#------------------------------------------------------------------------------ #$Date: 2022-06-24 09:58:32 +0300 (Fri, 24 Jun 2022) $ #$Revision: 276219 $ #$URL: file:///home/coder/svn-repositories/cod/cif/8/10/54/8105488.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_8105488 loop_ _publ_author_name 'Tan, Ming Yueh' 'Ho, Sheng Zhou' 'Tan, Kong Wai' 'Tiekink, Edward R.T.' _publ_section_title ; Crystal structure of 3-ethyl-1-[(E)-[(2E)-3-phenylprop-2-en-1-ylidene]amino]thiourea, C12H15N3S ; _journal_issue 6 _journal_name_full 'Zeitschrift f\"ur Kristallographie - New Crystal Structures' _journal_page_first 1439 _journal_page_last 1441 _journal_paper_doi 10.1515/ncrs-2020-0351 _journal_volume 235 _journal_year 2020 _chemical_formula_moiety 'C12 H15 N3 S1' _chemical_formula_sum 'C12 H15 N3 S' _chemical_formula_weight 233.33 _space_group_crystal_system orthorhombic _space_group_IT_number 61 _space_group_name_Hall '-P 2ac 2ab' _space_group_name_H-M_alt 'P b c a' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 11.9612(5) _cell_length_b 8.1215(3) _cell_length_c 27.5865(12) _cell_measurement_reflns_used 2214 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 73.9990 _cell_measurement_theta_min 3.7190 _cell_volume 2679.83(19) _computing_cell_refinement 'CrysAlis PRO [1]' _computing_data_collection 'CrysAlis PRO [1]' _computing_data_reduction 'CrysAlis PRO [1]' _computing_molecular_graphics 'ORTEP-3 for Windows [4]' _computing_publication_material 'SHELXL-2018/3 [3]' _computing_structure_refinement 'SHELXL-2018/3 [3]' _computing_structure_solution 'SHELXL-97 [2]' _diffrn_ambient_temperature 293(2) _diffrn_detector_area_resol_mean 10.4041 _diffrn_measured_fraction_theta_full 0.991 _diffrn_measured_fraction_theta_max 0.960 _diffrn_measurement_device_type 'Agilent Technologies SuperNova Dual diffractometer with Atlas detector' _diffrn_measurement_method '\w scan' _diffrn_radiation_monochromator Mirror _diffrn_radiation_source 'SuperNova (Cu) X-ray Source' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0242 _diffrn_reflns_av_unetI/netI 0.0221 _diffrn_reflns_Laue_measured_fraction_full 0.991 _diffrn_reflns_Laue_measured_fraction_max 0.960 _diffrn_reflns_limit_h_max 6 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 33 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 5668 _diffrn_reflns_point_group_measured_fraction_full 0.991 _diffrn_reflns_point_group_measured_fraction_max 0.960 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 74.176 _diffrn_reflns_theta_min 4.894 _exptl_absorpt_coefficient_mu 1.964 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.71451 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'CrysAlis PRO [1]' _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.157 _exptl_crystal_description slab _exptl_crystal_F_000 992 _exptl_crystal_size_max 0.500 _exptl_crystal_size_mid 0.500 _exptl_crystal_size_min 0.200 _refine_diff_density_max 0.249 _refine_diff_density_min -0.263 _refine_diff_density_rms 0.057 _refine_ls_extinction_coef 0.0055(5) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.037 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 153 _refine_ls_number_reflns 2612 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.037 _refine_ls_R_factor_all 0.0630 _refine_ls_R_factor_gt 0.0520 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0904P)^2^+0.2162P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1395 _refine_ls_wR_factor_ref 0.1514 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 2077 _reflns_number_total 2612 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file suppl_ncrs-2020-0351_suppl.cif _cod_data_source_block shelx _cod_original_formula_sum 'C12 H15 N3 S1' _cod_database_code 8105488 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.440 _shelx_estimated_absorpt_t_max 0.695 _shelx_res_file ; TITL exp_6994 shelx.res created by SHELXL-2018/3 at 01:03:31 on 09-Jul-2020 CELL 1.54184 11.9612 8.1215 27.5865 90.000 90.000 90.000 ZERR 4 0.0005 0.0003 0.0012 0.000 0.000 0.000 LATT 1 SYMM 1/2 - X, - Y, 1/2 + Z SYMM 1/2 + X, 1/2 - Y, - Z SYMM - X, 1/2 + Y, 1/2 - Z SFAC C H N S UNIT 96 120 24 8 MERG 2 FMAP 2 PLAN 5 SIZE 0.200 0.500 0.500 ACTA BOND $H CONF DFIX 0.86 0.01 N1 H1n N2 H2n L.S. 18 TEMP 20.00 WGHT 0.090400 0.216200 EXTI 0.005451 FVAR 5.41950 S1 4 0.407687 1.079943 0.563486 11.00000 0.07633 0.08959 = 0.07636 -0.02356 -0.02282 0.00269 N1 3 0.203997 0.967551 0.544220 11.00000 0.07831 0.09583 = 0.07778 -0.02770 0.00374 -0.01590 H1N 2 0.160636 0.895415 0.531375 11.00000 -1.20000 N2 3 0.337728 0.906721 0.489137 11.00000 0.06413 0.06497 = 0.05840 -0.00562 -0.00964 -0.00593 H2N 2 0.405986 0.907700 0.478678 11.00000 -1.20000 N3 3 0.257873 0.823824 0.462765 11.00000 0.06940 0.05620 = 0.05635 -0.00245 -0.00892 -0.00765 C1 1 0.309452 0.978989 0.531349 11.00000 0.07340 0.05543 = 0.05900 -0.00183 -0.01165 0.00192 C2 1 0.158178 1.025904 0.589850 11.00000 0.10298 0.13121 = 0.09599 -0.04052 0.02080 -0.01692 AFIX 23 H2A 2 0.197919 1.124233 0.599923 11.00000 -1.20000 H2B 2 0.168847 0.942470 0.614581 11.00000 -1.20000 AFIX 0 C3 1 0.038601 1.063200 0.585348 11.00000 0.11319 0.12604 = 0.17806 -0.03393 0.04640 0.01615 AFIX 137 H3A 2 0.028524 1.153114 0.563184 11.00000 -1.50000 H3B 2 0.009184 1.092909 0.616522 11.00000 -1.50000 H3C 2 -0.000141 0.967978 0.573391 11.00000 -1.50000 AFIX 0 C4 1 0.289043 0.770114 0.421320 11.00000 0.06435 0.04946 = 0.05731 0.00315 -0.00607 -0.00445 AFIX 43 H4 2 0.362028 0.787942 0.410951 11.00000 -1.20000 AFIX 0 C5 1 0.212358 0.682529 0.390656 11.00000 0.06119 0.04866 = 0.05554 0.00387 -0.00191 -0.00571 AFIX 43 H5 2 0.141266 0.659052 0.402428 11.00000 -1.20000 AFIX 0 C6 1 0.238978 0.633517 0.345990 11.00000 0.05962 0.04965 = 0.05776 0.00325 -0.00120 -0.00528 AFIX 43 H6 2 0.310561 0.659404 0.335262 11.00000 -1.20000 AFIX 0 C7 1 0.167746 0.543515 0.312103 11.00000 0.06433 0.04604 = 0.05181 0.00410 -0.00396 0.00041 C8 1 0.060327 0.492896 0.323680 11.00000 0.06530 0.06025 = 0.06540 0.00591 -0.01043 -0.00340 AFIX 43 H8 2 0.030544 0.519669 0.353807 11.00000 -1.20000 AFIX 0 C9 1 -0.002867 0.403859 0.291403 11.00000 0.07735 0.07224 = 0.09898 0.00292 -0.02550 -0.01208 AFIX 43 H9 2 -0.074344 0.369578 0.300014 11.00000 -1.20000 AFIX 0 C10 1 0.038560 0.365706 0.246999 11.00000 0.12052 0.08585 = 0.10224 -0.02147 -0.04273 -0.01237 AFIX 43 H10 2 -0.004487 0.305024 0.225343 11.00000 -1.20000 AFIX 0 C11 1 0.142997 0.416042 0.234070 11.00000 0.13477 0.10660 = 0.06963 -0.03082 -0.01033 0.00160 AFIX 43 H11 2 0.170577 0.391110 0.203416 11.00000 -1.20000 AFIX 0 C12 1 0.208666 0.504737 0.266590 11.00000 0.09016 0.08081 = 0.06087 -0.01085 0.00240 -0.00389 AFIX 43 H12 2 0.280185 0.537972 0.257693 11.00000 -1.20000 AFIX 0 HKLF 4 REM exp_6994 REM wR2 = 0.1514, GooF = S = 1.037, Restrained GooF = 1.037 for all data REM R1 = 0.0520 for 2077 Fo > 4sig(Fo) and 0.0630 for all 2612 data REM 153 parameters refined using 2 restraints END WGHT 0.0811 0.2479 REM Highest difference peak 0.249, deepest hole -0.263, 1-sigma level 0.057 Q1 1 0.1895 0.5403 0.2943 11.00000 0.05 0.25 Q2 1 0.1991 0.5836 0.3276 11.00000 0.05 0.22 Q3 1 0.3410 1.0796 0.5790 11.00000 0.05 0.22 Q4 1 0.1251 0.5343 0.3203 11.00000 0.05 0.21 Q5 1 0.4565 1.1036 0.5321 11.00000 0.05 0.21 ; _shelx_hkl_file ; 0 0 3 59.1045 12.5118 1 0 0 4 256942. 777.697 1 0 0 5-22.0133 16.1813 1 0 0 6 545957. 1404.57 1 0 0 7-8.36670 22.1111 1 0 0 8 234810. 1082.79 1 0 0 9 7.30960 25.1462 1 0 0 10 70011.6 665.068 1 0 0 11-49.1942 28.5075 1 0 0 12 48392.6 620.138 1 0 0 13-18.0132 36.9893 1 0 0 14 28372.4 532.581 1 0 0 15 26.7615 43.8657 1 0 0 16 2095.82 164.207 1 0 0 17 43.9677 50.0222 1 0 0 18 17.1678 45.9677 1 0 0 19 72.2969 57.1475 1 0 0 20 253.554 68.2129 1 0 0 21 56.0064 60.1072 2 0 0 21 121.688 63.2851 1 0 0 22 2027.12 212.251 2 0 0 22 2119.63 195.122 1 0 0 23 75.3787 81.1427 2 0 0 24 8520.24 428.656 2 0 0 25-49.3181 85.1506 2 0 0 26 6654.75 379.682 2 0 0 27 167.697 84.7333 2 0 0 28 2216.32 211.919 2 0 0 29-16.7012 63.0666 2 0 0 30 1568.28 160.680 2 0 0 31 40.8723 49.5930 2 0 0 32 223.089 59.8721 2 -1 0 0 53.7692 7.29870 1 -1 0 1 19.1757 7.32574 1 -1 0 2 60897.6 340.525 1 1 0 3 22.5399 8.18375 1 1 0 4 401939. 849.411 1 1 0 5 9.34022 10.6793 1 1 0 6 81644.5 491.723 1 1 0 7 20.0640 19.5997 1 -1 0 8 19563.6 335.361 1 1 0 8 20494.1 298.094 1 1 0 9 50.3281 21.5562 1 -1 0 9 55.1320 33.6364 1 -1 0 10 2795.39 146.393 1 1 0 10 3065.08 135.886 1 -1 0 11 13.2389 34.8105 1 1 0 11 27.2374 24.0536 1 1 0 12 83586.1 789.168 1 -1 0 12 80202.4 841.392 1 -1 0 13 50.9000 43.6496 1 1 0 13-13.5945 37.2904 1 -1 0 14 60911.7 815.017 1 1 0 14 64721.7 778.713 1 1 0 15 137.218 54.7287 1 -1 0 15 80.5789 53.8783 1 -1 0 16 744.957 105.885 1 1 0 16 918.640 106.280 1 1 0 17 106.920 49.1800 1 -1 0 17-33.5112 51.1917 1 1 0 18 1885.44 165.231 1 -1 0 18 1639.64 160.615 1 1 0 19-69.3391 53.7632 1 -1 0 19 35.9981 49.6407 1 -1 0 20 256.887 81.8785 1 1 0 20 180.170 68.1770 2 -1 0 21 54.6869 58.4699 1 1 0 21-8.71873 44.2656 2 -1 0 22 1110.90 155.904 1 -1 0 22 1018.02 161.947 2 1 0 22 1132.38 156.388 2 -1 0 23 3.81778 34.6000 1 1 0 23-193.798 79.9440 2 -1 0 23-137.554 90.2756 2 -1 0 24 1011.56 163.415 2 1 0 24 834.591 137.731 2 -1 0 25-94.4051 109.779 2 1 0 25-13.4163 97.9441 2 1 0 26 607.814 128.378 2 -1 0 26 553.045 133.386 2 1 0 27 287.004 91.5450 2 -1 0 27 33.7122 89.9968 2 1 0 28 18187.1 552.019 2 -1 0 28 17823.3 595.771 2 1 0 29 165.263 65.5555 2 -1 0 29 25.1998 60.1427 2 -1 0 30 2533.21 211.496 2 -1 0 31 50.1602 62.8612 2 -1 0 32 18.9516 39.9951 2 -1 0 33-41.0021 38.9674 2 -2 0 0 244869. 649.736 1 -2 0 -1 16.2105 7.19013 1 -2 0 1 8.02910 12.4247 1 -2 0 -2 237141. 440.976 1 -2 0 2 240462. 815.360 1 -2 0 3-1.06397 16.6828 1 -2 0 -3 27.0864 5.17012 1 -2 0 4 4639.46 142.408 1 2 0 7-3.76996 12.0405 1 2 0 8 48926.3 433.762 1 -2 0 8 50902.7 586.521 1 -2 0 9 21.6166 32.4515 1 2 0 9 27.1762 20.1011 1 -2 0 10 13446.4 338.368 1 2 0 10 13862.8 270.954 1 2 0 11 5.37840 19.3908 1 -2 0 11-44.9243 42.7865 1 -2 0 12 17327.0 420.292 1 2 0 12 17246.2 344.371 1 -2 0 13-56.6965 63.4919 1 2 0 13-84.4638 39.8755 1 2 0 14 74157.8 793.670 1 -2 0 14 75995.7 949.477 1 2 0 15-10.9945 30.2756 1 -2 0 15 33.8013 57.4215 1 -2 0 16 90331.5 1130.57 1 2 0 16 86843.9 935.226 1 -2 0 17 0.31667 59.2568 1 -2 0 18 4992.87 292.303 1 -2 0 19 49.7207 65.6999 1 -2 0 20 141.099 66.1948 1 -2 0 21 10.3796 68.5161 2 -2 0 21 158.443 71.3779 1 -2 0 22 6298.15 372.241 1 -2 0 22 6359.63 385.640 2 -2 0 23-168.199 95.9586 2 -2 0 23 72.6518 68.7817 1 -2 0 24-21.9457 90.1524 2 -2 0 25 134.975 118.008 2 -2 0 26 44138.7 1007.72 2 -2 0 27 20.9400 102.343 2 -2 0 28 2.92051 80.3328 2 -2 0 29 4.94907 74.1593 2 -2 0 30 38.8884 69.5321 2 -2 0 31 31.3866 57.1530 2 -2 0 32 452.228 85.1603 2 -2 0 33 10.9104 40.7310 2 -3 0 0 2516.74 81.8320 1 -3 0 -1 30.8518 14.4737 1 -3 0 1-20.7676 17.6553 1 -3 0 -2 347090. 707.882 1 -3 0 2 346992. 1168.20 1 -3 0 3 14.9370 27.5674 1 -3 0 -3 3.77413 6.56751 1 -3 0 4 262983. 1171.32 1 -3 0 5-10.9570 32.9883 1 -3 0 6 46856.0 559.734 1 -3 0 7 27.5236 29.6695 1 -3 0 8 77212.5 787.182 1 -3 0 9 12.0484 35.0316 1 -3 0 10 15738.1 397.011 1 -3 0 11 7.15315 55.4631 1 -3 0 12 204996. 1538.63 1 -3 0 13-91.0850 56.7750 1 -3 0 14 1438.43 145.520 1 -3 0 15-85.5138 58.1007 1 -3 0 16 90.9983 72.9601 1 -3 0 17-21.4664 59.6429 1 -3 0 18 10344.2 440.858 1 -3 0 19 166.737 79.8403 1 -3 0 20 10199.4 465.800 1 -3 0 20 10119.9 481.173 2 -3 0 21-103.322 60.3425 1 -3 0 21 8.49608 71.6178 2 -3 0 22 15018.0 599.122 2 -3 0 22 15172.4 587.698 1 -3 0 23 102.840 91.3407 2 -3 0 24 24780.0 775.423 2 -3 0 25 100.435 113.014 2 -3 0 26 2191.42 242.052 2 -3 0 27-59.8665 101.373 2 -3 0 28 909.600 154.488 2 -3 0 29 12.0014 70.1997 2 -3 0 30 252.675 81.5386 2 -3 0 31-5.40184 62.5767 2 -3 0 32 266.990 70.4024 2 -3 0 33 104.356 43.4639 2 -4 0 0 67583.6 494.965 1 -4 0 1 25.4243 19.2016 1 -4 0 -1 4.00997 10.3090 1 -4 0 2 44062.4 472.436 1 -4 0 -2 45967.7 314.983 1 -4 0 -3-12.0410 5.32146 1 -4 0 3 13.6499 25.2232 1 -4 0 4 934.010 80.7338 1 -4 0 5-76.4725 34.4463 1 -4 0 6 5085.99 200.860 1 -4 0 7-1.76117 24.6981 1 -4 0 8 17020.2 404.365 1 -4 0 9-19.6845 54.2733 1 -4 0 10 32988.5 615.268 1 -4 0 11 104.167 51.3197 1 -4 0 12 51010.6 817.146 1 -4 0 13 14.1595 60.3486 1 -4 0 14 30208.2 682.200 1 -4 0 15-56.4429 74.0869 1 -4 0 16 72082.0 1120.31 1 -4 0 17 22.6763 72.5403 1 -4 0 18 2486.14 232.016 1 -4 0 19 45.5089 70.1874 2 -4 0 19 109.874 80.5731 1 -4 0 20 7818.55 432.080 2 -4 0 20 7998.94 433.243 1 -4 0 21 3.88302 79.9718 1 -4 0 21-137.250 96.4587 2 -4 0 22 96.4238 81.9179 2 -4 0 22 135.647 67.8372 1 -4 0 23-49.6406 100.087 2 -4 0 24 19389.5 689.688 2 -4 0 25 44.7501 99.7442 2 -4 0 26 6903.79 403.010 2 -4 0 27-143.395 96.0632 2 -4 0 28 1348.90 181.791 2 -4 0 29-43.7298 76.4295 2 -4 0 30 642.624 115.965 2 -4 0 31-74.5430 61.2881 2 -4 0 32 591.735 88.8457 2 -4 0 33 30.0312 34.0627 2 -5 0 0-41.7686 23.1793 1 -5 0 1-8.55136 23.8971 1 -5 0 -1-57.3813 21.1586 1 -5 0 -2 36596.0 307.260 1 -5 0 2 35822.3 470.495 1 -5 0 3 17.0389 25.7333 1 -5 0 4 3148.57 158.253 1 -5 0 5 23.0369 33.2376 1 -5 0 6 2139.25 146.742 1 -5 0 7-134.389 56.1696 1 -5 0 8 8438.96 309.658 1 -5 0 9-0.24871 49.9459 1 -5 0 10 7008.63 307.627 1 -5 0 11-8.29958 48.4679 1 -5 0 12 5245.58 283.704 1 -5 0 13-63.8757 66.6750 1 -5 0 14 32509.1 748.396 1 -5 0 15-15.0580 65.8108 1 -5 0 16 13657.3 521.624 1 -5 0 16 14914.6 554.402 2 -5 0 17 161.950 88.8967 2 -5 0 17 187.927 103.788 1 -5 0 18 9563.77 465.377 2 -5 0 18 9423.50 461.754 1 -5 0 19-339.767 116.827 1 -5 0 19 19.3301 84.5734 2 -5 0 20 8459.96 453.514 2 -5 0 20 8629.02 461.970 1 -5 0 21-20.6056 90.8335 2 -5 0 22 17376.1 652.347 2 -5 0 23 9.81903 82.3826 2 -5 0 24 8989.23 468.245 2 -5 0 25-6.46894 84.7582 2 -5 0 26 1164.60 171.325 2 -5 0 27-32.5754 98.9355 2 -5 0 28-41.6897 83.2803 2 -5 0 29-24.3871 78.4746 2 -5 0 30 510.245 97.0813 2 -5 0 31 3.15612 45.7022 2 -5 0 32 18.5917 41.7734 2 -6 0 1-11.3522 25.0472 1 -6 0 2 35470.6 511.053 1 -6 0 3 22.7365 28.0067 1 -6 0 4 40534.2 611.555 1 -6 0 5 62.2646 41.4357 1 -6 0 6 12435.6 371.516 1 -6 0 7 63.4903 48.1153 1 -6 0 8 70370.6 953.201 1 -6 0 9 120.686 69.2718 1 -6 0 10 158484. 1534.46 1 -6 0 11 46.7273 53.8400 1 -6 0 12 1194.51 157.041 1 -6 0 13 61.5815 77.0568 1 -6 0 14 2679.80 238.894 1 -6 0 15-15.1314 69.2511 1 -6 0 15-79.4113 78.2311 2 -6 0 16 6760.92 380.308 2 -6 0 16 6914.13 397.886 1 -6 0 17 160.666 89.1832 1 -6 0 17 19.6367 66.3410 2 -6 0 18 18140.6 640.097 2 -6 0 18 18782.0 672.612 1 -6 0 19-189.542 94.3534 2 -6 0 19 32.5836 58.9833 1 -6 0 20 132.583 84.9749 2 -6 0 21 75.8012 86.2437 2 -6 0 22 7683.33 429.294 2 -6 0 23 43.8015 89.6671 2 -6 0 24 3212.61 277.424 2 -6 0 25-78.7385 87.3306 2 -6 0 26 35.7972 79.8175 2 -6 0 27-21.8182 82.2714 2 -6 0 28 812.898 126.032 2 -6 0 29-23.0365 55.2890 2 -6 0 30 1208.05 122.296 2 -6 0 31 30.9869 37.3840 2 -7 0 4 3187.18 184.959 1 -7 0 5 48.3109 23.7568 1 -7 0 6 2223.01 170.124 1 -7 0 7-152.351 56.7511 1 -7 0 8 14763.1 467.094 1 -7 0 9 160.860 68.7076 1 -7 0 10 47704.8 897.307 1 -7 0 11 5.82791 63.4802 4 -7 0 11 191.249 80.7067 1 -7 0 12 9296.59 423.166 1 -7 0 13-77.6587 68.7049 1 -7 0 14 9532.23 456.158 1 -7 0 15 31.2634 59.2456 2 -7 0 15-80.4780 91.0375 1 -7 0 16 3078.89 259.679 2 -7 0 16 2421.27 243.636 1 -7 0 17-17.1959 73.2971 2 -7 0 17-126.785 105.041 1 -7 0 18 56466.0 1117.21 2 -7 0 19 88.6683 94.7682 2 -7 0 20 15632.8 597.328 2 -7 0 21 146.599 112.258 2 -7 0 21 249.609 99.6122 3 -7 0 22 6078.22 369.711 2 -7 0 22 6342.07 378.241 3 -7 0 23 200.466 88.2421 3 -7 0 23-43.0783 69.3713 2 -7 0 24 1908.95 204.047 2 -7 0 25-8.62332 75.8994 2 -7 0 26 1407.32 160.251 2 -7 0 27-165.344 73.1924 2 -7 0 28 130.575 52.5980 2 -7 0 29 12.9328 38.8207 2 -7 0 30-30.1008 35.8500 2 -8 0 6 400.997 108.734 3 -8 0 6 540.772 107.877 4 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362.355 1 2 -2 10 10373.6 222.387 1 -2 -2 10 10902.3 311.111 1 -2 -2 11 30004.1 535.420 1 -2 2 11 29856.1 611.480 1 -2 2 12 13005.4 420.884 1 2 -2 12 12921.7 281.827 1 -2 -2 12 12613.9 357.331 1 -2 -2 13 7934.91 294.960 1 2 -2 13 7992.42 233.176 1 -2 2 13 8271.62 349.454 1 -2 2 14 11866.2 432.232 1 -2 -2 14 12302.1 384.475 1 -2 2 15 6381.86 328.050 1 -2 -2 15 6489.32 290.607 1 -2 2 16 709.608 121.838 1 -2 -2 16 573.368 100.879 1 -2 -2 17 552.074 105.212 1 -2 2 18 1154.86 172.778 2 -2 -2 18 1081.30 141.360 1 -2 2 19 124.720 88.5539 2 -2 -2 19 286.933 83.2239 1 -2 -2 20 1791.53 185.255 1 -2 2 20 1789.84 219.237 2 -2 -2 21 25187.9 690.675 1 -2 2 21 26692.2 818.908 2 -2 2 22 6143.01 403.382 2 -2 -2 22 5735.97 343.345 1 -2 2 23-86.0962 120.616 2 -2 2 24 553.279 151.041 2 -2 2 25 472.803 136.222 2 -2 2 26 480.272 132.543 2 -2 2 27 934.223 158.459 2 -2 -2 27 983.728 157.352 2 -2 2 28 2642.95 239.846 2 -2 -2 28 2902.54 238.711 2 -2 2 29 89.1117 86.3107 2 -2 -2 29 129.734 79.7749 2 -2 2 30 79.4995 64.7564 2 -2 -2 30 97.1074 70.6805 2 -2 -2 31 1940.74 162.612 2 -2 2 31 2069.38 168.962 2 -2 -2 32 133.711 54.2998 2 -2 2 32 164.401 55.2615 2 -3 -2 0 44.5228 35.5647 1 -3 -2 -1 188696. 1066.91 1 -3 -2 1 188033. 1065.19 1 -3 -2 2 22453.6 375.008 1 -3 -2 -2 21948.1 370.548 1 -3 -2 3 168494. 1049.71 1 -3 -2 -3 166693. 1039.15 1 3 -2 4 411.724 38.0172 1 -3 -2 4 542.617 71.7801 1 3 -2 5 4370.09 107.493 1 -3 -2 5 4185.90 177.759 1 3 -2 6 1887.73 68.9146 1 -3 -2 6 1961.07 127.179 1 -3 2 6 1959.11 137.553 1 -3 -2 7 279907. 1496.44 1 -3 2 7 272305. 1631.90 1 -3 2 8 110484. 1088.24 1 -3 -2 8 115138. 1000.49 1 -3 -2 9 81749.8 868.483 1 -3 2 9 76032.7 950.359 1 -3 -2 10 6374.50 254.963 1 -3 2 10 6058.18 283.672 1 -3 2 11 33873.8 689.636 1 -3 -2 11 35013.8 616.284 1 -3 2 12 73779.7 1054.63 1 -3 -2 12 77467.2 929.135 1 -3 2 13 235.442 89.2234 1 -3 -2 13 165.764 60.2280 1 -3 2 14 1018.42 147.737 1 -3 -2 14 223.605 77.3069 1 -3 2 15 14139.8 513.083 1 -3 -2 15 14701.5 458.495 1 -3 2 16 5639.57 337.250 1 -3 -2 16 6046.42 305.503 1 -3 2 17 14701.5 581.966 2 -3 2 17 14104.7 542.524 1 -3 -2 17 14356.0 485.997 1 -3 -2 18 19178.0 580.602 1 -3 2 18 17949.2 657.575 2 -3 -2 19 2581.15 225.743 1 -3 2 19 2877.78 275.923 2 -3 -2 20 7088.49 377.806 1 -3 2 20 7404.30 441.941 2 -3 2 21 160.434 103.008 2 -3 -2 21-126.804 92.9877 1 -3 2 22 13606.9 607.535 2 -3 2 23 257.202 125.995 2 -3 2 24 3.70217 94.3364 2 -3 2 25 639.160 148.915 2 -3 2 26 40.0361 89.2822 2 -3 -2 26-27.3850 85.2514 2 -3 2 27 967.561 169.168 2 -3 -2 27 778.811 146.751 2 -3 2 28 2748.30 243.740 2 -3 -2 28 2964.77 239.990 2 -3 -2 29 2791.34 221.777 2 -3 2 29 2721.06 228.046 2 -3 2 30 2263.09 191.835 2 -3 -2 30 2446.55 196.310 2 -3 2 31 1249.06 132.254 2 -3 -2 31 1359.43 136.532 2 -3 -2 32 12.2146 46.4392 2 -3 2 32 24.8899 38.8490 2 -4 -2 0 90112.3 773.288 1 -4 -2 1 5422.62 195.348 1 -4 -2 -1 5275.84 187.134 1 -4 -2 2 42378.3 552.628 1 -4 -2 -2 41007.4 512.953 1 -4 -2 3 65198.1 707.647 1 4 -2 3 64669.9 420.770 1 -4 -2 4 1224.27 101.383 1 -4 -2 -4 1375.25 97.6093 1 -4 2 5 410.716 66.8727 1 -4 -2 5 421.162 67.5237 1 -4 -2 -5 478.284 62.9588 1 -4 -2 -6 7453.99 231.730 1 -4 2 6 7159.38 268.989 1 -4 -2 6 7503.50 258.353 1 -4 -2 7 595.143 82.1640 1 -4 2 7 550.165 91.3290 1 -4 -2 8 13704.9 371.173 1 -4 2 8 13729.3 413.186 1 -4 -2 9 1379.83 128.403 1 -4 2 9 1162.77 131.277 1 -4 -2 10 688.467 100.588 1 -4 2 10 599.668 112.543 1 -4 2 11 50713.4 895.190 1 -4 -2 11 53311.3 790.188 1 -4 2 12 4676.50 283.962 1 -4 -2 12 4661.59 248.893 1 -4 2 13 1369.73 171.654 1 -4 -2 13 1258.44 149.033 1 -4 2 14 1603.00 183.466 1 -4 -2 14 849.938 122.253 1 -4 2 15 2719.78 247.674 1 -4 -2 15 2555.75 207.758 1 -4 2 16 2666.07 256.449 2 -4 -2 16 2865.95 225.031 1 -4 2 16 2753.29 254.070 1 -4 2 17 1469.72 192.686 1 -4 2 17 1809.78 221.912 2 -4 -2 17 1427.33 163.545 1 -4 2 18 649.431 135.448 2 -4 2 18 746.759 163.501 1 -4 -2 18 833.151 139.389 1 -4 -2 19 21677.9 660.131 1 -4 2 19 21952.3 760.657 2 -4 2 20 2714.70 279.110 2 -4 -2 20 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15 179.857 91.9365 2 -4 -3 15 409.755 110.365 1 -4 -3 16 7180.72 360.045 1 -4 3 16 6961.43 424.390 2 -4 3 17 2689.93 276.461 2 -4 -3 17 2520.56 223.762 1 -4 3 18 16694.7 677.316 2 -4 -3 18 16449.3 569.210 1 -4 -3 19 1181.29 174.388 1 -4 3 19 1425.09 219.733 2 -4 3 20 390.533 132.070 2 -4 3 21 51.1138 100.797 2 -4 3 22 4787.96 371.429 2 -4 3 23 883.059 171.854 2 -4 3 24 4921.75 363.319 2 -4 3 25 37.0854 87.9966 2 -4 3 26 2883.47 263.194 2 -4 -3 27 1469.13 170.669 2 -4 3 27 1311.50 176.992 2 -4 -3 28 170.774 84.4124 2 -4 3 28 72.1800 74.6643 2 -4 -3 29 392.633 90.6975 2 -4 3 29 307.712 93.9273 2 -4 -3 30 1792.71 147.242 2 -4 3 30 1750.35 153.426 2 -4 -3 31 21.4941 35.2254 2 -4 3 31 50.6807 46.8438 2 -5 -3 0 20.5896 38.1623 1 -5 -3 1 21877.3 475.767 1 -5 -3 -1 21896.1 468.347 1 -5 -3 2 51413.3 736.175 1 -5 -3 -2 51094.4 721.179 1 -5 -3 -3 406.264 77.0193 1 -5 -3 3 402.710 82.2533 1 -5 -3 4 83671.3 956.928 1 -5 -3 -4 83978.5 909.997 1 -5 -3 5 30985.0 589.913 1 -5 -3 -5 29826.5 545.921 1 -5 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126.887 2 -5 -3 29 373.406 84.0706 2 -5 3 29 330.345 82.3448 2 -5 -3 30 697.863 89.8475 2 -5 3 30 835.274 101.045 2 -6 -3 0-1.35177 28.4158 1 -6 -3 1 61.9179 36.8672 1 -6 -3 -1 131.373 53.1893 1 -6 -3 2 194.400 52.7226 1 -6 -3 -2 624.705 90.0123 1 -6 -3 3 6498.36 276.190 1 -6 -3 -3 6753.94 268.407 1 -6 -3 4 1397.03 132.465 1 -6 -3 -4 1636.72 135.664 1 -6 -3 -5 479.335 72.0324 1 -6 -3 5 217.665 61.5770 1 -6 -3 6 3074.33 204.425 1 -6 -3 7 4466.52 248.181 1 -6 -3 8 18.4641 51.6552 1 -6 -3 9 2045.42 183.526 4 -6 3 -9 1880.14 220.302 3 -6 -3 9 1901.17 177.775 1 -6 -3 10 431.354 101.021 1 -6 -3 10 482.990 101.891 4 -6 3 -10 642.357 141.787 3 -6 3 11 1982.86 203.364 2 -6 -3 11 2146.90 187.529 4 -6 3 -11 2226.48 247.175 3 -6 -3 11 1880.05 177.435 1 -6 3 12 496.946 114.320 2 -6 3 -12 552.338 150.522 3 -6 -3 12 512.340 107.582 1 -6 -3 12 640.715 113.128 4 -6 3 13 164.545 71.4947 2 -6 -3 13 66.4105 61.2479 4 -6 -3 13 154.402 86.7176 1 -6 3 14 126.512 86.2202 2 -6 -3 14-20.1197 44.6077 4 -6 -3 14 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66.2612 4 -12 3 -4-8.55719 86.6740 3 -12 3 5-80.0947 83.8914 3 -12 -3 5 177.104 90.6915 3 -12 3 -5 90.0617 106.219 3 -12 3 6 717.238 143.263 3 -12 -3 6 589.907 137.594 3 -12 3 -6 824.563 161.913 3 -12 3 7 72.1541 82.8466 3 -12 -3 7-111.771 88.0381 3 -12 3 -7 108.821 96.6480 3 -12 3 8 838.610 146.957 3 -12 -3 8 916.832 159.334 3 -12 3 -8 1055.51 171.314 3 -12 3 9 206.193 87.3863 3 -12 -3 9 311.167 109.676 3 -12 3 -9 371.137 125.871 3 -12 3 10-91.6330 69.9015 3 -12 -3 10 132.294 84.2818 3 -12 3 11-8.89546 52.3859 3 -12 -3 11-42.4147 78.7871 3 -12 -3 12 128.244 81.1272 3 -12 -3 13 446.408 111.012 3 -12 -3 14 923.772 133.780 3 -12 -3 15 111.594 68.8820 3 -12 -3 16 810.955 110.324 3 -12 -3 17 238.466 66.1709 3 -13 3 0 16.0775 68.7484 3 -13 3 -1 381.835 113.292 3 -13 3 1 561.364 125.537 3 -13 -3 2 36.6869 38.3049 3 -13 3 -2 116.663 83.2422 3 -13 3 2 50.0103 77.8468 3 -13 -3 3 19.5791 45.0910 3 -13 3 -3 9.76694 70.4457 3 -13 3 3 0.69050 76.2651 3 -13 -3 4 170.214 74.4558 3 -13 3 -4 327.563 100.475 3 -13 3 4 283.980 98.1718 3 -13 -3 5-38.9159 49.5788 3 -13 3 5-2.85067 70.0358 3 -13 3 -5-28.3340 67.9250 3 -13 -3 6 756.397 119.393 3 -13 3 -6 759.266 130.101 3 -13 3 6 640.668 115.911 3 -13 -3 7 105.955 68.7246 3 -13 3 7 112.731 70.5965 3 -13 -3 8 30.3265 66.7621 3 -13 3 8 41.2929 51.8103 3 -13 -3 9 27.3202 58.8057 3 -13 3 9-77.7954 53.2127 3 -13 -3 10 165.946 65.5612 3 -13 -3 11 187.934 66.3352 3 -13 -3 12 10.9908 43.9262 3 -13 -3 13 43.6434 47.6761 3 -14 3 0 1196.66 124.324 3 -14 3 -1 191.893 60.8524 3 -14 3 1 174.701 58.9894 3 -14 3 -2 33.7388 56.0810 3 -14 3 2 33.6707 43.4407 3 -14 3 3 43.3686 47.2735 3 0 -4 1 30134.1 591.847 1 0 -4 2 1093.30 125.382 1 0 -4 3 45179.8 693.905 1 0 -4 4 12335.5 358.626 1 0 -4 5 1895.19 144.200 1 0 -4 6 1788.71 149.273 1 0 -4 7 71046.1 865.039 1 0 -4 8 24604.1 511.757 1 0 -4 9 47007.1 721.638 1 0 -4 10 15452.6 413.310 1 0 -4 11 18000.8 449.762 1 0 -4 12 481.153 80.2500 1 0 -4 13 7437.91 303.127 1 0 -4 14 23342.2 548.573 1 0 -4 15 13746.3 423.635 1 0 4 15 15338.1 574.867 2 0 4 16 9744.53 466.564 2 0 -4 16 8617.66 345.563 1 0 4 17 5059.64 342.464 2 0 4 18 11799.1 528.899 2 0 4 19 52848.4 1115.29 2 0 4 20 25930.1 787.275 2 0 4 21 28323.9 822.572 2 0 4 22 12678.9 548.946 2 0 4 23 2383.76 241.542 2 0 4 24 479.685 119.008 2 0 4 25 420.029 108.870 2 0 4 26 2504.38 219.497 2 0 4 27 1257.59 148.892 2 0 -4 28 656.863 102.559 2 0 4 28 691.661 110.211 2 0 4 29 1160.65 120.838 2 0 -4 29 1293.13 122.962 2 0 -4 30 157.416 47.2025 2 -1 -4 0-103.075 59.6866 1 -1 -4 1 5106.65 248.114 1 -1 -4 2 805.869 106.532 1 1 -4 2 938.109 109.494 1 -1 -4 3 1594.57 141.593 1 1 -4 3 1478.61 130.607 1 -1 -4 4 10075.0 331.487 1 1 -4 4 9722.44 312.815 1 -1 -4 5 105.126 49.8024 1 1 -4 5 101.700 48.2356 1 1 -4 6 3639.66 192.399 1 -1 -4 6 3399.34 202.462 1 -1 -4 7 113331. 1126.62 1 1 -4 7 113346. 1041.63 1 -1 -4 8 104575. 1098.60 1 1 -4 8 104225. 1006.29 1 -1 -4 9 35916.9 651.881 1 1 -4 9 35740.3 602.166 1 1 -4 10 25887.3 509.653 1 -1 -4 10 25813.7 552.911 1 1 -4 11 277.868 70.7943 1 -1 -4 11 738.070 105.986 1 1 -4 12 18383.0 439.735 1 -1 -4 12 18745.4 488.365 1 -1 -4 13 8463.33 337.929 1 1 -4 13 8258.56 301.427 1 -1 4 14 2750.66 249.967 2 -1 -4 14 2670.45 200.800 1 1 4 15 5159.45 328.073 2 -1 4 15 5493.45 358.396 2 -1 -4 15 5105.37 277.554 1 -1 4 16 956.907 163.129 2 1 4 16 1133.90 164.902 2 -1 -4 16 860.783 120.927 1 -1 4 17 40.5554 86.6412 2 1 4 17 104.017 82.1611 2 -1 4 18 29093.9 851.742 2 1 4 18 29527.2 808.296 2 1 4 19 16433.0 609.557 2 -1 4 19 18120.3 680.683 2 1 4 20 696.802 138.750 2 -1 4 20 1118.70 189.896 2 1 4 21 58.2877 83.2275 2 -1 4 21 57.2433 83.7137 2 1 4 22 1142.59 168.608 2 -1 4 22 983.965 175.892 2 1 4 23 245.258 83.8600 2 -1 4 23 158.312 96.5788 2 1 4 24 12.7612 49.1393 2 -1 4 24 11.1568 77.8353 2 1 4 25 300.173 93.3217 2 -1 4 25 234.495 101.700 2 1 4 26-11.7415 55.6648 2 -1 4 26-18.2123 72.1378 2 -1 4 27 185.378 77.5202 2 1 -4 28 692.719 98.2162 2 -1 4 28 786.893 123.129 2 -1 -4 29 223.186 70.3382 2 -1 4 29 134.338 64.1635 2 -1 -4 30-49.9920 42.6004 2 -1 4 30 89.2973 48.1187 2 -2 -4 0 50283.4 787.866 1 -2 -4 1 17747.1 459.229 1 -2 -4 -1 17477.9 470.483 1 -2 -4 2 148.617 72.7475 1 2 -4 2 37.9418 53.4472 1 -2 -4 -2 92.0253 62.7335 1 -2 -4 3 34249.5 627.158 1 2 -4 3 33570.0 582.515 1 -2 -4 4 60754.5 834.086 1 2 -4 4 58602.2 744.325 1 -2 -4 5 107810. 1121.20 1 2 -4 5 104156. 968.338 1 -2 -4 6 115108. 1169.66 1 2 -4 6 117544. 1018.03 1 -2 -4 7 90249.8 1041.70 1 2 -4 7 90584.5 894.141 1 -2 -4 8 2801.18 196.530 1 2 -4 8 2550.60 155.830 1 -2 -4 9 2792.55 190.107 1 2 -4 9 2598.07 155.175 1 -2 -4 10 294.844 86.2776 1 2 -4 10 417.049 71.6604 1 -2 -4 11 2004.17 169.266 1 -2 -4 12 5741.83 285.607 1 -2 -4 13 10127.5 388.520 1 -2 4 13 10951.2 495.899 2 -2 4 14 247.070 100.526 2 -2 -4 14 281.916 75.1287 1 -2 4 15 1729.69 209.173 2 -2 -4 15 1847.56 178.254 1 -2 4 16 747.713 152.736 2 -2 -4 16 395.106 95.7959 1 -2 4 17 319.661 108.599 2 -2 -4 17 411.304 97.9696 1 -2 4 18 4870.91 366.503 2 -2 -4 18 4484.41 292.090 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39.1310 2 -4 -5 0 12204.2 465.668 4 -4 -5 0 11690.1 449.763 1 -4 -5 1 58.9552 73.7333 1 -4 -5 1-162.706 83.5386 4 -4 -5 -1 88.0631 88.4027 4 -4 -5 -1 135.514 78.8331 1 -4 -5 2 7279.66 353.914 1 -4 -5 2 7414.26 359.096 4 -4 -5 -2 6851.86 354.874 4 -4 -5 -2 6586.65 343.870 1 -4 -5 -3 971.609 141.359 1 -4 -5 3 822.949 138.456 1 -4 -5 3 807.167 126.966 4 -4 -5 -3 652.289 119.419 4 -4 -5 4 40.9071 69.1729 1 -4 -5 -4 71.1471 67.8151 1 -4 -5 4-6.84043 57.7527 4 -4 5 4 2.17082 51.5311 2 -4 -5 -5 268.868 80.2327 1 -4 -5 5 279.926 83.4002 4 -4 -5 -5 317.214 88.3870 4 -4 5 5 298.971 112.093 2 -4 -5 6 18494.3 571.231 1 -4 5 6 17026.6 617.650 2 -4 -5 6 18364.3 551.865 4 -4 -5 -6 16640.9 558.463 4 -4 -5 -6 16274.7 564.174 1 -4 -5 7 42895.0 864.507 1 -4 5 7 39726.9 953.702 2 -4 -5 7 41253.2 820.097 4 -4 -5 -7 36808.9 835.724 4 -4 -5 -7 37265.1 864.335 1 -4 -5 8 1876.83 194.346 1 -4 5 8 2259.36 242.967 2 -4 -5 8 1958.78 192.474 4 -4 -5 -8 1712.78 204.307 1 -4 -5 -9 474.394 134.198 1 -4 -5 9 720.985 138.791 1 -4 -5 9 587.140 110.211 4 -4 -5 -9 563.942 114.286 4 -4 5 9 491.540 126.815 2 -4 -5 10 1969.44 196.320 1 -4 5 10 1768.82 227.948 2 -4 -5 -10 1632.95 191.298 1 -4 -5 10 2080.93 190.639 4 -4 -5 11 2040.87 204.513 1 -4 5 11 1951.19 240.361 2 -4 -5 11 1906.66 182.461 4 -4 -5 12 3998.95 280.995 1 -4 5 12 3885.09 333.174 2 -4 -5 12 4025.14 259.005 4 -4 -5 13 852.552 146.211 1 -4 -5 13 853.102 129.631 4 -4 5 13 845.559 179.716 2 -4 5 14 5631.92 406.328 2 -4 -5 14 5902.90 306.320 4 -4 -5 14 6585.39 369.081 1 -4 5 15 357.731 130.005 2 -4 5 16-89.8832 97.2259 2 -4 5 17 1289.81 204.867 2 -4 5 18-39.1806 93.2042 2 -4 5 19 5479.44 407.314 2 -4 5 20 1252.94 201.745 2 -4 5 21 2356.81 261.100 2 -4 5 22 5710.14 386.212 2 -4 5 23 827.286 164.049 2 -4 5 24 76.2991 80.7447 2 -4 5 25 692.358 134.577 2 -4 5 26 41.1869 66.3347 2 -4 5 27 1364.92 143.163 2 -4 -5 27 1363.47 128.002 2 -4 -5 28 333.281 63.1565 2 -4 5 28 263.230 63.8222 2 -5 5 0 31.3694 56.0723 2 -5 -5 0 162.823 90.7092 4 -5 5 1 23185.1 696.428 2 -5 -5 1 23802.4 648.756 1 -5 -5 -1 23340.4 643.203 1 -5 -5 1 24056.1 658.544 4 -5 -5 -1 23987.5 666.902 4 -5 -5 -2 574.654 120.779 1 -5 -5 2 457.812 114.811 4 -5 -5 -2 458.516 122.931 4 -5 5 2 390.627 112.817 2 -5 -5 2 496.849 114.238 1 -5 -5 3 4774.04 297.155 1 -5 5 3 4443.04 311.734 2 -5 -5 -3 4641.82 298.132 4 -5 -5 -3 4265.48 281.164 1 -5 -5 3 4889.11 302.790 4 -5 5 -3 4410.51 315.694 3 -5 -5 -4 212.562 90.4867 1 -5 -5 4 301.238 92.4602 4 -5 -5 -4 305.910 96.1206 4 -5 5 4 547.734 122.682 2 -5 -5 4 279.591 97.0120 1 -5 5 5 13111.5 543.783 2 -5 -5 5 14138.1 500.755 4 -5 -5 -5 12678.8 496.775 4 -5 -5 -5 12464.0 482.139 1 -5 -5 6 6021.07 335.798 1 -5 5 6 5524.06 361.595 2 -5 -5 6 6254.41 337.017 4 -5 -5 -6 5481.20 331.561 4 -5 -5 -6 5662.38 326.505 1 -5 -5 7 12634.5 479.161 1 -5 5 7 12385.7 542.990 2 -5 -5 7 13353.9 488.572 4 -5 -5 -7 11703.1 472.023 4 -5 -5 -7 11819.3 472.490 1 -5 -5 8 74.7111 82.2257 4 -5 -5 8 13.3738 61.9744 1 -5 -5 -8 104.448 74.0059 4 -5 5 8-92.8598 85.0559 2 -5 -5 9 6068.24 344.680 1 -5 5 9 4818.49 351.187 2 -5 -5 9 5557.91 316.757 4 -5 -5 -9 4962.76 307.785 4 -5 -5 -9 4955.96 321.570 1 -5 -5 10 2968.55 236.319 1 -5 -5 10 2979.84 234.499 4 -5 5 10 2688.61 273.192 2 -5 -5 11 4740.40 305.450 1 -5 5 11 4077.87 333.220 2 -5 -5 11 4268.30 274.467 4 -5 -5 12 382.141 104.971 1 -5 -5 12 546.206 110.741 4 -5 5 12 474.307 130.705 2 -5 -5 13 158.127 80.2620 4 -5 5 13 205.175 104.832 2 -5 -5 14 314.332 91.2109 4 -5 5 14 528.861 144.572 2 -5 -5 15 299.888 78.4017 4 -5 5 15 274.600 122.687 2 -5 5 16 527.642 136.540 2 -5 5 17 4999.23 387.248 2 -5 5 18 4262.90 352.811 2 -5 5 19 109.192 98.7327 2 -5 5 20 125.233 112.639 2 -5 5 21 424.970 138.802 2 -5 5 22 23.0703 87.0570 2 -5 5 23 4973.11 326.063 2 -5 5 24 596.174 122.713 2 -5 5 25 360.112 94.2401 2 -5 5 26 1312.52 143.428 2 -5 -5 26 1307.60 124.089 2 -5 -5 27 90.8305 47.4640 2 -5 5 27 19.4950 45.0209 2 -6 -5 0 3964.53 275.519 1 -6 -5 0 3347.94 264.969 4 -6 -5 1 5734.86 326.412 1 -6 -5 -1 6165.22 338.200 1 -6 -5 1 5835.24 341.195 4 -6 -5 -1 5944.51 344.566 4 -6 5 -1 5161.62 352.619 3 -6 -5 2 3823.69 263.384 1 -6 -5 -2 3094.37 242.324 1 -6 -5 2 3826.09 277.169 4 -6 -5 -2 3685.57 277.109 4 -6 5 -2 4007.25 313.436 3 -6 -5 -3-73.0435 41.5288 1 -6 -5 3 51.9419 70.2488 4 -6 -5 -3 160.112 85.1514 4 -6 5 -3 229.267 100.440 3 -6 -5 4 7630.58 376.527 1 -6 5 4 7428.16 405.839 2 -6 -5 -4 8296.84 390.562 1 -6 -5 4 7931.64 388.862 4 -6 -5 -4 6812.88 367.069 4 -6 5 -4 7730.93 446.941 3 -6 -5 -5 268.082 77.6483 1 -6 -5 5 198.129 76.8454 1 -6 -5 5 104.045 89.2780 4 -6 -5 -5 52.2173 64.7203 4 -6 5 5 103.207 81.7002 2 -6 -5 6 166.906 72.7171 1 -6 -5 -6 405.970 105.471 4 -6 5 6 326.765 98.3384 2 -6 -5 7 566.047 122.201 1 -6 -5 7 413.304 116.236 4 -6 -5 -7 374.861 95.8536 4 -6 5 7 591.682 128.514 2 -6 -5 8 787.672 132.421 1 -6 -5 -8 954.665 147.196 4 -6 5 8 966.679 167.034 2 -6 -5 9 83.5563 64.9622 1 -6 -5 9 104.456 85.7746 4 -6 5 9 179.390 81.2779 2 -6 5 10 1964.15 235.696 2 -6 -5 10 2441.43 220.320 4 -6 -5 11 1578.24 181.127 4 -6 5 11 1234.86 186.614 2 -6 5 12 1970.65 237.362 2 -6 -5 12 2308.48 207.565 4 -6 5 13 2012.04 242.850 2 -6 -5 13 1993.32 192.917 4 -6 5 14 1598.15 219.318 2 -6 -5 14 2078.50 192.776 4 -6 5 15 1290.21 195.284 2 -6 -5 15 1302.26 150.851 4 -6 -5 16 194.817 68.6481 4 -6 5 16 255.418 112.426 2 -6 -5 17 1070.86 131.090 4 -6 5 17 834.000 169.762 2 -6 5 18 129.031 100.214 2 -6 5 19 100.407 87.5611 2 -6 5 20 1837.66 220.387 2 -6 5 21 487.196 126.309 2 -6 5 22 636.194 129.633 2 -6 5 23 53.9417 64.6773 2 -6 -5 24 157.483 63.7525 2 -6 5 24 94.9452 65.3007 2 -6 -5 25-4.68747 40.6939 2 -6 5 25 12.9173 54.3654 2 -6 5 26 677.329 90.1264 2 -6 -5 26 532.365 68.2704 2 -7 -5 0 16.2770 81.6521 4 -7 -5 0 220.394 75.7216 1 -7 -5 1 2452.27 212.152 1 -7 -5 1 3146.61 263.174 4 -7 -5 -1 2965.00 254.729 4 -7 5 -1 3055.92 290.491 3 -7 -5 2 12488.5 477.467 1 -7 -5 2 13329.7 519.577 4 -7 -5 -2 12415.5 503.338 4 -7 5 -2 12941.6 579.443 3 -7 -5 3 1790.94 187.651 1 -7 -5 -3 2157.19 220.393 4 -7 -5 3 2278.26 230.088 4 -7 5 -3 1964.08 243.958 3 -7 -5 4 1989.25 198.936 1 -7 -5 4 2105.13 215.520 4 -7 -5 -4 2107.64 213.182 4 -7 5 -4 1694.15 228.759 3 -7 -5 5 1310.77 157.613 1 -7 -5 5 1201.47 169.894 4 -7 -5 -5 1087.65 165.968 4 -7 5 -5 1372.92 217.194 3 -7 -5 6 726.361 144.809 4 -7 -5 -6 913.289 143.802 4 -7 -5 7 89.3430 83.2595 4 -7 -5 -7 77.3578 79.7586 4 -7 -5 8 964.862 152.729 4 -7 5 8 887.374 169.847 2 -7 5 9 9112.61 464.822 2 -7 -5 9 9298.00 426.211 4 -7 5 10 3773.43 305.920 2 -7 -5 10 4192.69 287.677 4 -7 5 11 3384.94 290.506 2 -7 -5 11 4001.87 279.611 4 -7 5 12 1856.12 224.826 2 -7 -5 12 1744.00 184.498 4 -7 -5 13-6.60368 61.2754 4 -7 5 13-17.8301 56.3624 2 -7 -5 14 47.7122 62.0510 4 -7 5 14 188.638 91.6168 2 -7 5 15 1942.92 221.612 2 -7 -5 15 2005.57 181.868 4 -7 -5 16-40.6276 52.3562 4 -7 5 16-94.5371 78.4468 2 -7 -5 17 584.280 102.657 4 -7 5 17 504.141 125.552 2 -7 -5 18 974.128 115.403 4 -7 5 18 1081.36 164.860 2 -7 5 19 591.829 129.670 2 -7 5 20 76.5359 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6 23 718.943 134.020 2 -2 6 24 394.204 102.876 2 -2 6 25 88.5770 58.0642 2 -2 6 26 413.427 79.1202 2 -3 -6 0 229.484 106.209 1 -3 6 0-66.7950 77.2735 2 -3 -6 0 72.0467 100.596 4 3 -6 0 250.480 90.6931 1 -3 6 -1 10830.5 519.874 2 -3 6 1 10855.6 518.538 2 -3 -6 1 12259.3 502.391 4 -3 -6 -1 11028.2 486.099 4 -3 -6 1 11163.0 492.172 1 -3 -6 -1 11221.6 495.442 1 3 -6 1 9650.15 420.228 1 3 -6 -1 10255.4 452.739 1 -3 6 -2 7261.67 431.864 2 -3 6 2 7212.96 429.819 2 -3 -6 2 7391.80 397.805 1 -3 -6 2 7609.16 397.023 4 -3 -6 -2 7988.84 414.905 4 -3 -6 -2 6873.44 391.927 1 3 -6 -2 6911.48 384.332 1 -3 -6 -3 399.052 111.524 1 -3 -6 3 518.618 124.939 1 -3 6 3 513.260 146.170 2 -3 -6 3 703.263 141.130 4 -3 -6 -3 534.909 132.006 4 -3 -6 4 8091.69 405.734 4 -3 6 4 8452.56 467.438 2 -3 -6 4 8318.95 425.660 1 -3 -6 -4 8030.00 422.720 4 -3 -6 -4 7490.16 418.518 1 3 6 5 87.8043 77.3415 2 -3 -6 5 209.037 93.0341 4 -3 6 5 121.181 82.1357 2 -3 -6 -5 215.133 105.009 4 -3 -6 5 366.696 114.230 1 3 6 6 7653.44 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254.456 2 -3 6 15 64.3363 113.885 2 -3 6 16 1240.67 205.688 2 -3 6 17 4319.52 361.293 2 -3 6 18 6658.03 436.121 2 -3 6 19 171.150 121.191 2 -3 6 20 1674.87 216.991 2 -3 6 21 899.389 163.792 2 -3 6 22 13.8378 76.1702 2 -3 6 23-10.4634 77.0707 2 -3 6 24 233.734 89.3491 2 -3 6 25 619.060 100.865 2 -3 6 26 356.259 80.6167 2 -4 6 0 30849.4 870.977 2 -4 -6 0 32683.0 839.088 1 -4 -6 0 32490.3 830.145 4 -4 -6 -1 116.911 95.1401 1 -4 6 -1 136.382 88.9934 2 -4 6 1 205.466 109.501 2 -4 -6 1 201.213 106.726 4 -4 -6 -1 281.372 113.643 4 -4 6 2 9177.97 486.209 2 -4 -6 2 9745.54 456.104 1 -4 -6 2 10312.5 462.880 4 -4 -6 -2 9720.65 461.146 4 -4 -6 -2 8679.12 440.661 1 -4 -6 3 119.442 86.7942 1 -4 6 3 276.047 120.320 2 -4 -6 3 298.249 107.056 4 -4 -6 -3 352.428 109.930 1 -4 -6 -3 92.3978 89.0941 4 -4 -6 4 2771.63 252.616 1 -4 6 4 2457.72 258.192 2 -4 -6 4 2697.77 241.089 4 -4 -6 -4 2551.75 243.144 4 -4 -6 -4 2355.85 243.399 1 -4 -6 5 2997.94 264.155 1 -4 6 5 2838.38 279.224 2 -4 -6 5 3086.56 258.683 4 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7 53.7613 74.3392 4 -5 -6 -7 157.131 96.3909 4 -5 6 7 262.614 112.673 2 -5 6 8 5588.73 394.635 2 -5 -6 8 6200.77 348.477 4 -5 -6 -8 5748.84 353.765 4 -5 6 9 1814.96 242.127 2 -5 -6 9 1960.05 202.840 4 -5 -6 -9 1919.03 210.116 4 -5 -6 10 119.725 74.8029 4 -5 -6 -10-94.6814 72.2451 4 -5 6 10 190.813 111.658 2 -5 -6 11 263.903 95.7960 4 -5 6 11 315.623 131.134 2 -5 6 12 1716.23 231.415 2 -5 -6 12 1548.95 174.049 4 -5 -6 13 132.285 81.0172 4 -5 6 13 106.430 82.1142 2 -5 -6 14-97.7669 66.7029 4 -5 6 14 10.3109 88.8490 2 -5 -6 15 42.2514 57.8573 4 -5 6 15 47.9157 83.5268 2 -5 6 16 534.203 147.662 2 -5 6 17 24.3105 85.7667 2 -5 6 18-4.51897 85.1323 2 -5 6 19 97.3249 98.2145 2 -5 6 20 179.401 102.976 2 -5 6 21 873.273 148.137 2 -5 6 22 33.1444 62.0479 2 -5 6 23 21.4187 64.6889 2 -5 6 24 281.215 78.1350 2 -5 -6 25 294.856 57.4126 2 -5 6 25 195.318 61.1086 2 -6 -6 0 450.849 134.571 4 -6 6 1 7835.76 427.291 2 -6 -6 1 7271.55 397.276 4 -6 -6 -1 7325.64 403.668 4 -6 6 2 4661.32 334.681 2 -6 -6 2 4628.31 321.241 4 -6 -6 -2 4825.97 332.272 4 -6 6 3 29.3999 94.4160 2 -6 -6 3 1.25315 99.0697 4 -6 -6 -3 199.630 102.136 4 -6 6 4 2347.48 248.347 2 -6 -6 4 2429.52 235.793 4 -6 -6 -4 2340.75 239.332 4 -6 -6 5 265.696 116.885 4 -6 -6 -5 405.604 129.436 4 -6 6 5 660.379 158.217 2 -6 6 6 9785.66 499.482 2 -6 -6 6 10816.0 472.563 4 -6 -6 -6 10259.2 468.457 4 -6 6 7 4541.99 348.027 2 -6 -6 7 4889.90 319.127 4 -6 -6 -7 4531.69 310.737 4 -6 6 8 5886.01 399.735 2 -6 -6 8 6487.20 357.586 4 -6 -6 -8 5847.42 345.684 4 -6 -6 9 38.4012 89.9901 4 -6 -6 -9-8.60117 66.2189 4 -6 6 9 41.2568 86.8356 2 -6 6 10 3352.94 306.886 2 -6 -6 10 3434.06 261.134 4 -6 -6 11-17.6042 72.4857 4 -6 6 11 96.6790 87.6126 2 -6 -6 12-7.94100 72.1879 4 -6 6 12 83.6075 89.6200 2 -6 -6 13 285.996 90.8860 4 -6 6 13 309.450 121.416 2 -6 6 14 1476.97 208.357 2 -6 -6 14 1308.70 148.078 4 -6 -6 15 20.7079 50.4585 4 -6 6 15 11.6111 83.5494 2 -6 6 16 2006.79 232.854 2 -6 -6 16 2042.74 163.009 4 -6 6 17 935.612 160.280 2 -6 6 18 399.110 106.747 2 -6 6 19-13.1923 75.2295 2 -6 6 20-22.1219 67.7498 2 -6 6 21 97.8339 73.1540 2 -6 6 22 635.450 107.947 2 -6 -6 23 197.979 50.8841 2 -6 6 23 79.9998 53.7432 2 -7 -6 0 85.6246 90.5005 4 -7 -6 1 593.915 148.303 4 -7 -6 -1 686.890 149.817 4 -7 -6 2 4146.58 306.457 4 -7 -6 -2 4090.41 303.359 4 -7 -6 3 2930.79 260.806 4 -7 -6 -3 3247.86 274.411 4 -7 -6 4 13873.7 533.069 4 -7 -6 -4 14050.3 542.100 4 -7 -6 5 599.212 145.233 4 -7 -6 -5 806.746 151.125 4 -7 6 6 5487.59 356.583 2 -7 -6 6 5681.25 343.913 4 -7 -6 -6 5460.53 337.172 4 -7 -6 7 231.954 116.971 4 -7 -6 -7 372.665 103.023 4 -7 6 7 335.590 102.813 2 -7 6 8 2298.81 240.199 2 -7 -6 8 2330.95 223.395 4 -7 -6 -8 2298.29 214.188 4 -7 -6 9 40.4486 83.1447 4 -7 6 9 47.7681 69.2467 2 -7 -6 10 21.4657 79.0968 4 -7 6 10 71.8568 74.4053 2 -7 -6 11 268.493 93.7881 4 -7 6 11 243.532 94.3343 2 -7 -6 12 253.953 82.5818 4 -7 6 12 394.032 118.500 2 -7 -6 13-63.6401 64.0878 4 -7 6 13-65.9988 63.7275 2 -7 -6 14 100.936 59.2986 4 -7 6 14 299.818 105.737 2 -7 -6 15-124.302 63.6373 4 -7 6 15 34.4195 72.0966 2 -7 -6 16 204.231 64.9361 4 -7 6 16 239.642 89.9739 2 -7 -6 17 38.1954 45.2680 4 -7 6 17-7.70111 68.6239 2 -7 6 18 26.2708 69.2050 2 -7 6 19 522.356 108.092 2 -7 6 20 348.151 86.7374 2 -7 6 21 527.948 88.1337 2 -7 -6 22 53.4846 48.1376 3 -8 -6 0 949.121 150.524 4 -8 -6 1 968.402 156.941 4 -8 -6 -1 995.016 158.902 4 -8 -6 2 2760.55 247.294 4 -8 -6 -2 2750.83 243.525 4 -8 -6 3 530.524 133.019 4 -8 -6 -3 597.526 129.851 4 -8 -6 4 143.605 103.932 4 -8 -6 -4 38.4725 68.6845 4 -8 -6 5 145.757 104.858 4 -8 -6 -5-104.112 77.8483 4 -8 -6 6-62.5720 90.8667 4 -8 -6 -6 51.0974 66.9615 4 -8 -6 7 1267.36 166.895 4 -8 -6 -7 969.771 137.955 4 -8 -6 8 19.1805 80.5345 4 -8 -6 9 1016.23 147.228 4 -8 -6 10 163.491 88.8887 4 -8 -6 11 97.1156 60.5482 3 -8 -6 11-4.64487 64.5786 4 -8 -6 12 14.9850 65.6114 3 -8 -6 12 29.1799 56.9766 4 -8 -6 13 163.129 71.8437 3 -8 -6 13 76.8319 65.2828 4 -8 6 13 141.522 69.3595 2 -8 -6 14 376.843 97.6434 3 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206.113 109.085 1 0 -7 -2-108.317 89.7487 1 0 -7 2-9.01319 71.9614 1 0 7 2 23.2942 94.1994 2 0 -7 3 158.664 76.9756 1 0 7 3 22.6192 94.7308 2 0 7 4-7.91070 84.7290 2 0 7 5 45.1352 88.5123 2 0 -7 5-38.9878 104.728 4 0 7 6-144.918 111.650 2 0 -7 6-30.3769 89.2815 4 0 7 7 265.479 119.024 2 0 -7 7-17.9434 70.8406 4 0 7 8 25.4916 97.2597 2 0 -7 8-58.7419 73.2010 4 0 7 9 41.3546 102.086 2 0 -7 9 21.1260 63.3129 4 0 7 10-73.2771 109.700 2 0 7 11-83.6305 103.352 2 0 7 12 21.4316 103.660 2 0 7 13 102.168 108.080 2 0 7 14-26.1111 80.3068 2 0 7 15-29.6619 97.3673 2 0 7 16-49.8221 91.7788 2 0 7 17-227.341 100.410 2 0 7 18-6.28156 81.5884 2 0 7 19-48.9564 72.9286 2 0 7 20-30.7655 65.0916 2 0 7 21-165.799 71.4589 2 0 7 22-13.6295 47.8011 2 0 7 23-48.4179 34.2623 2 -1 -7 0 575.168 125.303 1 1 -7 0 521.593 117.198 1 -1 7 1 3845.36 342.416 2 -1 -7 1 4089.91 313.147 1 1 -7 1 3685.09 293.084 1 -1 -7 -1 3803.50 313.762 1 1 -7 -1 3446.48 290.306 1 -1 7 2 4190.05 358.728 2 -1 -7 2 4208.18 315.304 4 1 -7 2 3879.49 292.944 1 1 -7 -2 4043.03 319.705 1 -1 7 3 2472.31 278.759 2 -1 -7 3 2660.04 253.280 4 1 7 4 715.875 165.276 2 -1 7 4 667.076 160.365 2 -1 -7 4 883.819 158.531 4 1 7 5 1302.45 206.242 2 -1 -7 5 1516.14 192.959 4 -1 7 5 1141.88 202.267 2 1 7 6 3539.71 322.651 2 -1 7 6 3034.51 308.218 2 -1 -7 6 3161.26 263.112 4 1 7 7 3377.18 312.754 2 -1 7 7 3358.94 327.324 2 -1 -7 7 4097.13 293.465 4 1 -7 7 3791.89 278.057 4 1 7 8-4.92957 94.4380 2 -1 7 8 30.8155 107.330 2 -1 -7 8-26.8339 86.5942 4 1 -7 8-5.58021 85.6131 4 1 7 9 519.516 149.993 2 -1 7 9 497.848 157.824 2 -1 -7 9 592.398 118.609 4 1 7 10-28.5872 112.058 2 -1 -7 10 44.0664 68.7089 4 -1 7 10-44.7338 92.4489 2 1 7 11 188.085 105.983 2 -1 7 11 144.746 116.570 2 1 7 12 18.7614 94.0683 2 -1 7 12 237.047 129.340 2 1 7 13 156.590 108.487 2 -1 7 13 371.258 149.209 2 1 7 14 902.216 165.302 2 -1 7 14 915.707 186.588 2 1 7 15 5105.18 347.829 2 -1 7 15 5199.05 380.159 2 -1 -7 -15 4961.52 302.404 4 1 7 16 217.431 96.9980 2 -1 7 16 314.171 128.641 2 1 7 17 118.701 73.7615 2 -1 7 17 96.3161 96.7630 2 1 7 18-65.0734 66.6009 2 -1 7 18-85.8692 91.5347 2 1 7 19 378.620 101.408 2 -1 7 19 232.015 92.8620 2 1 7 20 695.007 107.625 2 -1 7 20 753.297 129.530 2 1 7 21 334.968 76.2398 2 -1 7 21 196.119 85.5662 2 -1 7 22 196.480 71.7986 2 -1 7 23 1131.36 118.785 2 -2 -7 0 1817.02 223.326 4 -2 7 1 1410.13 220.564 2 -2 -7 1 1440.43 203.190 4 -2 -7 -1 1506.57 206.109 4 -2 7 2 1244.70 198.998 2 -2 -7 2 1505.44 196.366 4 -2 -7 -2 1235.57 194.337 4 -2 7 3 996.195 183.451 2 -2 -7 3 1034.03 173.800 4 -2 -7 -3 1021.08 172.190 4 -2 7 4 13.1927 85.1255 2 -2 -7 4 84.1256 88.7847 4 -2 -7 -4-163.348 102.692 4 -2 7 5 1355.78 210.922 2 -2 -7 5 1228.22 180.653 4 2 7 6 318.647 132.411 2 -2 7 6 410.153 154.929 2 -2 -7 6 392.403 106.739 4 2 7 7 15.5251 82.0042 2 -2 7 7 96.4303 97.3080 2 -2 -7 7 160.101 85.1162 4 2 7 8 2169.42 250.409 2 -2 7 8 1997.99 259.571 2 -2 -7 8 2473.43 225.817 4 2 7 9 923.002 170.379 2 -2 -7 9 789.971 140.228 4 -2 7 9 970.306 203.898 2 -2 -7 -9 820.676 157.546 4 2 7 10 4395.63 340.151 2 -2 7 10 5009.52 393.402 2 -2 -7 10 5259.66 306.719 4 -2 -7 -10 4626.83 328.501 4 2 7 11 7647.08 440.447 2 -2 7 11 7922.60 489.339 2 -2 -7 11 8493.35 373.426 4 -2 -7 -11 7596.22 408.543 4 2 7 12 1312.19 192.923 2 -2 7 12 1357.83 226.356 2 -2 -7 -12 1393.53 187.959 4 2 7 13 2004.02 227.042 2 -2 7 13 2213.37 269.151 2 -2 -7 -13 2262.45 224.356 4 2 7 14 44.5138 76.1906 2 -2 7 14 254.867 136.555 2 -2 -7 -14 125.031 92.4205 4 2 7 15 1106.11 172.083 2 -2 7 15 1206.65 200.348 2 2 7 16 454.834 116.581 2 -2 7 16 355.652 136.718 2 2 7 17 80.6828 66.4024 2 -2 7 17 32.2931 97.6996 2 -2 7 18 333.040 122.037 2 -2 7 19 774.440 145.282 2 -2 7 20 64.9319 74.9150 2 -2 7 21 704.386 123.353 2 -2 7 22 13.8720 59.4818 2 -2 7 23-46.0163 49.0246 2 -3 -7 0-15.0901 90.2705 4 -3 7 1 3204.66 308.919 2 -3 -7 1 3543.25 293.829 4 -3 -7 -1 3459.06 292.753 4 -3 7 2 3859.00 337.148 2 -3 -7 2 3945.16 311.094 4 -3 -7 -2 3591.48 303.843 4 -3 7 3 80.0067 106.900 2 -3 -7 3 124.082 92.4227 4 -3 -7 -3-59.8478 113.844 4 -3 7 4 287.840 125.073 2 -3 -7 4 523.951 142.027 4 -3 -7 -4 495.549 146.768 4 -3 7 5 969.914 185.249 2 -3 -7 5 915.685 161.034 4 -3 -7 -5 672.884 149.246 4 -3 7 6 53.0885 108.799 2 -3 -7 6-21.5353 88.7547 4 -3 -7 -6-2.33794 88.1742 4 -3 7 7 160.450 112.797 2 -3 -7 7 108.818 89.6647 4 -3 -7 -7-43.1383 93.1021 4 -3 -7 8 60.1846 74.9056 4 -3 7 8 28.4209 104.680 2 -3 -7 -8-21.0827 106.079 4 -3 -7 9 862.643 141.173 4 -3 7 9 698.775 169.010 2 -3 -7 -9 767.902 150.459 4 -3 -7 10 308.038 102.030 4 -3 7 10 212.688 134.470 2 -3 -7 -10 220.096 97.7194 4 -3 7 11 5634.89 415.093 2 -3 -7 11 5464.44 305.769 4 -3 -7 -11 5104.42 330.181 4 -3 7 12 4164.24 360.883 2 -3 -7 12 4377.50 264.998 4 -3 -7 -12 4417.96 301.514 4 -3 -7 13 86.0579 64.4174 4 -3 -7 -13-37.5709 75.0096 4 -3 7 13-5.72351 103.597 2 -3 7 14 478.912 148.528 2 -3 7 15 440.463 145.321 2 -3 7 16 166.404 110.702 2 -3 7 17-24.7167 95.5156 2 -3 7 18 1908.14 221.787 2 -3 7 19 20.2784 82.7244 2 -3 7 20 29.4327 73.0693 2 -3 7 21 105.280 74.2092 2 -3 7 22 371.770 88.0621 2 -3 7 23-11.2675 44.1879 2 -4 -7 0 13459.4 547.911 4 -4 -7 1 4595.36 328.577 4 -4 -7 -1 4539.65 332.796 4 -4 7 2 179.407 120.101 2 -4 -7 2 175.235 111.131 4 -4 -7 -2 90.1608 88.8874 4 -4 7 3 3453.19 320.343 2 -4 -7 3 3738.95 290.356 4 -4 -7 -3 3680.84 303.326 4 -4 7 4 225.079 115.962 2 -4 -7 4 266.476 105.767 4 -4 -7 -4 122.274 105.460 4 -4 7 5 3013.69 300.340 2 -4 -7 5 3161.59 262.279 4 -4 -7 -5 3231.71 278.454 4 -4 7 6 35.8621 108.935 2 -4 -7 6 221.037 111.426 4 -4 -7 -6 140.243 98.7137 4 -4 7 7 3425.26 321.590 2 -4 -7 7 3245.21 260.574 4 -4 -7 -7 3233.29 273.670 4 -4 -7 8 1037.35 157.027 4 -4 7 8 1053.76 201.338 2 -4 -7 -8 1067.54 171.006 4 -4 -7 9 1049.96 155.913 4 -4 7 9 852.421 180.126 2 -4 -7 -9 955.753 159.209 4 -4 -7 10 951.972 147.086 4 -4 -7 -10 926.409 149.919 4 -4 7 10 824.800 174.518 2 -4 -7 11 901.475 136.539 4 -4 -7 -11 1009.08 158.564 4 -4 7 11 1084.10 198.730 2 -4 -7 12 66.1567 65.7923 4 -4 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1982.48 198.384 4 -5 -7 -9 1959.36 208.043 4 -5 -7 10 132.530 81.9917 4 -5 -7 -10-0.36502 66.7204 4 -5 7 10 88.6167 90.3382 2 -5 7 11 2316.35 254.700 2 -5 -7 11 2387.78 204.032 4 -5 -7 -11 2644.11 215.421 4 -5 7 12 3961.92 329.538 2 -5 -7 12 4073.46 252.355 4 -5 7 13 1502.60 212.100 2 -5 -7 13 1314.32 144.799 4 -5 -7 14 1210.21 129.946 4 -5 7 14 922.971 173.550 2 -5 7 15 381.648 121.204 2 -5 7 16 1035.62 166.743 2 -5 7 17 980.821 160.384 2 -5 7 18 154.453 86.3156 2 -5 7 19-26.3541 61.6727 2 -5 7 20 62.3732 58.5474 2 -5 7 21 206.446 72.3355 2 -5 7 22 201.452 59.4185 2 -6 -7 0 1202.58 176.478 4 -6 -7 1 1100.44 173.240 4 -6 -7 -1 908.721 158.873 4 -6 -7 2 63.3117 103.677 4 -6 -7 -2 63.3380 85.3992 4 -6 -7 3 8307.20 412.798 4 -6 -7 -3 8193.19 415.211 4 -6 7 4 1343.72 185.342 2 -6 -7 4 1529.05 196.942 4 -6 -7 -4 1467.20 189.208 4 -6 -7 5 1229.90 176.702 4 -6 -7 -5 1123.62 170.764 4 -6 7 5 1052.40 171.234 2 -6 7 6 2852.72 268.963 2 -6 -7 6 2791.68 242.632 4 -6 -7 -6 2591.38 231.901 4 -6 -7 7 36.1074 87.2830 4 -6 7 7-19.0540 77.0714 2 -6 -7 -7-48.2652 80.1848 4 -6 -7 8 44.5531 74.6826 4 -6 7 8 53.6943 76.8279 2 -6 -7 -8 36.0361 73.1361 4 -6 7 9 1962.42 227.744 2 -6 -7 9 1908.85 193.875 4 -6 -7 -9 2115.89 197.924 4 -6 -7 10 95.0497 79.1009 4 -6 -7 -10 128.607 81.4330 4 -6 7 10 84.2556 90.5488 2 -6 -7 11 13.9688 69.4003 4 -6 7 11 17.4641 79.5238 2 -6 -7 12 3.09484 59.6602 4 -6 7 12 85.3344 87.1369 2 -6 -7 13 297.159 77.3365 4 -6 7 13 408.121 120.216 2 -6 -7 14 30.1311 47.0052 4 -6 7 14 67.0411 80.6850 2 -6 -7 15 419.196 71.7845 4 -6 7 15 393.919 106.434 2 -6 7 16 118.294 74.0466 2 -6 7 17 528.527 105.574 2 -6 7 18 421.567 95.1607 2 -6 7 19-4.05185 46.8707 2 -6 7 20 48.4338 44.2908 2 -7 -7 0 23.9851 80.9760 4 -7 -7 1 321.306 111.046 4 -7 -7 -1 280.915 105.869 4 -7 -7 2 129.643 102.362 4 -7 -7 -2 28.8211 75.8864 4 -7 -7 3 1281.32 169.522 4 -7 -7 -3 1408.08 175.835 4 -7 -7 4 1634.27 189.869 4 -7 -7 -4 1854.81 193.933 4 -7 -7 5 2746.66 237.824 4 -7 -7 -5 2471.85 219.850 4 -7 -7 6 1602.02 182.260 4 -7 -7 -6 1346.46 165.978 4 -7 7 7 2029.06 203.484 2 -7 -7 7 1912.09 194.417 4 -7 -7 -7 1975.75 187.106 4 -7 -7 8 502.586 116.847 4 -7 7 8 446.852 109.443 2 -7 -7 -8 393.911 93.8852 4 -7 -7 9 164.445 75.0223 4 -7 7 9 191.928 81.3211 2 -7 -7 -9 240.548 78.6910 4 -7 -7 10 30.1278 65.5443 4 -7 7 10-110.531 71.4924 2 -7 -7 11 160.033 66.5444 4 -7 7 11 135.172 81.6476 2 -7 -7 12 129.032 61.4846 4 -7 7 12 252.681 83.2344 2 -7 -7 13 216.478 63.7158 4 -7 7 13 188.683 79.6805 2 -7 -7 14 39.4752 40.6024 4 -7 7 14 33.0700 68.0806 2 -7 -7 15 705.475 81.9993 4 -7 7 15 767.872 110.820 2 -7 7 16 368.687 83.0031 2 -7 7 17 162.210 57.8002 2 -8 -7 0 404.076 107.771 4 -8 -7 1 425.687 109.298 4 -8 -7 -1 403.740 109.328 4 -8 -7 2-102.410 85.2141 4 -8 -7 -2-30.6990 72.2903 4 -8 -7 3 455.408 111.241 4 -8 -7 -3 344.633 91.8240 4 -8 -7 4 1978.77 190.469 4 -8 -7 -4 2069.00 189.627 4 -8 -7 5 365.857 107.514 4 -8 -7 -5 348.527 89.2135 4 -8 -7 6 1499.08 166.309 4 -8 -7 -6 1399.34 148.187 4 -8 -7 7 496.301 105.824 4 -8 -7 -7 172.488 69.9765 4 -8 -7 8 292.420 84.7758 4 -8 -7 9-6.02585 54.0945 4 -8 -7 10 430.466 88.7020 4 -8 -7 11 681.881 99.6791 4 -8 -7 12 8.83571 42.8218 4 -8 -7 13 527.618 80.2782 4 -8 -7 14-32.8398 38.8268 4 -9 -7 0-43.6258 62.5899 4 -9 -7 1 365.265 87.3926 4 -9 -7 -1 364.585 89.7798 4 -9 -7 2 38.3250 61.7405 4 -9 -7 -2 66.8942 63.2739 4 -9 -7 3 28.9247 69.0232 4 -9 -7 -3 54.2526 59.4252 4 -9 -7 4 30.9076 59.0471 4 -9 -7 -4 10.8242 47.6451 4 -9 -7 5 324.761 84.2014 4 -9 -7 -5 254.114 63.5480 4 -9 -7 6 420.862 90.6840 4 -9 -7 7 1187.74 130.317 4 -9 -7 8 1125.12 122.452 4 -9 -7 9 360.514 79.1291 4 -9 -7 10-53.1329 52.9142 4 -9 -7 11 254.647 58.6562 4 -9 -7 12 316.784 55.1407 4 -10 -7 0 38.9190 45.1659 4 -10 -7 -1-12.4716 43.4741 4 -10 -7 1 2.53607 41.1739 4 -10 -7 -2 80.5601 41.7511 4 -10 -7 2 85.8539 50.5988 4 -10 -7 3 606.461 87.1844 4 -10 -7 -3 472.597 66.9153 4 -10 -7 4 59.7521 44.6312 4 -10 -7 5 311.112 68.8338 4 -10 -7 6 451.634 75.4115 4 -10 -7 7 14.9675 44.2417 4 -10 -7 8 68.8230 45.7213 4 -10 -7 9 336.897 57.3231 4 0 -8 0 21.2134 97.7351 4 0 -8 1 8916.92 446.577 4 0 -8 2 5343.20 348.283 4 0 -8 3 5133.06 335.359 4 0 -8 4 617.230 141.269 4 0 -8 5 6233.98 355.206 4 0 -8 6 2939.35 245.076 4 0 -8 7 3587.66 259.677 4 0 8 8 1602.46 228.951 2 0 -8 8 1495.40 169.727 4 0 8 9 109.727 111.108 2 0 -8 9 186.246 86.0720 4 0 8 10 1631.73 220.808 2 0 8 11 363.092 128.629 2 0 8 12 2085.39 226.596 2 0 8 13 595.515 139.982 2 0 -8 -13 586.177 117.677 4 0 8 14 101.151 92.2072 2 0 -8 -14 12.0246 72.8313 4 0 8 15 111.832 78.2635 2 0 -8 -15 19.1002 65.5533 4 0 8 16 1259.44 157.006 2 0 -8 -16 1183.22 124.588 4 0 8 17 804.945 123.237 2 0 8 18 168.803 68.3185 2 -1 -8 0 37.3773 93.6700 4 -1 -8 1 58.2089 91.5404 4 -1 -8 -1 15.2104 98.5809 4 -1 -8 2 61.5737 103.459 4 -1 -8 -2 62.1767 93.0194 4 -1 -8 3 3614.02 287.052 4 -1 -8 -3 3664.05 300.476 4 1 -8 3 3321.17 270.818 4 -1 -8 4 496.129 126.314 4 1 -8 4 622.832 135.212 4 -1 -8 -4 583.649 142.578 4 -1 -8 5-39.3392 89.0621 4 1 -8 5 16.7669 78.8222 4 -1 -8 -5 73.0530 105.857 4 -1 -8 6 50.0690 80.6252 4 1 -8 6 52.8928 83.2004 4 -1 -8 -6 41.8076 95.7195 4 -1 8 7 582.496 159.501 2 -1 -8 7 532.316 125.083 4 1 -8 7 396.319 105.871 4 -1 -8 -7 756.810 159.093 4 -1 8 8 278.107 128.763 2 -1 -8 8 315.126 96.1796 4 1 -8 8 638.852 115.183 4 -1 -8 -8 438.731 121.148 4 -1 8 9 2041.29 250.900 2 -1 -8 9 1947.50 181.578 4 -1 -8 -9 1772.30 200.255 4 -1 8 10 4296.74 342.307 2 -1 -8 10 4384.91 252.187 4 -1 -8 -10 3901.96 283.025 4 -1 8 11 7519.78 437.730 2 -1 -8 -11 7434.39 372.860 4 -1 8 12 9058.73 469.677 2 -1 -8 -12 9004.72 396.309 4 -1 8 13 1959.58 222.604 2 -1 -8 -13 2111.24 194.503 4 -1 8 14 1196.61 180.116 2 -1 -8 -14 1138.79 143.936 4 -1 8 15 918.556 151.234 2 -1 -8 -15 893.853 118.264 4 1 -8 -16 1051.34 123.099 4 -1 8 16 861.003 136.886 2 -1 8 17 89.8163 71.6031 2 -1 8 18 553.949 105.449 2 -1 8 19 164.389 62.7296 2 -2 -8 0 162.648 106.869 4 -2 -8 1 750.979 152.466 4 -2 -8 -1 1012.42 172.608 4 -2 -8 2 33.6826 95.1715 4 -2 -8 -2 53.5177 97.7452 4 -2 -8 3 219.652 99.0351 4 -2 -8 -3 78.9524 102.268 4 -2 -8 4 26.4520 96.3008 4 -2 -8 -4 61.4071 98.2028 4 2 -8 4 59.3903 84.7343 4 -2 -8 5 132.319 104.863 4 -2 -8 -5 29.2325 95.4438 4 2 -8 5 203.713 96.1989 4 -2 8 6 176.248 118.176 2 -2 -8 6 114.741 89.9913 4 -2 -8 -6 23.2392 98.1792 4 2 -8 6 76.5851 72.3135 4 -2 8 7 66.7720 118.645 2 -2 -8 7-81.0339 89.5617 4 2 -8 7-89.6899 79.4869 4 -2 -8 -7-34.7148 89.5430 4 -2 8 8-109.985 108.007 2 -2 -8 8 56.7430 80.7147 4 -2 -8 -8 18.8895 88.7117 4 -2 8 9 126.350 112.317 2 -2 -8 9 204.751 79.7791 4 -2 -8 -9 119.811 85.2853 4 -2 -8 10 1005.72 133.206 4 -2 8 10 840.734 175.891 2 -2 -8 -10 714.933 138.323 4 -2 8 11 56.3738 108.835 2 -2 -8 11 59.3457 62.1931 4 -2 -8 -11-48.5618 94.8831 4 -2 8 12 1370.34 207.723 2 -2 -8 -12 1444.87 165.120 4 -2 8 13 2647.90 261.913 2 -2 -8 -13 2314.37 193.088 4 -2 8 14 4827.00 327.160 2 -2 -8 -14 4623.95 247.080 4 -2 8 15-58.3150 89.1066 2 -2 8 16 360.302 105.471 2 -2 8 17 401.314 100.600 2 2 -8 -17 451.946 79.2070 4 -2 8 18 92.3045 65.8204 2 -2 8 19 169.783 67.7656 2 -2 8 20 112.745 51.4578 2 -3 -8 0 10.3846 90.0356 4 -3 -8 1 1498.19 195.785 4 -3 -8 -1 1483.75 198.641 4 -3 -8 2 1602.74 201.125 4 -3 -8 -2 1386.88 192.236 4 -3 -8 3 846.398 149.456 4 -3 -8 -3 833.680 155.155 4 -3 -8 4 2701.59 241.236 4 -3 -8 -4 2821.77 254.952 4 -3 -8 5 1242.56 170.658 4 -3 -8 -5 1252.22 182.664 4 3 -8 5 1458.65 169.565 4 -3 -8 6 927.927 147.473 4 -3 8 6 1076.47 194.196 2 -3 -8 -6 811.217 150.562 4 3 -8 6 901.078 132.689 4 -3 8 7 1760.20 233.447 2 -3 -8 7 1944.24 195.471 4 -3 -8 -7 2018.17 211.770 4 -3 8 8 17.8639 105.907 2 -3 -8 8-14.4236 78.3653 4 -3 -8 -8-48.7953 95.1151 4 -3 -8 9 1198.44 148.255 4 -3 8 9 1079.45 187.827 2 -3 -8 -9 879.984 138.578 4 -3 8 10 60.3327 92.9283 2 -3 -8 10 206.892 84.2670 4 -3 -8 -10 39.4492 86.4003 4 -3 8 11 58.3881 103.966 2 -3 -8 11-4.40479 55.0838 4 -3 -8 -11-13.4657 77.8478 4 -3 8 12 1139.23 186.631 2 -3 -8 12 1146.31 122.675 4 -3 -8 -12 1206.35 144.078 4 -3 8 13 1501.79 200.082 2 -3 -8 -13 1540.96 147.756 4 -3 8 14 556.240 140.400 2 -3 8 15 1500.77 183.943 2 -3 8 16 186.087 94.3730 2 -3 8 17 1222.62 150.092 2 -3 8 18 346.817 89.0765 2 -3 8 19 146.576 58.6455 2 -4 -8 0 1484.20 188.499 4 -4 -8 1-2.70537 94.9152 4 -4 -8 -1 18.3467 92.8948 4 -4 -8 2 1522.28 190.428 4 -4 -8 -2 1514.01 189.749 4 -4 -8 3 67.9268 90.1597 4 -4 -8 -3 121.608 95.5384 4 -4 -8 4 74.6636 85.0182 4 -4 -8 -4 14.9004 94.1073 4 -4 -8 5 1625.15 184.845 4 -4 -8 -5 1432.40 183.612 4 -4 -8 6 64.9841 78.1129 4 -4 -8 -6-0.73110 77.1475 4 -4 8 7 595.360 152.934 2 -4 -8 7 707.244 124.641 4 -4 -8 -7 444.808 114.289 4 -4 8 8 352.989 122.171 2 -4 -8 8 522.830 117.687 4 -4 -8 -8 186.148 88.1528 4 -4 8 9 200.231 108.661 2 -4 -8 9 247.744 82.6580 4 -4 -8 -9 182.763 82.0384 4 -4 8 10 303.062 124.917 2 -4 -8 10 272.259 80.4778 4 -4 -8 -10 367.830 94.6354 4 -4 -8 11 33.3014 53.5320 4 -4 8 11 53.5865 93.9710 2 -4 -8 -11 6.27218 66.0486 4 -4 8 12 1761.25 206.414 2 -4 -8 12 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71.3214 4 1 -9 -7-2.42841 71.1814 4 -1 -9 8 167.320 59.2876 4 -1 -9 -8 41.4707 68.7153 4 1 -9 -8 119.698 81.7962 4 -1 -9 -9 111.912 76.6683 4 1 -9 -9 69.0358 69.8675 4 -1 -9 -10 60.2217 66.7013 4 1 -9 -10 125.053 73.6611 4 -1 -9 -11-21.5211 50.6755 4 1 -9 -11-18.1799 56.4658 4 -1 -9 -12 172.846 59.1420 4 1 -9 -12 200.500 64.8687 4 -1 -9 -13-63.4567 40.9295 4 1 -9 -13-32.8350 45.0934 4 -2 -9 0 600.823 123.193 4 2 -9 0 793.853 134.168 4 -2 -9 1 36.8469 79.0031 4 -2 -9 -1 0.31385 78.7480 4 2 -9 1-3.38243 76.1837 4 2 -9 -1-13.1252 72.3319 4 -2 -9 2 681.642 120.818 4 -2 -9 -2 605.478 119.350 4 2 -9 2 635.871 120.064 4 2 -9 -2 675.738 123.480 4 -2 -9 3 32.2498 71.6264 4 -2 -9 -3 4.02727 84.5299 4 2 -9 3-68.3017 77.6077 4 2 -9 -3 25.6231 76.0396 4 -2 -9 4 312.042 95.6616 4 -2 -9 -4 276.814 95.0784 4 2 -9 4 329.777 87.4573 4 2 -9 -4 338.908 104.654 4 -2 -9 5-17.2775 72.1601 4 -2 -9 -5 32.1830 72.7431 4 2 -9 5-4.21365 58.9903 4 2 -9 -5-36.3090 81.9456 4 -2 -9 6 1716.16 157.770 4 -2 -9 -6 1584.31 161.924 4 -2 -9 7 249.581 78.3069 4 -2 -9 -7 240.896 89.5309 4 -2 -9 8 730.083 101.207 4 -2 -9 -8 661.002 110.342 4 2 -9 -8 727.128 120.901 4 -2 -9 9-108.804 49.6620 4 -2 -9 -9 9.93915 59.6435 4 2 -9 -9 29.6816 67.8437 4 -2 -9 -10 261.236 70.3803 4 2 -9 -10 328.075 89.4814 4 -2 -9 -11 296.869 65.0121 4 2 -9 -11 439.756 89.6357 4 -2 -9 -12 11.5794 40.6271 4 2 -9 -12-23.1435 50.5405 4 2 -9 -13 114.512 51.3930 4 -3 -9 0-38.5703 80.4015 4 3 -9 0-71.1258 78.0907 4 -3 -9 1 0.29023 72.9269 4 -3 -9 -1 11.0835 74.2707 4 3 -9 1-16.4387 65.6989 4 3 -9 -1 4.69638 68.9339 4 -3 -9 2 15.6947 69.6581 4 -3 -9 -2 56.3942 74.1667 4 3 -9 2 59.3195 62.2285 4 -3 -9 3 1489.33 155.790 4 -3 -9 -3 1447.61 157.608 4 3 -9 3 1539.04 146.691 4 -3 -9 4-4.81149 62.1794 4 -3 -9 -4-7.23007 71.0882 4 3 -9 4 18.5495 60.8628 4 -3 -9 5 159.935 77.6365 4 -3 -9 -5 122.264 80.4032 4 -3 -9 6 437.967 93.3206 4 -3 -9 -6 621.141 105.781 4 -3 -9 7 20.3365 51.6408 4 -3 -9 -7 56.0753 60.5072 4 -3 -9 8 963.216 110.030 4 -3 -9 -8 1015.47 118.699 4 -3 -9 9 48.4304 42.5435 4 -3 -9 -9 38.3649 51.9479 4 -3 -9 -10 10.5760 41.4342 4 -3 -9 -11 125.488 46.7263 4 3 -9 -11 154.482 66.7495 4 3 -9 -12 314.772 70.6864 4 3 -9 -13 1044.96 99.4026 4 -4 -9 0 1172.62 138.440 4 4 -9 0 1160.77 130.262 4 -4 -9 1 332.376 91.7200 4 -4 -9 -1 390.279 100.002 4 4 -9 1 276.796 82.8634 4 4 -9 -1 350.507 88.8583 4 -4 -9 2 83.0319 71.4663 4 -4 -9 -2 99.7581 69.8033 4 4 -9 2 186.661 68.4324 4 -4 -9 3-12.6713 65.8890 4 -4 -9 -3 23.8188 60.1242 4 4 -9 3 20.6465 50.8039 4 -4 -9 4 656.105 104.595 4 -4 -9 -4 557.572 102.459 4 -4 -9 5 633.323 103.607 4 -4 -9 -5 534.704 99.0698 4 -4 -9 6 133.613 61.9717 4 -4 -9 -6 207.022 68.9961 4 -4 -9 7 547.598 88.5117 4 -4 -9 -7 541.270 92.1188 4 -4 -9 8 427.406 74.3442 4 -4 -9 -8 562.895 86.0809 4 -4 -9 9 125.792 45.4131 4 -4 -9 -9 100.071 46.2848 4 4 -9 -12 81.5629 47.0294 4 -5 -9 0 47.9538 60.1045 4 5 -9 0-61.0041 51.1303 4 -5 -9 1 65.6362 56.0298 4 -5 -9 -1 1.82322 52.2978 4 5 -9 1 130.168 56.5861 4 5 -9 -1 103.216 57.1343 4 -5 -9 2 295.094 74.0614 4 -5 -9 -2 309.058 82.0333 4 -5 -9 3 113.528 65.8783 4 -5 -9 -3 127.421 63.9611 4 -5 -9 4 1878.94 147.349 4 -5 -9 -4 1804.15 144.003 4 -5 -9 5 32.3725 51.5518 4 -5 -9 -5 45.7553 46.1175 4 -5 -9 6 110.459 55.7200 4 -5 -9 -6 73.7583 48.7556 4 -5 -9 7 449.228 75.0575 4 -5 -9 -7 313.657 63.2149 4 -5 -9 8 477.689 69.5016 4 -6 -9 0 61.7921 47.9908 4 -6 -9 1 162.921 56.4110 4 -6 -9 -1 101.675 50.7382 4 -6 -9 2 34.0196 43.2002 4 -6 -9 -2 13.5576 43.3375 4 6 -9 -2 47.5556 40.2677 4 -6 -9 3 89.6891 50.6916 4 -6 -9 -3 101.616 47.9702 4 -6 -9 4-74.6412 48.0110 4 -6 -9 -4-15.1438 34.6962 4 -6 -9 5-71.6177 43.4723 4 -6 -9 -5 9.83357 34.7880 4 -6 -9 6 73.6711 34.4789 4 0 -10 0 431.946 68.2330 4 0 -10 1 108.306 47.3085 4 0 -10 -1 101.090 48.6506 4 0 -10 -2 324.218 64.2545 4 0 -10 -3 88.7538 47.3913 4 0 -10 -4 342.452 63.7594 4 0 -10 -5 600.324 76.7556 4 -1 -10 0 11.3355 35.7487 4 1 -10 0-31.9572 38.2830 4 -1 -10 1 423.389 68.1053 4 -1 -10 -1 414.708 68.7739 4 1 -10 -1 425.630 69.7664 4 -1 -10 -2 143.044 50.8796 4 1 -10 -2 147.632 46.5869 4 -1 -10 -3 27.7736 39.8777 4 1 -10 -3 73.7185 48.5401 4 -1 -10 -4 27.7664 37.6386 4 1 -10 -4 62.8496 43.0461 4 -1 -10 -5 942.358 87.8668 4 1 -10 -5 927.616 90.1995 4 -2 -10 0 167.754 47.5413 4 -2 -10 1 41.2928 37.9201 4 -2 -10 -1 97.8789 45.6306 4 -2 -10 -2 209.830 51.6970 4 -2 -10 -3 326.071 60.1909 4 0 0 0 0.00 0.00 0 TITL exp_6994 in Pbca REM Pbca (#61, found as Pcab in ba-c setting) CELL 1.54184 11.961169 8.121533 27.586518 90.0000 90.0000 90.0000 ZERR 4.00 0.000475 0.000346 0.001197 0.0000 0.0000 0.0000 LATT 1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H N S UNIT 132.00 132.00 12.00 4.00 TREF HKLF 4 END ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S1 S 0.40769(5) 1.07994(8) 0.56349(2) 0.0808(3) Uani 1 1 d . . . . . N1 N 0.20400(17) 0.9676(3) 0.54422(8) 0.0840(6) Uani 1 1 d D . . . . H1N H 0.161(2) 0.895(3) 0.5314(10) 0.101 Uiso 1 1 d D U . . . N2 N 0.33773(15) 0.9067(2) 0.48914(6) 0.0625(4) Uani 1 1 d D . . . . H2N H 0.4060(10) 0.908(3) 0.4787(8) 0.075 Uiso 1 1 d D U . . . N3 N 0.25787(14) 0.82382(19) 0.46276(6) 0.0607(4) Uani 1 1 d . . . . . C1 C 0.30945(17) 0.9790(2) 0.53135(7) 0.0626(5) Uani 1 1 d . . . . . C2 C 0.1582(3) 1.0259(5) 0.58985(11) 0.1101(10) Uani 1 1 d . . . . . H2A H 0.197919 1.124233 0.599923 0.132 Uiso 1 1 calc R U . . . H2B H 0.168847 0.942470 0.614581 0.132 Uiso 1 1 calc R U . . . C3 C 0.0386(3) 1.0632(5) 0.58535(17) 0.1391(14) Uani 1 1 d . . . . . H3A H 0.028524 1.153114 0.563184 0.209 Uiso 1 1 calc R U . . . H3B H 0.009184 1.092909 0.616522 0.209 Uiso 1 1 calc R U . . . H3C H -0.000141 0.967978 0.573391 0.209 Uiso 1 1 calc R U . . . C4 C 0.28904(16) 0.7701(2) 0.42132(6) 0.0570(4) Uani 1 1 d . . . . . H4 H 0.362028 0.787942 0.410951 0.068 Uiso 1 1 calc R U . . . C5 C 0.21236(16) 0.6825(2) 0.39066(6) 0.0551(4) Uani 1 1 d . . . . . H5 H 0.141266 0.659052 0.402428 0.066 Uiso 1 1 calc R U . . . C6 C 0.23898(15) 0.6335(2) 0.34599(6) 0.0557(4) Uani 1 1 d . . . . . H6 H 0.310561 0.659404 0.335262 0.067 Uiso 1 1 calc R U . . . C7 C 0.16775(15) 0.5435(2) 0.31210(6) 0.0541(4) Uani 1 1 d . . . . . C8 C 0.06033(17) 0.4929(2) 0.32368(7) 0.0636(5) Uani 1 1 d . . . . . H8 H 0.030544 0.519669 0.353807 0.076 Uiso 1 1 calc R U . . . C9 C -0.0029(2) 0.4039(3) 0.29140(10) 0.0829(7) Uani 1 1 d . . . . . H9 H -0.074344 0.369578 0.300014 0.099 Uiso 1 1 calc R U . . . C10 C 0.0386(3) 0.3657(4) 0.24700(12) 0.1029(9) Uani 1 1 d . . . . . H10 H -0.004487 0.305024 0.225343 0.123 Uiso 1 1 calc R U . . . C11 C 0.1430(3) 0.4160(4) 0.23407(10) 0.1037(9) Uani 1 1 d . . . . . H11 H 0.170577 0.391110 0.203416 0.124 Uiso 1 1 calc R U . . . C12 C 0.2087(2) 0.5047(3) 0.26659(8) 0.0773(6) Uani 1 1 d . . . . . H12 H 0.280185 0.537972 0.257693 0.093 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S1 0.0763(4) 0.0896(4) 0.0764(4) -0.0236(3) -0.0228(3) 0.0027(3) N1 0.0783(12) 0.0958(14) 0.0778(12) -0.0277(11) 0.0037(10) -0.0159(11) N2 0.0641(9) 0.0650(9) 0.0584(9) -0.0056(7) -0.0096(7) -0.0059(7) N3 0.0694(9) 0.0562(9) 0.0563(8) -0.0025(7) -0.0089(7) -0.0076(7) C1 0.0734(12) 0.0554(9) 0.0590(10) -0.0018(8) -0.0117(9) 0.0019(9) C2 0.103(2) 0.131(2) 0.0960(19) -0.0405(19) 0.0208(17) -0.0169(18) C3 0.113(3) 0.126(3) 0.178(4) -0.034(2) 0.046(3) 0.016(2) C4 0.0643(10) 0.0495(9) 0.0573(10) 0.0031(8) -0.0061(8) -0.0044(8) C5 0.0612(10) 0.0487(8) 0.0555(9) 0.0039(7) -0.0019(8) -0.0057(7) C6 0.0596(10) 0.0497(8) 0.0578(10) 0.0032(8) -0.0012(8) -0.0053(7) C7 0.0643(10) 0.0460(8) 0.0518(9) 0.0041(7) -0.0040(8) 0.0004(7) C8 0.0653(11) 0.0602(10) 0.0654(11) 0.0059(9) -0.0104(9) -0.0034(9) C9 0.0774(14) 0.0722(14) 0.0990(18) 0.0029(12) -0.0255(13) -0.0121(11) C10 0.121(2) 0.0858(16) 0.102(2) -0.0215(15) -0.0427(18) -0.0124(17) C11 0.135(3) 0.107(2) 0.0696(14) -0.0308(14) -0.0103(16) 0.0016(18) C12 0.0902(15) 0.0808(14) 0.0609(11) -0.0108(11) 0.0024(11) -0.0039(12) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C1 N1 C2 125.0(2) . . C1 N1 H1N 121(2) . . C2 N1 H1N 111(2) . . C1 N2 N3 119.72(17) . . C1 N2 H2N 121.4(16) . . N3 N2 H2N 118.9(16) . . C4 N3 N2 115.91(17) . . N1 C1 N2 116.35(18) . . N1 C1 S1 124.18(16) . . N2 C1 S1 119.46(16) . . N1 C2 C3 111.2(3) . . N1 C2 H2A 109.4 . . C3 C2 H2A 109.4 . . N1 C2 H2B 109.4 . . C3 C2 H2B 109.4 . . H2A C2 H2B 108.0 . . C2 C3 H3A 109.5 . . C2 C3 H3B 109.5 . . H3A C3 H3B 109.5 . . C2 C3 H3C 109.5 . . H3A C3 H3C 109.5 . . H3B C3 H3C 109.5 . . N3 C4 C5 120.61(18) . . N3 C4 H4 119.7 . . C5 C4 H4 119.7 . . C6 C5 C4 122.65(17) . . C6 C5 H5 118.7 . . C4 C5 H5 118.7 . . C5 C6 C7 126.97(17) . . C5 C6 H6 116.5 . . C7 C6 H6 116.5 . . C12 C7 C8 117.99(19) . . C12 C7 C6 119.22(18) . . C8 C7 C6 122.79(17) . . C9 C8 C7 121.1(2) . . C9 C8 H8 119.4 . . C7 C8 H8 119.4 . . C10 C9 C8 120.3(2) . . C10 C9 H9 119.9 . . C8 C9 H9 119.9 . . C9 C10 C11 120.2(2) . . C9 C10 H10 119.9 . . C11 C10 H10 119.9 . . C10 C11 C12 120.2(3) . . C10 C11 H11 119.9 . . C12 C11 H11 119.9 . . C7 C12 C11 120.2(3) . . C7 C12 H12 119.9 . . C11 C12 H12 119.9 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 S1 C1 1.685(2) . N1 C1 1.314(3) . N1 C2 1.452(3) . N1 H1N 0.859(10) . N2 C1 1.347(3) . N2 N3 1.377(2) . N2 H2N 0.866(10) . N3 C4 1.279(2) . C2 C3 1.467(5) . C2 H2A 0.9700 . C2 H2B 0.9700 . C3 H3A 0.9600 . C3 H3B 0.9600 . C3 H3C 0.9600 . C4 C5 1.436(2) . C4 H4 0.9300 . C5 C6 1.333(2) . C5 H5 0.9300 . C6 C7 1.461(2) . C6 H6 0.9300 . C7 C12 1.384(3) . C7 C8 1.386(3) . C8 C9 1.374(3) . C8 H8 0.9300 . C9 C10 1.357(4) . C9 H9 0.9300 . C10 C11 1.362(5) . C10 H10 0.9300 . C11 C12 1.393(4) . C11 H11 0.9300 . C12 H12 0.9300 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 C1 N2 N3 C4 174.56(17) . . . . C2 N1 C1 N2 175.2(3) . . . . C2 N1 C1 S1 -6.1(4) . . . . N3 N2 C1 N1 -1.3(3) . . . . N3 N2 C1 S1 179.89(13) . . . . C1 N1 C2 C3 154.8(3) . . . . N2 N3 C4 C5 -179.71(15) . . . . N3 C4 C5 C6 175.63(17) . . . . C4 C5 C6 C7 179.69(17) . . . . C5 C6 C7 C12 178.93(19) . . . . C5 C6 C7 C8 -1.8(3) . . . . C12 C7 C8 C9 1.4(3) . . . . C6 C7 C8 C9 -177.88(18) . . . . C7 C8 C9 C10 -1.0(3) . . . . C8 C9 C10 C11 -0.3(4) . . . . C9 C10 C11 C12 1.0(5) . . . . C8 C7 C12 C11 -0.6(3) . . . . C6 C7 C12 C11 178.7(2) . . . . C10 C11 C12 C7 -0.6(4) . . . .