C1 C2 -77.6(4) . . . . ? C9 Zr1 C1 C2 -98.5(4) 6_557 . . . ? C11 Zr1 C1 C2 -49.5(4) . . . . ? C8 Zr1 C1 C2 158.0(5) 6_557 . . . ? C8 Zr1 C1 C2 179.4(4) . . . . ? C10 Zr1 C1 C2 -37.9(4) . . . . ? C10 Zr1 C1 C2 -79.8(4) 6_557 . . . ? C7 Zr1 C1 C2 164.7(5) . . . . ? C1 Zr1 C1 Si1 169.0(3) 6_557 . . . ? C2 Zr1 C1 Si1 122.9(7) . . . . ? C2 Zr1 C1 Si1 142.5(5) 6_557 . . . ? C9 Zr1 C1 Si1 45.3(6) . . . . ? C9 Zr1 C1 Si1 24.4(5) 6_557 . . . ? C11 Zr1 C1 Si1 73.5(5) . . . . ? C8 Zr1 C1 Si1 -79.1(6) 6_557 . . . ? C8 Zr1 C1 Si1 -57.7(5) . . . . ? C10 Zr1 C1 Si1 85.0(5) . . . . ? C10 Zr1 C1 Si1 43.2(4) 6_557 . . . ? C7 Zr1 C1 Si1 -72.4(5) . . . . ? Si1 C1 C2 C2 178.52(19) . . . 6_557 ? Zr1 C1 C2 C2 -43.2(3) . . . 6_557 ? Si1 C1 C2 Zr1 -138.3(5) . . . . ? C1 Zr1 C2 C2 20.0(2) 6_557 . . 6_557 ? C1 Zr1 C2 C2 146.4(3) . . . 6_557 ? C9 Zr1 C2 C2 -82.49(10) . . . 6_557 ? C9 Zr1 C2 C2 -116.11(9) 6_557 . . 6_557 ? C11 Zr1 C2 C2 -85.32(6) . . . 6_557 ? C8 Zr1 C2 C2 92.3(8) 6_557 . . 6_557 ? C8 Zr1 C2 C2 145.4(4) . . . 6_557 ? C10 Zr1 C2 C2 -63.96(4) . . . 6_557 ? C10 Zr1 C2 C2 -116.11(4) 6_557 . . 6_557 ? C7 Zr1 C2 C2 129.6(3) . . . 6_557 ? C1 Zr1 C2 C1 -126.3(5) 6_557 . . . ? C2 Zr1 C2 C1 -146.4(3) 6_557 . . . ? C9 Zr1 C2 C1 131.1(3) . . . . ? C9 Zr1 C2 C1 97.5(4) 6_557 . . . ? C11 Zr1 C2 C1 128.3(4) . . . . ? C8 Zr1 C2 C1 -54.1(10) 6_557 . . . ? C8 Zr1 C2 C1 -1.0(6) . . . . ? C10 Zr1 C2 C1 149.7(4) . . . . ? C10 Zr1 C2 C1 97.5(4) 6_557 . . . ? C7 Zr1 C2 C1 -16.8(5) . . . . ? C1 Zr1 C6 C7 -81.9(5) 6_557 . . 6_557 ? C1 Zr1 C6 C7 -166.9(5) . . . 6_557 ? C2 Zr1 C6 C7 -141.7(5) . . . 6_557 ? C2 Zr1 C6 C7 -107.1(5) 6_557 . . 6_557 ? C9 Zr1 C6 C7 36.5(5) . . . 6_557 ? C9 Zr1 C6 C7 74.7(5) 6_557 . . 6_557 ? C11 Zr1 C6 C7 55.6(5) . . . 6_557 ? C8 Zr1 C6 C7 36.8(5) 6_557 . . 6_557 ? C8 Zr1 C6 C7 74.4(6) . . . 6_557 ? C10 Zr1 C6 C7 -0.8(7) . . . 6_557 ? C10 Zr1 C6 C7 112.0(4) 6_557 . . 6_557 ? C7 Zr1 C6 C7 111.2(10) . . . 6_557 ? C1 Zr1 C6 C7 166.9(5) 6_557 . . . ? C1 Zr1 C6 C7 81.9(5) . . . . ? C2 Zr1 C6 C7 107.1(5) . . . . ? C2 Zr1 C6 C7 141.7(5) 6_557 . . . ? C9 Zr1 C6 C7 -74.7(5) . . . . ? C9 Zr1 C6 C7 -36.5(5) 6_557 . . . ? C11 Zr1 C6 C7 -55.6(5) . . . . ? C8 Zr1 C6 C7 -74.4(6) 6_557 . . . ? C8 Zr1 C6 C7 -36.8(5) . . . . ? C10 Zr1 C6 C7 -112.0(4) . . . . ? C10 Zr1 C6 C7 0.8(7) 6_557 . . . ? C7 C6 C7 C8 -0.3(10) 6_557 . . . ? Zr1 C6 C7 C8 67.8(5) . . . . ? C7 C6 C7 Zr1 -68.0(6) 6_557 . . . ? C1 Zr1 C7 C8 -127.8(6) 6_557 . . . ? C1 Zr1 C7 C8 152.0(6) . . . . ? C2 Zr1 C7 C8 161.2(6) . . . . ? C2 Zr1 C7 C8 -164.9(5) 6_557 . . . ? C9 Zr1 C7 C8 9.4(7) . . . . ? C9 Zr1 C7 C8 37.9(6) 6_557 . . . ? C11 Zr1 C7 C8 62.0(7) . . . . ? C8 Zr1 C7 C8 -34.5(7) 6_557 . . . ? C10 Zr1 C7 C8 5.1(9) . . . . ? C10 Zr1 C7 C8 67.5(6) 6_557 . . . ? C1 Zr1 C7 C6 -14.8(6) 6_557 . . . ? C1 Zr1 C7 C6 -95.1(5) . . . . ? C2 Zr1 C7 C6 -85.8(5) . . . . ? C2 Zr1 C7 C6 -52.0(6) 6_557 . . . ? C9 Zr1 C7 C6 122.4(5) . . . . ? C9 Zr1 C7 C6 150.9(5) 6_557 . . . ? C11 Zr1 C7 C6 175.0(3) . . . . ? C8 Zr1 C7 C6 78.5(6) 6_557 . . . ? C8 Zr1 C7 C6 113.0(8) . . . . ? C10 Zr1 C7 C6 118.1(5) . . . . ? C10 Zr1 C7 C6 -179.5(4) 6_557 . . . ? C6 C7 C8 C8 0.2(6) . . . 6_557 ? Zr1 C7 C8 C8 67.8(2) . . . 6_557 ? C6 C7 C8 Zr1 -67.6(5) . . . . ? C1 Zr1 C8 C8 -45.0(3) 6_557 . . 6_557 ? C1 Zr1 C8 C8 -146.3(2) . . . 6_557 ? C2 Zr1 C8 C8 -145.7(4) . . . 6_557 ? C2 Zr1 C8 C8 -82.1(8) 6_557 . . 6_557 ? C9 Zr1 C8 C8 72.10(6) . . . 6_557 ? C9 Zr1 C8 C8 102.28(7) 6_557 . . 6_557 ? C11 Zr1 C8 C8 100.7(2) . . . 6_557 ? C10 Zr1 C8 C8 66.58(11) . . . 6_557 ? C10 Zr1 C8 C8 121.84(10) 6_557 . . 6_557 ? C7 Zr1 C8 C8 -116.6(6) . . . 6_557 ? C1 Zr1 C8 C7 71.6(8) 6_557 . . . ? C1 Zr1 C8 C7 -29.7(7) . . . . ? C2 Zr1 C8 C7 -29.1(8) . . . . ? C2 Zr1 C8 C7 34.5(12) 6_557 . . . ? C9 Zr1 C8 C7 -171.3(6) . . . . ? C9 Zr1 C8 C7 -141.1(7) 6_557 . . . ? C11 Zr1 C8 C7 -142.7(5) . . . . ? C8 Zr1 C8 C7 116.6(6) 6_557 . . . ? C10 Zr1 C8 C7 -176.8(5) . . . . ? C10 Zr1 C8 C7 -121.5(6) 6_557 . . . ? C1 Zr1 C9 C9 -153.66(16) 6_557 . . 6_557 ? C1 Zr1 C9 C9 -39.6(2) . . . 6_557 ? C2 Zr1 C9 C9 -80.53(17) . . . 6_557 ? C2 Zr1 C9 C9 -116.70(15) 6_557 . . 6_557 ? C11 Zr1 C9 C9 -76.988(3) . . . 6_557 ? C8 Zr1 C9 C9 101.3(3) 6_557 . . 6_557 ? C8 Zr1 C9 C9 72.7(2) . . . 6_557 ? C10 Zr1 C9 C9 -116.685(6) . . . 6_557 ? C10 Zr1 C9 C9 -36.860(2) 6_557 . . 6_557 ? C7 Zr1 C9 C9 67.9(2) . . . 6_557 ? C1 Zr1 C9 C10 -36.98(16) 6_557 . . . ? C1 Zr1 C9 C10 77.1(2) . . . . ? C2 Zr1 C9 C10 36.15(17) . . . . ? C2 Zr1 C9 C10 -0.01(15) 6_557 . . . ? C9 Zr1 C9 C10 116.685(6) 6_557 . . . ? C11 Zr1 C9 C10 39.696(3) . . . . ? C8 Zr1 C9 C10 -142.0(3) 6_557 . . . ? C8 Zr1 C9 C10 -170.6(2) . . . . ? C10 Zr1 C9 C10 79.825(7) 6_557 . . . ? C7 Zr1 C9 C10 -175.4(2) . . . . ? C9 C9 C10 C11 -1.5 6_557 . . . ? Zr1 C9 C10 C11 -68.587(7) . . . . ? C9 C9 C10 Zr1 67.081(7) 6_557 . . . ? C1 Zr1 C10 C11 -104.89(14) 6_557 . . . ? C1 Zr1 C10 C11 -22.59(18) . . . . ? C2 Zr1 C10 C11 -42.54(14) . . . . ? C2 Zr1 C10 C11 -71.77(14) 6_557 . . . ? C9 Zr1 C10 C11 108.241(4) . . . . ? C9 Zr1 C10 C11 73.407(4) 6_557 . . . ? C8 Zr1 C10 C11 145.5(3) 6_557 . . . ? C8 Zr1 C10 C11 118.5(2) . . . . ? C10 Zr1 C10 C11 32.900(4) 6_557 . . . ? C7 Zr1 C10 C11 115.7(4) . . . . ? C1 Zr1 C10 C9 146.87(14) 6_557 . . . ? C1 Zr1 C10 C9 -130.83(18) . . . . ? C2 Zr1 C10 C9 -150.78(14) . . . . ? C2 Zr1 C10 C9 179.99(14) 6_557 . . . ? C9 Zr1 C10 C9 -34.834(4) 6_557 . . . ? C11 Zr1 C10 C9 -108.241(4) . . . . ? C8 Zr1 C10 C9 37.3(3) 6_557 . . . ? C8 Zr1 C10 C9 10.3(2) . . . . ? C10 Zr1 C10 C9 -75.341(6) 6_557 . . . ? C7 Zr1 C10 C9 7.5(4) . . . . ? C9 C10 C11 C10 2.6 . . . 6_557 ? Zr1 C10 C11 C10 -64.872(12) . . . 6_557 ? C9 C10 C11 Zr1 67.513(12) . . . . ? C1 Zr1 C11 C10 76.23(14) 6_557 . . . ? C1 Zr1 C11 C10 161.65(14) . . . . ? C2 Zr1 C11 C10 135.89(14) . . . . ? C2 Zr1 C11 C10 101.99(14) 6_557 . . . ? C9 Zr1 C11 C10 -41.089(1) . . . . ? C9 Zr1 C11 C10 -81.030(6) 6_557 . . . ? C8 Zr1 C11 C10 -43.1(3) 6_557 . . . ? C8 Zr1 C11 C10 -79.0(3) . . . . ? C10 Zr1 C11 C10 -122.120(6) 6_557 . . . ? C7 Zr1 C11 C10 -112.4(4) . . . . ? C1 Zr1 C11 C10 -161.65(14) 6_557 . . 6_557 ? C1 Zr1 C11 C10 -76.23(14) . . . 6_557 ? C2 Zr1 C11 C10 -101.99(14) . . . 6_557 ? C2 Zr1 C11 C10 -135.89(14) 6_557 . . 6_557 ? C9 Zr1 C11 C10 81.031(6) . . . 6_557 ? C9 Zr1 C11 C10 41.1 6_557 . . 6_557 ? C8 Zr1 C11 C10 79.0(3) 6_557 . . 6_557 ? C8 Zr1 C11 C10 43.1(3) . . . 6_557 ? C10 Zr1 C11 C10 122.120(7) . . . 6_557 ? C7 Zr1 C11 C10 9.7(4) . . . 6_557 ? C16 Si18 C12 C13 -142.9(10) . . . . ? C15 Si18 C12 C13 95.2(8) . . . . ? C14 Si18 C12 C13 -27.1(14) . . . . ? C16 Si18 C12 Zr2 -38.4(12) . . . . ? C15 Si18 C12 Zr2 -160.3(7) . . . . ? C14 Si18 C12 Zr2 77.5(14) . . . . ? C12 Zr2 C12 C13 -49.0(6) 6_557 . . . ? C13 Zr2 C12 C13 -20.6(5) 6_557 . . . ? C20 Zr2 C12 C13 91.3(9) . . . . ? C19 Zr2 C12 C13 -157.4(6) . . . . ? C19 Zr2 C12 C13 179.4(5) 6_557 . . . ? C18 Zr2 C12 C13 -125.5(6) . . . . ? C18 Zr2 C12 C13 -165.4(6) 6_557 . . . ? C17 Zr2 C12 C13 -135.0(6) . . . . ? C24 Zr2 C12 C13 46.8(7) . . . . ? C21 Zr2 C12 C13 74.8(10) . . . . ? C12 Zr2 C12 Si18 -168.0(5) 6_557 . . . ? C13 Zr2 C12 Si18 -119.0(10) . . . . ? C13 Zr2 C12 Si18 -139.6(8) 6_557 . . . ? C20 Zr2 C12 Si18 -27.7(11) . . . . ? C19 Zr2 C12 Si18 83.6(8) . . . . ? C19 Zr2 C12 Si18 60.4(8) 6_557 . . . ? C18 Zr2 C12 Si18 115.5(7) . . . . ? C18 Zr2 C12 Si18 75.6(8) 6_557 . . . ? C17 Zr2 C12 Si18 106.0(7) . . . . ? C24 Zr2 C12 Si18 -72.2(9) . . . . ? C21 Zr2 C12 Si18 -44.2(13) . . . . ? Si18 C12 C13 C13 -178.2(2) . . . 6_557 ? Zr2 C12 C13 C13 44.6(4) . . . 6_557 ? Si18 C12 C13 Zr2 137.2(6) . . . . ? C12 Zr2 C13 C13 -21.6(3) 6_557 . . 6_557 ? C12 Zr2 C13 C13 -144.2(5) . . . 6_557 ? C20 Zr2 C13 C13 101.0(3) . . . 6_557 ? C19 Zr2 C13 C13 -89.1(10) . . . 6_557 ? C19 Zr2 C13 C13 -145.2(5) 6_557 . . 6_557 ? C18 Zr2 C13 C13 -69.5(4) . . . 6_557 ? C18 Zr2 C13 C13 -128.5(4) 6_557 . . 6_557 ? C17 Zr2 C13 C13 -95.84(14) . . . 6_557 ? C24 Zr2 C13 C13 85.0(2) . . . 6_557 ? C21 Zr2 C13 C13 81.3(6) . . . 6_557 ? C12 Zr2 C13 C12 122.5(7) 6_557 . . . ? C13 Zr2 C13 C12 144.2(5) 6_557 . . . ? C20 Zr2 C13 C12 -114.8(5) . . . . ? C19 Zr2 C13 C12 55.1(13) . . . . ? C19 Zr2 C13 C12 -1.0(8) 6_557 . . . ? C18 Zr2 C13 C12 74.7(7) . . . . ? C18 Zr2 C13 C12 15.7(7) 6_557 . . . ? C17 Zr2 C13 C12 48.3(6) . . . . ? C24 Zr2 C13 C12 -130.8(6) . . . . ? C21 Zr2 C13 C12 -134.5(7) . . . . ? C12 Zr2 C17 C18 78.8(8) 6_557 . . . ? C12 Zr2 C17 C18 162.8(8) . . . . ? C13 Zr2 C17 C18 137.9(8) . . . . ? C13 Zr2 C17 C18 103.6(8) 6_557 . . . ? C20 Zr2 C17 C18 -59.2(8) . . . . ? C19 Zr2 C17 C18 -39.0(7) . . . . ? C19 Zr2 C17 C18 -79.5(9) 6_557 . . . ? C18 Zr2 C17 C18 -118.4(15) 6_557 . . . ? C24 Zr2 C17 C18 -59.2(8) . . . . ? C21 Zr2 C17 C18 -39.1(10) . . . . ? C12 Zr2 C17 C18 -162.8(8) 6_557 . . 6_557 ? C12 Zr2 C17 C18 -78.8(8) . . . 6_557 ? C13 Zr2 C17 C18 -103.6(8) . . . 6_557 ? C13 Zr2 C17 C18 -137.9(8) 6_557 . . 6_557 ? C20 Zr2 C17 C18 59.2(8) . . . 6_557 ? C19 Zr2 C17 C18 79.5(9) . . . 6_557 ? C19 Zr2 C17 C18 39.0(7) 6_557 . . 6_557 ? C18 Zr2 C17 C18 118.4(15) . . . 6_557 ? C24 Zr2 C17 C18 59.2(8) . . . 6_557 ? C21 Zr2 C17 C18 79.3(9) . . . 6_557 ? C18 C17 C18 C19 4.2(15) 6_557 . . . ? Zr2 C17 C18 C19 69.0(6) . . . . ? C18 C17 C18 Zr2 -64.8(9) 6_557 . . . ? C12 Zr2 C18 C17 -97.4(8) 6_557 . . . ? C12 Zr2 C18 C17 -18.9(9) . . . . ? C13 Zr2 C18 C17 -55.5(9) . . . . ? C13 Zr2 C18 C17 -88.6(8) 6_557 . . . ? C20 Zr2 C18 C17 132.8(8) . . . . ? C19 Zr2 C18 C17 111.3(10) . . . . ? C19 Zr2 C18 C17 74.9(8) 6_557 . . . ? C18 Zr2 C18 C17 34.7(9) 6_557 . . . ? C24 Zr2 C18 C17 175.6(13) . . . . ? C21 Zr2 C18 C17 148.7(9) . . . . ? C12 Zr2 C18 C19 151.2(7) 6_557 . . . ? C12 Zr2 C18 C19 -130.3(7) . . . . ? C13 Zr2 C18 C19 -166.8(6) . . . . ? C13 Zr2 C18 C19 160.1(6) 6_557 . . . ? C20 Zr2 C18 C19 21.5(8) . . . . ? C19 Zr2 C18 C19 -36.5(7) 6_557 . . . ? C18 Zr2 C18 C19 -76.7(7) 6_557 . . . ? C17 Zr2 C18 C19 -111.3(10) . . . . ? C24 Zr2 C18 C19 64.3(14) . . . . ? C21 Zr2 C18 C19 37.3(8) . . . . ? C17 C18 C19 C19 -2.5(9) . . . 6_557 ? Zr2 C18 C19 C19 67.3(2) . . . 6_557 ? C17 C18 C19 Zr2 -69.8(7) . . . . ? C12 Zr2 C19 C19 -144.7(3) 6_557 . . 6_557 ? C12 Zr2 C19 C19 -47.2(4) . . . 6_557 ? C13 Zr2 C19 C19 -85.0(10) . . . 6_557 ? C13 Zr2 C19 C19 -145.3(5) 6_557 . . 6_557 ? C20 Zr2 C19 C19 86.36(18) . . . 6_557 ? C18 Zr2 C19 C19 -114.8(7) . . . 6_557 ? C18 Zr2 C19 C19 -37.0(4) 6_557 . . 6_557 ? C17 Zr2 C19 C19 -76.7(3) . . . 6_557 ? C24 Zr2 C19 C19 102.1(4) . . . 6_557 ? C21 Zr2 C19 C19 103.1(5) . . . 6_557 ? C12 Zr2 C19 C18 -29.9(7) 6_557 . . . ? C12 Zr2 C19 C18 67.6(9) . . . . ? C13 Zr2 C19 C18 29.8(14) . . . . ? C13 Zr2 C19 C18 -30.5(9) 6_557 . . . ? C20 Zr2 C19 C18 -158.8(7) . . . . ? C19 Zr2 C19 C18 114.8(7) 6_557 . . . ? C18 Zr2 C19 C18 77.8(10) 6_557 . . . ? C17 Zr2 C19 C18 38.1(6) . . . . ? C24 Zr2 C19 C18 -143.1(7) . . . . ? C21 Zr2 C19 C18 -142.1(9) . . . . ? C12 Zr2 C20 C21 -19(4) 6_557 . . . ? C12 Zr2 C20 C21 -142(3) . . . . ? C13 Zr2 C20 C21 -100(3) . . . . ? C13 Zr2 C20 C21 -61(3) 6_557 . . . ? C19 Zr2 C20 C21 83(3) . . . . ? C19 Zr2 C20 C21 115(3) 6_557 . . . ? C18 Zr2 C20 C21 72(3) . . . . ? C18 Zr2 C20 C21 126(3) 6_557 . . . ? C17 Zr2 C20 C21 99(3) . . . . ? C24 Zr2 C20 C21 -81(3) . . . . ? C12 Zr2 C20 C21 142(3) 6_557 . . 6_557 ? C12 Zr2 C20 C21 19(4) . . . 6_557 ? C13 Zr2 C20 C21 61(3) . . . 6_557 ? C13 Zr2 C20 C21 100(3) 6_557 . . 6_557 ? C19 Zr2 C20 C21 -115(3) . . . 6_557 ? C19 Zr2 C20 C21 -83(3) 6_557 . . 6_557 ? C18 Zr2 C20 C21 -126(3) . . . 6_557 ? C18 Zr2 C20 C21 -72(3) 6_557 . . 6_557 ? C17 Zr2 C20 C21 -99(3) . . . 6_557 ? C24 Zr2 C20 C21 81(3) . . . 6_557 ? C21 Zr2 C20 C21 162(7) . . . 6_557 ? C12 Zr2 C20 C22 1(3) 6_557 . . . ? C12 Zr2 C20 C22 -122(2) . . . . ? C13 Zr2 C20 C22 -80(2) . . . . ? C13 Zr2 C20 C22 -41(2) 6_557 . . . ? C19 Zr2 C20 C22 104(2) . . . . ? C19 Zr2 C20 C22 136(2) 6_557 . . . ? C18 Zr2 C20 C22 93(2) . . . . ? C18 Zr2 C20 C22 147(2) 6_557 . . . ? C17 Zr2 C20 C22 120(2) . . . . ? C24 Zr2 C20 C22 -60(2) . . . . ? C21 Zr2 C20 C22 21(4) . . . . ? C12 Zr2 C20 C22 122(2) 6_557 . . 6_557 ? C12 Zr2 C20 C22 -1(3) . . . 6_557 ? C13 Zr2 C20 C22 41(2) . . . 6_557 ? C13 Zr2 C20 C22 80(2) 6_557 . . 6_557 ? C19 Zr2 C20 C22 -136(2) . . . 6_557 ? C19 Zr2 C20 C22 -104(2) 6_557 . . 6_557 ? C18 Zr2 C20 C22 -147(2) . . . 6_557 ? C18 Zr2 C20 C22 -93(2) 6_557 . . 6_557 ? C17 Zr2 C20 C22 -120(2) . . . 6_557 ? C24 Zr2 C20 C22 60(2) . . . 6_557 ? C21 Zr2 C20 C22 141(5) . . . 6_557 ? C12 Zr2 C20 C25 102.9(19) 6_557 . . 6_557 ? C12 Zr2 C20 C25 -20(2) . . . 6_557 ? C13 Zr2 C20 C25 22(2) . . . 6_557 ? C13 Zr2 C20 C25 60.8(19) 6_557 . . 6_557 ? C19 Zr2 C20 C25 -155(2) . . . 6_557 ? C19 Zr2 C20 C25 -122.8(19) 6_557 . . 6_557 ? C18 Zr2 C20 C25 -165.8(19) . . . 6_557 ? C18 Zr2 C20 C25 -112(2) 6_557 . . 6_557 ? C17 Zr2 C20 C25 -138.7(19) . . . 6_557 ? C24 Zr2 C20 C25 41.3(19) . . . 6_557 ? C21 Zr2 C20 C25 122(4) . . . 6_557 ? C12 Zr2 C20 C25 20(2) 6_557 . . . ? C12 Zr2 C20 C25 -102.9(19) . . . . ? C13 Zr2 C20 C25 -60.8(19) . . . . ? C13 Zr2 C20 C25 -22(2) 6_557 . . . ? C19 Zr2 C20 C25 122.8(19) . . . . ? C19 Zr2 C20 C25 155(2) 6_557 . . . ? C18 Zr2 C20 C25 112(2) . . . . ? C18 Zr2 C20 C25 165.8(19) 6_557 . . . ? C17 Zr2 C20 C25 138.7(19) . . . . ? C24 Zr2 C20 C25 -41.3(19) . . . . ? C21 Zr2 C20 C25 39(4) . . . . ? C21 C20 C21 C22 10(21) 6_557 . . . ? C22 C20 C21 C22 5(10) 6_557 . . . ? C25 C20 C21 C22 -4(10) 6_557 . . . ? C25 C20 C21 C22 -9(7) . . . . ? Zr2 C20 C21 C22 61(7) . . . . ? C22 C20 C21 C21 -10(21) . . . 6_557 ? C22 C20 C21 C21 -6(11) 6_557 . . 6_557 ? C25 C20 C21 C21 -14(13) 6_557 . . 6_557 ? C25 C20 C21 C21 -20(18) . . . 6_557 ? Zr2 C20 C21 C21 51(15) . . . 6_557 ? C21 C20 C21 C25 20(18) 6_557 . . . ? C22 C20 C21 C25 9(7) . . . . ? C22 C20 C21 C25 14(8) 6_557 . . . ? C25 C20 C21 C25 6(5) 6_557 . . . ? Zr2 C20 C21 C25 70(4) . . . . ? C21 C20 C21 C23 16(16) 6_557 . . . ? C22 C20 C21 C23 5(6) . . . . ? C22 C20 C21 C23 10(5) 6_557 . . . ? C25 C20 C21 C23 2(4) 6_557 . . . ? C25 C20 C21 C23 -4(3) . . . . ? Zr2 C20 C21 C23 66.5(13) . . . . ? C21 C20 C21 Zr2 -51(15) 6_557 . . . ? C22 C20 C21 Zr2 -61(7) . . . . ? C22 C20 C21 Zr2 -56(4) 6_557 . . . ? C25 C20 C21 Zr2 -65(3) 6_557 . . . ? C25 C20 C21 Zr2 -70(4) . . . . ? C12 Zr2 C21 C20 164(3) 6_557 . . . ? C12 Zr2 C21 C20 50(4) . . . . ? C13 Zr2 C21 C20 91(3) . . . . ? C13 Zr2 C21 C20 126(3) 6_557 . . . ? C19 Zr2 C21 C20 -93(3) . . . . ? C19 Zr2 C21 C20 -63(3) 6_557 . . . ? C18 Zr2 C21 C20 -112(3) . . . . ? C18 Zr2 C21 C20 -59(3) 6_557 . . . ? C17 Zr2 C21 C20 -93(3) . . . . ? C24 Zr2 C21 C20 86(3) . . . . ? C12 Zr2 C21 C22 17(3) 6_557 . . . ? C12 Zr2 C21 C22 -98(3) . . . . ? C13 Zr2 C21 C22 -57(3) . . . . ? C13 Zr2 C21 C22 -21(3) 6_557 . . . ? C20 Zr2 C21 C22 -147(5) . . . . ? C19 Zr2 C21 C22 120(3) . . . . ? C19 Zr2 C21 C22 150(3) 6_557 . . . ? C18 Zr2 C21 C22 101(3) . . . . ? C18 Zr2 C21 C22 154(3) 6_557 . . . ? C17 Zr2 C21 C22 120(3) . . . . ? C24 Zr2 C21 C22 -61(3) . . . . ? C12 Zr2 C21 C21 154.4(5) 6_557 . . 6_557 ? C12 Zr2 C21 C21 40.1(7) . . . 6_557 ? C13 Zr2 C21 C21 81.2(5) . . . 6_557 ? C13 Zr2 C21 C21 116.7(4) 6_557 . . 6_557 ? C20 Zr2 C21 C21 -10(3) . . . 6_557 ? C19 Zr2 C21 C21 -102.2(3) . . . 6_557 ? C19 Zr2 C21 C21 -72.1(3) 6_557 . . 6_557 ? C18 Zr2 C21 C21 -121.2(3) . . . 6_557 ? C18 Zr2 C21 C21 -68.5(3) 6_557 . . 6_557 ? C17 Zr2 C21 C21 -102.1(4) . . . 6_557 ? C24 Zr2 C21 C21 76.7(5) . . . 6_557 ? C12 Zr2 C21 C25 40(2) 6_557 . . . ? C12 Zr2 C21 C25 -74(2) . . . . ? C13 Zr2 C21 C25 -33(2) . . . . ? C13 Zr2 C21 C25 3(2) 6_557 . . . ? C20 Zr2 C21 C25 -124(4) . . . . ? C19 Zr2 C21 C25 143.8(19) . . . . ? C19 Zr2 C21 C25 173.9(19) 6_557 . . . ? C18 Zr2 C21 C25 124.9(19) . . . . ? C18 Zr2 C21 C25 177.6(18) 6_557 . . . ? C17 Zr2 C21 C25 144.0(18) . . . . ? C24 Zr2 C21 C25 -37.2(19) . . . . ? C12 Zr2 C21 C23 58.8(9) 6_557 . . . ? C12 Zr2 C21 C23 -55.5(12) . . . . ? C13 Zr2 C21 C23 -14.4(10) . . . . ? C13 Zr2 C21 C23 21.1(9) 6_557 . . . ? C20 Zr2 C21 C23 -105(3) . . . . ? C19 Zr2 C21 C23 162.1(9) . . . . ? C19 Zr2 C21 C23 -167.7(8) 6_557 . . . ? C18 Zr2 C21 C23 143.2(8) . . . . ? C18 Zr2 C21 C23 -164.1(7) 6_557 . . . ? C17 Zr2 C21 C23 162.3(7) . . . . ? C24 Zr2 C21 C23 -18.9(8) . . . . ? C20 C21 C22 C25 20(17) . . . . ? C21 C21 C22 C25 23(14) 6_557 . . . ? C23 C21 C22 C25 12(10) . . . . ? Zr2 C21 C22 C25 82(13) . . . . ? C20 C21 C22 C23 8(9) . . . . ? C21 C21 C22 C23 11(5) 6_557 . . . ? C25 C21 C22 C23 -12(10) . . . . ? Zr2 C21 C22 C23 69(3) . . . . ? C21 C21 C22 C20 3(6) 6_557 . . . ? C25 C21 C22 C20 -20(17) . . . . ? C23 C21 C22 C20 -8(9) . . . . ? Zr2 C21 C22 C20 61(7) . . . . ? C20 C21 C22 C24 4(8) . . . . ? C21 C21 C22 C24 7(3) 6_557 . . . ? C25 C21 C22 C24 -16(12) . . . . ? C23 C21 C22 C24 -3.7(19) . . . . ? Zr2 C21 C22 C24 65.7(16) . . . . ? C20 C21 C22 Zr2 -61(7) . . . . ? C21 C21 C22 Zr2 -59(2) 6_557 . . . ? C25 C21 C22 Zr2 -82(13) . . . . ? C23 C21 C22 Zr2 -69(3) . . . . ? C21 C20 C22 C25 -160(17) . . . . ? C21 C20 C22 C25 25(14) 6_557 . . . ? C22 C20 C22 C25 23(14) 6_557 . . . ? C25 C20 C22 C25 16(11) 6_557 . . . ? Zr2 C20 C22 C25 85(13) . . . . ? C21 C20 C22 C21 -174(12) 6_557 . . . ? C22 C20 C22 C21 -176(8) 6_557 . . . ? C25 C20 C22 C21 177(9) 6_557 . . . ? C25 C20 C22 C21 160(17) . . . . ? Zr2 C20 C22 C21 -114(8) . . . . ? C21 C20 C22 C23 -172(9) . . . . ? C21 C20 C22 C23 14(6) 6_557 . . . ? C22 C20 C22 C23 12(4) 6_557 . . . ? C25 C20 C22 C23 4.5(17) 6_557 . . . ? C25 C20 C22 C23 -12(10) . . . . ? Zr2 C20 C22 C23 73(3) . . . . ? C21 C20 C22 C24 -176(8) . . . . ? C21 C20 C22 C24 10(5) 6_557 . . . ? C22 C20 C22 C24 8(3) 6_557 . . . ? C25 C20 C22 C24 1.2(17) 6_557 . . . ? C25 C20 C22 C24 -15(12) . . . . ? Zr2 C20 C22 C24 70.1(15) . . . . ? C21 C20 C22 Zr2 114(8) . . . . ? C21 C20 C22 Zr2 -60(5) 6_557 . . . ? C22 C20 C22 Zr2 -62(2) 6_557 . . . ? C25 C20 C22 Zr2 -69(2) 6_557 . . . ? C25 C20 C22 Zr2 -85(13) . . . . ? C12 Zr2 C22 C25 88(17) 6_557 . . . ? C12 Zr2 C22 C25 5(19) . . . . ? C13 Zr2 C22 C25 26(17) . . . . ? C13 Zr2 C22 C25 54(17) 6_557 . . . ? C20 Zr2 C22 C25 -93(16) . . . . ? C19 Zr2 C22 C25 -164(17) . . . . ? C19 Zr2 C22 C25 -138(17) 6_557 . . . ? C18 Zr2 C22 C25 168(16) . . . . ? C18 Zr2 C22 C25 -143(16) 6_557 . . . ? C17 Zr2 C22 C25 173(15) . . . . ? C24 Zr2 C22 C25 -10(15) . . . . ? C21 Zr2 C22 C25 -107(16) . . . . ? C12 Zr2 C22 C21 -165(3) 6_557 . . . ? C12 Zr2 C22 C21 113(4) . . . . ? C13 Zr2 C22 C21 133(3) . . . . ? C13 Zr2 C22 C21 161(3) 6_557 . . . ? C20 Zr2 C22 C21 14(2) . . . . ? C19 Zr2 C22 C21 -57(3) . . . . ? C19 Zr2 C22 C21 -31(3) 6_557 . . . ? C18 Zr2 C22 C21 -84(3) . . . . ? C18 Zr2 C22 C21 -36(4) 6_557 . . . ? C17 Zr2 C22 C21 -80(3) . . . . ? C24 Zr2 C22 C21 97(3) . . . . ? C12 Zr2 C22 C23 85(3) 6_557 . . . ? C12 Zr2 C22 C23 3(5) . . . . ? C13 Zr2 C22 C23 24(4) . . . . ? C13 Zr2 C22 C23 51(3) 6_557 . . . ? C20 Zr2 C22 C23 -96(3) . . . . ? C19 Zr2 C22 C23 -167(3) . . . . ? C19 Zr2 C22 C23 -141(3) 6_557 . . . ? C18 Zr2 C22 C23 166(3) . . . . ? C18 Zr2 C22 C23 -145(3) 6_557 . . . ? C17 Zr2 C22 C23 170.7(19) . . . . ? C24 Zr2 C22 C23 -12(2) . . . . ? C21 Zr2 C22 C23 -110(4) . . . . ? C12 Zr2 C22 C20 -178.9(19) 6_557 . . . ? C12 Zr2 C22 C20 99(3) . . . . ? C13 Zr2 C22 C20 119(2) . . . . ? C13 Zr2 C22 C20 147.0(19) 6_557 . . . ? C19 Zr2 C22 C20 -71(2) . . . . ? C19 Zr2 C22 C20 -45(2) 6_557 . . . ? C18 Zr2 C22 C20 -98.3(17) . . . . ? C18 Zr2 C22 C20 -49(2) 6_557 . . . ? C17 Zr2 C22 C20 -93.6(15) . . . . ? C24 Zr2 C22 C20 83.4(16) . . . . ? C21 Zr2 C22 C20 -14(2) . . . . ? C12 Zr2 C22 C24 97.7(19) 6_557 . . . ? C12 Zr2 C22 C24 15(4) . . . . ? C13 Zr2 C22 C24 36(2) . . . . ? C13 Zr2 C22 C24 63.6(19) 6_557 . . . ? C20 Zr2 C22 C24 -83.4(16) . . . . ? C19 Zr2 C22 C24 -154.5(19) . . . . ? C19 Zr2 C22 C24 -128.3(18) 6_557 . . . ? C18 Zr2 C22 C24 178.3(15) . . . . ? C18 Zr2 C22 C24 -132.8(16) 6_557 . . . ? C17 Zr2 C22 C24 -177.0(9) . . . . ? C21 Zr2 C22 C24 -97(3) . . . . ? C25 C22 C23 C24 -115(59) . . . . ? C21 C22 C23 C24 -16(9) . . . . ? C20 C22 C23 C24 -14(7) . . . . ? Zr2 C22 C23 C24 55(7) . . . . ? C21 C22 C23 C25 99(64) . . . . ? C20 C22 C23 C25 101(64) . . . . ? C24 C22 C23 C25 115(59) . . . . ? Zr2 C22 C23 C25 169(63) . . . . ? C25 C22 C23 C23 -109(62) . . . 6_557 ? C21 C22 C23 C23 -10(5) . . . 6_557 ? C20 C22 C23 C23 -8(3) . . . 6_557 ? C24 C22 C23 C23 6(5) . . . 6_557 ? Zr2 C22 C23 C23 60(2) . . . 6_557 ? C25 C22 C23 C25 -105(63) . . . 6_557 ? C21 C22 C23 C25 -6(3) . . . 6_557 ? C20 C22 C23 C25 -4.4(16) . . . 6_557 ? C24 C22 C23 C25 9(7) . . . 6_557 ? Zr2 C22 C23 C25 63.6(14) . . . 6_557 ? C25 C22 C23 C21 -99(64) . . . . ? C20 C22 C23 C21 2(2) . . . . ? C24 C22 C23 C21 16(9) . . . . ? Zr2 C22 C23 C21 70(3) . . . . ? C25 C22 C23 Zr2 -169(63) . . . . ? C21 C22 C23 Zr2 -70(3) . . . . ? C20 C22 C23 Zr2 -68.1(16) . . . . ? C24 C22 C23 Zr2 -55(7) . . . . ? C20 C21 C23 C24 -5(4) . . . . ? C22 C21 C23 C24 170(5) . . . . ? C21 C21 C23 C24 -2(3) 6_557 . . . ? C25 C21 C23 C24 -176(7) . . . . ? Zr2 C21 C23 C24 71(3) . . . . ? C20 C21 C23 C25 170(8) . . . . ? C22 C21 C23 C25 -15(11) . . . . ? C21 C21 C23 C25 173(7) 6_557 . . . ? Zr2 C21 C23 C25 -114(8) . . . . ? C20 C21 C23 C23 -3(3) . . . 6_557 ? C22 C21 C23 C23 172(4) . . . 6_557 ? C21 C21 C23 C23 0.001(11) 6_557 . . 6_557 ? C25 C21 C23 C23 -173(7) . . . 6_557 ? Zr2 C21 C23 C23 72.9(4) . . . 6_557 ? C20 C21 C23 C22 -175(6) . . . . ? C21 C21 C23 C22 -172(4) 6_557 . . . ? C25 C21 C23 C22 15(11) . . . . ? Zr2 C21 C23 C22 -99(4) . . . . ? C20 C21 C23 C25 -2(4) . . . 6_557 ? C22 C21 C23 C25 173(3) . . . 6_557 ? C21 C21 C23 C25 1.6(18) 6_557 . . 6_557 ? C25 C21 C23 C25 -172(9) . . . 6_557 ? Zr2 C21 C23 C25 74.6(19) . . . 6_557 ? C20 C21 C23 Zr2 -76(3) . . . . ? C22 C21 C23 Zr2 99(4) . . . . ? C21 C21 C23 Zr2 -72.9(4) 6_557 . . . ? C25 C21 C23 Zr2 114(7) . . . . ? C12 Zr2 C23 C24 117(4) 6_557 . . . ? C12 Zr2 C23 C24 34(4) . . . . ? C13 Zr2 C23 C24 55(4) . . . . ? C13 Zr2 C23 C24 86(4) 6_557 . . . ? C20 Zr2 C23 C24 -93(4) . . . . ? C19 Zr2 C23 C24 -133(4) . . . . ? C19 Zr2 C23 C24 -98(4) 6_557 . . . ? C18 Zr2 C23 C24 -166(3) . . . . ? C18 Zr2 C23 C24 -77(4) 6_557 . . . ? C17 Zr2 C23 C24 -171(3) . . . . ? C21 Zr2 C23 C24 -114(4) . . . . ? C12 Zr2 C23 C25 -96(6) 6_557 . . . ? C12 Zr2 C23 C25 -179(6) . . . . ? C13 Zr2 C23 C25 -159(6) . . . . ? C13 Zr2 C23 C25 -127(6) 6_557 . . . ? C20 Zr2 C23 C25 54(6) . . . . ? C19 Zr2 C23 C25 13(6) . . . . ? C19 Zr2 C23 C25 48(6) 6_557 . . . ? C18 Zr2 C23 C25 -20(6) . . . . ? C18 Zr2 C23 C25 69(7) 6_557 . . . ? C17 Zr2 C23 C25 -25(7) . . . . ? C24 Zr2 C23 C25 146(7) . . . . ? C21 Zr2 C23 C25 33(6) . . . . ? C12 Zr2 C23 C23 133.5(3) 6_557 . . 6_557 ? C12 Zr2 C23 C23 50.5(3) . . . 6_557 ? C13 Zr2 C23 C23 70.8(3) . . . 6_557 ? C13 Zr2 C23 C23 102.7(3) 6_557 . . 6_557 ? C20 Zr2 C23 C23 -76.5(4) . . . 6_557 ? C19 Zr2 C23 C23 -116.8(5) . . . 6_557 ? C19 Zr2 C23 C23 -82.1(5) 6_557 . . 6_557 ? C18 Zr2 C23 C23 -150.3(7) . . . 6_557 ? C18 Zr2 C23 C23 -61.0(9) 6_557 . . 6_557 ? C17 Zr2 C23 C23 -155(2) . . . 6_557 ? C24 Zr2 C23 C23 16(4) . . . 6_557 ? C21 Zr2 C23 C23 -97.3(8) . . . 6_557 ? C12 Zr2 C23 C22 -95(4) 6_557 . . . ? C12 Zr2 C23 C22 -178(4) . . . . ? C13 Zr2 C23 C22 -157(4) . . . . ? C13 Zr2 C23 C22 -126(4) 6_557 . . . ? C20 Zr2 C23 C22 55(4) . . . . ? C19 Zr2 C23 C22 15(4) . . . . ? C19 Zr2 C23 C22 50(4) 6_557 . . . ? C18 Zr2 C23 C22 -19(4) . . . . ? C18 Zr2 C23 C22 71(4) 6_557 . . . ? C17 Zr2 C23 C22 -23(5) . . . . ? C24 Zr2 C23 C22 148(7) . . . . ? C21 Zr2 C23 C22 34(4) . . . . ? C12 Zr2 C23 C25 152(4) 6_557 . . 6_557 ? C12 Zr2 C23 C25 69(4) . . . 6_557 ? C13 Zr2 C23 C25 90(4) . . . 6_557 ? C13 Zr2 C23 C25 122(4) 6_557 . . 6_557 ? C20 Zr2 C23 C25 -58(4) . . . 6_557 ? C19 Zr2 C23 C25 -98(4) . . . 6_557 ? C19 Zr2 C23 C25 -63(4) 6_557 . . 6_557 ? C18 Zr2 C23 C25 -131(4) . . . 6_557 ? C18 Zr2 C23 C25 -42(4) 6_557 . . 6_557 ? C17 Zr2 C23 C25 -136(4) . . . 6_557 ? C24 Zr2 C23 C25 35(6) . . . 6_557 ? C21 Zr2 C23 C25 -78(4) . . . 6_557 ? C12 Zr2 C23 C21 -129.2(8) 6_557 . . . ? C12 Zr2 C23 C21 147.8(8) . . . . ? C13 Zr2 C23 C21 168.1(9) . . . . ? C13 Zr2 C23 C21 -160.0(9) 6_557 . . . ? C20 Zr2 C23 C21 20.9(8) . . . . ? C19 Zr2 C23 C21 -19.5(10) . . . . ? C19 Zr2 C23 C21 15.3(10) 6_557 . . . ? C18 Zr2 C23 C21 -53.0(11) . . . . ? C18 Zr2 C23 C21 36.3(15) 6_557 . . . ? C17 Zr2 C23 C21 -58(2) . . . . ? C24 Zr2 C23 C21 114(4) . . . . ? C25 C23 C24 C23 3(12) . . . 6_557 ? C22 C23 C24 C23 17(13) . . . 6_557 ? C25 C23 C24 C23 1(5) 6_557 . . 6_557 ? C21 C23 C24 C23 8(9) . . . 6_557 ? Zr2 C23 C24 C23 70(8) . . . 6_557 ? C25 C23 C24 C25 2(7) . . . 6_557 ? C23 C23 C24 C25 -1(5) 6_557 . . 6_557 ? C22 C23 C24 C25 15(10) . . . 6_557 ? C21 C23 C24 C25 6(5) . . . 6_557 ? Zr2 C23 C24 C25 69(4) . . . 6_557 ? C23 C23 C24 C25 -3(12) 6_557 . . . ? C22 C23 C24 C25 13(10) . . . . ? C25 C23 C24 C25 -2(7) 6_557 . . . ? C21 C23 C24 C25 4(7) . . . . ? Zr2 C23 C24 C25 67(7) . . . . ? C25 C23 C24 C22 -13(10) . . . . ? C23 C23 C24 C22 -17(13) 6_557 . . . ? C25 C23 C24 C22 -15(10) 6_557 . . . ? C21 C23 C24 C22 -9(5) . . . . ? Zr2 C23 C24 C22 54(6) . . . . ? C25 C23 C24 C22 -5(9) . . . 6_557 ? C23 C23 C24 C22 -9(6) 6_557 . . 6_557 ? C22 C23 C24 C22 8(7) . . . 6_557 ? C25 C23 C24 C22 -7(4) 6_557 . . 6_557 ? C21 C23 C24 C22 -1(3) . . . 6_557 ? Zr2 C23 C24 C22 62(2) . . . 6_557 ? C25 C23 C24 Zr2 -67(7) . . . . ? C23 C23 C24 Zr2 -70(8) 6_557 . . . ? C22 C23 C24 Zr2 -54(6) . . . . ? C25 C23 C24 Zr2 -69(4) 6_557 . . . ? C21 C23 C24 Zr2 -62.5(14) . . . . ? C25 C22 C24 C23 -139(41) . . . 6_557 ? C21 C22 C24 C23 -4(4) . . . 6_557 ? C23 C22 C24 C23 -169(9) . . . 6_557 ? C20 C22 C24 C23 -3(3) . . . 6_557 ? Zr2 C22 C24 C23 69(3) . . . 6_557 ? C25 C22 C24 C23 31(36) . . . . ? C21 C22 C24 C23 165(8) . . . . ? C20 C22 C24 C23 166(8) . . . . ? Zr2 C22 C24 C23 -121(8) . . . . ? C25 C22 C24 C25 -137(42) . . . 6_557 ? C21 C22 C24 C25 -3(2) . . . 6_557 ? C23 C22 C24 C25 -168(9) . . . 6_557 ? C20 C22 C24 C25 -2(2) . . . 6_557 ? Zr2 C22 C24 C25 71(2) . . . 6_557 ? C21 C22 C24 C25 134(42) . . . . ? C23 C22 C24 C25 -31(36) . . . . ? C20 C22 C24 C25 135(41) . . . . ? Zr2 C22 C24 C25 -152(41) . . . . ? C25 C22 C24 C22 -142(39) . . . 6_557 ? C21 C22 C24 C22 -8(4) . . . 6_557 ? C23 C22 C24 C22 -173(6) . . . 6_557 ? C20 C22 C24 C22 -7(3) . . . 6_557 ? Zr2 C22 C24 C22 66(2) . . . 6_557 ? C25 C22 C24 Zr2 152(41) . . . . ? C21 C22 C24 Zr2 -74(3) . . . . ? C23 C22 C24 Zr2 121(8) . . . . ? C20 C22 C24 Zr2 -72.6(15) . . . . ? C12 Zr2 C24 C23 148(4) 6_557 . . 6_557 ? C12 Zr2 C24 C23 63(4) . . . 6_557 ? C13 Zr2 C24 C23 89(4) . . . 6_557 ? C13 Zr2 C24 C23 122(4) 6_557 . . 6_557 ? C20 Zr2 C24 C23 -74(4) . . . 6_557 ? C19 Zr2 C24 C23 -94(4) . . . 6_557 ? C19 Zr2 C24 C23 -55(4) 6_557 . . 6_557 ? C18 Zr2 C24 C23 -130(3) . . . 6_557 ? C18 Zr2 C24 C23 -19(5) 6_557 . . 6_557 ? C17 Zr2 C24 C23 -74(4) . . . 6_557 ? C21 Zr2 C24 C23 -95(4) . . . 6_557 ? C12 Zr2 C24 C23 -63(4) 6_557 . . . ? C12 Zr2 C24 C23 -148(4) . . . . ? C13 Zr2 C24 C23 -122(4) . . . . ? C13 Zr2 C24 C23 -89(4) 6_557 . . . ? C20 Zr2 C24 C23 74(4) . . . . ? C19 Zr2 C24 C23 55(4) . . . . ? C19 Zr2 C24 C23 94(4) 6_557 . . . ? C18 Zr2 C24 C23 19(5) . . . . ? C18 Zr2 C24 C23 130(3) 6_557 . . . ? C17 Zr2 C24 C23 74(4) . . . . ? C21 Zr2 C24 C23 54(4) . . . . ? C12 Zr2 C24 C25 166(5) 6_557 . . 6_557 ? C12 Zr2 C24 C25 81(5) . . . 6_557 ? C13 Zr2 C24 C25 107(5) . . . 6_557 ? C13 Zr2 C24 C25 141(5) 6_557 . . 6_557 ? C20 Zr2 C24 C25 -56(5) . . . 6_557 ? C19 Zr2 C24 C25 -76(5) . . . 6_557 ? C19 Zr2 C24 C25 -37(5) 6_557 . . 6_557 ? C18 Zr2 C24 C25 -112(5) . . . 6_557 ? C18 Zr2 C24 C25 -1(6) 6_557 . . 6_557 ? C17 Zr2 C24 C25 -56(5) . . . 6_557 ? C21 Zr2 C24 C25 -77(5) . . . 6_557 ? C12 Zr2 C24 C25 -81(5) 6_557 . . . ? C12 Zr2 C24 C25 -166(5) . . . . ? C13 Zr2 C24 C25 -141(5) . . . . ? C13 Zr2 C24 C25 -107(5) 6_557 . . . ? C20 Zr2 C24 C25 56(5) . . . . ? C19 Zr2 C24 C25 37(5) . . . . ? C19 Zr2 C24 C25 76(5) 6_557 . . . ? C18 Zr2 C24 C25 1(6) . . . . ? C18 Zr2 C24 C25 112(5) 6_557 . . . ? C17 Zr2 C24 C25 56(5) . . . . ? C21 Zr2 C24 C25 36(5) . . . . ? C12 Zr2 C24 C22 -86(3) 6_557 . . . ? C12 Zr2 C24 C22 -170(3) . . . . ? C13 Zr2 C24 C22 -145(3) . . . . ? C13 Zr2 C24 C22 -111(3) 6_557 . . . ? C20 Zr2 C24 C22 52(3) . . . . ? C19 Zr2 C24 C22 33(3) . . . . ? C19 Zr2 C24 C22 72(3) 6_557 . . . ? C18 Zr2 C24 C22 -3(3) . . . . ? C18 Zr2 C24 C22 108(3) 6_557 . . . ? C17 Zr2 C24 C22 52(3) . . . . ? C21 Zr2 C24 C22 32(3) . . . . ? C12 Zr2 C24 C22 170(3) 6_557 . . 6_557 ? C12 Zr2 C24 C22 86(3) . . . 6_557 ? C13 Zr2 C24 C22 111(3) . . . 6_557 ? C13 Zr2 C24 C22 145(3) 6_557 . . 6_557 ? C20 Zr2 C24 C22 -52(3) . . . 6_557 ? C19 Zr2 C24 C22 -72(3) . . . 6_557 ? C19 Zr2 C24 C22 -33(3) 6_557 . . 6_557 ? C18 Zr2 C24 C22 -108(3) . . . 6_557 ? C18 Zr2 C24 C22 3(3) 6_557 . . 6_557 ? C17 Zr2 C24 C22 -52(3) . . . 6_557 ? C21 Zr2 C24 C22 -73(3) . . . 6_557 ? C24 C23 C25 C22 76(63) . . . . ? C23 C23 C25 C22 77(63) 6_557 . . . ? C25 C23 C25 C22 77(63) 6_557 . . . ? C21 C23 C25 C22 69(60) . . . . ? Zr2 C23 C25 C22 11(62) . . . . ? C23 C23 C25 C24 1(4) 6_557 . . . ? C22 C23 C25 C24 -76(63) . . . . ? C25 C23 C25 C24 1(4) 6_557 . . . ? C21 C23 C25 C24 -7(12) . . . . ? Zr2 C23 C25 C24 -65(7) . . . . ? C24 C23 C25 C21 7(12) . . . . ? C23 C23 C25 C21 8(9) 6_557 . . . ? C22 C23 C25 C21 -69(60) . . . . ? C25 C23 C25 C21 8(9) 6_557 . . . ? Zr2 C23 C25 C21 -58(6) . . . . ? C24 C23 C25 C23 -1(4) . . . 6_557 ? C22 C23 C25 C23 -77(63) . . . 6_557 ? C25 C23 C25 C23 0.00(5) 6_557 . . 6_557 ? C21 C23 C25 C23 -8(9) . . . 6_557 ? Zr2 C23 C25 C23 -66(3) . . . 6_557 ? C24 C23 C25 C20 3(9) . . . . ? C23 C23 C25 C20 4(6) 6_557 . . . ? C22 C23 C25 C20 -73(61) . . . . ? C25 C23 C25 C20 4(6) 6_557 . . . ? C21 C23 C25 C20 -4(3) . . . . ? Zr2 C23 C25 C20 -62(3) . . . . ? C24 C23 C25 Zr2 65(6) . . . . ? C23 C23 C25 Zr2 66(3) 6_557 . . . ? C22 C23 C25 Zr2 -11(62) . . . . ? C25 C23 C25 Zr2 66(3) 6_557 . . . ? C21 C23 C25 Zr2 58(6) . . . . ? C21 C22 C25 C23 -84(64) . . . . ? C20 C22 C25 C23 -79(62) . . . . ? C24 C22 C25 C23 -36(29) . . . . ? Zr2 C22 C25 C23 -10(61) . . . . ? C21 C22 C25 C24 -48(41) . . . . ? C23 C22 C25 C24 36(29) . . . . ? C20 C22 C25 C24 -43(38) . . . . ? Zr2 C22 C25 C24 25(37) . . . . ? C23 C22 C25 C21 84(64) . . . . ? C20 C22 C25 C21 5(4) . . . . ? C24 C22 C25 C21 48(41) . . . . ? Zr2 C22 C25 C21 74(6) . . . . ? C21 C22 C25 C23 -31(25) . . . 6_557 ? C23 C22 C25 C23 54(45) . . . 6_557 ? C20 C22 C25 C23 -26(21) . . . 6_557 ? C24 C22 C25 C23 18(18) . . . 6_557 ? Zr2 C22 C25 C23 43(20) . . . 6_557 ? C21 C22 C25 C20 -5(4) . . . . ? C23 C22 C25 C20 79(62) . . . . ? C24 C22 C25 C20 43(38) . . . . ? Zr2 C22 C25 C20 69(2) . . . . ? C21 C22 C25 Zr2 -74(6) . . . . ? C23 C22 C25 Zr2 10(61) . . . . ? C20 C22 C25 Zr2 -69(2) . . . . ? C24 C22 C25 Zr2 -25(37) . . . . ? C23 C24 C25 C23 -178(9) 6_557 . . . ? C25 C24 C25 C23 -178(6) 6_557 . . . ? C22 C24 C25 C23 137(43) . . . . ? C22 C24 C25 C23 176(8) 6_557 . . . ? Zr2 C24 C25 C23 110(8) . . . . ? C23 C24 C25 C22 46(42) 6_557 . . . ? C23 C24 C25 C22 -137(43) . . . . ? C25 C24 C25 C22 45(42) 6_557 . . . ? C22 C24 C25 C22 39(40) 6_557 . . . ? Zr2 C24 C25 C22 -27(39) . . . . ? C23 C24 C25 C21 8(7) 6_557 . . . ? C23 C24 C25 C21 -174(10) . . . . ? C25 C24 C25 C21 8(7) 6_557 . . . ? C22 C24 C25 C21 -37(37) . . . . ? C22 C24 C25 C21 2(4) 6_557 . . . ? Zr2 C24 C25 C21 -64(3) . . . . ? C23 C24 C25 C23 178(9) . . . 6_557 ? C25 C24 C25 C23 -1(2) 6_557 . . 6_557 ? C22 C24 C25 C23 -46(43) . . . 6_557 ? C22 C24 C25 C23 -7(4) 6_557 . . 6_557 ? Zr2 C24 C25 C23 -72(5) . . . 6_557 ? C23 C24 C25 C20 5(6) 6_557 . . . ? C23 C24 C25 C20 -177(9) . . . . ? C25 C24 C25 C20 5(5) 6_557 . . . ? C22 C24 C25 C20 -40(39) . . . . ? C22 C24 C25 C20 -1(2) 6_557 . . . ? Zr2 C24 C25 C20 -66.8(18) . . . . ? C23 C24 C25 Zr2 72(5) 6_557 . . . ? C23 C24 C25 Zr2 -110(8) . . . . ? C25 C24 C25 Zr2 71(4) 6_557 . . . ? C22 C24 C25 Zr2 27(39) . . . . ? C22 C24 C25 Zr2 65.3(14) 6_557 . . . ? C20 C21 C25 C23 -11(10) . . . . ? C22 C21 C25 C23 155(19) . . . . ? C21 C21 C25 C23 -7(8) 6_557 . . . ? Zr2 C21 C25 C23 61(7) . . . . ? C20 C21 C25 C22 -166(12) . . . . ? C21 C21 C25 C22 -162(12) 6_557 . . . ? C23 C21 C25 C22 -155(19) . . . . ? Zr2 C21 C25 C22 -94(13) . . . . ? C20 C21 C25 C24 -9(7) . . . . ? C22 C21 C25 C24 157(16) . . . . ? C21 C21 C25 C24 -5(5) 6_557 . . . ? C23 C21 C25 C24 2(4) . . . . ? Zr2 C21 C25 C24 63(4) . . . . ? C20 C21 C25 C23 -7(5) . . . 6_557 ? C22 C21 C25 C23 159(14) . . . 6_557 ? C21 C21 C25 C23 -2(3) 6_557 . . 6_557 ? C23 C21 C25 C23 5(5) . . . 6_557 ? Zr2 C21 C25 C23 65.7(18) . . . 6_557 ? C22 C21 C25 C20 166(12) . . . . ? C21 C21 C25 C20 4(4) 6_557 . . . ? C23 C21 C25 C20 11(10) . . . . ? Zr2 C21 C25 C20 72(5) . . . . ? C20 C21 C25 Zr2 -72(4) . . . . ? C22 C21 C25 Zr2 94(13) . . . . ? C21 C21 C25 Zr2 -68.0(11) 6_557 . . . ? C23 C21 C25 Zr2 -61(7) . . . . ? C21 C20 C25 C23 170(8) . . . . ? C21 C20 C25 C23 -1(7) 6_557 . . . ? C22 C20 C25 C23 159(17) . . . . ? C22 C20 C25 C23 1(4) 6_557 . . . ? C25 C20 C25 C23 -4(6) 6_557 . . . ? Zr2 C20 C25 C23 70(5) . . . . ? C21 C20 C25 C22 12(11) . . . . ? C21 C20 C25 C22 -160(12) 6_557 . . . ? C22 C20 C25 C22 -158(13) 6_557 . . . ? C25 C20 C25 C22 -163(11) 6_557 . . . ? Zr2 C20 C25 C22 -89(12) . . . . ? C21 C20 C25 C24 171(6) . . . . ? C21 C20 C25 C24 0(6) 6_557 . . . ? C22 C20 C25 C24 160(15) . . . . ? C22 C20 C25 C24 2(2) 6_557 . . . ? C25 C20 C25 C24 -3(4) 6_557 . . . ? Zr2 C20 C25 C24 71(3) . . . . ? C21 C20 C25 C21 -171(8) 6_557 . . . ? C22 C20 C25 C21 -12(11) . . . . ? C22 C20 C25 C21 -170(6) 6_557 . . . ? C25 C20 C25 C21 -175(5) 6_557 . . . ? Zr2 C20 C25 C21 -100(5) . . . . ? C21 C20 C25 C23 173(6) . . . 6_557 ? C21 C20 C25 C23 2(4) 6_557 . . 6_557 ? C22 C20 C25 C23 161(13) . . . 6_557 ? C22 C20 C25 C23 3.3(12) 6_557 . . 6_557 ? C25 C20 C25 C23 -2(3) 6_557 . . 6_557 ? Zr2 C20 C25 C23 72.7(14) . . . 6_557 ? C21 C20 C25 Zr2 100(5) . . . . ? C21 C20 C25 Zr2 -71(4) 6_557 . . . ? C22 C20 C25 Zr2 89(12) . . . . ? C22 C20 C25 Zr2 -69.4(18) 6_557 . . . ? C25 C20 C25 Zr2 -74.5(17) 6_557 . . . ? C12 Zr2 C25 C23 84(6) 6_557 . . . ? C12 Zr2 C25 C23 1(7) . . . . ? C13 Zr2 C25 C23 21(6) . . . . ? C13 Zr2 C25 C23 50(6) 6_557 . . . ? C20 Zr2 C25 C23 -112(5) . . . . ? C19 Zr2 C25 C23 -168(6) . . . . ? C19 Zr2 C25 C23 -139(6) 6_557 . . . ? C18 Zr2 C25 C23 163(5) . . . . ? C18 Zr2 C25 C23 -136(6) 6_557 . . . ? C17 Zr2 C25 C23 167(3) . . . . ? C24 Zr2 C25 C23 -17(3) . . . . ? C21 Zr2 C25 C23 -132(6) . . . . ? C12 Zr2 C25 C22 -93(17) 6_557 . . . ? C12 Zr2 C25 C22 -176(15) . . . . ? C13 Zr2 C25 C22 -155(17) . . . . ? C13 Zr2 C25 C22 -126(17) 6_557 . . . ? C20 Zr2 C25 C22 72(18) . . . . ? C19 Zr2 C25 C22 16(17) . . . . ? C19 Zr2 C25 C22 45(17) 6_557 . . . ? C18 Zr2 C25 C22 -13(18) . . . . ? C18 Zr2 C25 C22 47(17) 6_557 . . . ? C17 Zr2 C25 C22 -9(20) . . . . ? C24 Zr2 C25 C22 167(21) . . . . ? C21 Zr2 C25 C22 51(17) . . . . ? C12 Zr2 C25 C24 101(4) 6_557 . . . ? C12 Zr2 C25 C24 18(6) . . . . ? C13 Zr2 C25 C24 38(5) . . . . ? C13 Zr2 C25 C24 67(4) 6_557 . . . ? C20 Zr2 C25 C24 -95(4) . . . . ? C19 Zr2 C25 C24 -151(4) . . . . ? C19 Zr2 C25 C24 -122(4) 6_557 . . . ? C18 Zr2 C25 C24 -179(3) . . . . ? C18 Zr2 C25 C24 -119(4) 6_557 . . . ? C17 Zr2 C25 C24 -175.9(14) . . . . ? C21 Zr2 C25 C24 -115(5) . . . . ? C12 Zr2 C25 C21 -144.0(17) 6_557 . . . ? C12 Zr2 C25 C21 133(2) . . . . ? C13 Zr2 C25 C21 153.3(17) . . . . ? C13 Zr2 C25 C21 -177.4(18) 6_557 . . . ? C20 Zr2 C25 C21 20.8(15) . . . . ? C19 Zr2 C25 C21 -35.6(18) . . . . ? C19 Zr2 C25 C21 -7(2) 6_557 . . . ? C18 Zr2 C25 C21 -64(2) . . . . ? C18 Zr2 C25 C21 -4(3) 6_557 . . . ? C17 Zr2 C25 C21 -61(4) . . . . ? C24 Zr2 C25 C21 115(5) . . . . ? C12 Zr2 C25 C23 118(3) 6_557 . . 6_557 ? C12 Zr2 C25 C23 35(4) . . . 6_557 ? C13 Zr2 C25 C23 56(3) . . . 6_557 ? C13 Zr2 C25 C23 85(3) 6_557 . . 6_557 ? C20 Zr2 C25 C23 -76.9(19) . . . 6_557 ? C19 Zr2 C25 C23 -133(2) . . . 6_557 ? C19 Zr2 C25 C23 -104(2) 6_557 . . 6_557 ? C18 Zr2 C25 C23 -161.8(15) . . . 6_557 ? C18 Zr2 C25 C23 -102(3) 6_557 . . 6_557 ? C17 Zr2 C25 C23 -158.2(13) . . . 6_557 ? C24 Zr2 C25 C23 18(2) . . . 6_557 ? C21 Zr2 C25 C23 -98(3) . . . 6_557 ? C12 Zr2 C25 C20 -164.8(15) 6_557 . . . ? C12 Zr2 C25 C20 112(3) . . . . ? C13 Zr2 C25 C20 132.5(16) . . . . ? C13 Zr2 C25 C20 161.8(16) 6_557 . . . ? C19 Zr2 C25 C20 -56.4(15) . . . . ? C19 Zr2 C25 C20 -27.4(17) 6_557 . . . ? C18 Zr2 C25 C20 -84.9(13) . . . . ? C18 Zr2 C25 C20 -25(2) 6_557 . . . ? C17 Zr2 C25 C20 -81(3) . . . . ? C24 Zr2 C25 C20 95(4) . . . . ? C21 Zr2 C25 C20 -20.8(15) . . . . ? C26 C27 C28 C28 41(2) . . . 3_566 ? C26 C27 C28 C27 39(5) . . . 3_566 ? C28 C27 C28 C27 -1(3) 3_566 . . 3_566 ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 395.97 37.53 16.98 o 2 0 0 157189.80 135092.41 5630.11 o 3 0 0 84.57 224.01 31.77 o 4 0 0 1520.62 937.54 52.60 o 5 0 0 5.73 73.16 39.45 o 6 0 0 6793.77 7058.23 185.80 o 7 0 0 489.50 860.72 41.36 o 8 0 0 62234.63 70599.65 1444.41 o 9 0 0 35.75 72.55 17.40 o 10 0 0 33597.97 35323.92 517.35 o 11 0 0 356.34 894.71 31.09 o 12 0 0 4938.15 4870.18 97.01 o 13 0 0 209.29 389.23 29.71 o 14 0 0 1531.14 1493.66 55.69 o 15 0 0 80.81 235.38 25.83 o 1 1 0 1980.79 101.93 8.30 o 2 1 0 1523.11 690.61 21.00 o 3 1 0 41992.73 46975.37 739.96 o 4 1 0 1475.80 1273.88 28.27 o 5 1 0 519.41 422.33 23.12 o 6 1 0 878.32 1026.94 34.73 o 7 1 0 19344.39 21467.56 309.37 o 8 1 0 154.98 170.34 32.42 o 9 1 0 105.76 31.56 11.62 o 10 1 0 18.98 75.58 13.42 o 11 1 0 4.64 44.82 14.64 o 12 1 0 361.31 263.08 17.09 o 13 1 0 671.70 553.00 27.06 o 14 1 0 486.16 516.02 20.15 o 15 1 0 1012.62 979.30 57.82 o 0 2 0 1884.31 1432.57 131.11 o 1 2 0 496.07 501.25 37.07 o 2 2 0 8938.19 9929.13 255.44 o 3 2 0 54094.98 52606.55 895.56 o 4 2 0 5.34 34.92 17.48 o 5 2 0 34954.03 35352.30 563.39 o 6 2 0 31.18 30.62 25.68 o 7 2 0 351.52 376.12 22.39 o 8 2 0 901.04 1020.73 21.67 o 9 2 0 1431.52 1837.82 27.08 o 10 2 0 444.02 475.68 16.63 o 11 2 0 675.00 681.44 19.37 o 12 2 0 103.86 98.92 16.04 o 13 2 0 1506.10 1288.97 27.21 o 14 2 0 8.64 23.01 16.38 o 15 2 0 354.06 294.18 25.80 o 1 3 0 16893.16 15519.28 293.64 o 2 3 0 1542.35 1040.17 38.23 o 3 3 0 971.98 2108.04 52.79 o 4 3 0 203.37 30.10 19.88 o 5 3 0 123.20 174.45 25.25 o 6 3 0 984.72 1291.53 45.46 o 7 3 0 23732.07 23561.42 323.28 o 8 3 0 38.25 153.57 12.77 o 9 3 0 1623.43 1850.61 32.85 o 10 3 0 2058.91 2094.16 46.14 o 11 3 0 466.21 544.75 24.76 o 12 3 0 1528.43 1459.65 30.09 o 13 3 0 1033.92 1214.64 39.28 o 14 3 0 531.63 517.84 24.97 o 15 3 0 1512.49 1799.18 60.94 o 0 4 0 28426.86 36225.04 1078.14 o 1 4 0 6316.52 5721.98 62.76 o 2 4 0 7129.33 5939.33 134.15 o 3 4 0 6779.46 6153.52 123.49 o 4 4 0 30283.64 32493.92 613.45 o 5 4 0 838.16 591.82 36.65 o 6 4 0 47368.55 45768.34 680.43 o 7 4 0 409.93 857.49 25.03 o 8 4 0 15867.74 16429.56 304.73 o 9 4 0 196.07 216.03 13.80 o 10 4 0 11846.46 10450.78 114.35 o 11 4 0 1102.62 1072.69 22.54 o 12 4 0 7091.15 6921.26 117.25 o 13 4 0 1295.37 971.98 32.12 o 14 4 0 3241.71 3266.24 62.67 o 15 4 0 493.93 483.74 30.78 o 1 5 0 458.74 626.47 23.86 o 2 5 0 7829.82 6852.04 154.78 o 3 5 0 261.47 300.17 26.31 o 4 5 0 2894.77 3811.72 84.50 o 5 5 0 360.56 336.87 28.26 o 6 5 0 7600.13 7384.76 140.28 o 7 5 0 166.33 143.36 12.87 o 8 5 0 1602.10 1233.37 33.40 o 9 5 0 833.64 463.33 17.29 o 10 5 0 2242.32 2052.95 77.54 o 11 5 0 87.93 331.28 20.83 o 12 5 0 2591.51 2843.65 51.06 o 13 5 0 321.26 502.08 22.40 o 14 5 0 135.59 156.16 21.34 o 15 5 0 40.09 13.44 19.77 o 0 6 0 3928.36 5441.21 157.39 o 1 6 0 18577.24 17608.60 266.73 o 2 6 0 7354.49 7240.17 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2377.62 39.05 o 8 8 0 1815.79 1845.92 48.75 o 9 8 0 618.86 865.95 30.45 o 10 8 0 5865.60 6151.68 156.39 o 11 8 0 886.36 895.74 51.38 o 12 8 0 2923.54 2854.48 117.42 o 13 8 0 1337.56 1312.50 38.40 o 14 8 0 454.13 516.81 28.06 o 1 9 0 200.92 164.25 27.16 o 2 9 0 3596.74 2751.89 62.75 o 3 9 0 327.51 309.57 22.11 o 4 9 0 863.68 914.55 27.64 o 5 9 0 1682.84 1084.93 27.88 o 6 9 0 237.73 145.14 19.22 o 7 9 0 31.71 170.06 17.71 o 8 9 0 635.07 676.42 58.70 o 9 9 0 735.44 608.70 23.33 o 10 9 0 2729.48 2402.51 128.33 o 11 9 0 63.29 156.89 19.58 o 12 9 0 1306.27 1573.81 115.06 o 13 9 0 235.08 380.96 33.54 o 0 10 0 2606.87 3103.80 88.17 o 1 10 0 9262.93 9357.92 176.89 o 2 10 0 29.92 55.51 18.30 o 3 10 0 15121.19 17751.93 286.95 o 4 10 0 1417.06 1407.89 35.01 o 5 10 0 14654.09 14592.14 204.08 o 6 10 0 1303.98 1518.34 31.83 o 7 10 0 12774.71 12622.68 167.84 o 8 10 0 180.59 122.20 18.46 o 9 10 0 7775.86 7459.40 140.64 o 10 10 0 0.13 8.90 21.42 o 11 10 0 4227.63 4669.27 150.77 o 12 10 0 176.25 171.01 27.42 o 13 10 0 2548.07 2059.15 66.13 o 1 11 0 1099.09 1346.65 25.84 o 2 11 0 2394.67 1593.33 35.32 o 3 11 0 1988.30 2509.85 50.66 o 4 11 0 596.42 896.78 33.27 o 5 11 0 45.41 0.88 18.60 o 6 11 0 473.35 272.75 19.98 o 7 11 0 6.61 67.18 19.72 o 8 11 0 167.18 246.24 23.09 o 9 11 0 112.25 106.71 20.71 o 10 11 0 42.79 115.84 26.31 o 11 11 0 362.83 361.25 35.42 o 12 11 0 0.38 -3.57 24.51 o 0 12 0 1173.80 1027.65 37.54 o 1 12 0 3797.70 4254.04 150.74 o 2 12 0 451.31 780.01 26.23 o 3 12 0 9994.22 9216.48 156.68 o 4 12 0 496.23 995.33 32.89 o 5 12 0 11700.42 10954.37 150.84 o 6 12 0 38.33 216.71 25.13 o 7 12 0 4112.13 4273.34 91.55 o 8 12 0 60.84 413.74 23.68 o 9 12 0 889.96 1066.25 60.13 o 10 12 0 47.75 128.65 43.05 o 11 12 0 1359.09 1413.47 45.61 o 1 13 0 202.86 103.69 19.76 o 2 13 0 181.33 218.50 21.92 o 3 13 0 984.27 846.67 25.48 o 4 13 0 449.30 322.90 25.44 o 5 13 0 50.94 158.72 23.86 o 6 13 0 641.57 884.05 36.58 o 7 13 0 86.49 128.07 24.52 o 8 13 0 707.03 830.35 48.05 o 9 13 0 616.93 565.20 33.95 o 10 13 0 880.07 828.88 98.69 o 11 13 0 653.14 636.18 25.54 o 0 14 0 5078.68 6392.36 124.60 o 1 14 0 18014.88 19478.73 293.05 o 2 14 0 1163.60 933.59 39.56 o 3 14 0 8366.48 8124.18 155.32 o 4 14 0 18.88 188.66 21.03 o 5 14 0 3834.04 4879.70 83.08 o 6 14 0 100.58 155.66 35.38 o 7 14 0 4169.39 4215.04 214.61 o 8 14 0 979.25 892.92 47.90 o 9 14 0 4404.14 4692.47 135.75 o 10 14 0 706.12 717.90 38.48 o 1 15 0 80.75 149.78 21.08 o 2 15 0 124.83 22.80 20.66 o 3 15 0 27.51 157.86 23.67 o 4 15 0 92.68 143.36 26.87 o 5 15 0 110.50 133.25 25.58 o 6 15 0 2.54 84.52 23.79 o 7 15 0 272.25 409.40 25.88 o 8 15 0 39.07 70.17 19.05 o 9 15 0 187.37 135.88 17.36 o 0 16 0 1092.55 1832.62 60.65 o 1 16 0 3925.26 5221.75 89.96 o 2 16 0 1845.89 2107.91 54.33 o 3 16 0 2239.90 1929.84 44.08 o 4 16 0 1574.78 985.02 30.31 o 5 16 0 2394.71 1824.94 45.58 o 6 16 0 669.46 836.31 30.85 o 7 16 0 3913.55 4248.06 92.40 o 1 17 0 17.59 14.95 21.23 o 2 17 0 2.13 97.68 24.64 o 3 17 0 97.54 42.60 20.79 o 4 17 0 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1 960.16 937.79 16.03 o 13 2 1 2925.37 2976.33 40.33 o 14 2 1 403.39 335.16 14.75 o 15 2 1 3656.80 3477.33 99.08 o 1 3 1 8935.19 6736.25 119.70 o 2 3 1 462.69 287.33 14.56 o 3 3 1 1033.36 824.18 20.89 o 4 3 1 883.34 1391.99 29.44 o 5 3 1 78.55 12.86 18.59 o 6 3 1 5540.26 4980.77 72.30 o 7 3 1 4062.17 4221.04 41.86 o 8 3 1 312.78 312.45 11.16 o 9 3 1 140.39 243.22 13.79 o 10 3 1 245.49 240.08 11.90 o 11 3 1 514.09 692.55 20.28 o 12 3 1 683.04 778.25 17.81 o 13 3 1 181.67 256.46 13.98 o 14 3 1 533.60 522.35 17.17 o 15 3 1 78.87 60.77 17.35 o 0 4 1 43128.86 42066.17 1019.93 o 1 4 1 1185.86 1279.00 27.22 o 2 4 1 2346.03 2568.10 47.75 o 3 4 1 903.59 669.13 19.51 o 4 4 1 63603.61 62405.96 923.48 o 5 4 1 236.33 205.57 24.18 o 6 4 1 17098.59 17275.14 205.77 o 7 4 1 714.70 1065.47 17.32 o 8 4 1 181.77 300.08 11.60 o 9 4 1 537.32 482.78 20.61 o 10 4 1 2054.44 2306.62 27.50 o 11 4 1 177.51 126.51 12.08 o 12 4 1 3522.95 3434.72 33.50 o 13 4 1 1.97 2.19 13.14 o 14 4 1 1652.77 1637.03 34.14 o 15 4 1 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629.28 546.59 22.82 o 5 7 1 2.47 38.15 12.75 o 6 7 1 11.51 61.82 12.02 o 7 7 1 456.60 523.78 17.96 o 8 7 1 5.50 19.82 10.04 o 9 7 1 970.11 1096.35 27.98 o 10 7 1 379.23 430.96 13.62 o 11 7 1 2020.29 2059.14 60.67 o 12 7 1 11.21 -16.75 19.14 o 13 7 1 599.24 654.53 17.18 o 14 7 1 423.49 534.13 17.69 o 0 8 1 58835.98 58994.66 1243.95 o 1 8 1 510.37 503.45 24.85 o 2 8 1 45221.85 45169.51 761.10 o 3 8 1 2059.91 1964.23 60.95 o 4 8 1 21729.07 22290.78 329.55 o 5 8 1 1101.23 1150.63 23.26 o 6 8 1 9311.76 9666.14 99.81 o 7 8 1 844.11 774.39 16.05 o 8 8 1 9021.05 8690.16 89.68 o 9 8 1 619.53 664.90 16.17 o 10 8 1 7953.74 8516.60 137.47 o 11 8 1 258.37 291.56 16.82 o 12 8 1 3104.97 3183.59 75.43 o 13 8 1 12.68 12.88 14.20 o 14 8 1 1722.58 1462.92 59.54 o 1 9 1 142.43 75.73 22.54 o 2 9 1 2250.06 2423.56 49.36 o 3 9 1 182.99 117.88 15.29 o 4 9 1 755.53 851.00 20.59 o 5 9 1 269.40 160.52 12.51 o 6 9 1 178.38 70.56 12.69 o 7 9 1 1108.51 1035.14 28.97 o 8 9 1 65.64 84.72 18.98 o 9 9 1 385.81 384.01 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42164.87 531.44 o 2 6 3 878.71 664.03 27.07 o 3 6 3 22200.34 21088.18 340.53 o 4 6 3 32.42 96.94 23.31 o 5 6 3 24782.48 24769.47 269.25 o 6 6 3 147.59 179.42 10.50 o 7 6 3 4840.23 4788.44 46.27 o 8 6 3 5628.07 5439.48 56.18 o 9 6 3 4598.33 4459.16 44.47 o 10 6 3 1815.77 2040.79 30.77 o 11 6 3 7222.55 7558.94 74.23 o 12 6 3 494.51 434.15 18.64 o 13 6 3 2806.76 2728.66 64.84 o 14 6 3 74.87 83.10 13.72 o 1 7 3 5172.46 5601.04 74.60 o 2 7 3 58.97 69.12 23.27 o 3 7 3 1568.95 1399.39 48.44 o 4 7 3 1489.99 1471.71 24.60 o 5 7 3 2653.02 2483.19 32.02 o 6 7 3 792.69 585.96 14.57 o 7 7 3 6076.04 6047.29 54.96 o 8 7 3 17.21 32.80 9.95 o 9 7 3 341.83 371.22 27.67 o 10 7 3 394.96 441.05 18.86 o 11 7 3 71.82 142.52 14.82 o 12 7 3 263.64 372.56 20.18 o 13 7 3 219.75 254.81 22.25 o 14 7 3 322.57 318.86 16.28 o 0 8 3 79852.71 80338.66 1353.42 o 1 8 3 2542.20 2408.16 36.54 o 2 8 3 35437.11 36374.70 417.47 o 3 8 3 326.82 203.47 17.60 o 4 8 3 7616.48 7566.09 90.83 o 5 8 3 4.00 11.83 11.22 o 6 8 3 9544.30 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0 4 4 9086.97 9550.43 168.90 o 1 4 4 1541.02 1601.30 30.44 o 2 4 4 26347.04 22802.94 363.54 o 3 4 4 628.63 791.31 26.36 o 4 4 4 78498.52 79896.23 966.08 o 5 4 4 65.75 65.28 19.97 o 6 4 4 44948.01 46905.27 507.52 o 7 4 4 1161.35 1083.85 16.98 o 8 4 4 5830.42 6063.92 51.82 o 9 4 4 856.00 896.34 29.52 o 10 4 4 8270.13 8614.97 76.60 o 11 4 4 674.53 734.21 17.38 o 12 4 4 7898.48 8450.11 107.52 o 13 4 4 501.26 392.31 16.79 o 14 4 4 4283.96 4268.19 110.24 o 15 4 4 306.71 304.00 18.93 o 1 5 4 638.53 548.16 22.03 o 2 5 4 6289.15 6095.11 99.43 o 3 5 4 494.83 530.81 19.95 o 4 5 4 41.84 16.68 21.48 o 5 5 4 299.81 145.41 14.22 o 6 5 4 4122.24 3752.50 41.52 o 7 5 4 78.92 101.79 9.29 o 8 5 4 751.46 764.93 23.86 o 9 5 4 11.61 78.60 11.53 o 10 5 4 66.14 77.16 13.03 o 11 5 4 52.50 51.53 14.09 o 12 5 4 90.95 134.58 13.64 o 13 5 4 25.19 37.51 14.33 o 14 5 4 306.59 323.50 17.85 o 0 6 4 1868.29 1389.73 44.36 o 1 6 4 48722.39 48383.94 587.15 o 2 6 4 3638.87 3383.25 52.97 o 3 6 4 8385.09 8389.49 131.18 o 4 6 4 3235.00 3529.53 57.04 o 5 6 4 2205.23 2004.14 28.11 o 6 6 4 1992.89 2129.42 27.35 o 7 6 4 12854.12 12409.34 103.16 o 8 6 4 260.89 138.47 10.05 o 9 6 4 12821.08 12677.24 136.01 o 10 6 4 69.89 74.86 13.19 o 11 6 4 3985.25 4004.26 58.37 o 12 6 4 161.34 227.75 14.63 o 13 6 4 1187.07 1257.68 28.46 o 14 6 4 76.47 73.76 14.93 o 1 7 4 66.38 117.84 17.46 o 2 7 4 994.55 1302.63 32.42 o 3 7 4 106.48 114.22 20.82 o 4 7 4 1229.09 953.97 24.56 o 5 7 4 928.94 1044.53 19.02 o 6 7 4 240.51 146.90 12.02 o 7 7 4 1476.76 1176.73 19.12 o 8 7 4 127.43 156.67 11.35 o 9 7 4 300.02 343.85 17.66 o 10 7 4 932.70 1015.28 21.36 o 11 7 4 1319.34 1376.79 22.83 o 12 7 4 1130.20 1425.65 50.70 o 13 7 4 1379.28 1323.68 44.44 o 14 7 4 486.09 510.03 37.71 o 0 8 4 18544.36 18513.25 277.28 o 1 8 4 21218.58 20740.13 234.72 o 2 8 4 5172.52 5461.86 68.81 o 3 8 4 1233.76 1155.55 28.15 o 4 8 4 1204.62 1197.39 23.45 o 5 8 4 13.81 42.20 11.52 o 6 8 4 4462.36 4052.97 41.72 o 7 8 4 3393.80 3447.18 56.06 o 8 8 4 4848.89 4994.00 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4 93.91 35.50 14.45 o 3 11 4 1359.45 1658.85 31.69 o 4 11 4 25.17 86.24 15.45 o 5 11 4 453.78 644.51 18.82 o 6 11 4 20.08 29.69 15.06 o 7 11 4 1476.22 1863.25 39.53 o 8 11 4 17.56 11.03 16.34 o 9 11 4 41.79 30.36 16.92 o 10 11 4 46.81 27.79 15.91 o 11 11 4 5.75 54.86 15.34 o 12 11 4 227.99 282.36 29.26 o 0 12 4 1708.54 2627.88 62.31 o 1 12 4 6381.31 5843.49 84.11 o 2 12 4 130.60 265.54 17.80 o 3 12 4 7911.56 9011.22 196.91 o 4 12 4 22.37 295.48 19.59 o 5 12 4 7079.66 8265.24 90.46 o 6 12 4 91.87 202.43 15.91 o 7 12 4 4207.20 3695.16 49.80 o 8 12 4 10.90 137.88 17.49 o 9 12 4 1951.68 1665.33 39.60 o 10 12 4 28.72 44.93 16.01 o 11 12 4 1560.01 1643.77 51.68 o 1 13 4 224.83 162.87 14.33 o 2 13 4 1188.31 1822.74 27.76 o 3 13 4 51.81 29.38 15.38 o 4 13 4 988.61 861.04 19.29 o 5 13 4 152.92 65.27 18.66 o 6 13 4 202.67 120.21 15.62 o 7 13 4 432.22 327.08 18.54 o 8 13 4 353.04 314.00 17.96 o 9 13 4 640.47 794.90 44.06 o 10 13 4 921.30 969.64 50.29 o 0 14 4 209.03 222.81 45.62 o 1 14 4 8819.37 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135.08 o 3 8 9 1004.31 1029.45 21.29 o 4 8 9 7309.99 6979.83 67.07 o 5 8 9 453.60 458.68 12.95 o 6 8 9 7500.39 7133.72 70.13 o 7 8 9 144.33 142.93 12.61 o 8 8 9 7241.04 6629.36 68.88 o 9 8 9 155.22 82.62 14.53 o 10 8 9 5505.66 5341.55 106.26 o 11 8 9 56.27 137.46 17.58 o 12 8 9 2713.87 3050.09 73.73 o 13 8 9 52.59 65.32 14.70 o 1 9 9 584.77 517.68 14.43 o 2 9 9 1.45 15.82 13.68 o 3 9 9 680.97 735.80 22.19 o 4 9 9 47.36 22.56 12.21 o 5 9 9 461.53 470.44 14.46 o 6 9 9 72.10 74.19 13.50 o 7 9 9 206.86 204.40 13.54 o 8 9 9 669.45 681.76 17.34 o 9 9 9 216.52 288.02 16.15 o 10 9 9 364.66 403.32 17.87 o 11 9 9 80.28 182.79 16.38 o 12 9 9 191.31 197.82 20.18 o 0 10 9 11775.54 10988.06 147.64 o 1 10 9 3729.28 4186.12 48.32 o 2 10 9 7292.59 7345.12 72.73 o 3 10 9 1700.75 1270.36 23.81 o 4 10 9 2675.10 3104.60 59.69 o 5 10 9 911.94 753.55 17.38 o 6 10 9 2404.08 2063.06 53.85 o 7 10 9 950.98 1117.67 29.72 o 8 10 9 3510.40 3559.44 76.44 o 9 10 9 392.85 423.19 16.81 o 10 10 9 1739.00 1825.99 33.16 o 11 10 9 316.96 312.08 15.63 o 12 10 9 748.79 891.92 40.36 o 1 11 9 58.94 79.11 15.12 o 2 11 9 0.29 28.13 14.05 o 3 11 9 22.98 94.11 12.42 o 4 11 9 196.63 117.42 12.36 o 5 11 9 732.82 441.55 17.73 o 6 11 9 658.23 624.35 17.21 o 7 11 9 1042.11 868.74 26.72 o 8 11 9 511.39 412.04 16.89 o 9 11 9 452.32 561.03 17.64 o 10 11 9 224.12 300.11 15.14 o 11 11 9 469.12 461.11 18.30 o 0 12 9 7793.36 6861.46 93.78 o 1 12 9 119.95 151.61 17.33 o 2 12 9 8749.92 9173.71 92.64 o 3 12 9 173.67 178.61 13.43 o 4 12 9 9955.76 9495.40 99.32 o 5 12 9 327.62 411.61 14.00 o 6 12 9 6094.71 5860.05 83.37 o 7 12 9 10.46 44.39 14.49 o 8 12 9 3245.29 2827.03 58.90 o 9 12 9 7.55 43.48 14.10 o 10 12 9 2745.47 2648.36 116.52 o 1 13 9 60.73 53.30 14.39 o 2 13 9 87.67 93.52 13.03 o 3 13 9 10.25 -0.86 12.83 o 4 13 9 13.40 20.15 13.10 o 5 13 9 173.31 138.40 13.05 o 6 13 9 142.17 99.35 12.09 o 7 13 9 127.10 122.19 10.91 o 8 13 9 67.42 167.97 14.02 o 9 13 9 8.10 19.31 13.73 o 0 14 9 4081.31 4116.05 132.88 o 1 14 9 649.02 548.73 40.16 o 2 14 9 3442.00 3146.04 55.61 o 3 14 9 212.89 273.02 14.48 o 4 14 9 2317.05 2492.65 43.23 o 5 14 9 29.79 51.32 12.51 o 6 14 9 2000.86 2036.44 34.28 o 7 14 9 124.65 185.73 14.25 o 8 14 9 2542.50 2304.16 80.09 o 1 15 9 2.02 3.02 16.12 o 2 15 9 31.11 64.29 17.78 o 3 15 9 88.07 46.32 12.48 o 4 15 9 46.91 53.84 11.14 o 5 15 9 209.55 286.75 13.32 o 6 15 9 266.68 328.13 19.00 o 7 15 9 333.28 332.60 24.65 o 0 16 9 3372.10 2804.26 66.35 o 1 16 9 595.62 528.34 49.11 o 2 16 9 2858.55 2817.20 118.04 o 3 16 9 928.93 1017.91 34.19 o 4 16 9 2508.73 2164.73 53.40 o 5 16 9 1020.32 1047.36 27.64 o 1 17 9 8.81 44.57 12.75 o 2 17 9 3.38 34.57 15.03 o 3 17 9 83.71 115.32 16.00 o 0 0 10 295.23 1425.80 106.86 o 1 0 10 675.70 578.04 28.33 o 2 0 10 22955.89 24883.07 613.54 o 3 0 10 27.22 129.47 52.43 o 4 0 10 74003.12 79855.07 2363.81 o 5 0 10 48.14 30.77 21.62 o 6 0 10 25150.19 23209.04 443.14 o 7 0 10 212.98 237.80 15.47 o 8 0 10 3788.19 3389.73 41.19 o 9 0 10 47.05 74.10 15.01 o 10 0 10 6530.51 6674.48 85.53 o 11 0 10 105.23 49.24 16.36 o 12 0 10 8013.00 8306.46 133.31 o 13 0 10 129.97 65.43 27.63 o 14 0 10 5107.21 4744.74 122.10 o 1 1 10 2364.66 2699.11 51.14 o 2 1 10 1236.77 1222.92 35.93 o 3 1 10 2721.95 2919.28 67.90 o 4 1 10 447.35 267.06 25.55 o 5 1 10 361.69 163.34 15.32 o 6 1 10 0.87 85.14 15.70 o 7 1 10 310.86 417.60 11.08 o 8 1 10 6.38 3.07 10.29 o 9 1 10 504.46 626.74 13.00 o 10 1 10 198.51 228.81 12.65 o 11 1 10 1772.82 1656.81 39.69 o 12 1 10 357.05 341.50 22.56 o 13 1 10 499.15 461.49 18.41 o 14 1 10 74.60 77.81 17.19 o 0 2 10 1123.90 1457.67 44.40 o 1 2 10 13320.57 12830.06 187.52 o 2 2 10 331.08 249.03 17.24 o 3 2 10 112.49 132.04 16.54 o 4 2 10 698.64 768.76 33.13 o 5 2 10 1225.29 1322.17 25.46 o 6 2 10 802.52 933.62 24.29 o 7 2 10 1338.20 1473.65 16.90 o 8 2 10 10.04 20.99 10.86 o 9 2 10 2696.82 2605.68 26.59 o 10 2 10 19.65 51.84 11.58 o 11 2 10 529.78 580.27 20.79 o 12 2 10 4.40 -4.79 16.44 o 13 2 10 67.44 140.82 16.38 o 14 2 10 12.90 22.04 13.29 o 1 3 10 3925.36 3464.73 58.37 o 2 3 10 606.75 488.81 19.35 o 3 3 10 4172.66 4673.10 88.36 o 4 3 10 13.53 94.38 14.66 o 5 3 10 26.09 18.04 14.40 o 6 3 10 2791.42 2503.35 36.07 o 7 3 10 435.55 534.75 13.01 o 8 3 10 2245.74 2075.32 23.31 o 9 3 10 1164.39 1247.28 17.55 o 10 3 10 327.89 331.68 15.65 o 11 3 10 3238.69 3153.03 42.91 o 12 3 10 130.67 162.28 15.72 o 13 3 10 1130.44 1085.79 31.16 o 14 3 10 456.02 633.42 57.85 o 0 4 10 20965.90 20262.17 555.53 o 1 4 10 3235.73 3513.35 47.57 o 2 4 10 35181.24 34199.29 347.30 o 3 4 10 421.79 432.21 16.27 o 4 4 10 33688.89 33616.93 393.44 o 5 4 10 74.57 41.57 14.51 o 6 4 10 15382.75 15103.34 124.05 o 7 4 10 493.14 428.11 13.09 o 8 4 10 5924.84 6323.81 55.86 o 9 4 10 515.36 543.72 23.10 o 10 4 10 5543.84 5992.76 58.62 o 11 4 10 262.16 394.58 22.72 o 12 4 10 4278.64 4476.17 79.66 o 13 4 10 153.16 113.36 14.59 o 14 4 10 2981.13 2692.34 45.65 o 1 5 10 388.40 386.13 15.95 o 2 5 10 4609.40 3984.25 45.74 o 3 5 10 535.99 676.30 17.88 o 4 5 10 726.38 1029.34 23.20 o 5 5 10 219.22 120.52 10.95 o 6 5 10 2505.01 2107.68 51.23 o 7 5 10 10.22 36.94 13.03 o 8 5 10 1655.06 1283.13 35.01 o 9 5 10 141.74 131.63 14.10 o 10 5 10 79.18 79.31 13.00 o 11 5 10 99.01 53.28 13.47 o 12 5 10 57.24 71.50 14.63 o 13 5 10 22.17 8.15 13.63 o 0 6 10 85.48 -26.59 26.59 o 1 6 10 29531.14 28505.42 333.34 o 2 6 10 872.37 761.60 18.85 o 3 6 10 4860.33 5047.48 60.42 o 4 6 10 1909.15 1820.26 37.62 o 5 6 10 1773.81 1997.28 27.85 o 6 6 10 1250.05 1479.42 20.88 o 7 6 10 8677.40 8227.18 74.20 o 8 6 10 426.51 212.44 17.43 o 9 6 10 5986.22 4793.63 64.21 o 10 6 10 136.90 176.90 14.01 o 11 6 10 2138.18 2269.55 53.57 o 12 6 10 87.88 114.43 18.41 o 13 6 10 837.78 1105.03 38.77 o 1 7 10 178.15 147.50 16.01 o 2 7 10 233.09 228.13 16.08 o 3 7 10 12.01 55.90 13.01 o 4 7 10 46.90 127.19 12.27 o 5 7 10 540.86 476.56 14.27 o 6 7 10 62.90 26.37 11.34 o 7 7 10 1331.39 1154.09 21.39 o 8 7 10 400.77 371.68 16.03 o 9 7 10 1348.92 1152.17 20.60 o 10 7 10 459.55 583.49 16.71 o 11 7 10 477.55 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11738.72 128.25 o 6 10 10 69.24 101.88 13.96 o 7 10 10 6816.49 6891.87 108.88 o 8 10 10 393.46 292.69 15.94 o 9 10 10 4096.39 3571.30 49.15 o 10 10 10 75.05 171.61 18.77 o 11 10 10 2986.62 2764.19 105.07 o 1 11 10 264.85 338.89 15.94 o 2 11 10 255.44 202.96 13.56 o 3 11 10 461.07 507.66 14.22 o 4 11 10 0.30 10.52 11.88 o 5 11 10 213.97 261.53 14.42 o 6 11 10 60.43 22.93 14.72 o 7 11 10 664.89 765.28 28.60 o 8 11 10 1.21 10.74 15.98 o 9 11 10 15.32 22.44 15.02 o 10 11 10 85.95 72.12 20.10 o 11 11 10 32.83 57.49 17.02 o 0 12 10 147.12 103.10 25.33 o 1 12 10 5182.57 4545.44 58.67 o 2 12 10 110.36 81.16 13.46 o 3 12 10 3984.72 4307.84 71.67 o 4 12 10 107.65 314.51 13.34 o 5 12 10 2989.03 3410.16 57.01 o 6 12 10 15.49 127.04 12.41 o 7 12 10 3193.32 2785.33 32.29 o 8 12 10 36.91 95.33 14.17 o 9 12 10 2565.29 2122.54 35.45 o 10 12 10 53.75 81.12 16.43 o 1 13 10 135.06 61.25 14.82 o 2 13 10 265.55 449.71 15.77 o 3 13 10 138.84 115.05 12.85 o 4 13 10 592.59 545.71 15.36 o 5 13 10 97.26 106.54 12.01 o 6 13 10 312.22 165.29 15.15 o 7 13 10 477.63 468.96 20.30 o 8 13 10 296.76 212.90 13.39 o 9 13 10 306.30 361.65 39.49 o 0 14 10 42.67 84.75 26.55 o 1 14 10 2819.44 2728.70 79.79 o 2 14 10 195.04 192.25 15.89 o 3 14 10 3759.18 4024.20 64.96 o 4 14 10 1189.36 1097.08 23.44 o 5 14 10 3901.87 3673.68 92.73 o 6 14 10 452.51 474.31 18.15 o 7 14 10 2551.59 2224.48 94.93 o 8 14 10 33.39 73.75 19.51 o 1 15 10 16.64 37.65 16.10 o 2 15 10 0.46 62.44 23.04 o 3 15 10 57.10 93.43 17.87 o 4 15 10 19.14 45.95 16.96 o 5 15 10 2.19 22.98 15.20 o 6 15 10 12.58 0.02 14.67 o 7 15 10 42.74 57.23 24.47 o 0 16 10 848.06 617.13 33.73 o 1 16 10 2168.74 1630.09 60.10 o 2 16 10 428.65 441.67 23.37 o 3 16 10 4106.72 3973.66 67.68 o 4 16 10 95.94 232.19 15.69 o 5 16 10 3684.66 3894.29 75.72 o 1 17 10 48.80 52.77 21.97 o 2 17 10 117.96 191.16 23.75 o 1 1 11 159.04 142.73 21.91 o 2 1 11 1632.36 1443.51 36.04 o 3 1 11 648.58 578.38 25.03 o 4 1 11 705.19 580.27 20.80 o 5 1 11 85.58 110.75 14.07 o 6 1 11 724.71 787.15 20.11 o 7 1 11 1260.23 1160.82 23.71 o 8 1 11 130.40 121.18 11.08 o 9 1 11 1137.88 1085.79 17.24 o 10 1 11 2551.38 2434.02 26.20 o 11 1 11 299.20 321.63 25.19 o 12 1 11 1861.93 1625.72 38.78 o 13 1 11 142.23 160.69 15.71 o 14 1 11 414.32 394.14 28.70 o 0 2 11 75.55 137.67 32.91 o 1 2 11 21999.98 23068.76 296.04 o 2 2 11 101.30 64.05 18.94 o 3 2 11 58578.79 60454.19 699.02 o 4 2 11 106.19 191.54 15.19 o 5 2 11 36126.30 36001.24 476.80 o 6 2 11 107.27 138.74 12.99 o 7 2 11 7644.57 7312.95 59.71 o 8 2 11 138.71 163.86 12.49 o 9 2 11 6350.30 6851.23 65.03 o 10 2 11 6.37 16.53 12.15 o 11 2 11 6510.07 6909.76 86.03 o 12 2 11 14.91 40.10 16.72 o 13 2 11 5044.67 4361.16 118.81 o 14 2 11 253.17 234.64 14.12 o 1 3 11 208.77 134.30 16.99 o 2 3 11 2.31 12.51 17.42 o 3 3 11 5359.09 4728.52 65.63 o 4 3 11 2.67 29.97 14.30 o 5 3 11 63.52 55.41 16.51 o 6 3 11 44.36 86.62 13.03 o 7 3 11 468.17 562.55 18.15 o 8 3 11 191.70 229.60 12.94 o 9 3 11 20.36 24.50 12.11 o 10 3 11 744.68 604.92 17.48 o 11 3 11 93.03 66.76 15.39 o 12 3 11 71.98 3.73 16.34 o 13 3 11 3.29 47.88 17.62 o 14 3 11 3.28 31.59 13.92 o 0 4 11 44427.45 40740.45 1066.94 o 1 4 11 105.80 70.22 16.69 o 2 4 11 14860.00 14382.29 181.76 o 3 4 11 1290.83 1080.95 22.37 o 4 4 11 278.17 358.11 15.95 o 5 4 11 1673.06 1781.51 28.39 o 6 4 11 3201.93 3945.61 37.43 o 7 4 11 1061.10 1121.25 18.27 o 8 4 11 5569.34 5112.23 47.60 o 9 4 11 81.46 70.99 15.24 o 10 4 11 2153.51 2165.64 37.19 o 11 4 11 31.79 52.24 14.40 o 12 4 11 359.78 374.43 17.38 o 13 4 11 16.48 4.64 14.29 o 1 5 11 12.11 82.02 15.56 o 2 5 11 918.70 1200.19 22.34 o 3 5 11 91.06 94.78 13.38 o 4 5 11 499.49 595.34 18.16 o 5 5 11 126.85 127.46 12.60 o 6 5 11 476.89 527.65 15.46 o 7 5 11 728.89 650.12 17.91 o 8 5 11 870.76 824.39 25.55 o 9 5 11 539.93 522.11 17.95 o 10 5 11 1143.89 1113.44 36.02 o 11 5 11 413.42 546.32 20.74 o 12 5 11 495.45 441.12 17.37 o 13 5 11 599.27 618.58 32.31 o 0 6 11 3513.10 3051.99 87.83 o 1 6 11 9953.34 9556.81 135.65 o 2 6 11 2803.08 3155.02 48.41 o 3 6 11 6375.19 6500.12 97.85 o 4 6 11 24.95 12.47 12.99 o 5 6 11 2851.94 2936.59 45.04 o 6 6 11 819.05 736.98 17.89 o 7 6 11 5612.29 5214.62 57.92 o 8 6 11 1200.78 1389.52 25.53 o 9 6 11 6563.65 6362.93 76.14 o 10 6 11 922.78 676.84 18.29 o 11 6 11 3338.68 3299.50 106.37 o 12 6 11 281.36 301.82 17.52 o 13 6 11 1678.75 1540.80 44.52 o 1 7 11 924.40 920.34 24.75 o 2 7 11 105.45 148.08 15.80 o 3 7 11 975.98 976.55 23.41 o 4 7 11 3.94 10.59 13.59 o 5 7 11 953.85 876.34 18.90 o 6 7 11 151.35 154.56 14.36 o 7 7 11 1570.26 1504.20 40.46 o 8 7 11 25.28 90.76 15.21 o 9 7 11 171.27 199.80 16.20 o 10 7 11 23.88 22.58 14.80 o 11 7 11 27.22 29.66 16.79 o 12 7 11 216.43 214.93 18.59 o 13 7 11 576.27 639.17 26.70 o 0 8 11 13424.49 14686.72 262.24 o 1 8 11 2116.07 2133.70 51.75 o 2 8 11 9227.59 8818.22 119.11 o 3 8 11 293.85 306.15 29.79 o 4 8 11 4542.58 4037.28 76.10 o 5 8 11 412.81 359.97 15.53 o 6 8 11 7558.40 7864.13 83.31 o 7 8 11 925.70 982.94 22.29 o 8 8 11 6293.08 6549.22 90.50 o 9 8 11 194.05 275.79 16.82 o 10 8 11 3452.05 2788.16 67.58 o 11 8 11 13.34 17.24 23.49 o 12 8 11 1997.75 1714.25 61.98 o 1 9 11 2.25 7.88 22.13 o 2 9 11 243.53 512.33 22.66 o 3 9 11 62.81 50.53 14.29 o 4 9 11 3.31 3.85 15.57 o 5 9 11 218.94 339.10 16.08 o 6 9 11 1050.40 1375.92 44.32 o 7 9 11 338.07 247.12 17.09 o 8 9 11 460.12 356.58 19.46 o 9 9 11 51.14 -0.95 17.69 o 10 9 11 31.56 23.27 19.07 o 11 9 11 94.44 63.93 18.90 o 12 9 11 43.80 106.84 21.62 o 0 10 11 4544.34 3370.38 117.00 o 1 10 11 2704.10 3227.34 63.54 o 2 10 11 3678.15 3517.15 104.64 o 3 10 11 467.19 345.21 16.53 o 4 10 11 2809.80 3125.37 60.11 o 5 10 11 385.18 409.67 17.75 o 6 10 11 2413.38 2328.25 51.85 o 7 10 11 782.03 904.44 35.99 o 8 10 11 2272.48 1843.49 31.75 o 9 10 11 744.29 814.55 37.45 o 10 10 11 1191.23 1194.09 35.10 o 11 10 11 195.53 178.98 17.98 o 1 11 11 17.43 35.25 22.79 o 2 11 11 83.35 79.97 15.86 o 3 11 11 123.81 271.41 16.53 o 4 11 11 265.28 318.08 15.80 o 5 11 11 600.36 394.44 15.40 o 6 11 11 304.94 199.21 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15 11 122.11 157.25 26.37 o 2 15 11 105.90 42.83 29.23 o 3 15 11 439.78 543.45 32.48 o 4 15 11 2.36 13.68 23.33 o 5 15 11 231.21 173.36 23.19 o 6 15 11 166.89 86.02 19.04 o 0 16 11 2253.93 1964.86 107.47 o 1 16 11 323.91 441.86 26.27 o 2 16 11 2297.67 1777.71 100.30 o 3 16 11 656.57 607.77 25.88 o 4 16 11 2118.85 2204.97 115.61 o 0 0 12 26456.06 32124.22 952.92 o 1 0 12 260.50 99.76 23.98 o 2 0 12 23872.07 23070.54 482.05 o 3 0 12 390.76 115.15 25.81 o 4 0 12 32555.09 31005.62 666.82 o 5 0 12 72.29 56.82 25.65 o 6 0 12 9518.46 9107.15 138.02 o 7 0 12 552.45 431.65 33.05 o 8 0 12 12834.10 13311.09 149.55 o 9 0 12 194.35 159.57 17.25 o 10 0 12 9486.63 9985.25 120.20 o 11 0 12 0.73 42.86 14.79 o 12 0 12 5534.82 5183.97 109.15 o 13 0 12 90.13 85.79 27.08 o 14 0 12 2350.59 2158.42 92.68 o 1 1 12 328.14 296.45 17.61 o 2 1 12 23.83 39.78 16.84 o 3 1 12 202.78 205.59 16.66 o 4 1 12 24.71 31.85 14.53 o 5 1 12 43.10 90.98 13.97 o 6 1 12 10.59 112.48 17.77 o 7 1 12 779.98 869.73 15.56 o 8 1 12 374.52 384.80 15.95 o 9 1 12 623.22 473.83 13.64 o 10 1 12 325.26 327.40 13.55 o 11 1 12 352.61 325.99 16.86 o 12 1 12 81.02 133.55 17.24 o 13 1 12 77.74 51.46 17.01 o 14 1 12 37.66 71.96 14.50 o 0 2 12 2921.14 2671.00 53.15 o 1 2 12 514.30 651.40 18.48 o 2 2 12 110.37 195.27 14.73 o 3 2 12 39.77 78.24 14.57 o 4 2 12 380.20 276.22 14.98 o 5 2 12 123.52 47.57 12.73 o 6 2 12 155.67 155.01 12.45 o 7 2 12 1594.22 1496.15 21.07 o 8 2 12 292.30 358.30 14.11 o 9 2 12 920.50 1055.89 17.75 o 10 2 12 0.50 35.07 12.85 o 11 2 12 337.88 325.99 14.42 o 12 2 12 8.55 9.66 13.34 o 13 2 12 130.17 114.21 15.08 o 14 2 12 0.93 32.69 21.28 o 1 3 12 339.07 367.46 16.54 o 2 3 12 320.17 371.75 16.74 o 3 3 12 603.54 494.42 17.17 o 4 3 12 303.07 126.33 14.83 o 5 3 12 521.30 492.61 14.70 o 6 3 12 420.86 549.75 13.44 o 7 3 12 1516.91 1801.99 30.03 o 8 3 12 947.50 941.76 21.46 o 9 3 12 836.83 791.54 17.46 o 10 3 12 470.04 508.51 15.49 o 11 3 12 794.66 677.15 19.94 o 12 3 12 258.86 296.26 18.63 o 13 3 12 485.42 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146.51 123.00 17.08 o 2 8 23 1509.67 1420.06 30.86 o 3 8 23 251.76 334.42 17.57 o 4 8 23 1014.79 1306.29 28.34 o 5 8 23 48.79 113.15 15.92 o 1 9 23 49.47 121.12 14.12 o 2 9 23 35.85 53.85 16.63 o 3 9 23 102.45 150.91 15.36 o 0 0 24 610.70 515.97 149.75 o 1 0 24 311.72 365.90 37.67 o 2 0 24 1736.22 2097.54 89.67 o 3 0 24 110.23 211.59 37.24 o 4 0 24 5890.01 5992.50 119.75 o 5 0 24 239.72 361.74 38.92 o 6 0 24 2645.88 2306.34 67.52 o 7 0 24 2.48 1.73 22.93 o 1 1 24 110.45 91.55 16.50 o 2 1 24 38.69 73.38 15.45 o 3 1 24 357.42 332.59 16.94 o 4 1 24 2.51 64.96 17.24 o 5 1 24 0.77 3.74 17.08 o 6 1 24 47.84 83.45 14.93 o 7 1 24 2.61 20.78 16.54 o 0 2 24 4.79 -31.33 31.33 o 1 2 24 434.62 561.38 21.36 o 2 2 24 17.47 26.48 17.99 o 3 2 24 4.85 19.40 17.88 o 4 2 24 522.19 514.25 22.30 o 5 2 24 17.18 0.86 16.73 o 6 2 24 77.09 77.33 17.70 o 7 2 24 148.17 145.99 16.60 o 1 3 24 336.98 229.96 17.44 o 2 3 24 380.40 456.32 19.13 o 3 3 24 1044.20 880.13 23.61 o 4 3 24 4.63 28.91 17.74 o 5 3 24 4.56 14.19 19.27 o 6 3 24 306.34 328.13 18.48 o 7 3 24 3.38 24.97 19.81 o 0 4 24 590.74 771.62 49.31 o 1 4 24 12.71 11.68 21.37 o 2 4 24 998.71 1211.90 30.27 o 3 4 24 2.12 30.34 17.43 o 4 4 24 1454.19 1292.67 27.72 o 5 4 24 1.96 59.63 15.85 o 6 4 24 1171.06 931.81 30.59 o 1 5 24 44.48 105.23 17.80 o 2 5 24 373.58 196.36 18.02 o 3 5 24 159.33 348.95 21.88 o 4 5 24 0.42 28.63 19.94 o 5 5 24 11.59 29.27 27.23 o 6 5 24 310.00 141.46 21.92 o 0 6 24 9.82 33.60 24.78 o 1 6 24 1855.91 1606.52 30.91 o 2 6 24 119.74 74.93 15.91 o 3 6 24 485.54 438.07 19.83 o 4 6 24 412.68 560.82 24.91 o 5 6 24 255.15 405.40 17.64 o 1 7 24 17.03 61.16 14.66 o 2 7 24 34.48 103.11 15.31 o 3 7 24 48.52 34.23 15.37 o 4 7 24 70.35 86.06 15.04 o 0 8 24 1050.98 1035.21 38.57 o 1 8 24 934.27 694.17 18.71 o 2 8 24 477.59 401.35 19.47 o 3 8 24 22.33 37.72 14.95 o 1 1 25 26.30 42.36 16.17 o 2 1 25 204.39 183.48 16.24 o 3 1 25 22.79 76.61 15.88 o 4 1 25 34.04 54.82 16.67 o 5 1 25 22.60 14.67 15.72 o 6 1 25 2.70 16.44 15.29 o 0 2 25 85.41 174.08 29.34 o 1 2 25 842.79 935.30 27.33 o 2 2 25 5.84 42.91 16.00 o 3 2 25 1740.05 2020.88 41.71 o 4 2 25 20.82 56.85 14.52 o 5 2 25 1646.78 1294.33 27.79 o 6 2 25 23.99 104.91 14.57 o 1 3 25 23.11 13.90 17.34 o 2 3 25 15.90 36.35 16.04 o 3 3 25 3.69 49.67 15.99 o 4 3 25 7.96 3.46 18.31 o 5 3 25 9.16 29.68 14.41 o 0 4 25 855.03 1175.03 37.38 o 1 4 25 2.04 1.30 18.41 o 2 4 25 406.43 377.56 19.03 o 3 4 25 105.13 61.70 16.85 o 4 4 25 108.55 57.93 18.28 o 5 4 25 99.41 119.75 14.90 o 1 5 25 5.12 57.13 21.54 o 2 5 25 29.75 13.52 18.09 o 3 5 25 0.27 25.18 18.41 o 4 5 25 11.67 19.30 19.83 o 0 6 25 181.47 112.86 23.45 o 1 6 25 950.97 1098.30 28.10 o 2 6 25 85.39 97.61 15.56 o 3 6 25 723.29 635.16 27.12 o 1 7 25 43.95 48.81 12.67 o 0 0 26 2002.86 1965.30 100.35 o 1 0 26 14.15 12.75 19.88 o 2 0 26 1888.17 2063.34 64.91 o 3 0 26 50.48 62.41 22.55 o 4 0 26 550.74 588.00 35.12 o 1 1 26 0.18 9.54 13.12 o 2 1 26 51.50 72.31 13.42 o 3 1 26 19.07 8.57 13.86 o 4 1 26 17.24 12.82 14.99 o 0 2 26 45.59 177.57 25.72 o 1 2 26 60.18 81.08 16.85 o 2 2 26 52.59 54.92 15.60 o 3 2 26 118.59 96.34 16.97 o 4 2 26 16.18 34.12 15.25 o 1 3 26 3.50 33.57 16.78 o 2 3 26 107.81 65.11 17.93 o 3 3 26 36.54 91.25 15.38 o 0 4 26 1166.36 1217.18 35.30 o 1 4 26 11.98 7.36 19.03 o 2 4 26 908.63 943.78 28.83 o 3 4 26 11.16 -0.67 16.69 o 1 5 26 19.63 47.44 23.40 o 2 5 26 44.69 32.61 19.18 o 1 1 27 82.58 185.37 16.52 o 2 1 27 257.45 194.69 14.22 o 0 2 27 135.39 273.04 46.92 o 1 2 27 2186.57 1884.61 44.76 o