#------------------------------------------------------------------------------ #$Date: 2022-06-23 12:36:15 +0300 (Thu, 23 Jun 2022) $ #$Revision: 276190 $ #$URL: file:///home/coder/svn-repositories/cod/cif/8/10/54/8105484.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_8105484 loop_ _publ_author_name 'Guerrab, Walid' 'Mague, Joel T.' 'Ramli, Youssef' _publ_section_title ; Synthesis and crystal structure of 3-octyl-5,5-diphenylimidazolidine-2,4-dione, C23H28N2O2 ; _journal_issue 6 _journal_name_full 'Zeitschrift f\"ur Kristallographie - New Crystal Structures' _journal_page_first 1425 _journal_page_last 1427 _journal_paper_doi 10.1515/ncrs-2020-0347 _journal_volume 235 _journal_year 2020 _chemical_formula_moiety 'C23 H28 N2 O2' _chemical_formula_sum 'C23 H28 N2 O2' _chemical_formula_weight 364.47 _chemical_name_systematic ; 3-octyl-5,5-diphenylimidazolidine-2,4-dione ; _space_group_crystal_system orthorhombic _space_group_IT_number 61 _space_group_name_Hall '-P 2ac 2ab' _space_group_name_H-M_alt 'P b c a' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 10.713(2) _cell_length_b 15.689(3) _cell_length_c 24.485(5) _cell_measurement_reflns_used 9175 _cell_measurement_temperature 120(2) _cell_measurement_theta_max 26.6320 _cell_measurement_theta_min 2.4478 _cell_volume 4115.3(14) _computing_cell_refinement 'SAINT [1]' _computing_data_collection 'APEX3 [1]' _computing_data_reduction 'SAINT [1]' _computing_molecular_graphics 'DIAMOND [4]' _computing_publication_material 'SHELXTL [1]' _computing_structure_refinement 'SHELXL-2018/1 [3]' _computing_structure_solution 'SHELXT [2]' _diffrn_ambient_temperature 120(2) _diffrn_detector_area_resol_mean 8.3333 _diffrn_measured_fraction_theta_full 0.995 _diffrn_measured_fraction_theta_max 0.988 _diffrn_measurement_device_type 'Bruker Smart APEX CCD' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0450 _diffrn_reflns_av_unetI/netI 0.0420 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.988 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 32 _diffrn_reflns_limit_l_min -32 _diffrn_reflns_number 37198 _diffrn_reflns_point_group_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.988 _diffrn_reflns_theta_full 28.500 _diffrn_reflns_theta_max 28.834 _diffrn_reflns_theta_min 1.663 _diffrn_source 'fine-focus sealed tube' _exptl_absorpt_coefficient_mu 0.075 _exptl_absorpt_correction_T_max 0.99 _exptl_absorpt_correction_T_min 0.86 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS [5]' _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.177 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 1568 _exptl_crystal_size_max 0.268 _exptl_crystal_size_mid 0.212 _exptl_crystal_size_min 0.173 _exptl_transmission_factor_max 0.928 _exptl_transmission_factor_min 0.808 _refine_diff_density_max 0.593 _refine_diff_density_min -0.388 _refine_diff_density_rms 0.052 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.079 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 325 _refine_ls_number_reflns 5321 _refine_ls_number_restraints 7 _refine_ls_restrained_S_all 1.099 _refine_ls_R_factor_all 0.0819 _refine_ls_R_factor_gt 0.0581 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0901P)^2^+1.1449P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1584 _refine_ls_wR_factor_ref 0.1734 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 3818 _reflns_number_total 5321 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file suppl_ncrs-2020-0347_suppl.cif _cod_data_source_block JTM1029_0m_a _cod_original_cell_volume 4115.2(14) _cod_database_code 8105484 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.980 _shelx_estimated_absorpt_t_max 0.987 _shelx_res_file ; TITL JTM1029_0m_a.res in Pbca JTM1029_0m_a.res created by SHELXL-2018/1 at 09:21:19 on 11-Dec-2018 REM Old TITL JTM1029_0m in Pbca REM SHELXT solution in Pbca REM R1 0.183, Rweak 0.005, Alpha 0.018, Orientation as input REM Formula found by SHELXT: C23 N O3 CELL 0.71073 10.7126 15.6893 24.4848 90.000 90.000 90.000 ZERR 8.000 0.0022 0.0032 0.0049 0.000 0.000 0.000 LATT 1 SYMM 1/2-X, -Y, 1/2+Z SYMM -X, 1/2+Y, 1/2-Z SYMM 1/2+X, 1/2-Y, -Z SFAC C H N O UNIT 184 224 16 16 TEMP -153 SIZE 0.173 0.212 0.268 L.S. 5 BOND $H EXYZ C7 C7A EADP C7 C7A EADP C8 C8A EADP C9 C9A EADP C10 C10A EADP C11 C11A LIST 4 EQIV $1 -x+1, -y+1, -z+1 HTAB N2 O2_$1 MPLA C12 > C17 MPLA N1 > C3 MPLA C18 > C23 CONF ACTA 57 FMAP 2 PLAN 5 WGHT 0.090100 1.144900 FVAR 0.34821 0.68417 O1 4 0.335314 0.680219 0.339350 11.00000 0.04591 0.03852 = 0.03099 0.00977 -0.01507 -0.00317 O2 4 0.336004 0.481478 0.475183 11.00000 0.02437 0.03366 = 0.03469 0.01063 -0.00232 -0.00374 N1 3 0.307845 0.573155 0.401911 11.00000 0.02496 0.02918 = 0.02368 0.00203 -0.00523 -0.00038 N2 3 0.480080 0.584438 0.451338 11.00000 0.02180 0.02676 = 0.02346 0.00605 -0.00368 -0.00116 H2 2 0.538909 0.566002 0.476021 11.00000 0.04499 C1 1 0.498553 0.645481 0.407079 11.00000 0.02766 0.02257 = 0.02039 0.00248 -0.00128 -0.00002 C2 1 0.371591 0.637956 0.377493 11.00000 0.03125 0.02744 = 0.02330 -0.00012 -0.00480 0.00067 C3 1 0.373328 0.539812 0.446297 11.00000 0.02254 0.02578 = 0.02410 0.00119 -0.00028 0.00251 C4 1 0.189871 0.538764 0.380852 11.00000 0.02306 0.03657 = 0.03147 -0.00011 -0.00658 -0.00075 H4A 2 0.139410 0.522808 0.412886 11.00000 0.03723 H4B 2 0.147124 0.585640 0.364003 11.00000 0.03834 C5 1 0.211262 0.466561 0.340900 11.00000 0.02863 0.03576 = 0.03483 -0.00301 -0.00603 0.00020 H5A 2 0.245413 0.415944 0.360721 11.00000 0.03353 H5B 2 0.270189 0.485359 0.314027 11.00000 0.03728 C6 1 0.091864 0.441422 0.311861 11.00000 0.03931 0.03991 = 0.04538 -0.00377 -0.01664 0.00069 H6A 2 0.025284 0.421082 0.341140 11.00000 0.06683 H6B 2 0.058901 0.495011 0.296667 11.00000 0.07095 PART 1 C7 1 0.106925 0.375753 0.267365 21.00000 0.06481 0.03550 = 0.04277 -0.00136 -0.01918 0.00103 AFIX 23 H7A 2 0.140811 0.322192 0.282764 21.00000 -1.20000 H7B 2 0.165522 0.396798 0.239156 21.00000 -1.20000 AFIX 0 C8 1 -0.023458 0.359468 0.241782 21.00000 0.05869 0.03995 = 0.02891 0.00210 -0.01351 -0.00108 AFIX 23 H8A 2 -0.080554 0.340867 0.271257 21.00000 -1.20000 H8B 2 -0.055531 0.414372 0.227633 21.00000 -1.20000 AFIX 0 C9 1 -0.030180 0.294960 0.196416 21.00000 0.03771 0.04891 = 0.03963 -0.00501 -0.00384 -0.00638 AFIX 23 H9A 2 -0.118996 0.282916 0.188335 21.00000 -1.20000 H9B 2 0.008621 0.241203 0.209069 21.00000 -1.20000 AFIX 0 C10 1 0.033964 0.323154 0.144130 21.00000 0.04281 0.06039 = 0.03945 -0.00318 -0.00302 -0.00952 AFIX 23 H10A 2 0.002819 0.380240 0.133587 21.00000 -1.20000 H10B 2 0.124932 0.327704 0.150632 21.00000 -1.20000 AFIX 0 C11 1 0.010471 0.261319 0.098092 21.00000 0.06427 0.08364 = 0.04546 -0.01876 0.00910 -0.01105 AFIX 33 H11A 2 0.053012 0.281315 0.065056 21.00000 -1.50000 H11B 2 0.042580 0.204985 0.108171 21.00000 -1.50000 H11C 2 -0.079444 0.257482 0.091139 21.00000 -1.50000 AFIX 0 PART 2 SAME 0.003 C7 > C11 C7A 1 0.106925 0.375753 0.267365 -21.00000 0.06481 0.03550 = 0.04277 -0.00136 -0.01918 0.00103 AFIX 23 H7C 2 0.105359 0.319574 0.285764 -21.00000 -1.20000 H7D 2 0.192592 0.383068 0.252941 -21.00000 -1.20000 AFIX 0 C8A 1 0.022539 0.367554 0.217922 -21.00000 0.05869 0.03995 = 0.02891 0.00210 -0.01351 -0.00108 AFIX 23 H8C 2 -0.062119 0.352740 0.231067 -21.00000 -1.20000 H8D 2 0.016812 0.424293 0.200408 -21.00000 -1.20000 AFIX 0 C9A 1 0.058097 0.304322 0.174852 -21.00000 0.03771 0.04891 = 0.03963 -0.00501 -0.00384 -0.00638 AFIX 23 H9C 2 0.073624 0.248257 0.192118 -21.00000 -1.20000 H9D 2 0.136410 0.322955 0.157012 -21.00000 -1.20000 AFIX 0 C10A 1 -0.043530 0.295096 0.132000 -21.00000 0.04281 0.06039 = 0.03945 -0.00318 -0.00302 -0.00952 AFIX 23 H10C 2 -0.117489 0.267700 0.148721 -21.00000 -1.20000 H10D 2 -0.068744 0.352372 0.119108 -21.00000 -1.20000 AFIX 0 C11A 1 -0.000852 0.242793 0.084043 -21.00000 0.06427 0.08364 = 0.04546 -0.01876 0.00910 -0.01105 AFIX 33 H11D 2 -0.068781 0.238320 0.057389 -21.00000 -1.50000 H11E 2 0.071382 0.270304 0.066943 -21.00000 -1.50000 H11F 2 0.022657 0.185667 0.096544 -21.00000 -1.50000 AFIX 0 PART 0 C12 1 0.520787 0.735139 0.429658 11.00000 0.02678 0.02424 = 0.02094 0.00142 -0.00165 0.00252 C13 1 0.421745 0.785530 0.446996 11.00000 0.02704 0.03121 = 0.03628 -0.00099 -0.00229 0.00456 H13 2 0.340540 0.764080 0.442671 11.00000 0.03531 C14 1 0.442978 0.865040 0.469292 11.00000 0.03718 0.03295 = 0.04697 -0.00717 -0.00121 0.01177 H14 2 0.374805 0.900711 0.480612 11.00000 0.05926 C15 1 0.564009 0.895379 0.474659 11.00000 0.04560 0.02838 = 0.05314 -0.01355 -0.00619 0.00481 H15 2 0.578949 0.953616 0.491602 11.00000 0.04396 C16 1 0.663707 0.845774 0.457776 11.00000 0.03349 0.03624 = 0.05895 -0.01521 -0.00489 -0.00127 H16 2 0.751237 0.867871 0.460220 11.00000 0.05261 C17 1 0.642062 0.765730 0.435506 11.00000 0.02825 0.03051 = 0.04206 -0.00973 -0.00118 0.00288 H17 2 0.711823 0.734002 0.422700 11.00000 0.04184 C18 1 0.600929 0.618214 0.367241 11.00000 0.03249 0.02795 = 0.02630 -0.00613 0.00490 -0.00420 C19 1 0.616412 0.663526 0.319053 11.00000 0.05165 0.05330 = 0.02814 0.00243 0.00865 -0.00004 H19 2 0.564616 0.709051 0.312055 11.00000 0.05784 C20 1 0.711217 0.642365 0.283005 11.00000 0.06764 0.07721 = 0.03097 -0.00523 0.01878 -0.01154 H20 2 0.720231 0.671808 0.253874 11.00000 0.07176 C21 1 0.790648 0.576583 0.294863 11.00000 0.05428 0.06790 = 0.05497 -0.02777 0.02882 -0.00849 H21 2 0.856549 0.563917 0.269300 11.00000 0.07600 C22 1 0.775748 0.530478 0.342211 11.00000 0.05377 0.04948 = 0.07768 -0.01376 0.02982 0.00788 H22 2 0.831863 0.483386 0.352977 11.00000 0.07137 C23 1 0.680257 0.551222 0.378666 11.00000 0.04169 0.03327 = 0.05149 -0.00115 0.01639 0.00421 H23 2 0.671259 0.517338 0.412824 11.00000 0.05051 HKLF 4 REM JTM1029_0m_a.res in Pbca REM R1 = 0.0581 for 3818 Fo > 4sig(Fo) and 0.0819 for all 5321 data REM 325 parameters refined using 7 restraints END WGHT 0.0899 1.1457 REM Highest difference peak 0.593, deepest hole -0.388, 1-sigma level 0.052 Q1 1 -0.0085 0.3305 0.0942 11.00000 0.05 0.59 Q2 1 0.0550 0.3689 0.2330 11.00000 0.05 0.56 Q3 1 0.5075 0.6900 0.4171 11.00000 0.05 0.33 Q4 1 0.4369 0.6438 0.3919 11.00000 0.05 0.33 Q5 1 -0.0337 0.2538 0.1404 11.00000 0.05 0.32 ; _shelx_hkl_file ; -1 0 0 0.00 0.20 -1 0 0 0.60 0.20 -1 0 0 0.00 0.10 -2 0 0 907.11 73.99 -2 0 0 974.60 73.99 -2 0 0 985.80 73.99 -3 0 0 0.30 0.30 -3 0 0 1.50 0.40 -3 0 0 0.20 0.40 -4 0 0 74.99 5.70 -4 0 0 71.49 5.80 -4 0 0 71.29 5.80 -5 0 0 -0.90 0.50 -5 0 0 -0.40 0.60 -5 0 0 -0.20 0.60 -6 0 0 1559.04 121.99 -6 0 0 1554.94 121.99 -6 0 0 1606.24 121.89 -7 0 0 -0.60 0.90 -7 0 0 -0.50 0.80 7 0 0 0.80 0.70 -8 0 0 17.60 2.00 8 0 0 17.30 2.00 8 0 0 18.10 1.80 9 0 0 -0.40 1.20 -9 0 0 -1.40 1.10 -10 0 0 53.19 4.90 10 0 0 57.19 5.00 11 0 0 -1.10 1.60 -11 0 0 -0.70 1.70 -12 0 0 1.10 1.80 12 0 0 -2.00 1.90 -13 0 0 -1.40 2.10 13 0 0 0.00 2.60 14 0 0 -0.50 2.90 0 1 0 0.30 0.10 0 1 0 -0.20 0.10 0 -1 0 0.20 0.10 -1 1 0 2.20 0.30 -1 -1 0 3.10 0.30 -1 1 0 3.10 0.30 -1 1 0 1.90 0.30 1 1 0 2.60 0.30 2 1 0 82.39 6.40 -2 1 0 84.19 6.40 -2 -1 0 80.99 6.40 -2 1 0 81.09 6.30 2 1 0 82.09 6.30 -2 -1 0 77.49 6.40 -2 1 0 79.49 6.30 -3 -1 0 0.00 0.40 3 1 0 0.30 0.30 -3 1 0 -0.60 0.40 -3 -1 0 0.00 0.40 -3 1 0 0.00 0.40 -3 1 0 -0.30 0.40 -4 1 0 40.20 3.20 -4 1 0 40.10 3.20 4 1 0 36.40 3.10 -4 1 0 42.30 3.20 -4 -1 0 41.00 3.20 -4 -1 0 36.00 3.20 -5 -1 0 0.80 0.60 -5 -1 0 -0.30 0.70 -5 1 0 0.30 0.60 -5 1 0 -0.60 0.50 5 1 0 -0.30 0.40 -5 1 0 0.00 0.60 -6 1 0 11.00 1.30 -6 1 0 12.20 1.20 6 1 0 11.10 1.40 6 1 0 8.40 1.10 -6 1 0 10.00 1.20 -6 -1 0 11.60 1.30 -7 1 0 -0.30 0.80 -7 -1 0 0.00 0.80 -7 1 0 -0.30 0.90 7 1 0 -1.00 0.80 7 1 0 -0.70 0.70 -7 1 0 -0.40 0.90 -8 1 0 22.00 2.00 -8 -1 0 20.60 2.10 -8 1 0 18.00 2.20 -8 1 0 20.80 2.20 8 1 0 19.60 2.20 9 1 0 -1.20 1.40 -9 -1 0 -0.40 1.20 9 -1 0 1.70 1.40 -9 1 0 0.90 1.10 9 -1 0 0.40 1.20 -10 1 0 13.80 2.00 10 -1 0 17.20 2.30 10 1 0 13.40 2.10 -10 -1 0 13.10 2.00 -11 1 0 0.70 1.70 11 1 0 -2.50 1.60 11 -1 0 1.50 1.70 -11 -1 0 -3.30 1.70 12 -1 0 7.20 2.10 -12 -1 0 3.20 2.10 12 1 0 4.00 2.10 -12 1 0 3.70 2.00 -13 1 0 1.50 2.50 -13 -1 0 1.90 2.40 13 -1 0 0.00 2.30 13 1 0 -1.00 2.70 14 -1 0 7.80 3.00 14 1 0 3.00 3.00 0 -2 0 127.79 10.40 0 2 0 136.79 10.40 0 2 0 137.09 10.40 -1 2 0 0.10 0.20 1 -2 0 0.70 0.30 -1 2 0 0.10 0.30 1 2 0 0.80 0.20 -1 -2 0 -0.10 0.30 1 2 0 0.40 0.30 -2 2 0 8998.00 714.23 2 2 0 9277.97 714.23 2 2 0 9542.95 714.43 -2 2 0 9118.09 714.33 -2 2 0 8979.10 714.33 -2 -2 0 9461.25 714.43 3 2 0 -0.20 0.40 -3 -2 0 -0.40 0.40 -3 2 0 0.20 0.40 3 2 0 -0.10 0.20 -3 2 0 1.00 0.40 -3 2 0 0.30 0.40 -4 2 0 48.20 3.90 -4 -2 0 49.80 4.00 -4 2 0 51.59 4.00 4 2 0 49.70 3.90 -4 2 0 49.99 3.90 4 2 0 44.90 4.00 -5 2 0 -0.70 0.60 5 2 0 0.50 0.40 -5 2 0 1.20 0.70 -5 -2 0 -0.30 0.60 -5 2 0 0.60 0.60 5 2 0 0.90 0.70 6 2 0 0.90 0.80 6 2 0 0.00 0.50 -6 2 0 -0.10 0.80 -6 2 0 1.70 0.80 -6 2 0 0.90 0.70 -6 -2 0 -0.10 0.70 7 2 0 0.40 0.60 -7 2 0 -0.80 0.80 -7 -2 0 1.10 0.90 7 2 0 0.40 0.90 -7 2 0 0.20 0.80 -7 2 0 0.10 1.00 -8 2 0 148.29 11.60 -8 2 0 155.98 11.80 -8 -2 0 141.09 11.70 8 2 0 149.69 11.70 -8 2 0 142.79 11.70 -9 2 0 -0.30 1.30 9 2 0 0.40 1.30 -9 2 0 -1.20 1.10 -9 2 0 0.30 1.20 -9 -2 0 -1.60 1.30 10 -2 0 87.19 6.90 -10 2 0 84.19 6.90 -10 -2 0 82.39 6.90 10 2 0 74.29 7.00 -11 2 0 -0.60 1.80 11 -2 0 2.80 1.70 11 2 0 -0.60 1.70 -11 -2 0 1.50 1.60 -12 -2 0 5.30 2.20 -12 2 0 10.10 2.10 12 2 0 6.00 2.40 12 -2 0 10.80 2.40 -13 -2 0 3.20 2.50 13 -2 0 0.90 2.60 13 2 0 3.10 2.70 14 -2 0 -0.40 3.20 14 2 0 3.60 3.40 -14 -2 0 4.20 3.20 0 3 0 -0.40 0.30 0 -3 0 0.20 0.30 0 3 0 -0.20 0.30 -1 3 0 0.80 0.30 -1 -3 0 0.80 0.40 -1 3 0 -0.30 0.30 1 -3 0 -0.20 0.30 1 3 0 0.30 0.20 1 3 0 -0.10 0.30 2 3 0 554.14 42.30 -2 -3 0 552.44 42.30 2 -3 0 529.95 42.30 -2 3 0 544.65 42.30 2 3 0 559.24 42.30 -2 3 0 532.35 42.30 -3 -3 0 -0.70 0.50 -3 3 0 0.70 0.50 -3 3 0 0.40 0.40 3 3 0 0.20 0.20 -3 3 0 0.00 0.50 3 3 0 0.20 0.50 -4 -3 0 6.50 0.90 -4 3 0 8.00 0.90 4 3 0 8.40 0.90 -4 3 0 7.60 0.90 4 3 0 7.00 0.70 -4 3 0 8.00 1.00 -5 3 0 1.00 0.60 -5 3 0 -0.40 0.60 -5 3 0 -0.50 0.70 -5 -3 0 -0.80 0.70 5 3 0 -0.10 0.40 5 3 0 -0.10 0.70 -6 3 0 21.00 2.10 -6 3 0 25.00 2.20 6 3 0 22.70 1.90 -6 -3 0 25.10 2.20 -6 3 0 20.70 2.20 6 3 0 24.10 2.20 -7 3 0 -0.30 1.00 -7 3 0 -0.40 0.90 -7 3 0 -0.10 0.90 -7 -3 0 0.20 0.90 7 3 0 0.90 1.00 -8 3 0 1.20 1.10 -8 -3 0 1.20 1.00 8 3 0 2.80 1.20 -8 3 0 0.50 1.10 -8 3 0 3.40 1.30 -9 3 0 0.90 1.30 -9 -3 0 0.90 1.30 9 3 0 0.00 1.30 -9 3 0 2.10 1.20 -9 3 0 -1.00 1.20 10 -3 0 475.25 36.00 -10 -3 0 451.15 35.90 10 3 0 448.96 36.00 -10 3 0 448.16 35.90 -10 3 0 475.95 35.90 11 -3 0 -1.40 1.60 11 3 0 -0.70 1.70 -11 3 0 1.10 1.80 -11 -3 0 3.70 1.70 12 3 0 9.90 2.40 12 -3 0 11.50 2.50 -12 -3 0 9.50 2.30 -12 3 0 10.30 2.40 13 -3 0 -1.30 2.60 13 3 0 -0.50 2.40 -13 -3 0 2.80 2.50 14 3 0 -2.20 3.30 -14 -3 0 -0.90 3.10 0 4 0 607.44 47.60 0 4 0 618.84 47.50 0 -4 0 614.54 47.60 1 4 0 -0.10 0.40 1 4 0 0.40 0.30 -1 4 0 -0.10 0.30 1 -4 0 0.00 0.40 -1 -4 0 0.20 0.50 -1 4 0 0.10 0.40 2 4 0 971.90 77.49 2 -4 0 994.20 77.49 -2 -4 0 993.10 77.49 -2 4 0 1014.60 77.49 2 4 0 1022.50 77.49 -2 4 0 1005.10 77.49 3 -4 0 -0.70 0.50 -3 4 0 -0.60 0.40 -3 -4 0 2.30 0.60 -3 4 0 0.90 0.60 3 4 0 0.00 0.30 3 4 0 -0.40 0.50 -4 4 0 12.90 1.40 4 -4 0 13.90 1.40 4 4 0 15.40 1.50 -4 -4 0 11.30 1.40 -4 4 0 17.70 1.40 4 4 0 15.10 1.20 -5 4 0 0.10 0.60 -5 -4 0 -0.80 0.80 -5 4 0 0.10 0.70 -5 4 0 -1.30 0.70 5 4 0 0.10 0.30 5 4 0 0.10 0.70 -6 4 0 190.08 14.70 6 4 0 172.88 14.80 -6 -4 0 183.18 14.70 -6 4 0 189.78 14.70 -6 4 0 192.18 14.70 6 4 0 192.98 14.60 -7 4 0 0.10 1.00 -7 -4 0 0.00 0.90 -7 4 0 0.20 0.90 -7 4 0 0.10 0.90 7 4 0 0.30 1.00 -8 -4 0 19.70 2.10 -8 4 0 18.50 2.10 -8 4 0 20.50 2.10 -8 4 0 17.80 2.10 8 4 0 18.40 2.20 -9 4 0 -0.80 1.20 -9 -4 0 1.00 1.20 9 4 0 -1.50 1.30 -9 4 0 0.40 1.30 -9 4 0 1.00 1.40 -10 -4 0 13.00 2.10 10 4 0 8.20 2.00 -10 4 0 11.90 2.00 -10 4 0 12.60 2.00 -10 4 0 16.00 2.00 11 -4 0 -1.20 1.90 -11 -4 0 -0.60 1.80 11 4 0 -1.50 1.70 -11 4 0 0.40 1.80 12 4 0 0.20 2.10 -12 4 0 8.30 2.30 12 -4 0 2.70 2.30 -12 -4 0 4.90 2.00 -13 -4 0 1.80 2.60 13 4 0 -2.80 2.40 -14 -4 0 1.80 3.10 0 5 0 0.00 0.40 0 -5 0 0.70 0.50 0 5 0 0.00 0.40 -1 5 0 -0.30 0.50 -1 5 0 0.40 0.40 -1 -5 0 0.10 0.50 1 -5 0 -0.20 0.40 1 5 0 0.10 0.40 1 5 0 0.10 0.40 -2 5 0 0.40 0.50 2 -5 0 0.20 0.50 2 5 0 -0.10 0.50 -2 5 0 0.50 0.40 -2 -5 0 -0.80 0.50 2 5 0 0.30 0.30 3 5 0 0.20 0.30 -3 -5 0 1.00 0.60 3 -5 0 -0.50 0.50 -3 5 0 0.30 0.70 -3 5 0 -0.20 0.50 3 5 0 0.40 0.60 4 -5 0 0.60 0.70 -4 5 0 -0.10 0.50 -4 -5 0 1.10 0.70 -4 5 0 -0.20 0.70 4 5 0 1.20 0.30 4 5 0 -0.30 0.70 -5 -5 0 0.20 0.70 -5 5 0 0.00 0.70 -5 5 0 -0.20 0.60 5 -5 0 0.40 0.60 5 5 0 0.40 0.30 5 5 0 0.40 0.80 -6 5 0 39.50 3.60 6 -5 0 39.50 3.60 6 5 0 46.40 3.70 -6 5 0 42.90 3.60 -6 -5 0 42.40 3.70 -7 5 0 -0.40 1.00 -7 5 0 0.60 1.00 -7 5 0 0.90 1.00 -7 -5 0 -1.60 0.90 7 5 0 0.40 1.00 -8 5 0 482.05 38.30 -8 -5 0 467.35 38.30 -8 5 0 485.15 38.30 8 5 0 524.45 38.40 -8 5 0 501.45 38.30 -9 -5 0 1.10 1.30 -9 5 0 0.60 1.30 9 5 0 -1.30 1.30 -9 5 0 1.80 1.40 -9 5 0 -0.10 1.20 -10 -5 0 30.90 3.30 -10 5 0 35.10 3.30 -10 5 0 31.90 3.30 10 5 0 31.10 3.50 -10 5 0 33.10 3.30 -11 -5 0 -1.60 1.80 -11 5 0 0.10 1.80 -11 5 0 -1.00 3.00 11 5 0 0.20 1.80 11 -5 0 0.10 1.90 -12 -5 0 0.10 2.20 12 5 0 2.20 2.40 -13 -5 0 -2.30 2.60 13 5 0 1.10 2.50 -14 -5 0 -0.10 3.00 0 6 0 2.00 0.60 0 -6 0 0.40 0.50 0 6 0 2.10 0.50 -1 -6 0 0.00 0.60 1 6 0 0.20 0.40 -1 6 0 -0.20 0.50 -1 6 0 -0.10 0.40 1 -6 0 0.40 0.50 1 6 0 -0.70 0.50 -2 6 0 528.35 41.80 2 6 0 523.45 41.80 2 -6 0 544.85 41.80 -2 -6 0 538.85 41.80 2 6 0 536.55 41.70 -2 6 0 557.44 41.80 -3 6 0 0.70 0.70 -3 -6 0 0.50 0.70 -3 6 0 0.30 0.50 3 -6 0 0.00 0.60 3 6 0 0.00 0.40 3 6 0 -0.30 0.60 -4 6 0 347.87 26.60 -4 6 0 336.47 26.60 -4 -6 0 333.67 26.60 4 6 0 353.56 26.50 4 6 0 334.07 26.60 4 -6 0 340.07 26.60 5 -6 0 0.20 0.80 5 6 0 -0.30 0.80 -5 6 0 0.20 0.70 -5 6 0 -0.30 0.80 -5 -6 0 -0.50 0.80 5 6 0 0.00 0.30 -6 -6 0 48.90 4.40 -6 6 0 56.89 4.40 -6 6 0 57.79 4.50 6 6 0 49.90 4.50 6 -6 0 50.39 4.40 -7 6 0 0.50 1.10 -7 -6 0 0.70 1.00 7 -6 0 0.10 1.00 7 6 0 -0.10 1.10 -7 6 0 0.70 0.90 -8 -6 0 -1.00 1.30 -8 6 0 0.30 1.30 -8 6 0 -0.10 1.20 8 6 0 -1.70 1.20 8 -6 0 -0.30 1.20 -9 6 0 -0.30 1.30 9 -6 0 1.00 1.50 -9 6 0 1.70 1.50 9 6 0 0.10 1.40 -9 -6 0 -0.60 1.30 -10 6 0 74.89 6.50 10 -6 0 74.19 6.50 -10 -6 0 70.49 6.50 -10 6 0 72.99 6.40 10 6 0 83.09 6.60 -11 -6 0 1.40 1.60 11 6 0 1.10 1.90 -11 6 0 0.30 1.70 11 -6 0 -2.00 2.40 -12 -6 0 0.10 2.20 12 6 0 4.70 2.30 13 6 0 -0.60 2.70 -13 -6 0 -0.90 2.70 0 -7 0 0.70 0.60 0 7 0 0.90 0.50 0 7 0 0.10 0.60 -1 -7 0 -0.30 0.70 1 -7 0 -0.10 0.60 1 7 0 -0.40 0.60 1 7 0 -0.60 0.50 -1 7 0 0.30 0.50 -1 7 0 0.70 0.60 2 7 0 61.79 4.80 -2 7 0 65.29 4.80 2 7 0 58.79 4.90 -2 -7 0 52.49 4.90 -2 7 0 56.89 4.90 2 -7 0 61.59 4.90 3 7 0 0.40 0.50 -3 7 0 -0.50 0.70 3 7 0 0.60 0.80 3 -7 0 0.30 0.70 -3 -7 0 1.00 0.70 -3 7 0 0.50 0.60 -4 7 0 170.38 12.50 4 7 0 159.68 12.60 4 -7 0 154.28 12.50 4 7 0 160.08 12.40 -4 7 0 152.68 12.60 -4 -7 0 155.88 12.60 -5 7 0 0.60 0.70 -5 -7 0 -0.20 0.80 -5 7 0 -1.70 0.90 5 7 0 -0.30 0.90 5 -7 0 -0.70 0.80 -6 -7 0 2.40 1.10 6 -7 0 3.20 1.10 -6 7 0 2.80 1.00 6 7 0 0.80 1.10 -6 7 0 5.90 1.10 7 -7 0 -1.00 1.00 -7 7 0 -1.40 1.10 -7 -7 0 1.10 1.30 -7 7 0 -0.70 1.00 7 7 0 0.90 1.20 8 -7 0 47.10 4.10 -8 7 0 48.30 4.10 8 7 0 44.20 4.20 -8 7 0 40.30 4.10 -8 -7 0 45.80 4.10 -9 -7 0 -1.70 1.30 9 -7 0 0.30 1.50 -9 7 0 0.30 1.60 9 7 0 -1.60 1.40 -9 7 0 0.50 1.40 10 7 0 58.39 5.00 -10 7 0 45.80 5.00 10 -7 0 55.29 5.00 -10 -7 0 52.29 5.00 11 7 0 1.00 2.00 -11 7 0 -0.10 2.00 -11 -7 0 0.00 1.70 -12 -7 0 42.40 4.10 12 7 0 31.30 4.10 13 7 0 2.80 3.20 -13 -7 0 0.30 2.60 0 8 0 51.89 4.50 0 -8 0 57.39 4.50 0 8 0 56.59 4.50 1 8 0 -0.20 0.60 1 -8 0 -0.40 0.70 -1 8 0 0.40 0.70 1 8 0 0.30 0.60 -1 -8 0 -0.80 0.70 -1 8 0 0.60 0.60 2 8 0 528.35 40.10 -2 8 0 536.85 40.00 -2 8 0 498.85 40.10 -2 -8 0 494.55 40.10 2 -8 0 513.55 40.10 2 8 0 519.85 40.00 3 8 0 -0.20 0.60 -3 8 0 -0.50 0.80 3 -8 0 0.80 0.80 -3 8 0 0.00 0.60 -3 -8 0 0.70 0.80 3 8 0 0.90 0.90 4 8 0 -0.80 0.80 4 -8 0 -0.10 0.90 -4 8 0 0.50 0.80 4 8 0 -0.40 0.50 -4 8 0 0.50 0.60 -4 -8 0 1.00 0.90 5 -8 0 1.30 0.90 -5 -8 0 -0.10 0.90 -5 8 0 -0.30 0.80 5 8 0 0.60 1.00 -5 8 0 -0.30 0.90 -6 -8 0 15.30 1.70 -6 8 0 11.90 1.60 -6 8 0 13.00 1.50 6 8 0 9.40 1.60 6 -8 0 8.70 1.40 7 8 0 0.90 1.30 -7 8 0 0.40 1.10 7 -8 0 1.20 1.20 -7 -8 0 1.00 1.20 -7 8 0 0.80 1.20 -8 -8 0 170.48 13.80 8 -8 0 180.08 13.70 -8 8 0 165.08 13.70 8 8 0 175.08 13.80 -9 -8 0 1.50 1.70 9 -8 0 0.60 1.60 9 8 0 -1.30 1.60 -9 8 0 -0.40 1.70 -10 8 0 16.50 2.20 -10 -8 0 11.80 2.10 10 -8 0 14.00 2.40 10 8 0 10.10 2.30 -11 -8 0 -0.20 1.90 -11 8 0 1.20 2.10 11 8 0 -2.50 2.30 -12 -8 0 0.80 2.40 12 8 0 -0.80 2.50 -12 8 0 0.20 2.50 -13 -8 0 3.70 2.80 0 9 0 -0.20 0.70 0 -9 0 -0.10 0.90 0 9 0 -0.60 0.70 -1 9 0 0.30 0.60 1 9 0 0.40 0.70 1 9 0 -0.20 0.70 -1 -9 0 0.20 0.90 1 -9 0 0.10 0.80 -1 9 0 -0.20 0.80 -2 -9 0 376.36 29.50 -2 9 0 393.36 29.40 2 -9 0 381.36 29.40 2 9 0 376.66 29.40 2 9 0 373.16 29.40 -2 9 0 363.96 29.40 -3 9 0 0.00 0.70 -3 -9 0 0.80 0.90 3 -9 0 -0.30 0.80 3 9 0 -0.50 0.80 -3 9 0 0.20 0.90 3 9 0 0.10 0.60 4 9 0 442.86 34.60 -4 9 0 438.96 34.60 4 9 0 436.16 34.50 4 -9 0 439.26 34.60 -4 -9 0 442.56 34.60 -4 9 0 463.65 34.50 -5 9 0 -1.20 1.00 -5 9 0 -0.10 0.90 -5 -9 0 -0.10 1.10 5 -9 0 1.30 1.10 5 9 0 -0.10 1.00 -6 9 0 114.49 8.70 6 9 0 113.09 8.90 -6 -9 0 100.99 8.80 6 -9 0 103.29 8.80 -6 9 0 113.89 8.80 7 -9 0 0.70 1.30 -7 9 0 -1.70 1.20 7 9 0 -0.70 1.30 -7 -9 0 0.10 1.30 -8 9 0 116.19 9.60 8 -9 0 123.69 9.50 8 9 0 113.49 9.60 -8 -9 0 112.89 9.60 9 -9 0 -0.50 1.70 -9 -9 0 0.60 1.70 9 9 0 0.00 1.70 -9 9 0 -1.00 1.70 -10 -9 0 66.89 6.20 10 9 0 71.79 6.40 -10 9 0 75.69 6.40 -11 -9 0 -0.40 2.00 -11 9 0 -3.90 1.90 11 9 0 0.30 2.30 -12 -9 0 51.69 5.40 12 9 0 55.29 5.70 -12 9 0 60.29 5.70 0 10 0 1025.20 79.29 0 10 0 1013.80 79.29 0 -10 0 1030.20 79.39 1 10 0 0.00 0.90 -1 10 0 0.50 0.80 1 -10 0 0.10 0.90 1 10 0 0.10 0.80 -1 -10 0 0.50 0.90 -1 10 0 0.90 0.80 -2 10 0 50.59 4.30 2 -10 0 48.20 4.30 2 10 0 49.90 4.20 -2 -10 0 44.60 4.30 2 10 0 55.19 4.30 -2 10 0 55.29 4.20 3 -10 0 0.30 1.00 -3 10 0 -0.60 0.70 3 10 0 0.10 0.90 3 10 0 0.00 0.70 -3 10 0 -0.40 1.00 -3 -10 0 0.30 1.00 -4 -10 0 2.40 1.10 4 10 0 4.20 1.30 4 -10 0 1.70 1.00 -4 10 0 2.00 0.90 -4 10 0 7.30 1.40 -5 -10 0 0.60 1.10 -5 10 0 -1.00 1.10 5 -10 0 -0.10 1.20 5 10 0 1.20 1.30 -6 -10 0 121.29 10.20 6 10 0 130.39 10.20 6 -10 0 126.59 10.10 -6 10 0 127.69 10.20 -7 -10 0 1.10 1.30 7 -10 0 0.70 1.40 7 10 0 -0.90 1.40 -7 10 0 -0.60 1.40 -8 10 0 45.60 4.60 -8 -10 0 44.80 4.60 8 10 0 55.69 4.80 8 -10 0 58.69 4.70 9 -10 0 -0.10 1.80 -9 -10 0 1.50 1.70 9 10 0 -0.70 1.70 -9 10 0 -0.30 1.70 -10 -10 0 45.30 4.70 -10 10 0 53.69 4.70 10 10 0 43.50 4.70 11 10 0 -2.60 2.30 -11 10 0 -0.10 2.20 -11 -10 0 2.30 2.40 12 10 0 8.20 3.40 -12 -10 0 5.10 3.00 -12 10 0 7.10 2.70 0 11 0 -0.10 0.80 0 -11 0 -0.50 0.90 0 11 0 -0.40 1.00 -1 -11 0 0.90 1.00 1 11 0 0.40 0.90 -1 11 0 -0.30 0.80 1 11 0 0.10 0.90 1 -11 0 -0.70 1.00 -1 11 0 -0.50 0.90 2 -11 0 5.60 1.50 2 11 0 12.60 1.50 -2 11 0 11.20 1.60 -2 -11 0 9.70 1.60 2 11 0 11.80 1.40 -2 11 0 14.00 1.40 -3 11 0 -0.40 1.10 3 -11 0 0.80 1.20 -3 11 0 0.10 0.90 3 11 0 -1.00 0.80 3 11 0 -0.20 1.10 -3 -11 0 0.50 1.10 -4 11 0 -0.30 1.10 4 11 0 1.20 1.10 -4 -11 0 -1.10 1.10 4 -11 0 1.00 1.30 5 11 0 -0.80 1.20 -5 -11 0 1.10 1.30 5 -11 0 0.70 1.20 -5 11 0 -0.20 1.20 6 -11 0 28.60 3.00 -6 11 0 29.60 3.00 -6 -11 0 25.60 3.00 6 11 0 32.30 3.10 -7 -11 0 -1.30 1.40 7 11 0 0.90 1.80 7 -11 0 0.30 1.50 -7 11 0 -1.60 1.50 8 11 0 4.90 1.90 -8 -11 0 7.60 2.00 8 -11 0 5.70 2.00 -8 11 0 5.70 1.80 -9 -11 0 1.00 1.70 -9 11 0 -0.70 1.80 9 11 0 0.30 1.90 -10 11 0 17.30 3.00 -10 -11 0 19.90 3.00 10 11 0 18.80 3.00 -11 11 0 0.50 2.40 11 11 0 -3.20 2.60 -11 -11 0 -0.90 2.30 -12 11 0 28.50 4.20 -12 -11 0 25.10 4.40 0 12 0 81.69 7.60 0 -12 0 99.39 7.60 0 12 0 99.99 7.50 1 12 0 0.00 1.00 1 -12 0 -1.50 1.10 -1 -12 0 -0.30 1.10 -1 12 0 0.80 1.10 -1 12 0 0.40 0.90 1 12 0 0.60 1.10 2 -12 0 2.70 1.30 2 12 0 1.00 1.10 -2 -12 0 4.80 1.30 -2 12 0 4.10 1.40 2 12 0 2.10 1.10 -3 -12 0 0.70 1.20 -3 12 0 -1.10 1.20 3 -12 0 0.40 1.30 3 12 0 0.10 1.10 -4 12 0 57.69 5.10 -4 -12 0 53.89 5.00 4 -12 0 66.69 5.10 4 12 0 54.69 5.10 -5 12 0 0.80 1.40 -5 -12 0 1.50 1.40 5 12 0 -0.50 1.30 5 -12 0 -1.30 1.40 6 12 0 196.08 15.60 6 -12 0 205.48 15.50 -6 12 0 180.78 15.60 -6 -12 0 200.68 15.60 7 12 0 -1.10 1.60 7 -12 0 -0.20 1.70 -7 12 0 -1.40 1.50 -7 -12 0 -0.80 1.50 -8 -12 0 12.20 2.10 8 12 0 7.90 2.10 8 -12 0 9.70 2.20 -8 12 0 11.40 2.10 -9 -12 0 -0.10 1.90 9 12 0 -0.20 2.10 -9 12 0 -0.60 2.00 -10 -12 0 1.30 2.20 -10 12 0 2.40 2.50 10 12 0 3.20 2.80 -11 -12 0 0.20 2.50 11 12 0 -1.30 3.20 -11 12 0 -1.70 2.70 0 13 0 -0.10 1.10 0 13 0 1.30 1.10 0 -13 0 -0.20 1.20 -1 -13 0 0.90 1.30 1 13 0 0.60 1.30 1 -13 0 1.20 1.30 -1 13 0 0.50 1.30 1 13 0 -0.30 1.10 -2 13 0 173.78 13.80 2 13 0 169.38 13.80 2 13 0 168.08 13.70 -2 -13 0 176.68 13.80 2 -13 0 184.58 13.90 -3 13 0 -0.90 1.30 3 -13 0 -1.70 1.40 -3 -13 0 2.10 1.50 3 13 0 0.10 1.40 -4 -13 0 63.79 5.90 -4 13 0 68.49 5.90 4 -13 0 72.69 5.90 4 13 0 70.39 5.90 5 13 0 -2.40 1.70 -5 -13 0 -0.30 1.50 5 -13 0 1.00 1.50 -5 13 0 0.60 1.50 -6 13 0 80.39 6.70 6 13 0 76.79 6.70 -6 -13 0 78.59 6.80 6 -13 0 76.39 6.70 -7 -13 0 -0.50 1.50 -7 13 0 0.30 1.70 7 -13 0 -2.00 1.80 7 13 0 -0.80 1.80 -8 13 0 5.70 2.30 8 13 0 9.90 2.30 -8 -13 0 11.30 2.50 -9 13 0 -1.20 2.40 -9 -13 0 1.00 2.10 9 13 0 -1.50 2.20 10 13 0 26.60 4.00 -10 13 0 28.30 3.90 -10 -13 0 27.00 3.60 -11 13 0 -0.80 3.00 11 13 0 0.40 3.50 0 14 0 1.00 1.40 0 -14 0 -0.30 1.40 -1 14 0 -0.90 1.50 1 14 0 0.00 1.30 1 -14 0 1.00 1.40 -1 -14 0 1.10 1.50 1 14 0 0.30 1.30 2 14 0 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9.30 3 7 4 120.89 9.20 -3 7 -4 115.79 9.20 3 7 4 118.39 9.20 -3 -7 4 110.59 9.20 -3 -7 4 119.99 9.10 4 -7 4 1.60 0.70 4 7 -4 0.70 0.90 -4 7 4 3.00 0.60 -4 7 4 2.20 0.90 -4 -7 -4 0.90 0.90 4 7 4 1.20 0.90 -4 7 -4 1.20 0.80 4 -7 -4 2.80 0.90 -4 -7 4 2.20 0.40 4 7 4 0.80 0.70 -4 7 -4 4.30 0.90 -4 -7 4 1.00 0.90 5 7 -4 38.10 3.70 -5 7 4 39.70 3.60 5 -7 4 43.10 3.50 -5 7 4 44.10 3.40 -5 -7 -4 42.50 3.60 -5 7 -4 42.70 3.50 -5 7 -4 41.30 3.60 5 -7 -4 34.10 3.60 5 7 4 43.20 3.60 5 7 4 46.40 3.40 -5 -7 4 35.00 3.60 -6 -7 -4 2.60 1.10 -6 7 4 1.50 1.00 6 -7 4 0.20 0.90 6 7 -4 3.40 1.20 -6 7 4 0.60 0.80 -6 7 -4 0.90 1.10 -6 7 -4 2.10 1.20 -6 -7 4 1.00 1.00 6 -7 -4 0.70 1.10 6 7 4 0.70 1.00 -7 -7 -4 5.20 1.30 7 7 -4 3.20 1.40 -7 7 4 5.80 1.30 7 -7 4 4.70 1.20 -7 7 -4 3.40 1.30 7 -7 -4 10.50 1.50 7 7 4 6.60 1.40 -7 7 -4 5.00 1.30 -7 -7 4 4.90 1.30 8 7 -4 -1.00 1.40 -8 -7 -4 -0.20 1.20 -8 7 4 -0.30 1.20 8 7 4 -0.30 1.50 -8 7 -4 1.90 1.40 -8 -7 4 1.00 1.30 -8 7 -4 0.80 1.30 8 -7 -4 -2.10 1.20 -9 7 4 13.70 2.00 -9 -7 -4 14.00 2.00 9 7 -4 9.50 2.10 -9 7 -4 14.50 2.00 -9 -7 4 10.90 2.00 9 -7 -4 16.50 2.20 -9 7 -4 16.10 2.20 9 7 4 12.40 2.10 -10 -7 -4 7.90 2.10 10 -7 4 10.80 2.10 10 7 -4 11.90 2.50 -10 7 4 15.20 2.30 10 7 4 11.60 2.20 -10 7 -4 15.20 2.20 10 -7 -4 12.20 2.30 -10 -7 4 17.10 2.20 -11 7 4 1.40 2.10 11 7 -4 3.00 2.10 -11 -7 -4 0.20 2.00 11 -7 4 3.50 2.20 11 -7 -4 1.60 1.90 -11 -7 4 2.50 1.90 11 7 4 3.00 2.10 -11 7 -4 -0.20 2.00 12 7 -4 -1.10 2.40 12 -7 4 0.70 2.50 -12 -7 -4 -1.90 2.00 12 7 4 0.40 2.40 12 -7 -4 -3.60 2.40 -12 -7 4 0.30 2.20 -13 -7 -4 3.60 2.90 13 7 -4 4.70 3.00 13 7 4 6.40 3.30 -13 -7 4 0.40 2.70 0 8 -4 687.73 52.69 0 8 4 694.53 52.69 0 -8 4 688.93 52.69 0 8 -4 667.93 52.69 0 8 4 676.73 52.59 0 -8 -4 658.83 52.69 1 -8 4 4.60 0.90 -1 8 4 7.80 0.70 1 8 -4 6.20 0.90 -1 -8 -4 5.10 1.00 -1 8 4 4.70 0.90 1 8 -4 7.10 1.10 -1 8 -4 7.90 1.00 -1 8 -4 6.40 1.00 -1 -8 4 4.30 1.00 1 8 4 7.10 0.90 1 -8 -4 5.10 1.00 1 8 4 4.70 0.90 -2 8 4 140.99 10.30 -2 8 4 138.69 10.40 -2 -8 -4 125.19 10.40 2 8 -4 133.19 10.30 2 -8 4 131.69 10.40 2 8 -4 135.99 10.40 -2 8 -4 124.59 10.40 -2 8 -4 131.09 10.40 2 -8 -4 121.39 10.40 -2 -8 4 128.19 10.40 2 8 4 132.09 10.40 2 8 4 130.69 10.40 -3 8 4 -1.00 0.90 3 -8 4 0.40 0.70 3 8 -4 1.00 0.60 -3 -8 -4 1.00 0.80 -3 8 4 0.30 0.40 3 8 -4 -0.30 0.90 3 8 4 -0.40 0.70 3 8 4 1.50 0.80 -3 8 -4 0.20 0.80 -3 -8 4 -0.10 0.90 3 -8 -4 0.30 0.80 -3 8 -4 0.10 0.80 4 -8 4 0.50 0.80 -4 8 4 -0.60 0.90 -4 -8 -4 -0.40 0.90 -4 8 4 -0.30 0.50 4 8 -4 1.10 1.00 -4 8 -4 0.20 0.80 -4 -8 4 -0.60 0.90 4 8 4 0.00 0.70 4 8 4 0.00 0.80 4 -8 -4 0.00 1.00 -4 8 -4 -0.80 0.90 5 8 -4 7.30 1.40 5 -8 4 6.30 1.10 -5 8 4 7.90 1.20 -5 -8 -4 5.80 1.30 -5 8 -4 6.20 1.20 5 8 4 7.40 1.30 -5 -8 4 2.60 1.20 -5 8 -4 11.60 1.30 5 -8 -4 3.50 1.20 5 8 4 7.60 1.00 6 -8 4 63.49 5.50 -6 8 4 70.59 5.60 -6 -8 -4 66.39 5.60 6 8 -4 64.59 5.70 6 -8 -4 70.89 5.60 6 8 4 68.69 5.60 -6 8 -4 64.39 5.60 -6 8 -4 70.79 5.70 -6 -8 4 65.39 5.60 -7 -8 -4 1.10 1.30 7 -8 4 0.80 1.10 -7 8 4 1.70 1.40 7 8 -4 0.40 1.30 -7 8 -4 1.30 1.30 -7 -8 4 -0.80 1.20 -7 8 -4 -0.60 1.40 7 -8 -4 -0.30 1.20 7 8 4 0.00 1.20 -8 8 4 222.38 18.20 -8 -8 -4 228.98 18.30 8 8 -4 241.38 18.30 8 -8 -4 232.48 18.20 -8 8 -4 226.98 18.20 8 8 4 238.18 18.30 -8 -8 4 223.78 18.30 -8 8 -4 235.28 18.20 -9 -8 -4 10.40 2.10 9 8 -4 14.40 2.40 -9 8 4 12.50 2.20 -9 8 -4 16.00 2.30 9 8 4 17.90 2.30 -9 -8 4 12.00 2.20 -9 8 -4 18.00 2.30 9 -8 -4 16.50 2.40 10 8 -4 15.00 2.60 -10 8 4 18.70 2.40 -10 -8 -4 5.20 2.00 10 -8 -4 10.50 2.30 -10 -8 4 10.80 2.20 -10 8 -4 17.10 2.60 10 8 4 14.20 2.50 -11 -8 -4 26.60 3.40 11 -8 4 30.60 3.50 11 8 -4 33.40 3.80 -11 8 4 32.90 3.50 11 -8 -4 36.00 3.60 11 8 4 35.00 3.70 -11 -8 4 27.60 3.50 -12 -8 -4 2.00 2.50 12 8 -4 1.50 2.60 12 -8 4 4.20 2.70 12 8 4 -0.80 2.60 -12 -8 4 0.00 2.30 12 -8 -4 1.40 2.60 -13 -8 -4 4.70 2.80 0 9 -4 0.00 0.80 0 -9 4 1.20 0.90 0 -9 -4 -0.90 0.80 0 9 4 -0.80 0.70 0 9 -4 -0.30 0.80 0 9 4 -0.40 0.50 1 -9 4 1.70 0.90 -1 9 4 4.60 0.60 -1 9 4 3.00 0.90 1 9 -4 2.30 1.00 1 9 -4 3.20 0.80 -1 -9 -4 1.40 1.00 1 9 4 4.70 0.80 -1 9 -4 2.90 0.90 -1 9 -4 2.70 0.90 1 -9 -4 2.90 1.00 1 9 4 2.20 0.90 -1 -9 4 1.70 0.90 -2 9 4 3.60 0.60 2 9 -4 3.40 0.80 -2 9 4 2.50 0.90 2 -9 4 1.90 0.90 2 9 -4 1.80 0.90 -2 -9 -4 2.60 1.00 2 -9 -4 2.40 0.90 2 9 4 2.00 0.80 -2 9 -4 1.80 0.80 -2 -9 4 1.90 0.90 2 9 4 2.10 0.80 -2 9 -4 2.10 1.00 -3 9 4 -0.30 0.90 3 -9 4 0.20 0.80 3 9 -4 0.50 0.60 -3 -9 -4 0.90 0.90 3 9 -4 1.20 1.00 3 9 4 1.00 0.90 3 9 4 0.50 0.80 -3 9 -4 -0.80 0.90 3 -9 -4 0.40 0.90 -3 9 -4 0.90 0.80 -3 -9 4 0.20 0.90 4 9 -4 33.90 2.90 -4 -9 -4 32.50 2.90 4 -9 4 24.30 2.70 -4 9 4 33.60 2.80 -4 9 -4 31.00 2.90 4 9 4 26.20 2.60 4 9 4 33.40 2.80 -4 9 -4 33.10 2.80 -4 -9 4 24.20 2.80 4 -9 -4 26.90 2.80 -5 9 4 60.79 5.00 5 9 -4 62.09 5.10 5 -9 4 60.89 4.90 -5 -9 -4 56.09 5.00 -5 9 -4 58.29 5.00 5 -9 -4 68.29 5.10 -5 9 -4 55.69 5.10 5 9 4 59.99 5.00 -5 -9 4 56.79 5.10 -6 9 4 0.90 1.20 -6 -9 -4 6.50 1.40 6 -9 4 5.10 1.20 6 9 -4 5.80 1.50 6 -9 -4 5.70 1.30 -6 -9 4 2.80 1.30 -6 9 -4 3.40 1.30 -6 9 -4 3.70 1.20 6 9 4 5.30 1.30 -7 -9 -4 103.89 8.90 -7 9 4 112.79 9.00 7 9 -4 120.69 9.10 7 -9 -4 118.79 9.00 -7 9 -4 102.89 9.00 -7 -9 4 104.89 9.00 7 9 4 106.29 9.00 -7 9 -4 113.39 8.90 -8 9 4 1.80 1.60 -8 -9 -4 0.90 1.40 8 9 -4 2.50 1.70 -8 9 -4 1.50 1.50 -8 -9 4 0.70 1.50 8 -9 -4 1.50 1.50 8 9 4 4.80 1.60 -8 9 -4 1.30 1.40 9 9 -4 1.00 1.80 -9 9 4 -0.50 1.70 -9 -9 -4 -1.30 1.50 9 -9 -4 0.20 1.70 9 9 4 0.70 1.90 -9 9 -4 -1.40 1.60 -9 -9 4 -1.00 1.70 -10 9 4 63.19 5.90 -10 -9 -4 66.59 6.00 10 9 -4 63.09 6.10 10 9 4 59.19 6.00 -10 9 -4 73.09 6.00 -10 -9 4 66.59 6.00 10 -9 -4 74.79 6.00 11 9 -4 5.90 2.50 -11 -9 -4 7.70 2.40 11 -9 4 10.80 2.40 -11 9 4 9.50 2.50 11 9 4 6.00 2.70 -11 -9 4 4.30 2.30 11 -9 -4 8.80 2.40 -12 -9 -4 9.40 2.70 -12 9 4 8.90 3.50 12 -9 4 7.40 3.00 12 9 -4 11.00 3.10 12 9 4 10.40 3.30 -12 -9 4 9.40 2.80 -13 -9 -4 0.00 2.90 0 10 4 235.38 17.90 0 -10 -4 223.28 18.00 0 -10 4 223.18 18.00 0 10 -4 247.88 18.00 0 10 4 226.08 18.00 0 10 -4 218.68 17.90 1 10 -4 -0.50 0.80 1 10 -4 -0.10 0.90 1 -10 4 -0.60 0.90 -1 -10 -4 -0.50 0.90 -1 10 4 -0.50 0.90 -1 10 4 0.10 0.60 -1 10 -4 1.20 1.00 1 10 4 -0.30 0.80 -1 -10 4 1.40 1.00 -1 10 -4 0.50 0.90 1 10 4 0.80 0.80 1 -10 -4 -0.10 0.90 -2 -10 -4 3.20 1.10 -2 10 4 5.90 1.20 2 10 -4 3.50 0.90 2 -10 4 2.00 1.00 2 10 -4 5.70 1.20 2 10 4 6.00 1.00 2 10 4 3.10 0.90 -2 -10 4 5.90 1.20 -2 10 -4 4.30 1.10 2 -10 -4 3.40 1.10 -2 10 -4 4.90 1.00 -3 10 4 0.70 1.00 3 10 -4 1.00 0.80 -3 -10 -4 1.60 1.10 3 -10 4 1.90 1.00 3 10 -4 2.90 1.10 -3 10 -4 1.20 1.10 -3 10 -4 3.60 1.00 3 -10 -4 1.60 1.20 3 10 4 0.80 0.90 3 10 4 0.90 0.90 -3 -10 4 1.70 1.10 4 -10 4 4.40 1.20 -4 -10 -4 6.20 1.40 -4 10 4 8.50 1.30 4 10 -4 5.40 1.40 4 -10 -4 2.80 1.20 -4 10 -4 6.50 1.20 -4 10 -4 6.60 1.30 4 10 4 6.50 1.10 -4 -10 4 4.30 1.20 4 10 4 7.20 1.20 5 10 -4 0.60 1.20 -5 10 4 -0.40 1.10 -5 -10 -4 0.20 1.10 5 -10 4 -0.40 1.10 -5 10 -4 0.00 1.10 5 -10 -4 0.50 1.30 5 10 4 -1.50 1.10 -5 -10 4 2.10 1.20 -5 10 -4 1.00 1.20 6 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229.48 17.20 -5 11 -4 217.08 17.10 -5 -11 4 231.88 17.20 5 -11 -4 226.48 17.20 6 11 -4 5.60 1.90 -6 11 4 10.40 1.70 -6 -11 -4 12.00 1.80 -6 11 -4 10.40 1.90 -6 -11 4 8.50 1.80 6 -11 -4 7.20 1.80 -6 11 -4 4.70 1.60 6 11 4 7.20 1.60 -7 11 4 30.40 3.20 7 11 -4 29.30 3.30 -7 -11 -4 29.30 3.10 7 -11 -4 39.00 3.40 -7 11 -4 24.60 3.10 7 11 4 32.80 3.30 -7 -11 4 27.40 3.10 8 11 -4 2.90 1.80 -8 -11 -4 0.10 1.60 -8 11 4 0.80 1.60 8 11 4 5.10 1.80 8 -11 -4 2.20 1.70 -8 -11 4 5.10 1.70 -8 11 -4 6.00 1.70 9 11 -4 -0.10 2.00 -9 -11 -4 1.50 1.80 -9 11 4 2.00 2.00 9 -11 -4 1.30 2.10 9 11 4 -1.50 1.80 -9 -11 4 1.50 1.90 -9 11 -4 0.40 1.80 -10 11 4 0.80 2.10 -10 -11 -4 -0.30 2.00 10 11 -4 -0.80 2.40 -10 -11 4 1.50 2.40 -10 11 -4 1.80 2.40 10 11 4 -3.30 2.10 10 -11 -4 0.40 2.10 11 -11 4 7.70 2.60 11 11 -4 4.00 3.20 -11 11 4 4.90 2.60 -11 -11 -4 6.80 2.60 -11 -11 4 8.90 2.70 11 11 4 7.50 2.80 12 -11 4 23.10 4.00 -12 -11 -4 22.30 3.90 -12 11 4 22.30 4.00 0 -12 -4 15.50 1.90 0 12 4 13.20 1.70 0 12 -4 10.50 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5 145.79 12.60 1 11 5 163.18 12.60 1 -11 -5 168.68 12.70 1 11 5 171.68 12.60 2 -11 5 7.00 1.30 -2 11 5 6.80 1.40 -2 -11 -5 10.10 1.50 2 11 -5 7.90 1.20 2 11 -5 7.80 1.40 -2 11 -5 8.70 1.40 -2 11 -5 9.90 1.40 2 11 5 10.60 1.30 -2 -11 5 11.80 1.60 2 11 5 7.20 1.30 2 -11 -5 5.60 1.40 -3 -11 -5 8.30 1.40 3 11 -5 7.10 1.40 3 -11 5 6.70 1.30 -3 11 5 4.80 1.30 3 -11 -5 7.00 1.50 -3 11 -5 6.10 1.30 3 11 5 9.20 1.30 -3 11 -5 5.10 1.30 3 11 5 4.90 1.20 -3 -11 5 8.10 1.40 -4 -11 -5 328.97 26.20 4 11 -5 336.47 26.20 4 -11 5 334.67 26.10 -4 11 5 336.77 26.20 -4 -11 5 317.77 26.20 4 11 5 333.47 26.10 4 -11 -5 332.87 26.20 -4 11 -5 347.87 26.20 -4 11 -5 338.97 26.10 -5 -11 -5 6.20 1.50 -5 11 5 7.20 1.50 5 11 -5 7.40 1.80 5 -11 5 4.70 1.40 5 -11 -5 10.70 1.60 -5 -11 5 6.80 1.50 -5 11 -5 7.40 1.50 5 11 5 3.20 1.60 -5 11 -5 6.40 1.60 -6 11 5 75.39 6.00 6 11 -5 79.49 6.10 -6 -11 -5 64.89 5.90 -6 11 -5 68.39 5.90 6 11 5 67.09 5.90 -6 11 -5 65.89 6.00 -6 -11 5 67.49 5.90 6 -11 -5 69.89 5.90 7 11 -5 39.20 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2.10 5 -1 6 21.10 2.10 -5 -1 -6 18.70 2.10 -5 -1 -6 19.10 1.90 5 -1 -6 17.50 2.00 -5 1 -6 20.60 2.10 -5 -1 6 23.00 1.90 -5 1 -6 24.40 1.90 5 1 6 23.20 2.00 -5 -1 6 21.20 2.10 6 1 -6 78.89 6.80 -6 -1 -6 86.59 6.70 -6 -1 -6 78.19 6.80 -6 1 6 73.99 6.80 -6 1 6 81.39 6.70 6 -1 6 84.19 6.80 6 1 6 75.79 6.70 -6 1 -6 91.39 6.80 -6 -1 6 90.89 6.60 6 -1 -6 86.49 6.80 -6 1 -6 89.09 6.70 -6 -1 6 90.59 6.80 7 1 -6 6.20 1.30 -7 -1 -6 8.50 1.20 -7 1 6 11.30 1.40 -7 1 6 7.40 1.10 -7 -1 -6 7.50 1.40 7 -1 6 8.50 1.30 -7 1 -6 10.30 1.20 7 -1 -6 9.60 1.40 -7 -1 6 8.90 1.50 -7 1 -6 7.40 1.40 7 1 6 7.10 1.20 -7 -1 6 12.00 1.10 -8 1 6 93.69 7.60 -8 -1 -6 91.89 7.70 -8 1 6 93.49 7.70 -8 -1 -6 97.99 7.80 8 -1 6 89.79 7.70 8 1 -6 93.39 7.80 -8 1 -6 101.59 7.60 -8 1 -6 99.49 7.80 -8 -1 6 98.99 7.70 8 -1 -6 87.89 7.70 8 1 6 96.09 7.60 9 1 -6 12.00 1.90 -9 -1 -6 11.30 1.80 -9 1 6 15.70 1.90 9 -1 6 11.60 1.80 -9 -1 -6 12.30 2.00 -9 1 -6 16.30 1.80 9 -1 -6 11.90 1.90 -9 1 -6 17.50 2.10 -9 -1 6 14.40 2.10 -10 1 6 0.20 1.60 -10 -1 -6 0.60 1.40 -10 -1 -6 2.10 1.60 10 1 -6 0.80 1.60 -10 -1 6 1.00 1.50 10 -1 -6 1.30 1.70 -10 1 -6 4.30 1.70 11 1 -6 2.40 2.10 -11 1 6 0.50 1.70 -11 -1 -6 1.50 1.80 -11 1 -6 -0.60 1.90 -11 -1 6 -0.40 1.70 11 -1 -6 0.80 2.00 -12 1 6 4.50 2.40 12 1 -6 4.40 2.40 -12 -1 6 5.90 2.30 12 1 6 3.40 2.20 12 -1 -6 7.00 2.20 -12 1 -6 2.40 2.20 13 -1 6 12.30 2.90 13 1 -6 13.10 2.90 -13 1 6 7.70 2.70 -13 -1 6 16.70 3.10 13 1 6 10.70 2.90 14 1 -6 4.00 3.20 -14 1 6 2.10 3.30 14 -1 6 7.40 3.60 -14 -1 6 4.70 2.90 0 -2 -6 1777.42 137.59 0 2 -6 1750.82 137.59 0 -2 6 1846.92 137.49 0 -2 6 1744.03 137.59 0 2 6 1725.03 137.59 0 -2 -6 1812.52 137.49 -1 -2 -6 522.25 40.50 1 -2 6 528.15 40.40 -1 2 6 563.34 40.50 1 2 -6 500.55 40.50 1 -2 6 513.65 40.50 -1 2 -6 532.15 40.50 1 -2 -6 504.85 40.50 1 -2 -6 549.54 40.50 1 2 6 495.75 40.50 -1 -2 6 517.25 40.50 -1 -2 6 514.95 40.50 2 2 -6 31.20 2.70 2 -2 6 28.70 2.70 -2 2 6 30.90 2.70 -2 -2 -6 32.90 2.70 -2 -2 -6 35.60 2.70 -2 2 6 35.80 2.70 2 -2 -6 33.00 2.60 -2 -2 6 31.50 2.70 -2 -2 6 33.50 2.60 -2 2 -6 32.50 2.70 2 2 6 32.50 2.70 -3 -2 -6 169.88 12.90 -3 -2 -6 161.18 13.00 -3 2 6 162.78 12.90 3 2 -6 156.68 12.90 -3 2 6 170.98 12.90 3 -2 6 159.88 12.90 -3 2 -6 156.88 13.00 -3 -2 6 169.28 12.90 3 2 6 158.38 12.90 -3 -2 6 170.18 13.00 -3 2 -6 177.98 12.80 3 -2 -6 163.48 12.90 4 2 -6 428.06 34.10 -4 -2 -6 444.06 34.10 -4 2 6 438.06 34.10 -4 2 6 418.66 34.10 4 -2 6 447.36 34.10 -4 -2 -6 432.06 34.10 -4 2 -6 437.86 34.10 -4 2 -6 456.15 34.00 -4 -2 6 466.75 34.00 4 -2 -6 438.96 34.10 -4 -2 6 420.36 34.10 4 2 6 432.46 34.10 -5 -2 -6 468.35 35.60 -5 2 6 473.45 35.70 -5 -2 -6 438.86 35.70 5 -2 6 450.45 35.70 5 2 -6 447.76 35.70 -5 2 6 455.75 35.60 5 2 6 472.65 35.60 -5 -2 6 442.66 35.70 -5 -2 6 475.75 35.60 -5 2 -6 458.45 35.60 5 -2 -6 454.75 35.60 -5 2 -6 459.55 35.70 -6 2 6 1.40 0.80 6 2 -6 2.30 0.90 -6 -2 -6 0.90 0.80 -6 2 6 1.70 0.90 6 -2 6 1.30 0.90 -6 -2 -6 2.00 1.00 6 2 6 0.80 0.80 6 -2 -6 0.70 0.80 -6 -2 6 1.10 0.50 -6 2 -6 1.50 0.70 -6 2 -6 0.50 0.90 -6 -2 6 0.40 0.90 7 2 -6 -0.10 1.00 -7 -2 -6 -0.50 1.10 -7 -2 -6 -0.80 0.80 7 -2 6 0.60 0.90 -7 2 6 0.50 1.00 -7 2 6 0.30 0.90 -7 2 -6 0.10 0.80 -7 2 -6 -0.20 1.10 -7 -2 6 -1.20 0.90 7 2 6 0.40 0.90 7 -2 -6 0.10 0.90 -8 -2 -6 20.20 2.40 8 -2 6 20.20 2.20 -8 2 6 23.00 2.40 -8 -2 -6 25.50 2.30 -8 2 6 23.90 2.20 8 2 -6 20.30 2.40 8 2 6 19.50 2.20 8 -2 -6 18.70 2.30 -8 2 -6 24.50 2.30 -8 -2 6 18.70 2.30 -8 2 -6 20.30 2.30 9 2 -6 139.19 10.40 -9 -2 -6 120.29 10.30 9 -2 6 127.59 10.20 -9 -2 -6 131.59 10.20 -9 2 6 124.69 10.30 -9 -2 6 123.89 10.30 -9 2 -6 126.79 10.50 9 -2 -6 128.89 10.30 -9 2 -6 123.79 10.30 -10 2 6 6.30 1.80 -10 -2 -6 7.20 1.80 10 -2 6 3.10 1.60 -10 -2 -6 5.50 1.50 10 2 -6 3.70 1.70 10 -2 -6 0.10 1.60 -10 2 -6 5.10 1.80 -10 -2 6 4.50 1.60 11 2 -6 0.70 1.80 -11 2 6 4.60 2.00 -11 -2 6 4.00 2.00 11 -2 -6 3.40 2.00 -11 2 -6 0.10 1.80 11 2 6 0.10 1.70 -12 2 6 9.30 2.50 12 2 -6 12.50 2.50 12 2 6 4.50 2.30 -12 -2 6 8.80 2.30 -12 2 -6 9.30 2.40 13 2 -6 7.70 2.80 -13 2 6 8.70 2.90 13 2 6 9.50 2.70 -13 2 -6 3.80 2.80 -13 -2 6 6.20 2.60 -14 2 6 23.20 3.80 14 2 -6 22.50 4.00 14 -2 6 21.70 3.80 -14 -2 6 20.80 4.40 0 -3 6 0.20 0.40 0 -3 -6 0.10 0.40 0 -3 6 0.40 0.30 0 3 -6 -0.20 0.50 0 3 6 0.00 0.40 0 -3 -6 0.40 0.30 1 3 -6 4.60 0.80 -1 3 6 5.60 0.80 1 -3 6 6.60 0.80 -1 -3 -6 4.80 0.70 1 -3 6 5.90 0.60 -1 -3 -6 6.70 0.80 1 -3 -6 8.50 0.80 -1 3 -6 7.00 0.80 1 3 6 6.70 0.80 -1 -3 6 6.30 0.70 1 -3 -6 5.90 0.60 -1 -3 6 6.90 0.70 -2 -3 -6 444.46 34.50 2 -3 6 465.05 34.50 2 3 -6 438.96 34.60 2 -3 6 454.15 34.40 -2 -3 -6 442.96 34.50 -2 3 6 442.36 34.50 -2 3 -6 441.26 34.60 -2 -3 6 437.96 34.50 2 -3 -6 432.76 34.50 2 -3 -6 455.95 34.50 2 3 6 439.36 34.50 -2 -3 6 439.26 34.50 -3 3 6 597.44 45.70 3 -3 6 612.44 45.60 -3 -3 -6 567.04 45.60 -3 -3 -6 597.64 45.70 3 3 -6 573.64 45.70 3 -3 6 584.04 45.70 3 -3 -6 593.94 45.60 -3 3 -6 582.54 45.70 3 3 6 581.24 45.60 -3 -3 6 565.34 45.70 -3 -3 6 608.64 45.60 -4 3 6 29.10 2.40 -4 -3 -6 26.10 2.30 4 3 -6 21.20 2.40 -4 3 6 26.90 2.30 4 -3 6 24.00 2.30 -4 -3 -6 27.60 2.40 -4 3 -6 27.40 2.40 4 3 6 24.40 2.30 -4 -3 6 29.70 2.10 -4 -3 6 25.60 2.40 4 -3 -6 25.10 2.20 -5 -3 -6 36.90 3.50 5 -3 6 39.30 3.50 5 3 -6 41.20 3.60 -5 3 6 42.80 3.50 -5 3 6 40.00 3.60 -5 3 -6 45.90 3.60 -5 -3 6 45.70 3.30 -5 3 -6 44.40 3.40 5 3 6 39.30 3.50 -5 -3 6 37.50 3.50 5 -3 -6 38.60 3.40 -6 -3 -6 24.10 2.20 6 3 -6 23.60 2.40 6 -3 6 20.60 2.20 -6 3 6 22.10 2.20 -6 3 6 24.90 2.30 -6 -3 -6 22.70 2.40 6 -3 -6 22.10 2.30 -6 3 -6 24.10 2.40 -6 3 -6 28.50 2.20 -6 -3 6 27.70 2.40 6 3 6 23.30 2.20 -7 -3 -6 2.10 1.10 -7 3 6 -0.10 0.90 -7 -3 -6 1.10 0.90 -7 3 6 0.00 1.00 7 3 -6 0.80 1.10 7 -3 6 2.00 1.10 7 -3 -6 0.00 0.90 -7 3 -6 0.60 1.00 -7 3 -6 1.70 0.90 -7 -3 6 1.80 1.00 7 3 6 1.70 1.00 8 3 -6 83.59 6.70 -8 -3 -6 80.29 6.70 8 -3 6 90.39 6.70 -8 3 6 90.49 6.70 -8 -3 -6 73.29 6.60 -8 3 6 77.29 6.60 -8 3 -6 79.19 6.70 -8 3 -6 83.29 6.50 -8 -3 6 77.89 6.70 8 -3 -6 75.19 6.60 -9 3 6 0.80 1.30 9 -3 6 0.70 1.20 9 3 -6 0.10 1.40 -9 -3 -6 1.70 1.50 -9 3 6 -0.10 1.50 -9 -3 -6 -0.50 1.30 -9 -3 6 0.60 1.50 9 -3 -6 -0.30 1.20 -9 3 -6 -0.90 1.40 10 -3 6 1.70 1.60 -10 3 6 2.20 1.80 -10 -3 -6 0.40 1.50 10 3 -6 -0.60 1.60 10 -3 -6 1.80 1.50 -10 3 -6 0.40 1.60 10 3 6 -0.50 1.50 -10 -3 6 4.00 1.80 -11 3 6 2.70 1.80 11 3 -6 4.80 2.00 -11 -3 -6 3.30 1.90 -11 -3 6 4.30 2.00 -11 3 -6 1.60 2.10 11 3 6 2.00 1.80 12 3 -6 6.10 2.60 -12 3 6 4.70 2.40 12 3 6 2.70 2.20 -12 -3 6 0.10 2.30 -12 3 -6 0.10 2.10 13 3 -6 0.40 3.00 -13 3 6 4.80 2.50 -13 -3 6 2.20 2.80 13 3 6 1.00 2.50 -13 3 -6 5.10 3.10 -14 3 6 -2.50 2.90 14 3 -6 0.40 3.20 14 -3 6 0.30 3.40 0 -4 -6 17.60 1.40 0 -4 6 12.90 1.30 0 -4 -6 14.50 1.20 0 4 6 11.30 1.30 0 -4 6 13.70 1.30 0 4 -6 17.50 1.40 1 4 -6 964.60 77.59 -1 4 6 970.40 77.59 1 -4 6 1012.40 77.59 -1 -4 -6 977.40 77.59 -1 -4 -6 1012.10 77.59 1 -4 6 1060.99 77.59 -1 4 -6 1013.00 77.59 1 4 6 977.50 77.59 -1 -4 6 988.10 77.59 1 -4 -6 986.00 77.59 -1 -4 6 1029.50 77.59 1 -4 -6 1019.40 77.49 2 4 -6 422.16 32.70 2 -4 6 432.16 32.60 -2 -4 -6 425.36 32.60 -2 -4 -6 411.16 32.60 2 -4 6 402.16 32.60 -2 4 6 406.06 32.70 2 -4 -6 420.26 32.70 -2 -4 6 431.06 32.70 -2 4 -6 427.86 32.70 2 -4 -6 435.46 32.50 -2 -4 6 414.36 32.60 2 4 6 410.16 32.60 3 -4 6 106.49 8.40 -3 -4 -6 107.19 8.40 3 -4 6 110.79 8.30 3 4 -6 110.89 8.50 -3 4 6 110.79 8.40 -3 -4 -6 101.09 8.40 3 -4 -6 106.69 8.30 -3 -4 6 107.49 8.40 -3 -4 6 111.69 8.30 3 4 6 102.99 8.40 3 -4 -6 89.99 8.40 -3 4 -6 107.69 8.40 4 4 -6 154.98 13.60 4 -4 6 169.48 13.60 -4 -4 -6 163.38 13.60 -4 4 6 185.28 13.60 4 -4 6 172.38 13.50 -4 -4 -6 174.68 13.50 -4 -4 6 189.88 13.40 -4 4 -6 169.38 13.60 -4 -4 6 160.98 13.60 4 -4 -6 158.68 13.60 4 4 6 178.58 13.50 4 -4 -6 179.78 13.50 5 -4 6 169.68 13.40 5 4 -6 170.28 13.40 -5 4 6 185.78 13.40 -5 -4 -6 153.18 13.40 5 -4 6 179.18 13.30 -5 -4 -6 176.58 13.40 -5 4 6 156.18 13.40 5 -4 -6 176.58 13.30 -5 4 -6 169.98 13.40 -5 -4 6 163.18 13.40 5 4 6 164.48 13.30 -6 -4 -6 9.60 1.20 6 4 -6 6.70 1.30 -6 4 6 5.40 1.00 -6 4 6 6.00 1.20 -6 -4 -6 4.60 1.20 6 -4 6 5.80 1.10 -6 4 -6 6.10 1.20 -6 -4 6 4.20 1.10 6 -4 -6 8.00 1.00 6 4 6 7.00 1.10 -6 4 -6 8.70 1.00 -7 4 6 0.70 1.00 -7 -4 -6 1.90 1.00 7 -4 6 1.70 1.00 -7 4 6 3.50 1.10 7 4 -6 -0.50 1.10 -7 -4 -6 1.70 1.20 -7 -4 6 2.00 1.10 7 4 6 3.90 1.00 -7 4 -6 3.10 0.90 -7 4 -6 3.00 1.30 7 -4 -6 3.90 1.00 8 -4 6 2.20 1.30 -8 4 6 1.90 1.20 -8 -4 -6 -0.20 1.20 -8 4 6 2.50 1.20 8 4 -6 1.30 1.50 -8 -4 -6 2.70 1.20 -8 4 -6 0.10 1.80 -8 -4 6 2.30 1.20 -8 4 -6 2.10 1.30 8 -4 -6 0.70 1.10 9 4 -6 1.00 1.70 -9 4 6 0.60 1.30 -9 4 6 0.20 1.30 -9 -4 -6 1.60 1.30 9 -4 6 1.10 1.30 -9 -4 6 1.00 1.30 -9 4 -6 -1.60 1.50 9 4 6 -0.60 1.30 9 -4 -6 0.80 1.30 -10 4 6 14.70 2.10 10 4 -6 16.10 2.30 10 -4 6 18.80 2.30 -10 -4 -6 8.70 2.00 10 4 6 14.60 2.20 -10 4 -6 12.10 2.20 -10 -4 6 10.80 2.10 -11 4 6 23.20 3.10 11 4 -6 21.90 3.20 -11 -4 -6 23.60 3.10 11 -4 6 30.00 3.20 -11 4 -6 34.30 3.30 11 4 6 29.70 3.40 -11 -4 6 31.50 3.30 -12 4 6 -1.20 2.40 12 4 -6 0.00 2.20 -12 4 -6 1.40 2.20 12 4 6 -2.40 2.10 -12 -4 6 -1.00 2.00 -13 4 6 4.40 2.70 13 4 -6 2.40 2.80 -13 4 -6 2.00 2.70 13 4 6 4.70 3.00 -13 -4 6 2.00 2.60 14 -4 6 -2.70 3.00 -14 4 6 -3.90 3.20 0 -5 6 -0.20 0.50 0 5 6 0.40 0.30 0 -5 6 0.10 0.50 0 -5 -6 0.20 0.60 0 5 6 -0.80 0.50 0 5 -6 -0.50 0.60 1 5 -6 186.98 14.10 1 -5 6 181.78 14.00 -1 5 6 176.78 14.10 -1 -5 -6 183.88 14.10 -1 -5 -6 173.98 14.00 1 -5 6 184.58 14.00 1 -5 -6 181.18 14.10 -1 -5 6 179.28 14.00 -1 -5 6 177.38 14.00 -1 5 -6 179.38 14.10 1 5 6 174.78 14.00 -2 -5 -6 11.50 1.30 2 5 -6 15.70 1.40 -2 -5 -6 11.90 1.30 2 -5 6 12.60 1.30 2 -5 6 14.50 1.20 -2 5 6 12.40 1.30 -2 -5 6 13.20 1.20 -2 5 -6 13.60 1.30 -2 -5 6 12.70 1.30 2 -5 -6 11.70 1.30 2 5 6 10.60 1.20 3 -5 6 369.16 28.10 -3 5 6 344.57 28.20 3 -5 6 382.56 28.20 -3 -5 -6 352.36 28.20 -3 -5 -6 352.96 28.20 3 5 -6 360.76 28.20 3 -5 -6 360.96 28.10 3 5 6 355.26 28.20 -3 -5 6 367.76 28.20 -3 5 -6 359.36 28.20 3 -5 -6 366.76 28.20 -3 -5 6 371.86 28.10 -4 5 6 10.10 1.10 4 -5 6 5.90 1.10 -4 -5 -6 7.50 1.10 4 -5 6 9.60 0.90 -4 -5 -6 8.30 1.10 4 5 -6 6.60 1.20 -4 -5 6 9.40 0.80 4 -5 -6 8.80 1.20 -4 5 -6 11.90 1.30 4 -5 -6 8.70 0.90 -4 -5 6 5.30 1.10 4 5 6 8.40 1.10 5 -5 6 199.68 14.80 -5 -5 -6 180.48 14.90 -5 -5 -6 187.38 15.00 5 -5 6 179.98 14.90 5 5 -6 193.28 15.00 -5 5 6 198.18 14.90 5 -5 -6 199.98 14.80 5 5 6 201.18 14.90 5 -5 -6 178.08 14.90 -5 -5 6 175.48 14.90 -5 5 -6 188.28 14.90 -6 -5 -6 19.10 2.10 -6 -5 -6 22.30 2.00 6 -5 6 17.30 1.90 6 5 -6 16.10 2.00 -6 5 6 19.50 1.90 6 -5 6 20.80 1.80 6 -5 -6 17.40 1.80 6 5 6 20.50 1.90 -6 -5 6 13.90 1.90 6 -5 -6 19.60 2.00 -6 5 -6 15.30 1.90 -7 5 6 131.29 9.90 7 -5 6 121.29 9.90 -7 -5 -6 114.39 9.90 7 5 -6 127.59 10.00 -7 5 6 137.79 10.00 7 -5 6 124.59 9.80 7 -5 -6 122.99 9.90 -7 -5 6 120.39 9.90 -7 5 -6 133.99 10.00 7 5 6 111.99 9.90 8 5 -6 111.69 8.80 -8 5 6 104.89 8.70 -8 -5 -6 109.99 8.70 8 -5 6 103.69 8.70 8 5 6 114.99 8.80 -8 5 -6 104.79 8.70 -8 -5 6 105.29 8.80 -9 -5 -6 114.99 9.80 -9 5 6 123.49 9.80 9 -5 6 131.79 9.90 -9 5 6 116.29 9.90 9 5 -6 123.69 10.00 -9 5 -6 113.79 9.90 9 5 6 128.69 10.00 -9 -5 6 127.19 10.00 10 5 -6 35.20 3.60 -10 5 6 29.60 3.30 10 -5 6 32.40 3.40 -10 5 6 33.70 3.30 -10 -5 -6 34.00 3.40 -10 5 -6 30.40 3.40 -10 -5 6 30.70 3.40 10 5 6 34.50 3.50 11 5 -6 -2.20 2.00 -11 5 6 -0.20 1.90 11 -5 6 -0.10 2.00 -11 -5 -6 0.10 1.60 11 5 6 3.20 1.90 -11 -5 6 2.80 1.80 -11 5 -6 3.90 2.20 -12 -5 -6 2.70 3.40 -12 5 6 -0.60 2.10 12 5 -6 -1.00 2.40 12 5 6 -0.70 2.20 -12 -5 6 -0.60 2.10 -12 5 -6 1.00 2.50 -13 5 6 0.60 2.80 13 5 -6 3.10 2.90 -13 -5 6 6.30 3.00 13 5 6 0.90 2.60 -13 5 -6 2.90 2.70 0 6 6 2013.60 154.08 0 -6 6 1992.50 154.08 0 6 -6 1955.30 154.08 0 6 6 2027.80 153.98 0 -6 -6 1993.50 154.08 0 -6 6 1952.30 154.08 -1 -6 -6 16.60 1.70 1 6 -6 16.10 1.70 1 -6 6 15.80 1.50 -1 6 6 15.40 1.60 -1 -6 6 15.20 1.60 -1 6 -6 15.00 1.60 1 6 6 17.90 1.60 -1 -6 6 16.90 1.50 -1 6 -6 17.40 1.70 1 6 6 19.00 1.50 1 -6 -6 17.40 1.70 -2 -6 -6 142.29 12.20 2 6 -6 164.48 12.30 -2 6 6 138.09 12.20 2 -6 6 160.98 12.20 2 6 6 157.08 12.20 -2 6 -6 152.98 12.20 2 6 6 164.48 12.20 2 -6 -6 152.68 12.20 -2 6 -6 156.68 12.20 -2 -6 6 162.38 12.10 3 6 -6 40.70 3.40 -3 6 6 41.30 3.30 -3 -6 -6 40.30 3.30 3 -6 6 37.10 3.20 -3 -6 6 35.30 3.30 3 6 6 36.00 3.30 3 6 6 43.50 3.30 -3 -6 6 43.40 3.20 3 -6 -6 34.80 3.30 -3 6 -6 39.30 3.30 4 6 -6 22.30 2.10 -4 -6 -6 20.00 2.00 -4 6 6 19.00 2.00 4 -6 6 19.80 1.80 -4 -6 6 19.90 1.70 4 -6 -6 18.90 1.70 4 6 6 20.20 2.00 4 -6 -6 20.90 2.00 -4 6 -6 21.40 2.10 -4 -6 6 19.60 2.00 -4 6 -6 22.30 2.10 4 6 6 24.40 1.90 -5 -6 -6 14.20 1.50 5 -6 6 11.40 1.30 5 6 -6 9.30 1.50 -5 6 6 15.30 1.60 -5 -6 6 9.30 1.50 5 -6 -6 8.50 1.40 5 6 6 14.60 1.40 5 6 6 11.10 1.40 -5 6 -6 12.60 1.50 -5 6 -6 11.70 1.50 5 -6 -6 11.90 1.20 6 -6 6 174.08 14.40 -6 6 6 192.18 14.50 6 6 -6 169.28 14.50 -6 -6 -6 177.28 14.50 6 6 6 183.28 14.50 6 6 6 193.78 14.40 6 -6 -6 185.88 14.50 -6 6 -6 187.88 14.50 -6 -6 6 188.98 14.50 -7 -6 -6 17.90 1.90 7 6 -6 17.50 2.10 7 -6 6 21.30 2.10 -7 6 6 15.50 2.00 -7 -6 6 14.00 2.00 -7 6 -6 20.70 2.10 7 6 6 14.00 2.00 7 -6 -6 14.40 2.00 8 6 -6 3.80 1.60 8 -6 6 1.80 1.30 -8 6 6 0.30 1.20 -8 -6 -6 0.10 1.20 -8 -6 6 2.80 1.30 -8 6 -6 1.40 1.30 8 6 6 -0.10 1.30 8 -6 -6 0.80 1.40 9 -6 6 -0.20 1.40 -9 6 6 -0.60 1.30 -9 -6 -6 -0.10 1.50 9 6 -6 1.30 1.70 -9 6 -6 -1.00 1.60 9 6 6 0.30 1.50 -9 -6 6 1.80 1.40 9 -6 -6 0.60 1.50 10 -6 6 -0.30 1.80 -10 -6 -6 2.30 1.70 -10 6 6 2.60 1.80 10 6 -6 1.00 1.90 10 6 6 4.00 2.10 -10 6 -6 3.60 1.80 -10 -6 6 5.10 1.80 10 -6 -6 5.80 1.80 -11 -6 -6 16.00 2.30 11 6 -6 11.80 2.80 11 -6 6 12.30 2.50 -11 6 -6 16.10 2.50 11 6 6 18.10 2.60 11 -6 -6 13.90 2.60 -11 -6 6 7.60 2.30 -12 -6 -6 1.50 2.20 12 6 -6 -0.50 2.50 12 6 6 2.60 2.70 -12 -6 6 1.70 2.20 -12 6 -6 2.60 2.40 12 -6 -6 2.20 2.30 13 6 -6 23.40 4.00 -13 -6 6 20.20 3.60 13 6 6 23.00 3.70 13 -6 -6 28.00 4.00 -13 6 -6 26.90 3.80 0 7 -6 -1.00 0.80 0 -7 6 0.10 0.60 0 7 6 -0.60 0.60 0 7 -6 -0.20 0.70 0 -7 -6 0.20 0.80 0 7 6 0.50 0.40 -1 7 6 29.70 2.10 -1 7 6 22.70 2.40 1 7 -6 24.10 2.40 1 -7 6 26.40 2.30 -1 -7 -6 25.50 2.50 -1 7 -6 25.80 2.40 1 -7 -6 22.20 2.40 -1 7 -6 24.40 2.40 1 7 6 25.10 2.40 -1 -7 6 23.70 2.30 -1 -7 6 29.80 2.30 1 7 6 27.80 2.30 -2 7 6 125.09 10.20 -2 -7 -6 138.29 10.20 2 -7 6 131.39 10.20 2 7 -6 135.39 10.30 -2 7 -6 139.19 10.20 -2 -7 6 115.59 10.20 2 7 6 134.79 10.20 -2 7 -6 119.69 10.20 -2 -7 6 133.49 10.10 2 -7 -6 120.29 10.20 2 7 6 131.89 10.20 3 7 -6 73.89 5.90 -3 -7 -6 73.59 5.90 -3 7 6 79.49 5.90 3 -7 6 72.39 5.80 -3 -7 6 65.69 5.80 3 7 6 78.29 5.80 -3 7 -6 70.29 5.90 3 7 6 69.49 5.80 -3 -7 6 74.09 5.70 3 -7 -6 64.79 5.80 4 7 -6 47.00 3.80 -4 -7 -6 39.70 3.80 4 -7 6 42.60 3.60 -4 7 6 47.90 3.70 -4 -7 6 34.50 3.70 -4 -7 6 46.00 3.50 4 -7 -6 37.70 3.70 -4 7 -6 47.40 3.70 -4 7 -6 39.90 3.70 4 7 6 47.50 3.70 4 7 6 47.00 3.70 -5 -7 -6 115.39 9.40 5 -7 6 117.99 9.20 5 7 -6 120.89 9.40 -5 7 6 113.89 9.30 -5 7 -6 120.09 9.30 -5 7 -6 123.89 9.40 -5 -7 6 108.79 9.30 5 7 6 119.59 9.30 5 7 6 119.89 9.30 5 -7 -6 109.79 9.40 6 -7 6 129.79 10.10 -6 -7 -6 127.29 10.20 -6 7 6 115.19 10.20 6 7 -6 132.09 10.30 -6 7 -6 126.59 10.20 -6 -7 6 142.59 10.20 6 7 6 127.29 10.20 -6 7 -6 123.69 10.20 6 -7 -6 125.09 10.20 7 7 -6 13.80 2.00 -7 -7 -6 13.40 1.70 -7 7 6 16.50 1.80 7 7 6 16.00 1.90 -7 7 -6 10.70 1.80 -7 -7 6 12.30 1.80 7 -7 -6 16.00 1.90 -7 7 -6 13.70 1.90 -8 7 6 43.20 3.80 8 7 -6 34.60 3.90 -8 -7 -6 38.90 3.80 8 -7 6 42.60 3.80 -8 -7 6 39.70 3.80 -8 7 -6 46.00 4.00 8 -7 -6 40.30 3.90 8 7 6 39.60 3.90 9 7 -6 54.49 5.10 -9 -7 -6 54.39 4.80 -9 7 6 49.10 4.80 9 -7 6 50.39 4.70 -9 7 -6 50.99 4.80 9 7 6 54.79 4.80 9 -7 -6 51.29 4.90 -9 -7 6 49.10 4.70 10 7 -6 6.60 2.10 10 -7 6 6.20 1.90 -10 7 6 7.10 2.00 -10 -7 -6 7.40 2.00 10 -7 -6 9.10 2.10 10 7 6 6.40 2.00 -10 -7 6 3.30 1.80 -10 7 -6 6.20 1.90 -11 -7 -6 1.60 1.80 -11 7 6 2.20 2.10 11 -7 6 -2.40 1.80 11 7 -6 0.40 2.30 -11 7 -6 1.40 2.30 11 -7 -6 -0.20 1.90 -11 -7 6 -1.90 2.10 11 7 6 -0.80 2.00 -12 -7 -6 0.00 2.30 12 7 -6 -0.70 2.90 12 -7 6 -0.70 2.50 -12 -7 6 -1.60 2.20 12 7 6 2.80 2.50 -12 7 -6 1.30 2.50 12 -7 -6 -0.50 2.60 13 7 -6 14.70 4.00 13 -7 -6 21.60 3.80 -13 -7 6 15.90 3.70 0 8 6 693.13 53.59 0 8 -6 702.23 53.59 0 8 6 714.93 53.49 0 8 -6 675.03 53.59 0 -8 -6 676.23 53.59 0 -8 6 675.03 53.49 -1 8 6 11.50 1.40 1 8 -6 9.80 1.30 -1 8 6 13.60 1.10 1 -8 6 13.70 1.40 1 8 -6 14.00 1.50 -1 -8 -6 14.10 1.50 1 8 6 14.00 1.50 -1 8 -6 13.30 1.40 1 -8 -6 13.50 1.50 1 8 6 11.50 1.20 -1 8 -6 10.50 1.40 -1 -8 6 10.10 1.40 2 8 -6 219.48 17.40 2 -8 6 219.88 17.30 -2 8 6 209.58 17.40 -2 -8 -6 221.88 17.40 2 8 6 227.48 17.30 2 8 6 222.68 17.30 -2 -8 6 231.98 17.30 -2 8 -6 216.38 17.40 2 -8 -6 214.28 17.40 -2 -8 6 229.58 17.40 3 -8 6 22.90 2.10 -3 8 6 21.10 2.20 -3 -8 -6 22.20 2.20 3 8 -6 26.50 2.40 -3 -8 6 23.40 2.00 3 8 6 23.30 2.10 3 -8 -6 22.70 2.30 -3 -8 6 22.80 2.20 -3 8 -6 26.30 2.20 3 8 6 25.10 2.20 -3 8 -6 16.50 2.20 4 -8 6 0.30 0.80 -4 -8 -6 0.70 1.00 -4 8 6 -0.10 0.90 4 8 -6 0.00 1.00 4 8 6 1.20 0.80 -4 8 -6 0.00 0.90 -4 -8 6 -0.60 0.90 4 8 6 -0.40 0.90 -4 8 -6 0.30 0.90 4 -8 -6 1.30 1.00 -5 8 6 1.30 1.00 5 8 -6 0.70 1.10 5 -8 6 0.90 0.80 -5 -8 -6 1.80 1.10 5 8 6 1.30 0.90 -5 -8 6 1.70 1.20 -5 8 -6 0.00 0.90 5 8 6 0.40 0.90 5 -8 -6 1.10 1.00 -5 8 -6 0.50 1.00 -6 -8 -6 40.20 3.40 -6 8 6 34.30 3.40 6 8 -6 41.10 3.50 -6 8 -6 39.90 3.50 -6 -8 6 37.50 3.40 -6 8 -6 31.20 3.40 6 8 6 36.50 3.40 6 -8 -6 34.70 3.50 7 8 -6 3.20 1.50 -7 8 6 0.20 1.40 -7 -8 -6 1.20 1.30 -7 -8 6 1.90 1.30 -7 8 -6 0.70 1.40 -7 8 -6 -0.30 1.40 7 8 6 1.00 1.30 7 -8 -6 -0.10 1.30 8 -8 6 51.39 4.60 -8 -8 -6 51.99 4.50 8 8 -6 50.49 4.70 -8 8 6 51.89 4.70 -8 -8 6 49.40 4.60 8 8 6 53.69 4.60 8 -8 -6 44.90 4.70 -8 8 -6 51.09 4.70 -9 8 6 58.59 5.40 -9 -8 -6 54.09 5.40 9 -8 6 61.89 5.50 9 8 -6 76.59 5.70 9 8 6 62.29 5.60 -9 8 -6 57.49 5.60 -9 -8 6 61.19 5.50 9 -8 -6 70.39 5.60 10 8 -6 -0.30 2.20 10 -8 6 -1.40 2.00 -10 -8 -6 1.50 1.70 -10 8 6 2.00 1.70 -10 8 -6 -0.80 1.80 -10 -8 6 1.20 1.80 10 8 6 0.30 1.80 10 -8 -6 0.20 2.00 -11 8 6 1.00 2.20 -11 -8 -6 4.30 2.20 11 -8 6 0.40 2.20 11 8 -6 1.50 2.30 11 8 6 3.30 2.20 11 -8 -6 4.90 2.40 -11 8 -6 2.20 2.70 -11 -8 6 4.60 2.40 12 8 -6 1.40 2.70 12 -8 6 -1.20 2.60 -12 -8 -6 4.30 2.70 -12 -8 6 -0.70 2.40 12 -8 -6 1.00 2.70 12 8 6 2.70 3.00 13 -8 -6 1.10 3.40 0 9 6 -0.30 0.60 0 9 -6 1.00 0.80 0 -9 -6 -1.00 0.80 0 -9 6 0.30 0.70 0 9 6 0.20 0.80 0 9 -6 0.60 0.80 1 9 -6 15.20 1.50 -1 9 6 12.40 1.50 -1 -9 -6 14.20 1.60 1 9 -6 13.40 1.60 -1 9 6 12.50 1.20 1 -9 6 17.30 1.50 -1 -9 6 11.60 1.50 1 9 6 14.90 1.40 -1 9 -6 12.20 1.50 -1 9 -6 13.50 1.60 1 -9 -6 9.70 1.50 1 9 6 14.00 1.60 -2 -9 -6 -0.90 1.00 -2 9 6 0.30 0.80 2 -9 6 -0.10 0.80 2 9 -6 0.70 0.90 -2 -9 6 0.70 1.00 -2 -9 6 1.30 0.70 2 -9 -6 0.40 0.90 2 9 6 0.10 0.70 2 9 6 0.10 0.80 -2 9 -6 0.50 0.80 -2 9 -6 -0.40 1.00 3 9 -6 171.98 13.60 -3 -9 -6 166.68 13.60 -3 9 6 156.78 13.60 3 -9 6 177.98 13.50 3 -9 -6 169.58 13.60 -3 -9 6 186.38 13.50 3 9 6 179.98 13.60 -3 9 -6 177.08 13.60 3 9 6 181.88 13.60 -3 -9 6 167.78 13.60 -3 9 -6 150.38 13.60 -4 9 6 3.40 1.10 4 9 -6 4.00 1.20 -4 -9 -6 4.00 1.10 4 -9 6 2.30 0.90 4 9 6 3.80 1.10 -4 -9 6 1.80 1.10 -4 9 -6 4.50 1.10 4 -9 -6 6.70 1.30 4 9 6 3.80 1.00 -4 9 -6 1.90 1.10 5 -9 6 26.00 2.80 5 9 -6 36.80 3.10 -5 9 6 33.30 3.00 -5 -9 -6 27.40 2.90 5 9 6 30.90 2.80 -5 9 -6 23.70 2.80 -5 -9 6 34.80 2.90 5 -9 -6 29.90 2.90 -5 9 -6 25.90 2.90 6 9 -6 236.18 18.20 -6 9 6 233.98 18.10 -6 -9 -6 226.68 18.10 -6 9 -6 223.28 18.10 -6 -9 6 221.68 18.20 6 9 6 240.18 18.20 -6 9 -6 223.68 18.10 6 -9 -6 236.08 18.20 -7 9 6 57.49 4.80 7 9 -6 48.90 5.00 7 -9 -6 51.89 4.80 -7 9 -6 61.99 4.90 -7 9 -6 53.09 4.90 -7 -9 6 55.79 4.90 7 9 6 51.59 4.80 8 9 -6 11.50 2.00 -8 -9 -6 13.10 1.90 -8 9 6 7.20 2.00 8 9 6 9.20 1.90 8 -9 -6 6.30 1.80 -8 9 -6 8.20 1.90 -8 -9 6 8.90 1.80 -8 9 -6 7.90 1.80 9 -9 6 0.60 1.70 -9 -9 -6 0.10 1.60 -9 9 6 0.70 1.60 9 9 -6 -0.60 1.80 9 9 6 0.40 1.70 9 -9 -6 0.30 1.70 -9 9 -6 -1.10 1.80 -9 -9 6 -0.80 1.60 10 -9 6 12.20 2.70 10 9 -6 17.30 2.90 -10 -9 -6 21.40 2.60 -10 9 6 16.70 2.60 -10 -9 6 20.30 2.70 10 9 6 16.60 2.70 10 -9 -6 20.10 2.90 -11 9 6 2.80 2.20 -11 -9 -6 1.30 2.30 11 9 -6 2.60 2.50 11 -9 6 5.40 2.30 11 9 6 2.60 2.30 -11 -9 6 -0.30 2.40 11 -9 -6 2.40 2.50 12 -9 6 -0.10 2.60 -12 -9 -6 1.50 2.80 12 9 -6 -0.40 2.80 12 9 6 -0.80 2.70 -12 -9 6 3.30 2.70 12 -9 -6 -0.10 2.60 0 10 6 288.37 22.20 0 10 -6 285.77 22.30 0 10 6 274.57 22.30 0 -10 6 280.97 22.30 0 10 -6 298.07 22.30 0 -10 -6 281.17 22.30 1 -10 6 72.59 6.20 -1 10 6 73.89 6.20 1 10 -6 81.79 6.30 1 10 -6 72.99 6.20 -1 -10 -6 83.59 6.30 1 10 6 73.69 6.20 -1 10 -6 74.69 6.20 -1 -10 6 76.59 6.20 1 -10 -6 76.59 6.30 1 10 6 82.89 6.20 -1 10 -6 76.19 6.20 -2 -10 -6 102.19 8.30 2 -10 6 102.09 8.30 -2 10 6 105.29 8.30 2 10 -6 101.99 8.40 -2 10 -6 102.59 8.30 -2 -10 6 100.79 8.30 -2 10 -6 101.19 8.30 2 -10 -6 110.39 8.40 2 10 6 111.59 8.30 2 10 6 98.19 8.30 -3 10 6 2.10 1.20 3 10 -6 1.00 1.10 -3 -10 -6 1.90 1.10 3 -10 6 0.30 1.00 -3 -10 6 0.80 1.10 -3 -10 6 0.90 1.30 3 10 6 0.10 0.80 -3 10 -6 0.60 1.00 -3 10 -6 -0.80 1.00 3 -10 -6 -0.20 1.20 3 10 6 0.40 0.90 -4 10 6 38.50 3.30 -4 -10 -6 33.40 3.20 4 10 -6 28.30 3.30 4 -10 6 30.70 3.10 4 10 6 36.10 3.20 4 10 6 34.60 3.10 -4 10 -6 37.90 3.20 -4 10 -6 39.70 3.40 4 -10 -6 34.60 3.30 -5 -10 -6 14.20 1.90 5 10 -6 10.20 1.90 -5 10 6 15.10 1.80 5 -10 -6 14.00 2.00 -5 10 -6 13.30 1.80 -5 10 -6 14.60 1.70 5 10 6 11.00 1.70 -5 -10 6 13.60 1.80 -6 10 6 169.98 12.20 -6 -10 -6 147.69 12.10 6 10 -6 159.08 12.20 -6 10 -6 153.58 12.00 -6 -10 6 147.29 12.10 6 -10 -6 147.99 12.10 6 10 6 140.09 12.10 -6 10 -6 147.99 12.10 7 10 -6 16.10 2.20 -7 10 6 5.30 1.90 -7 -10 -6 9.50 1.90 -7 10 -6 7.80 1.80 7 10 6 9.30 1.80 -7 10 -6 9.10 1.90 7 -10 -6 12.60 2.10 -7 -10 6 13.00 1.90 -8 10 6 6.90 1.80 8 10 -6 5.00 2.10 -8 -10 -6 3.40 1.80 -8 -10 6 3.60 1.70 -8 10 -6 8.90 1.90 8 10 6 5.40 1.80 -8 10 -6 8.50 2.00 8 -10 -6 5.80 1.80 9 -10 6 9.70 2.30 9 10 -6 8.50 2.30 -9 10 6 7.00 2.00 -9 -10 -6 10.60 2.00 9 10 6 14.10 2.30 9 -10 -6 10.10 2.10 -9 -10 6 10.70 2.30 -10 10 6 0.20 2.20 10 -10 6 2.30 2.30 -10 -10 -6 0.30 2.10 10 10 -6 -2.40 2.20 -10 -10 6 1.00 2.30 10 -10 -6 0.00 2.00 10 10 6 1.20 2.10 -11 -10 -6 6.70 2.40 -11 10 6 6.30 2.70 11 -10 6 10.10 2.70 11 10 -6 6.80 3.10 -11 -10 6 7.90 2.50 11 -10 -6 14.20 3.00 11 10 6 10.50 2.80 12 -10 6 2.20 2.80 -12 10 6 -1.70 3.00 -12 -10 -6 1.80 2.70 12 10 6 -2.20 3.20 12 -10 -6 2.80 3.20 0 11 6 0.20 1.10 0 11 -6 0.60 1.00 0 -11 -6 -0.90 1.20 0 -11 6 0.30 0.90 0 11 -6 1.80 1.00 -1 -11 -6 31.10 3.00 1 11 -6 29.40 2.90 -1 11 6 32.60 3.00 1 -11 6 30.80 3.00 1 11 -6 32.30 3.10 1 11 6 30.80 2.80 -1 11 -6 35.20 3.00 1 11 6 31.90 3.00 -1 11 -6 28.20 2.90 -1 -11 6 34.40 3.10 1 -11 -6 34.60 3.00 2 11 -6 45.10 3.60 2 11 -6 46.70 3.90 2 -11 6 40.60 3.70 -2 -11 -6 40.40 3.80 -2 11 6 38.30 3.70 -2 11 -6 46.40 3.80 2 11 6 35.10 3.70 2 -11 -6 46.30 3.80 -2 -11 6 40.50 3.80 2 11 6 45.30 3.70 -2 11 -6 40.80 3.70 -3 11 6 2.10 1.20 -3 -11 -6 2.90 1.30 3 11 -6 2.90 1.30 3 -11 6 2.80 1.10 -3 -11 6 2.50 1.20 3 -11 -6 2.40 1.40 3 11 6 3.20 1.10 3 11 6 2.30 1.10 -3 11 -6 5.30 1.30 -3 11 -6 4.90 1.40 -4 -11 -6 75.39 6.50 4 11 -6 79.09 6.60 -4 11 6 89.99 6.60 4 -11 6 78.19 6.50 4 11 6 75.09 6.40 4 11 6 81.39 6.50 4 -11 -6 77.49 6.60 -4 -11 6 81.89 6.60 -4 11 -6 79.59 6.50 -4 11 -6 69.39 6.50 5 11 -6 2.80 1.50 -5 11 6 0.00 1.30 -5 -11 -6 1.90 1.40 5 11 6 0.00 1.20 -5 -11 6 2.00 1.50 -5 11 -6 0.60 1.10 -5 11 -6 0.10 1.40 5 -11 -6 -0.40 1.50 -6 11 6 11.00 2.00 -6 -11 -6 9.50 2.00 6 11 -6 15.20 2.20 -6 11 -6 8.10 1.90 -6 -11 6 11.60 1.90 6 -11 -6 17.30 2.10 -6 11 -6 13.60 1.90 6 11 6 14.00 1.90 7 11 -6 72.19 7.10 -7 11 6 94.39 7.20 -7 -11 -6 86.79 7.10 -7 -11 6 87.09 7.00 7 -11 -6 97.99 7.20 -7 11 -6 80.69 7.00 7 11 6 70.19 7.10 -7 11 -6 81.39 7.00 8 11 -6 15.50 2.50 -8 11 6 18.10 2.40 -8 -11 -6 9.20 2.10 8 11 6 19.90 2.50 8 -11 -6 19.20 2.40 -8 -11 6 13.50 2.30 -8 11 -6 17.00 2.60 -9 11 6 -0.40 1.80 9 11 -6 3.20 2.20 -9 -11 -6 2.20 2.00 9 11 6 -1.60 1.80 -9 -11 6 3.60 2.10 9 -11 -6 -1.30 1.90 -9 11 -6 0.00 1.90 -10 -11 -6 0.60 2.10 -10 11 6 7.00 2.30 10 11 -6 3.60 2.60 10 -11 6 4.10 2.50 10 11 6 3.50 2.30 -10 -11 6 3.50 2.50 10 -11 -6 4.40 2.50 11 -11 6 -0.60 2.60 11 11 -6 -0.10 2.80 -11 11 6 -1.50 2.50 -11 -11 -6 -1.10 2.40 11 11 6 0.10 2.70 -11 -11 6 -3.50 2.80 11 -11 -6 -1.10 2.40 -12 11 6 -0.90 3.30 12 -11 6 0.60 3.40 -12 -11 -6 3.80 2.80 12 -11 -6 -1.10 5.50 0 12 -6 0.80 1.20 0 -12 6 -0.20 1.20 0 12 -6 1.00 1.20 0 12 6 0.80 1.20 0 -12 -6 1.10 1.40 -1 12 6 129.89 9.20 1 -12 6 110.79 9.10 1 12 -6 107.99 9.20 1 12 -6 105.49 9.10 -1 -12 -6 114.79 9.20 1 12 6 112.09 9.20 -1 12 -6 114.39 9.20 -1 -12 6 115.59 9.20 -1 12 -6 117.09 9.20 1 -12 -6 117.39 9.20 -2 -12 -6 0.90 1.20 2 12 -6 -0.30 1.20 -2 12 6 0.10 1.30 2 -12 6 0.90 1.20 2 12 -6 0.10 1.10 -2 12 -6 0.60 1.10 -2 12 -6 0.40 1.20 2 -12 -6 0.70 1.30 2 12 6 -0.30 1.20 -2 -12 6 -0.50 1.30 2 12 6 0.60 1.20 3 -12 6 81.99 7.70 -3 12 6 96.89 7.80 -3 -12 -6 100.59 7.80 3 12 -6 96.79 7.80 3 -12 -6 98.49 7.80 3 12 6 93.59 7.70 -3 -12 6 97.49 7.70 -3 12 -6 91.79 7.70 -3 12 -6 95.19 7.70 3 12 6 95.49 7.70 4 12 -6 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2.50 -2 -5 14 27.10 2.50 -2 -5 14 30.30 2.50 2 -5 -14 27.20 2.50 -2 5 -14 25.20 2.60 2 5 14 26.50 2.60 3 5 -14 14.10 1.80 -3 -5 -14 15.70 1.60 3 -5 14 12.20 1.60 -3 -5 -14 12.50 1.60 -3 5 14 13.20 1.60 3 -5 -14 16.70 1.70 -3 5 -14 10.90 1.70 -3 -5 14 16.40 1.60 3 5 14 8.40 1.70 -3 -5 14 12.80 1.60 -4 5 14 58.49 5.10 4 -5 14 62.29 5.20 -4 -5 -14 61.59 5.10 -4 -5 -14 61.79 5.10 4 5 -14 69.89 5.30 -4 -5 14 62.49 5.00 4 5 14 62.09 5.20 -4 5 -14 54.39 5.20 -4 -5 14 59.19 5.20 4 -5 -14 63.39 5.20 -5 -5 -14 14.30 1.60 5 -5 14 12.60 1.80 -5 -5 -14 9.70 1.70 -5 5 14 13.60 1.80 5 5 -14 12.10 1.90 5 5 14 14.40 1.80 -5 5 -14 13.60 1.80 -5 -5 14 9.40 1.60 5 -5 -14 11.30 1.70 6 5 -14 4.50 1.80 6 -5 14 3.40 1.40 -6 -5 -14 4.30 1.50 -6 5 14 2.90 1.20 -6 -5 -14 4.90 1.30 6 5 14 4.70 1.50 -6 -5 14 1.60 1.50 -6 5 -14 5.60 1.50 6 -5 -14 3.10 1.40 7 5 -14 90.59 8.00 7 -5 14 91.99 7.80 -7 5 14 93.29 7.70 -7 -5 -14 96.69 7.90 -7 -5 14 96.69 7.80 -7 5 -14 81.39 7.80 7 -5 -14 100.99 7.90 7 5 14 104.09 7.90 -8 5 14 67.49 5.70 -8 -5 -14 59.09 6.00 8 -5 14 62.59 5.90 8 5 -14 74.69 6.00 8 -5 -14 62.99 5.80 -8 -5 14 72.69 6.00 -8 5 -14 64.99 5.80 9 5 -14 1.20 2.20 -9 5 14 1.00 1.70 9 -5 14 -1.90 1.70 -9 -5 -14 0.20 1.80 9 -5 -14 1.10 1.70 -9 5 -14 0.30 2.00 -9 -5 14 1.70 1.70 10 5 -14 18.10 3.00 10 -5 14 15.20 2.60 -10 -5 -14 20.90 3.00 -10 -5 14 17.60 2.80 -10 5 -14 17.70 2.80 10 -5 -14 19.40 2.80 11 5 -14 4.50 3.00 11 -5 14 7.40 2.70 -11 -5 -14 5.50 2.80 -11 -5 14 3.00 2.40 11 -5 -14 7.50 2.50 -11 5 -14 5.80 2.90 12 -5 14 17.70 3.50 12 5 -14 11.50 3.50 -12 5 -14 15.60 3.50 -12 -5 14 14.20 3.20 12 -5 -14 14.90 3.30 12 5 14 8.40 3.10 0 6 -14 73.49 6.70 0 -6 -14 85.99 6.60 0 -6 14 80.39 6.50 0 -6 -14 80.99 6.70 0 -6 14 89.29 6.70 1 -6 14 2.10 1.00 -1 6 14 3.30 1.20 1 6 -14 2.90 1.10 -1 -6 -14 3.40 1.10 -1 -6 -14 4.00 0.90 -1 -6 14 2.90 0.90 -1 -6 14 3.30 1.00 1 -6 -14 3.30 1.00 -1 6 -14 3.30 1.10 1 6 14 4.40 1.10 2 -6 14 0.20 1.00 2 6 -14 0.30 1.10 -2 6 14 -0.80 0.90 -2 -6 -14 -0.60 1.00 -2 -6 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14 245.18 18.30 2 -7 -14 243.38 18.40 -2 -7 14 234.98 18.30 2 7 14 237.68 18.40 -2 7 -14 228.68 18.40 3 7 -14 6.40 1.50 -3 -7 -14 2.20 1.20 -3 -7 -14 3.20 1.20 -3 7 14 2.00 1.10 3 -7 14 4.70 1.20 -3 -7 14 2.60 1.00 -3 7 -14 2.80 1.20 3 7 14 1.10 1.20 3 -7 -14 3.00 1.20 -3 -7 14 2.50 1.00 -4 7 14 26.40 2.80 4 -7 14 31.00 3.00 -4 -7 -14 31.70 2.90 -4 -7 -14 31.10 3.00 4 7 -14 31.40 3.10 -4 -7 14 32.60 2.90 4 -7 -14 28.80 3.00 4 7 14 25.90 2.90 -4 7 -14 29.50 3.00 -5 -7 -14 130.39 10.10 -5 7 14 117.59 10.00 -5 -7 -14 114.99 10.00 5 7 -14 138.39 10.20 5 -7 14 121.09 10.00 5 -7 -14 120.59 10.00 -5 -7 14 128.89 10.00 5 7 14 136.79 10.10 -5 7 -14 116.39 10.00 6 7 -14 1.10 1.80 -6 7 14 2.60 1.30 -6 -7 -14 1.80 1.60 6 -7 14 2.30 1.50 -6 -7 -14 1.50 1.40 -6 7 -14 2.40 1.50 -6 -7 14 0.50 1.40 6 7 14 4.70 1.60 6 -7 -14 1.70 1.50 -7 -7 -14 2.80 1.90 7 7 -14 5.50 1.90 7 -7 14 1.90 1.60 -7 -7 -14 2.70 1.50 -7 7 14 2.60 1.40 7 -7 -14 3.00 1.60 7 7 14 5.80 2.00 -7 7 -14 6.20 1.70 -7 -7 14 5.80 1.70 -8 7 14 41.30 4.20 8 -7 14 44.60 4.20 -8 -7 -14 40.50 4.30 8 7 -14 52.69 4.70 -8 -7 14 44.90 4.20 -8 7 -14 44.90 4.50 8 -7 -14 32.90 4.00 9 7 -14 4.30 2.20 9 -7 14 3.00 1.90 -9 -7 -14 2.40 2.10 -9 7 14 5.10 2.00 -9 7 -14 3.60 2.00 -9 -7 14 1.60 1.90 9 -7 -14 2.10 2.00 10 7 -14 12.10 2.90 10 -7 14 8.30 2.40 -10 -7 14 9.30 2.50 -10 7 -14 8.50 2.80 10 -7 -14 8.30 2.70 10 7 14 10.70 2.50 11 7 -14 1.70 3.20 11 -7 14 -1.30 2.40 -11 7 -14 2.70 2.60 -11 -7 14 3.80 2.80 11 7 14 2.00 2.90 11 -7 -14 4.20 2.60 12 -7 14 27.40 3.90 12 7 -14 23.80 5.00 -12 7 -14 25.20 4.50 0 8 14 55.09 5.00 0 -8 -14 58.89 5.10 0 8 -14 61.29 5.10 0 -8 14 60.99 5.00 1 8 -14 3.90 1.30 -1 -8 -14 4.20 1.20 1 -8 14 3.60 1.20 -1 8 14 4.20 1.20 1 -8 -14 6.00 1.40 -1 8 -14 4.50 1.30 -1 -8 14 2.10 1.10 1 8 14 3.50 1.20 -1 -8 14 2.60 1.00 -2 -8 -14 8.90 1.40 2 -8 14 8.20 1.50 -2 8 14 7.00 1.40 -2 -8 -14 6.50 1.30 2 8 -14 8.90 1.60 -2 -8 14 10.10 1.40 -2 8 -14 6.20 1.40 2 8 14 4.90 1.30 2 -8 -14 7.40 1.40 -2 -8 14 3.80 1.20 3 -8 14 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250.97 22.10 -3 0 22 6.70 1.80 -3 0 -22 7.50 1.80 3 0 -22 7.10 1.70 3 0 -22 11.00 1.70 3 0 22 9.50 2.10 4 0 22 1.20 1.70 -4 0 22 3.40 1.60 4 0 -22 3.00 1.50 -4 0 -22 0.30 1.60 4 0 -22 2.80 1.80 5 0 22 12.90 2.30 -5 0 22 8.40 2.10 -5 0 22 14.70 2.10 -5 0 -22 12.80 2.20 6 0 22 52.49 4.60 -6 0 22 46.80 4.50 -6 0 -22 36.10 4.30 7 0 22 1.60 2.40 -7 0 -22 1.20 2.00 -7 0 22 2.20 2.20 -8 0 -22 61.99 6.50 -8 0 22 75.99 6.50 8 0 22 74.39 6.90 9 0 22 3.30 3.00 -9 0 -22 5.90 2.60 -9 0 22 3.90 2.90 -10 0 -22 68.49 6.60 -10 0 22 61.39 6.40 10 0 22 59.69 6.40 0 1 22 0.30 1.40 0 -1 -22 0.60 1.40 0 1 -22 0.60 1.50 0 -1 22 0.10 1.40 1 1 -22 21.00 2.30 -1 -1 -22 16.30 2.20 1 -1 22 18.30 2.30 -1 1 22 12.90 2.20 1 -1 -22 19.10 2.30 -1 -1 22 19.50 2.40 -1 1 -22 18.30 2.30 1 1 22 15.60 2.30 2 1 -22 3.90 1.50 -2 1 22 4.00 1.50 2 -1 22 1.10 1.60 -2 -1 -22 4.10 1.60 2 -1 -22 3.80 1.60 -2 -1 22 7.80 1.60 -2 1 -22 5.50 1.60 2 1 22 0.80 1.80 2 -1 -22 6.60 1.50 3 1 -22 1.70 1.70 3 1 -22 2.70 1.40 -3 -1 -22 1.90 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6 -5 -28 8.00 3.10 -6 5 -28 16.40 5.30 6 5 28 10.90 3.80 7 -5 -28 2.30 3.80 0 -6 28 7.10 2.70 0 6 28 4.80 2.50 0 6 -28 -0.50 2.40 -1 6 28 16.20 2.90 1 6 -28 12.20 2.90 1 -6 28 13.80 3.20 -1 -6 28 15.40 3.10 1 6 28 15.20 2.90 -1 6 -28 12.40 2.90 2 -6 28 1.70 2.90 -2 6 28 0.60 2.40 2 6 -28 3.30 2.90 2 6 28 0.60 2.50 -2 6 -28 -0.10 2.70 -3 6 28 28.00 3.60 3 6 -28 21.20 3.60 3 -6 28 29.00 4.10 3 6 28 32.90 3.80 -3 6 -28 20.90 3.60 4 -6 28 -2.00 2.80 -4 6 28 3.40 2.50 4 6 -28 -2.20 3.10 4 -6 -28 1.90 2.80 -4 6 -28 1.20 2.50 4 6 28 2.80 2.70 5 6 -28 2.90 3.40 -5 6 28 0.10 2.50 5 -6 28 1.40 3.00 5 6 28 2.70 3.00 -5 6 -28 -0.40 2.60 5 -6 -28 1.60 2.90 6 6 -28 7.70 3.50 -6 6 28 2.70 3.10 6 -6 -28 7.00 3.60 6 6 28 14.80 3.90 0 7 28 1.30 2.80 0 7 -28 0.60 2.50 0 -7 28 -2.80 2.40 -1 7 28 8.40 2.70 1 -7 28 11.40 2.90 1 7 -28 5.20 2.90 -1 -7 28 3.70 2.50 1 7 28 10.30 2.90 -1 7 -28 9.80 2.80 2 -7 28 1.40 2.80 -2 7 28 10.90 2.70 2 7 -28 6.30 2.80 -2 7 -28 6.60 2.90 2 7 28 6.70 2.70 3 -7 28 15.10 3.20 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31 6.40 2.90 3 -2 31 8.60 3.40 -3 2 -31 11.30 3.10 3 2 31 5.10 3.60 -3 -2 31 7.50 3.10 -4 2 31 1.10 2.90 -4 2 -31 1.80 3.00 0 3 31 2.60 2.90 0 3 -31 -2.50 3.00 0 -3 31 -1.60 3.10 1 -3 31 6.40 3.20 1 3 -31 4.40 2.80 -1 3 31 5.60 3.00 -1 3 -31 5.70 2.90 1 3 31 4.40 3.00 -1 -3 31 6.70 3.00 2 -3 31 2.90 3.10 -2 3 31 -0.10 2.80 2 3 31 -0.50 3.00 -2 3 -31 -2.10 2.80 -2 -3 31 -0.30 2.80 3 -3 31 5.90 3.60 -3 3 31 0.90 3.10 -3 3 -31 2.10 3.30 -4 3 31 1.80 2.90 -4 3 -31 1.00 3.00 0 4 31 7.20 3.10 0 4 -31 10.90 3.40 0 -4 31 9.10 3.50 1 4 -31 8.60 3.10 1 -4 31 4.20 3.20 -1 4 31 14.00 3.50 1 4 31 10.10 3.30 -1 4 -31 8.20 3.10 -1 -4 31 9.10 3.10 -2 4 31 3.00 2.80 2 4 -31 1.10 3.00 2 -4 31 1.30 3.10 2 4 31 0.60 3.30 -2 -4 31 1.80 3.30 -2 4 -31 0.10 3.20 -3 4 31 9.80 3.40 -3 4 -31 2.20 3.00 -4 4 31 1.20 2.90 0 5 -31 1.20 2.90 0 5 31 -1.00 3.00 0 -5 31 -0.40 3.00 1 -5 31 5.10 3.30 1 5 -31 4.90 3.40 -1 5 31 -0.20 2.90 -1 -5 31 10.30 3.50 -1 5 -31 3.10 2.90 -2 5 31 1.80 3.70 2 5 -31 3.00 3.50 2 -5 31 6.10 3.50 -2 5 -31 6.40 3.10 3 5 -31 20.40 3.80 0 -6 31 6.40 3.70 0 6 -31 9.70 3.60 1 -6 31 2.50 3.50 1 6 -31 -0.10 3.00 -1 6 -31 -0.50 2.90 -1 -6 31 1.80 3.10 2 6 -31 -0.10 3.50 3 6 -31 -0.20 3.20 0 -7 31 0.90 3.20 1 -7 31 -1.20 3.60 0 0 32 79.89 7.70 1 0 32 0.50 3.50 -1 0 32 0.80 3.00 -2 0 32 12.50 3.40 -3 0 32 17.10 3.80 0 1 32 -1.80 3.40 0 -1 32 1.90 3.00 -1 1 32 2.20 3.40 1 -1 32 -2.60 3.40 1 1 32 -3.40 3.50 -1 -1 32 1.10 3.10 -2 1 32 -0.10 3.00 -2 -1 32 1.60 3.00 -3 1 32 1.30 3.00 -3 -1 32 -1.90 3.50 -3 1 -32 -0.40 3.10 0 2 32 2.70 3.10 0 -2 32 -0.10 3.10 -1 2 32 -1.00 3.00 1 -2 32 4.80 3.10 -1 -2 32 -2.10 3.00 -1 2 -32 4.20 3.10 -2 2 32 2.40 3.00 -2 2 -32 4.80 3.50 -2 -2 32 5.00 3.20 -3 2 32 5.30 3.10 -3 2 -32 0.10 3.10 0 -3 32 0.60 3.10 0 3 -32 -0.60 3.00 1 -3 32 3.40 3.60 -1 -3 32 1.80 3.20 -1 3 -32 0.90 3.40 -2 -3 32 3.80 3.50 -2 3 -32 -1.40 3.00 -3 3 -32 5.30 3.60 0 -4 32 0.10 3.20 0 4 -32 2.70 3.10 1 -4 32 8.80 4.50 1 4 -32 10.50 3.40 -1 4 -32 6.50 3.20 -1 -4 32 12.00 3.90 2 4 -32 0.40 3.90 -2 4 -32 5.80 3.60 -2 -4 32 0.50 4.20 0 -5 32 4.40 3.70 0 5 -32 -0.80 3.20 1 5 -32 3.20 3.20 -1 -5 32 0.80 3.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.33531(12) 0.68022(8) 0.33935(5) 0.0385(3) Uani 1 1 d . . . . . O2 O 0.33600(10) 0.48148(7) 0.47518(5) 0.0309(3) Uani 1 1 d . . . . . N1 N 0.30784(11) 0.57315(8) 0.40191(5) 0.0259(3) Uani 1 1 d . . . . . N2 N 0.48008(11) 0.58444(8) 0.45134(5) 0.0240(3) Uani 1 1 d . . . . . H2 H 0.539(2) 0.5660(13) 0.4760(8) 0.045(6) Uiso 1 1 d . . . . . C1 C 0.49855(13) 0.64548(9) 0.40708(6) 0.0235(3) Uani 1 1 d . . . . . C2 C 0.37159(15) 0.63796(10) 0.37749(6) 0.0273(3) Uani 1 1 d . . . . . C3 C 0.37333(13) 0.53981(9) 0.44630(6) 0.0241(3) Uani 1 1 d . . . . . C4 C 0.18987(14) 0.53876(11) 0.38085(7) 0.0304(3) Uani 1 1 d . . . . . H4A H 0.1394(18) 0.5228(12) 0.4129(8) 0.037(5) Uiso 1 1 d . . . . . H4B H 0.1471(17) 0.5856(13) 0.3640(8) 0.038(5) Uiso 1 1 d . . . . . C5 C 0.21126(16) 0.46656(11) 0.34090(7) 0.0331(4) Uani 1 1 d . . . . . H5A H 0.2454(17) 0.4159(12) 0.3607(7) 0.034(5) Uiso 1 1 d . . . . . H5B H 0.2702(19) 0.4854(12) 0.3140(8) 0.037(5) Uiso 1 1 d . . . . . C6 C 0.09186(18) 0.44142(12) 0.31186(8) 0.0415(4) Uani 1 1 d . . . . . H6A H 0.025(2) 0.4211(16) 0.3411(10) 0.067(7) Uiso 1 1 d . . . . . H6B H 0.059(2) 0.4950(17) 0.2967(11) 0.071(7) Uiso 1 1 d . . . . . C7 C 0.1069(2) 0.37575(12) 0.26736(8) 0.0477(5) Uani 0.684(2) 1 d D . P A 1 H7A H 0.140811 0.322192 0.282764 0.057 Uiso 0.684(2) 1 calc R U P A 1 H7B H 0.165522 0.396798 0.239156 0.057 Uiso 0.684(2) 1 calc R U P A 1 C8 C -0.0235(3) 0.35947(17) 0.24178(11) 0.0425(7) Uani 0.684(2) 1 d D . P A 1 H8A H -0.080554 0.340867 0.271257 0.051 Uiso 0.684(2) 1 calc R U P A 1 H8B H -0.055531 0.414372 0.227633 0.051 Uiso 0.684(2) 1 calc R U P A 1 C9 C -0.0302(2) 0.29496(18) 0.19642(10) 0.0421(6) Uani 0.684(2) 1 d D . P A 1 H9A H -0.118996 0.282916 0.188335 0.050 Uiso 0.684(2) 1 calc R U P A 1 H9B H 0.008621 0.241203 0.209069 0.050 Uiso 0.684(2) 1 calc R U P A 1 C10 C 0.0340(3) 0.3232(2) 0.14413(11) 0.0476(6) Uani 0.684(2) 1 d D . P A 1 H10A H 0.002819 0.380240 0.133587 0.057 Uiso 0.684(2) 1 calc R U P A 1 H10B H 0.124932 0.327704 0.150632 0.057 Uiso 0.684(2) 1 calc R U P A 1 C11 C 0.0105(6) 0.2613(4) 0.09809(18) 0.0645(10) Uani 0.684(2) 1 d D . P A 1 H11A H 0.053012 0.281315 0.065056 0.097 Uiso 0.684(2) 1 calc R U P A 1 H11B H 0.042580 0.204985 0.108171 0.097 Uiso 0.684(2) 1 calc R U P A 1 H11C H -0.079444 0.257482 0.091139 0.097 Uiso 0.684(2) 1 calc R U P A 1 C7A C 0.1069(2) 0.37575(12) 0.26736(8) 0.0477(5) Uani 0.316(2) 1 d D . P A 2 H7C H 0.105359 0.319574 0.285764 0.057 Uiso 0.316(2) 1 calc R U P A 2 H7D H 0.192592 0.383068 0.252941 0.057 Uiso 0.316(2) 1 calc R U P A 2 C8A C 0.0225(6) 0.3676(3) 0.21792(19) 0.0425(7) Uani 0.316(2) 1 d D . P A 2 H8C H -0.062119 0.352740 0.231067 0.051 Uiso 0.316(2) 1 calc R U P A 2 H8D H 0.016812 0.424293 0.200408 0.051 Uiso 0.316(2) 1 calc R U P A 2 C9A C 0.0581(5) 0.3043(4) 0.1749(2) 0.0421(6) Uani 0.316(2) 1 d D . P A 2 H9C H 0.073624 0.248257 0.192118 0.050 Uiso 0.316(2) 1 calc R U P A 2 H9D H 0.136410 0.322955 0.157012 0.050 Uiso 0.316(2) 1 calc R U P A 2 C10A C -0.0435(5) 0.2951(4) 0.1320(2) 0.0476(6) Uani 0.316(2) 1 d D . P A 2 H10C H -0.117489 0.267700 0.148721 0.057 Uiso 0.316(2) 1 calc R U P A 2 H10D H -0.068744 0.352372 0.119108 0.057 Uiso 0.316(2) 1 calc R U P A 2 C11A C -0.0009(13) 0.2428(10) 0.0840(4) 0.0645(10) Uani 0.316(2) 1 d D . P A 2 H11D H -0.068781 0.238320 0.057389 0.097 Uiso 0.316(2) 1 calc R U P A 2 H11E H 0.071382 0.270304 0.066943 0.097 Uiso 0.316(2) 1 calc R U P A 2 H11F H 0.022657 0.185667 0.096544 0.097 Uiso 0.316(2) 1 calc R U P A 2 C12 C 0.52079(13) 0.73514(9) 0.42966(6) 0.0240(3) Uani 1 1 d . . . . . C13 C 0.42174(15) 0.78553(10) 0.44700(7) 0.0315(3) Uani 1 1 d . . . . . H13 H 0.3405(18) 0.7641(12) 0.4427(8) 0.035(5) Uiso 1 1 d . . . . . C14 C 0.44298(17) 0.86504(11) 0.46929(8) 0.0390(4) Uani 1 1 d . . . . . H14 H 0.375(2) 0.9007(15) 0.4806(10) 0.059(6) Uiso 1 1 d . . . . . C15 C 0.56401(18) 0.89538(11) 0.47466(8) 0.0424(4) Uani 1 1 d . . . . . H15 H 0.5789(19) 0.9536(13) 0.4916(8) 0.044(5) Uiso 1 1 d . . . . . C16 C 0.66371(17) 0.84577(12) 0.45778(9) 0.0429(4) Uani 1 1 d . . . . . H16 H 0.751(2) 0.8679(14) 0.4602(9) 0.053(6) Uiso 1 1 d . . . . . C17 C 0.64206(15) 0.76573(10) 0.43551(7) 0.0336(4) Uani 1 1 d . . . . . H17 H 0.7118(19) 0.7340(13) 0.4227(8) 0.042(5) Uiso 1 1 d . . . . . C18 C 0.60093(15) 0.61821(10) 0.36724(6) 0.0289(3) Uani 1 1 d . . . . . C19 C 0.6164(2) 0.66353(14) 0.31905(7) 0.0444(4) Uani 1 1 d . . . . . H19 H 0.565(2) 0.7091(15) 0.3121(10) 0.058(7) Uiso 1 1 d . . . . . C20 C 0.7112(2) 0.64236(17) 0.28300(9) 0.0586(6) Uani 1 1 d . . . . . H20 H 0.720(3) 0.6718(16) 0.2539(12) 0.072(8) Uiso 1 1 d . . . . . C21 C 0.7906(2) 0.57658(16) 0.29486(10) 0.0590(6) Uani 1 1 d . . . . . H21 H 0.857(2) 0.5639(16) 0.2693(12) 0.076(8) Uiso 1 1 d . . . . . C22 C 0.7757(2) 0.53048(15) 0.34221(11) 0.0603(6) Uani 1 1 d . . . . . H22 H 0.832(2) 0.4834(17) 0.3530(11) 0.071(8) Uiso 1 1 d . . . . . C23 C 0.68026(18) 0.55122(11) 0.37867(9) 0.0421(4) Uani 1 1 d . . . . . H23 H 0.671(2) 0.5173(14) 0.4128(10) 0.051(6) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0459(7) 0.0385(7) 0.0310(6) 0.0098(5) -0.0151(5) -0.0032(5) O2 0.0244(5) 0.0337(6) 0.0347(6) 0.0106(5) -0.0023(4) -0.0037(4) N1 0.0250(6) 0.0292(6) 0.0237(6) 0.0020(5) -0.0052(5) -0.0004(5) N2 0.0218(6) 0.0268(6) 0.0235(6) 0.0061(5) -0.0037(5) -0.0012(5) C1 0.0277(7) 0.0226(7) 0.0204(7) 0.0025(5) -0.0013(5) 0.0000(5) C2 0.0313(8) 0.0274(7) 0.0233(7) -0.0001(6) -0.0048(6) 0.0007(6) C3 0.0225(7) 0.0258(7) 0.0241(7) 0.0012(5) -0.0003(5) 0.0025(5) C4 0.0231(7) 0.0366(9) 0.0315(8) -0.0001(6) -0.0066(6) -0.0008(6) C5 0.0286(8) 0.0358(9) 0.0348(8) -0.0030(7) -0.0060(7) 0.0002(7) C6 0.0393(10) 0.0399(10) 0.0454(10) -0.0038(8) -0.0166(8) 0.0007(8) C7 0.0648(13) 0.0355(9) 0.0428(10) -0.0014(8) -0.0192(9) 0.0010(9) C8 0.0587(19) 0.0400(12) 0.0289(14) 0.0021(12) -0.0135(12) -0.0011(12) C9 0.0377(12) 0.0489(14) 0.0396(13) -0.0050(11) -0.0038(10) -0.0064(11) C10 0.0428(15) 0.0604(17) 0.0394(14) -0.0032(12) -0.0030(12) -0.0095(12) C11 0.064(2) 0.084(3) 0.045(3) -0.0188(18) 0.009(2) -0.011(2) C7A 0.0648(13) 0.0355(9) 0.0428(10) -0.0014(8) -0.0192(9) 0.0010(9) C8A 0.0587(19) 0.0400(12) 0.0289(14) 0.0021(12) -0.0135(12) -0.0011(12) C9A 0.0377(12) 0.0489(14) 0.0396(13) -0.0050(11) -0.0038(10) -0.0064(11) C10A 0.0428(15) 0.0604(17) 0.0394(14) -0.0032(12) -0.0030(12) -0.0095(12) C11A 0.064(2) 0.084(3) 0.045(3) -0.0188(18) 0.009(2) -0.011(2) C12 0.0268(7) 0.0242(7) 0.0209(7) 0.0014(5) -0.0017(5) 0.0025(5) C13 0.0270(8) 0.0312(8) 0.0363(8) -0.0010(6) -0.0023(6) 0.0046(6) C14 0.0372(9) 0.0330(9) 0.0470(10) -0.0072(7) -0.0012(8) 0.0118(7) C15 0.0456(10) 0.0284(8) 0.0531(11) -0.0135(8) -0.0062(9) 0.0048(7) C16 0.0335(9) 0.0362(9) 0.0590(12) -0.0152(8) -0.0049(8) -0.0013(7) C17 0.0283(8) 0.0305(8) 0.0421(9) -0.0097(7) -0.0012(7) 0.0029(6) C18 0.0325(8) 0.0280(7) 0.0263(7) -0.0061(6) 0.0049(6) -0.0042(6) C19 0.0516(11) 0.0533(11) 0.0281(9) 0.0024(8) 0.0087(8) 0.0000(9) C20 0.0676(15) 0.0772(16) 0.0310(10) -0.0052(10) 0.0188(10) -0.0115(13) C21 0.0543(13) 0.0679(14) 0.0550(13) -0.0278(11) 0.0288(11) -0.0085(11) C22 0.0538(13) 0.0495(12) 0.0777(16) -0.0138(11) 0.0298(12) 0.0079(10) C23 0.0417(10) 0.0333(9) 0.0515(11) -0.0011(8) 0.0164(8) 0.0042(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C2 N1 C3 111.68(12) . . C2 N1 C4 123.47(13) . . C3 N1 C4 124.66(13) . . C3 N2 C1 112.85(12) . . C3 N2 H2 118.6(13) . . C1 N2 H2 127.0(13) . . N2 C1 C18 112.79(12) . . N2 C1 C12 110.86(11) . . C18 C1 C12 112.09(12) . . N2 C1 C2 100.29(11) . . C18 C1 C2 108.11(12) . . C12 C1 C2 112.12(12) . . O1 C2 N1 125.92(14) . . O1 C2 C1 127.07(14) . . N1 C2 C1 107.00(12) . . O2 C3 N2 127.83(13) . . O2 C3 N1 124.49(13) . . N2 C3 N1 107.66(12) . . N1 C4 C5 111.82(13) . . N1 C4 H4A 106.6(11) . . C5 C4 H4A 114.0(11) . . N1 C4 H4B 106.3(12) . . C5 C4 H4B 111.6(12) . . H4A C4 H4B 106.0(16) . . C4 C5 C6 111.72(14) . . C4 C5 H5A 109.6(10) . . C6 C5 H5A 109.3(10) . . C4 C5 H5B 108.2(12) . . C6 C5 H5B 108.3(12) . . H5A C5 H5B 109.7(16) . . C7A C6 C5 115.24(17) . . C7 C6 C5 115.24(17) . . C7A C6 H6A 110.8(14) . . C7 C6 H6A 110.8(14) . . C5 C6 H6A 109.2(13) . . C7A C6 H6B 110.4(15) . . C7 C6 H6B 110.4(15) . . C5 C6 H6B 104.9(15) . . H6A C6 H6B 106(2) . . C6 C7 C8 107.92(18) . . C6 C7 H7A 110.1 . . C8 C7 H7A 110.1 . . C6 C7 H7B 110.1 . . C8 C7 H7B 110.1 . . H7A C7 H7B 108.4 . . C9 C8 C7 116.9(2) . . C9 C8 H8A 108.1 . . C7 C8 H8A 108.1 . . C9 C8 H8B 108.1 . . C7 C8 H8B 108.1 . . H8A C8 H8B 107.3 . . C8 C9 C10 113.9(2) . . C8 C9 H9A 108.8 . . C10 C9 H9A 108.8 . . C8 C9 H9B 108.8 . . C10 C9 H9B 108.8 . . H9A C9 H9B 107.7 . . C11 C10 C9 111.5(3) . . C11 C10 H10A 109.3 . . C9 C10 H10A 109.3 . . C11 C10 H10B 109.3 . . C9 C10 H10B 109.3 . . H10A C10 H10B 108.0 . . C10 C11 H11A 109.5 . . C10 C11 H11B 109.5 . . H11A C11 H11B 109.5 . . C10 C11 H11C 109.5 . . H11A C11 H11C 109.5 . . H11B C11 H11C 109.5 . . C6 C7A C8A 124.8(2) . . C6 C7A H7C 106.1 . . C8A C7A H7C 106.1 . . C6 C7A H7D 106.1 . . C8A C7A H7D 106.1 . . H7C C7A H7D 106.3 . . C9A C8A C7A 117.8(3) . . C9A C8A H8C 107.8 . . C7A C8A H8C 107.8 . . C9A C8A H8D 107.8 . . C7A C8A H8D 107.8 . . H8C C8A H8D 107.2 . . C8A C9A C10A 111.6(4) . . C8A C9A H9C 109.3 . . C10A C9A H9C 109.3 . . C8A C9A H9D 109.3 . . C10A C9A H9D 109.3 . . H9C C9A H9D 108.0 . . C11A C10A C9A 111.9(5) . . C11A C10A H10C 109.2 . . C9A C10A H10C 109.2 . . C11A C10A H10D 109.2 . . C9A C10A H10D 109.2 . . H10C C10A H10D 107.9 . . C10A C11A H11D 109.5 . . C10A C11A H11E 109.5 . . H11D C11A H11E 109.5 . . C10A C11A H11F 109.5 . . H11D C11A H11F 109.5 . . H11E C11A H11F 109.5 . . C13 C12 C17 119.01(14) . . C13 C12 C1 120.97(13) . . C17 C12 C1 119.95(13) . . C14 C13 C12 120.60(16) . . C14 C13 H13 121.4(12) . . C12 C13 H13 118.0(12) . . C13 C14 C15 120.09(16) . . C13 C14 H14 121.0(14) . . C15 C14 H14 118.9(14) . . C16 C15 C14 119.98(16) . . C16 C15 H15 120.4(12) . . C14 C15 H15 119.6(12) . . C15 C16 C17 119.79(17) . . C15 C16 H16 120.6(13) . . C17 C16 H16 119.5(13) . . C16 C17 C12 120.53(15) . . C16 C17 H17 118.1(12) . . C12 C17 H17 121.3(12) . . C23 C18 C19 119.27(16) . . C23 C18 C1 121.70(14) . . C19 C18 C1 119.01(15) . . C20 C19 C18 120.4(2) . . C20 C19 H19 120.6(15) . . C18 C19 H19 118.9(15) . . C21 C20 C19 120.1(2) . . C21 C20 H20 120.9(19) . . C19 C20 H20 119.0(19) . . C20 C21 C22 120.20(19) . . C20 C21 H21 118.2(16) . . C22 C21 H21 121.6(16) . . C21 C22 C23 120.1(2) . . C21 C22 H22 123.2(15) . . C23 C22 H22 116.7(16) . . C18 C23 C22 119.94(19) . . C18 C23 H23 121.1(13) . . C22 C23 H23 118.9(13) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 O1 C2 1.2095(18) . O2 C3 1.2238(18) . N1 C2 1.363(2) . N1 C3 1.3953(18) . N1 C4 1.4677(19) . N2 C3 1.3466(19) . N2 C1 1.4597(18) . N2 H2 0.92(2) . C1 C18 1.529(2) . C1 C12 1.530(2) . C1 C2 1.546(2) . C4 C5 1.514(2) . C4 H4A 0.98(2) . C4 H4B 0.96(2) . C5 C6 1.516(2) . C5 H5A 1.000(19) . C5 H5B 0.96(2) . C6 C7A 1.508(3) . C6 C7 1.508(3) . C6 H6A 1.06(3) . C6 H6B 0.98(3) . C7 C8 1.552(3) . C7 H7A 0.9900 . C7 H7B 0.9900 . C8 C9 1.504(4) . C8 H8A 0.9900 . C8 H8B 0.9900 . C9 C10 1.519(3) . C9 H9A 0.9900 . C9 H9B 0.9900 . C10 C11 1.508(4) . C10 H10A 0.9900 . C10 H10B 0.9900 . C11 H11A 0.9800 . C11 H11B 0.9800 . C11 H11C 0.9800 . C7A C8A 1.516(4) . C7A H7C 0.9900 . C7A H7D 0.9900 . C8A C9A 1.497(4) . C8A H8C 0.9900 . C8A H8D 0.9900 . C9A C10A 1.519(4) . C9A H9C 0.9900 . C9A H9D 0.9900 . C10A C11A 1.504(5) . C10A H10C 0.9900 . C10A H10D 0.9900 . C11A H11D 0.9800 . C11A H11E 0.9800 . C11A H11F 0.9800 . C12 C13 1.390(2) . C12 C17 1.392(2) . C13 C14 1.381(2) . C13 H13 0.939(19) . C14 C15 1.387(3) . C14 H14 0.96(2) . C15 C16 1.385(2) . C15 H15 1.02(2) . C16 C17 1.389(2) . C16 H16 1.00(2) . C17 H17 0.95(2) . C18 C23 1.380(2) . C18 C19 1.387(2) . C19 C20 1.386(3) . C19 H19 0.92(2) . C20 C21 1.369(4) . C20 H20 0.86(3) . C21 C22 1.376(4) . C21 H21 0.96(3) . C22 C23 1.396(3) . C22 H22 0.99(3) . C23 H23 1.00(2) . loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag N2 H2 O2 0.92(2) 1.94(2) 2.8615(16) 175.4(19) 5_666 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 C3 N2 C1 C18 -107.46(14) . . . . C3 N2 C1 C12 125.91(13) . . . . C3 N2 C1 C2 7.31(15) . . . . C3 N1 C2 O1 -177.40(15) . . . . C4 N1 C2 O1 7.3(2) . . . . C3 N1 C2 C1 3.62(16) . . . . C4 N1 C2 C1 -171.67(13) . . . . N2 C1 C2 O1 174.72(15) . . . . C18 C1 C2 O1 -67.0(2) . . . . C12 C1 C2 O1 57.1(2) . . . . N2 C1 C2 N1 -6.32(14) . . . . C18 C1 C2 N1 111.95(13) . . . . C12 C1 C2 N1 -123.99(13) . . . . C1 N2 C3 O2 175.76(14) . . . . C1 N2 C3 N1 -5.64(16) . . . . C2 N1 C3 O2 179.66(14) . . . . C4 N1 C3 O2 -5.1(2) . . . . C2 N1 C3 N2 1.00(17) . . . . C4 N1 C3 N2 176.22(13) . . . . C2 N1 C4 C5 89.55(18) . . . . C3 N1 C4 C5 -85.13(18) . . . . N1 C4 C5 C6 -170.10(15) . . . . C4 C5 C6 C7A 174.32(16) . . . . C4 C5 C6 C7 174.32(16) . . . . C5 C6 C7 C8 -178.93(18) . . . . C6 C7 C8 C9 -179.5(2) . . . . C7 C8 C9 C10 -68.6(3) . . . . C8 C9 C10 C11 -172.8(3) . . . . C5 C6 C7A C8A -152.1(4) . . . . C6 C7A C8A C9A 174.1(4) . . . . C7A C8A C9A C10A 172.5(5) . . . . C8A C9A C10A C11A 170.9(9) . . . . N2 C1 C12 C13 -79.92(17) . . . . C18 C1 C12 C13 153.07(14) . . . . C2 C1 C12 C13 31.25(18) . . . . N2 C1 C12 C17 96.99(16) . . . . C18 C1 C12 C17 -30.02(19) . . . . C2 C1 C12 C17 -151.84(14) . . . . C17 C12 C13 C14 0.5(2) . . . . C1 C12 C13 C14 177.46(15) . . . . C12 C13 C14 C15 -0.1(3) . . . . C13 C14 C15 C16 -0.2(3) . . . . C14 C15 C16 C17 0.0(3) . . . . C15 C16 C17 C12 0.4(3) . . . . C13 C12 C17 C16 -0.7(3) . . . . C1 C12 C17 C16 -177.67(16) . . . . N2 C1 C18 C23 -11.0(2) . . . . C12 C1 C18 C23 115.02(16) . . . . C2 C1 C18 C23 -120.90(16) . . . . N2 C1 C18 C19 170.79(15) . . . . C12 C1 C18 C19 -63.24(19) . . . . C2 C1 C18 C19 60.84(18) . . . . C23 C18 C19 C20 -0.6(3) . . . . C1 C18 C19 C20 177.67(18) . . . . C18 C19 C20 C21 -0.2(3) . . . . C19 C20 C21 C22 0.9(4) . . . . C20 C21 C22 C23 -0.7(4) . . . . C19 C18 C23 C22 0.8(3) . . . . C1 C18 C23 C22 -177.44(18) . . . . C21 C22 C23 C18 -0.2(3) . . . .