Crystallography Open Database

Information card for entry 7717065

Preview

Coordinates	7717065.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H36 Co Mo6 O25 S6
Calculated formula	C12 H36 Co Mo6 O25 S6
Title of publication	Polyoxometalate-supported transition metal complexes for the oxidative cross-coupling of amines and alcohols.
Authors of publication	Pardiwala, Ankita; Desai, Meghal A.; Jangir, Ritambhara
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	42
Pages of publication	17207 - 17220
a	8.6329 ± 0.0009 Å
b	9.2575 ± 0.0009 Å
c	12.2531 ± 0.0013 Å
α	94.763 ± 0.004°
β	93.152 ± 0.004°
γ	91.312 ± 0.004°
Cell volume	974.03 ± 0.17 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0578
Residual factor for significantly intense reflections	0.0558
Weighted residual factors for significantly intense reflections	0.138
Weighted residual factors for all reflections included in the refinement	0.1404
Goodness-of-fit parameter for all reflections included in the refinement	1.236
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
296535 (current)	2024-12-06	cif/ Updating files of 7717064, 7717065, 7717066 Original log message: Adding full bibliography for 7717064--7717066.cif.	7717065.cif
294836	2024-09-21	cif/ Adding structures of 7717064, 7717065, 7717066 via cif-deposit CGI script.	7717065.cif