Crystallography Open Database

Information card for entry 7718324

Preview

Coordinates	7718324.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H22 Si2
Calculated formula	C26 H22 Si2
Title of publication	Synthesis and redox behavior of Si-Si dimeric 9-methylsilafluorene.
Authors of publication	Wentz, Kelsie E.; Molino, Andrew; Jiang, George Q.; Siegler, Maxime A.; Wilson, David J. D.; Thoi, V. Sara; Klausen, Rebekka S.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2025
Journal volume	54
Journal issue	15
Pages of publication	6167 - 6173
a	18.4395 ± 0.0008 Å
b	14.6169 ± 0.0005 Å
c	17.3824 ± 0.0007 Å
α	90°
β	112.872 ± 0.005°
γ	90°
Cell volume	4316.7 ± 0.3 Å³
Cell temperature	110 ± 2 K
Ambient diffraction temperature	110 ± 2 K
Number of distinct elements	3
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0572
Residual factor for significantly intense reflections	0.0425
Weighted residual factors for significantly intense reflections	0.1005
Weighted residual factors for all reflections included in the refinement	0.1081
Goodness-of-fit parameter for all reflections included in the refinement	1.022
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
300914 (current)	2025-07-06	cif/ Updating files of 7718324 Original log message: Adding full bibliography for 7718324.cif.	7718324.cif
298452	2025-03-15	cif/ Adding structures of 7718324 via cif-deposit CGI script.	7718324.cif