#------------------------------------------------------------------------------ #$Date: 2022-12-05 12:40:57 +0200 (Mon, 05 Dec 2022) $ #$Revision: 279704 $ #$URL: file:///home/coder/svn-repositories/cod/cif/8/10/63/8106328.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_8106328 loop_ _publ_author_name 'Luo, Guoyong' 'Yang, Wude' 'Lang, Tianqiong' 'Zhao, Chenliang' 'Zhang, Jingjie' _publ_section_title ; The crystal structure of (E)-2-(4-hydroxyphenyl)-5-(prop-1-en-1-yl)benzofuran-3-carbaldehyde, C18H14O3 ; _journal_issue 5 _journal_name_full 'Zeitschrift f\"ur Kristallographie - New Crystal Structures' _journal_page_first 873 _journal_page_last 874 _journal_paper_doi 10.1515/ncrs-2018-0066 _journal_volume 233 _journal_year 2018 _chemical_formula_moiety 'C18 H14 O3' _chemical_formula_sum 'C18 H14 O3' _chemical_formula_weight 278.29 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _cell_angle_alpha 90 _cell_angle_beta 99.964(8) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 11.115(4) _cell_length_b 6.878(3) _cell_length_c 18.024(7) _cell_measurement_reflns_used 1226 _cell_measurement_temperature 173 _cell_measurement_theta_max 24.32 _cell_measurement_theta_min 2.29 _cell_volume 1357.1(9) _computing_cell_refinement 'SAINT v8.34A (Bruker, 2013)' _computing_data_reduction 'SAINT v8.34A (Bruker, 2013)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 173 _diffrn_measured_fraction_theta_full 0.993 _diffrn_measured_fraction_theta_max 0.990 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0693 _diffrn_reflns_av_unetI/netI 0.0642 _diffrn_reflns_Laue_measured_fraction_full 0.993 _diffrn_reflns_Laue_measured_fraction_max 0.990 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 7 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 10517 _diffrn_reflns_point_group_measured_fraction_full 0.993 _diffrn_reflns_point_group_measured_fraction_max 0.990 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.481 _diffrn_reflns_theta_min 2.295 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.092 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.5980 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2014/5 (Bruker,2014/5) was used for absorption correction. wR2(int) was 0.0725 before and 0.0544 after correction. The Ratio of minimum to maximum transmission is 0.8020. The \l/2 correction factor is 0.00150. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.362 _exptl_crystal_description block _exptl_crystal_F_000 584 _exptl_crystal_size_max 0.28 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.233 _refine_diff_density_min -0.294 _refine_diff_density_rms 0.058 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.024 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 192 _refine_ls_number_reflns 3064 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.024 _refine_ls_R_factor_all 0.1090 _refine_ls_R_factor_gt 0.0601 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0969P)^2^+0.1139P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1613 _refine_ls_wR_factor_ref 0.1892 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 1861 _reflns_number_total 3064 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; mo_20171135-s-2_0m.res created by SHELXL-2014/7 TITL mo_20171135-s-2_0m_a.res in P2(1)/n REM Old TITL mo_20171135-S-2_0m in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.153, Rweak 0.008, Alpha 0.033, Orientation as input REM Formula found by SHELXT: C18 O3 CELL 0.71073 11.115 6.8779 18.0237 90 99.964 90 ZERR 4 0.0042 0.0026 0.0065 0 0.008 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H O UNIT 72 56 12 L.S. 20 PLAN 20 SIZE 0.28 0.15 0.12 TEMP -100.15 BOND $H list 4 fmap 2 acta REM REM REM WGHT 0.096900 0.113900 FVAR 0.35349 O1 3 0.640573 0.300639 0.213034 11.00000 0.03208 0.03197 = 0.02816 0.00025 0.00890 0.00304 O2 3 0.574563 0.288555 0.457143 11.00000 0.03870 0.07405 = 0.02722 -0.00148 0.00380 -0.00662 O3 3 0.066204 0.321943 0.102098 11.00000 0.03353 0.06404 = 0.04090 -0.00367 0.00808 0.00630 AFIX 147 H3 2 0.059353 0.271343 0.059154 11.00000 -1.50000 AFIX 0 C1 1 0.185462 0.319300 0.135912 11.00000 0.03012 0.03345 = 0.03005 0.00673 0.00793 0.00150 C2 1 0.274788 0.221093 0.106166 11.00000 0.03810 0.03061 = 0.02518 -0.00059 0.00768 0.00204 AFIX 43 H2 2 0.254126 0.153768 0.059683 11.00000 -1.20000 AFIX 0 C3 1 0.393538 0.220842 0.143849 11.00000 0.03719 0.02892 = 0.02447 -0.00064 0.01030 0.00326 AFIX 43 H3A 2 0.454400 0.155307 0.122303 11.00000 -1.20000 AFIX 0 C4 1 0.426528 0.314651 0.212962 11.00000 0.03506 0.02520 = 0.02804 0.00257 0.00742 0.00067 C5 1 0.334133 0.414325 0.241789 11.00000 0.04530 0.02714 = 0.02818 -0.00007 0.00968 0.00160 AFIX 43 H5 2 0.353923 0.480945 0.288481 11.00000 -1.20000 AFIX 0 C6 1 0.216434 0.417179 0.203922 11.00000 0.04124 0.02912 = 0.03345 0.00143 0.01462 0.00639 AFIX 43 H6 2 0.155618 0.486363 0.224203 11.00000 -1.20000 AFIX 0 C7 1 0.549684 0.304264 0.254487 11.00000 0.03505 0.02243 = 0.03087 0.00021 0.00863 -0.00234 C8 1 0.596050 0.296144 0.330508 11.00000 0.02861 0.03157 = 0.03180 -0.00131 0.00549 -0.00249 C9 1 0.526970 0.281454 0.390919 11.00000 0.03262 0.03916 = 0.03233 0.00017 0.00568 -0.00418 AFIX 43 H9 2 0.440909 0.265603 0.378707 11.00000 -1.20000 AFIX 0 C10 1 0.726620 0.287712 0.336844 11.00000 0.03189 0.02763 = 0.03503 -0.00237 0.01066 -0.00238 C11 1 0.825305 0.273233 0.396133 11.00000 0.03261 0.03830 = 0.03379 -0.00161 0.00786 -0.00467 AFIX 43 H11 2 0.811813 0.269693 0.446743 11.00000 -1.20000 AFIX 0 C12 1 0.943111 0.264053 0.380688 11.00000 0.03280 0.03169 = 0.04101 -0.00034 0.00868 0.00002 C13 1 0.960586 0.273936 0.305651 11.00000 0.03535 0.02944 = 0.04770 -0.00195 0.01387 -0.00237 AFIX 43 H13 2 1.041740 0.271299 0.295668 11.00000 -1.20000 AFIX 0 C14 1 0.865090 0.287369 0.245359 11.00000 0.03775 0.02830 = 0.03934 -0.00249 0.01554 0.00056 AFIX 43 H14 2 0.878242 0.293041 0.194708 11.00000 -1.20000 AFIX 0 C15 1 0.749307 0.291994 0.263654 11.00000 0.03604 0.02364 = 0.03098 -0.00057 0.00759 -0.00111 C16 1 1.044878 0.245053 0.444365 11.00000 0.03859 0.04814 = 0.04574 0.00099 0.00918 -0.00049 AFIX 43 H16 2 1.022698 0.242023 0.492943 11.00000 -1.20000 AFIX 0 C17 1 1.162641 0.231691 0.442937 11.00000 0.03778 0.04465 = 0.05224 -0.00116 0.00830 0.00292 AFIX 43 H17 2 1.187394 0.234773 0.395073 11.00000 -1.20000 AFIX 0 C18 1 1.259822 0.212164 0.510393 11.00000 0.04451 0.05718 = 0.06657 -0.00296 -0.00639 0.00113 AFIX 137 H18A 2 1.304378 0.090315 0.507273 11.00000 -1.50000 H18B 2 1.222672 0.211335 0.555897 11.00000 -1.50000 H18C 2 1.316503 0.321963 0.512491 11.00000 -1.50000 AFIX 0 HKLF 4 REM mo_20171135-s-2_0m_a.res in P2(1)/n REM R1 = 0.0601 for 1861 Fo > 4sig(Fo) and 0.1090 for all 3064 data REM 192 parameters refined using 0 restraints END WGHT 0.0968 0.1179 REM Highest difference peak 0.233, deepest hole -0.294, 1-sigma level 0.058 Q1 1 1.3864 0.2658 0.4982 11.00000 0.05 0.23 Q2 1 0.7869 0.2218 0.4602 11.00000 0.05 0.22 Q3 1 0.5254 0.3877 0.3368 11.00000 0.05 0.21 Q4 1 1.0360 0.1216 0.5128 11.00000 0.05 0.20 Q5 1 0.8062 0.3505 0.4589 11.00000 0.05 0.19 Q6 1 1.3784 0.2435 0.5368 11.00000 0.05 0.18 Q7 1 1.0379 0.0380 0.4378 11.00000 0.05 0.17 Q8 1 0.2452 0.3493 0.1131 11.00000 0.05 0.17 Q9 1 1.2202 0.0941 0.5613 11.00000 0.05 0.17 Q10 1 0.6159 0.0870 0.4459 11.00000 0.05 0.17 Q11 1 0.0395 0.1603 0.0304 11.00000 0.05 0.17 Q12 1 1.0896 0.0862 0.5719 11.00000 0.05 0.17 Q13 1 0.8455 0.3876 0.1446 11.00000 0.05 0.17 Q14 1 0.3742 0.1070 0.0256 11.00000 0.05 0.17 Q15 1 1.0862 0.3881 0.5731 11.00000 0.05 0.16 Q16 1 0.4122 0.3925 0.3373 11.00000 0.05 0.16 Q17 1 1.0805 0.2611 0.4008 11.00000 0.05 0.16 Q18 1 0.7471 0.3620 0.3009 11.00000 0.05 0.16 Q19 1 0.0014 0.0859 0.0380 11.00000 0.05 0.16 Q20 1 0.4075 0.3259 0.3364 11.00000 0.05 0.16 REM The information below was added by Olex2. REM REM R1 = 0.0601 for 1861 Fo > 4sig(Fo) and 0.1090 for all 11151 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.23, deepest hole -0.29 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.1090 REM R1_gt = 0.0601 REM wR_ref = 0.1892 REM GOOF = 1.024 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 11151 REM Reflections_gt = 1861 REM Parameters = n/a REM Hole = -0.29 REM Peak = 0.23 REM Flack = n/a ; _cod_data_source_file suppl_ncrs-2018-0066_suppl.cif _cod_data_source_block mo _cod_database_code 8106328 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.989 _shelx_estimated_absorpt_t_min 0.975 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2.a Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3A), C5(H5), C6(H6), C9(H9), C11(H11), C13(H13), C14(H14), C16(H16), C17(H17) 2.b Idealised Me refined as rotating group: C18(H18A,H18B,H18C) 2.c Idealised tetrahedral OH refined as rotating group: O3(H3) ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.64057(15) 0.3006(2) 0.21303(9) 0.0303(4) Uani 1 1 d . . . . . O2 O 0.57456(18) 0.2886(3) 0.45714(10) 0.0469(6) Uani 1 1 d . . . . . O3 O 0.06620(17) 0.3219(3) 0.10210(11) 0.0460(6) Uani 1 1 d . . . . . H3 H 0.0594 0.2713 0.0592 0.069 Uiso 1 1 calc GR . . . . C1 C 0.1855(2) 0.3193(4) 0.13591(14) 0.0309(6) Uani 1 1 d . . . . . C2 C 0.2748(2) 0.2211(4) 0.10617(13) 0.0310(6) Uani 1 1 d . . . . . H2 H 0.2541 0.1538 0.0597 0.037 Uiso 1 1 calc R . . . . C3 C 0.3935(2) 0.2208(4) 0.14385(13) 0.0296(6) Uani 1 1 d . . . . . H3A H 0.4544 0.1553 0.1223 0.036 Uiso 1 1 calc R . . . . C4 C 0.4265(2) 0.3147(3) 0.21296(13) 0.0292(6) Uani 1 1 d . . . . . C5 C 0.3341(2) 0.4143(4) 0.24179(13) 0.0331(6) Uani 1 1 d . . . . . H5 H 0.3539 0.4809 0.2885 0.040 Uiso 1 1 calc R . . . . C6 C 0.2164(2) 0.4172(4) 0.20392(14) 0.0336(6) Uani 1 1 d . . . . . H6 H 0.1556 0.4864 0.2242 0.040 Uiso 1 1 calc R . . . . C7 C 0.5497(2) 0.3043(3) 0.25449(13) 0.0291(6) Uani 1 1 d . . . . . C8 C 0.5961(2) 0.2961(4) 0.33051(14) 0.0306(6) Uani 1 1 d . . . . . C9 C 0.5270(3) 0.2815(4) 0.39092(14) 0.0347(6) Uani 1 1 d . . . . . H9 H 0.4409 0.2656 0.3787 0.042 Uiso 1 1 calc R . . . . C10 C 0.7266(2) 0.2877(4) 0.33684(14) 0.0309(6) Uani 1 1 d . . . . . C11 C 0.8253(2) 0.2732(4) 0.39613(15) 0.0346(6) Uani 1 1 d . . . . . H11 H 0.8118 0.2697 0.4467 0.042 Uiso 1 1 calc R . . . . C12 C 0.9431(2) 0.2641(4) 0.38069(15) 0.0349(6) Uani 1 1 d . . . . . C13 C 0.9606(3) 0.2739(4) 0.30565(16) 0.0367(6) Uani 1 1 d . . . . . H13 H 1.0417 0.2713 0.2957 0.044 Uiso 1 1 calc R . . . . C14 C 0.8651(2) 0.2874(4) 0.24536(15) 0.0341(6) Uani 1 1 d . . . . . H14 H 0.8782 0.2930 0.1947 0.041 Uiso 1 1 calc R . . . . C15 C 0.7493(2) 0.2920(4) 0.26365(14) 0.0300(6) Uani 1 1 d . . . . . C16 C 1.0449(3) 0.2451(4) 0.44437(17) 0.0439(7) Uani 1 1 d . . . . . H16 H 1.0227 0.2420 0.4929 0.053 Uiso 1 1 calc R . . . . C17 C 1.1626(3) 0.2317(4) 0.44294(18) 0.0448(7) Uani 1 1 d . . . . . H17 H 1.1874 0.2348 0.3951 0.054 Uiso 1 1 calc R . . . . C18 C 1.2598(3) 0.2122(5) 0.5104(2) 0.0580(9) Uani 1 1 d . . . . . H18A H 1.3044 0.0903 0.5073 0.087 Uiso 1 1 calc GR . . . . H18B H 1.2227 0.2113 0.5559 0.087 Uiso 1 1 calc GR . . . . H18C H 1.3165 0.3220 0.5125 0.087 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0321(10) 0.0320(10) 0.0282(9) 0.0002(7) 0.0089(7) 0.0030(8) O2 0.0387(12) 0.0741(15) 0.0272(10) -0.0015(9) 0.0038(8) -0.0066(10) O3 0.0335(11) 0.0640(15) 0.0409(11) -0.0037(10) 0.0081(9) 0.0063(9) C1 0.0301(14) 0.0335(15) 0.0300(12) 0.0067(11) 0.0079(10) 0.0015(11) C2 0.0381(15) 0.0306(14) 0.0252(12) -0.0006(10) 0.0077(11) 0.0020(11) C3 0.0372(15) 0.0289(14) 0.0245(12) -0.0006(10) 0.0103(10) 0.0033(11) C4 0.0351(15) 0.0252(13) 0.0280(12) 0.0026(10) 0.0074(10) 0.0007(11) C5 0.0453(17) 0.0271(14) 0.0282(12) -0.0001(10) 0.0097(11) 0.0016(12) C6 0.0412(16) 0.0291(14) 0.0335(13) 0.0014(11) 0.0146(11) 0.0064(12) C7 0.0351(15) 0.0224(13) 0.0309(13) 0.0002(10) 0.0086(11) -0.0023(10) C8 0.0286(14) 0.0316(14) 0.0318(13) -0.0013(11) 0.0055(10) -0.0025(11) C9 0.0326(15) 0.0392(15) 0.0323(13) 0.0002(11) 0.0057(11) -0.0042(12) C10 0.0319(14) 0.0276(14) 0.0350(13) -0.0024(11) 0.0107(11) -0.0024(11) C11 0.0326(15) 0.0383(15) 0.0338(14) -0.0016(11) 0.0079(11) -0.0047(12) C12 0.0328(15) 0.0317(15) 0.0410(15) -0.0003(11) 0.0087(12) 0.0000(11) C13 0.0354(16) 0.0294(14) 0.0477(16) -0.0019(12) 0.0139(12) -0.0024(12) C14 0.0377(16) 0.0283(14) 0.0393(14) -0.0025(11) 0.0155(12) 0.0006(11) C15 0.0360(14) 0.0236(13) 0.0310(13) -0.0006(10) 0.0076(11) -0.0011(11) C16 0.0386(17) 0.0481(18) 0.0457(16) 0.0010(13) 0.0092(13) -0.0005(13) C17 0.0378(17) 0.0447(17) 0.0522(17) -0.0012(14) 0.0083(13) 0.0029(13) C18 0.045(2) 0.057(2) 0.067(2) -0.0030(17) -0.0064(16) 0.0011(16) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C7 O1 C15 106.64(19) . . C1 O3 H3 109.5 . . O3 C1 C2 122.8(2) . . O3 C1 C6 117.6(2) . . C2 C1 C6 119.6(2) . . C1 C2 H2 120.0 . . C3 C2 C1 120.1(2) . . C3 C2 H2 120.0 . . C2 C3 H3A 119.3 . . C2 C3 C4 121.5(2) . . C4 C3 H3A 119.3 . . C3 C4 C5 117.4(2) . . C3 C4 C7 121.3(2) . . C5 C4 C7 121.3(2) . . C4 C5 H5 119.4 . . C6 C5 C4 121.3(2) . . C6 C5 H5 119.4 . . C1 C6 H6 119.9 . . C5 C6 C1 120.2(2) . . C5 C6 H6 119.9 . . O1 C7 C4 116.4(2) . . O1 C7 C8 111.1(2) . . C8 C7 C4 132.4(2) . . C7 C8 C9 126.7(2) . . C7 C8 C10 106.2(2) . . C10 C8 C9 126.9(2) . . O2 C9 C8 122.6(3) . . O2 C9 H9 118.7 . . C8 C9 H9 118.7 . . C11 C10 C8 135.4(2) . . C15 C10 C8 105.7(2) . . C15 C10 C11 118.8(2) . . C10 C11 H11 120.2 . . C12 C11 C10 119.6(2) . . C12 C11 H11 120.2 . . C11 C12 C13 119.0(3) . . C11 C12 C16 118.2(3) . . C13 C12 C16 122.8(3) . . C12 C13 H13 118.5 . . C14 C13 C12 123.1(3) . . C14 C13 H13 118.5 . . C13 C14 H14 122.2 . . C15 C14 C13 115.7(2) . . C15 C14 H14 122.2 . . O1 C15 C10 110.3(2) . . C14 C15 O1 125.9(2) . . C14 C15 C10 123.8(2) . . C12 C16 H16 115.7 . . C17 C16 C12 128.6(3) . . C17 C16 H16 115.7 . . C16 C17 H17 117.5 . . C16 C17 C18 125.1(3) . . C18 C17 H17 117.5 . . C17 C18 H18A 109.5 . . C17 C18 H18B 109.5 . . C17 C18 H18C 109.5 . . H18A C18 H18B 109.5 . . H18A C18 H18C 109.5 . . H18B C18 H18C 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 O1 C7 1.357(3) . O1 C15 1.384(3) . O2 C9 1.220(3) . O3 H3 0.8400 . O3 C1 1.360(3) . C1 C2 1.383(4) . C1 C6 1.389(3) . C2 H2 0.9500 . C2 C3 1.376(4) . C3 H3A 0.9500 . C3 C4 1.394(3) . C4 C5 1.407(4) . C4 C7 1.444(4) . C5 H5 0.9500 . C5 C6 1.367(3) . C6 H6 0.9500 . C7 C8 1.379(3) . C8 C9 1.440(4) . C8 C10 1.437(4) . C9 H9 0.9500 . C10 C11 1.396(3) . C10 C15 1.386(3) . C11 H11 0.9500 . C11 C12 1.386(4) . C12 C13 1.401(4) . C12 C16 1.471(4) . C13 H13 0.9500 . C13 C14 1.385(4) . C14 H14 0.9500 . C14 C15 1.383(4) . C16 H16 0.9500 . C16 C17 1.317(4) . C17 H17 0.9500 . C17 C18 1.486(4) . C18 H18A 0.9800 . C18 H18B 0.9800 . C18 H18C 0.9800 . loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma -1 0 0 -0.2 0.1 1 0 0 0.3 0.2 1 0 0 0.1 0.2 -1 0 0 0.1 0.2 2 0 0 7 0.8 2 0 0 5.5 0.7 3 0 0 0 0.5 3 0 0 -0.2 0.5 4 0 0 -0.1 0.6 4 0 0 0.5 0.6 5 0 0 0.5 0.9 5 0 0 -0.1 0.7 6 0 0 165.18 6.2 6 0 0 166.68 6.4 7 0 0 0.7 0.9 7 0 0 -0.6 0.8 9 0 0 0.4 1.3 9 0 0 -1 1.2 10 0 0 84.89 5.3 10 0 0 92.59 5.4 11 0 0 -1.7 1.5 11 0 0 0.7 1.5 12 0 0 1.2 1.8 12 0 0 2.3 1.9 13 0 0 0.9 2 13 0 0 -0.4 1.9 14 0 0 1.8 2.3 14 0 0 5 2.7 0 -1 0 -9.3 0.5 0 1 0 -9.2 0.5 -1 -1 0 15.4 0.8 1 -1 0 16.4 0.9 1 -1 0 16.4 0.8 -1 -1 0 15.1 0.8 -1 1 0 15.2 0.9 1 1 0 15.5 0.8 1 1 0 16.8 0.8 2 -1 0 174.68 4.8 2 -1 0 172.48 5.3 2 -1 0 174.08 5.3 2 1 0 174.18 5.2 2 1 0 177.18 5.2 3 -1 0 -0.4 0.6 3 -1 0 -0.1 0.2 3 1 0 0.2 0.5 3 1 0 0.6 0.6 5 -1 0 16 1.8 5 -1 0 18.9 2 5 1 0 17.7 1.9 5 1 0 14.5 1.6 6 -1 0 54.29 3.2 6 -1 0 64.99 3.3 6 1 0 52.49 3 6 1 0 52.79 3.2 7 -1 0 16.5 2.3 7 -1 0 16.4 2.1 7 1 0 17.4 2.2 7 1 0 15.8 2.1 8 -1 0 6.2 1.5 8 1 0 5.3 1.6 8 1 0 3.6 1.3 9 -1 0 3 1.5 -9 -1 0 6.4 1.4 9 -1 0 5.8 1.8 9 1 0 8.4 2 9 1 0 7.4 2.1 10 -1 0 3.1 1.6 10 -1 0 4.2 1.7 10 1 0 2.8 1.8 10 1 0 2.3 1.6 11 -1 0 1.5 1.6 11 -1 0 1.3 1.6 11 1 0 -1.1 1.6 11 1 0 0.1 1.5 12 -1 0 0.3 1.8 12 -1 0 -0.1 1.7 12 1 0 -1.2 1.7 12 1 0 1 2 13 -1 0 -0.4 1.9 13 1 0 3.7 2.2 13 1 0 0.9 2.2 14 -1 0 3 2.5 14 1 0 1 2.4 14 1 0 1.5 2.3 0 -2 0 9999 259.57 -1 -2 0 93.79 3.1 1 -2 0 86.79 3.2 -1 -2 0 93.49 3 1 -2 0 89.59 3.2 1 2 0 90.29 2.9 2 -2 0 89.99 3.1 2 -2 0 94.59 3.4 2 2 0 88.69 3.1 3 -2 0 4.7 0.6 3 -2 0 6.3 1.1 3 2 0 5.4 0.8 3 2 0 6.7 1 4 -2 0 4.6 0.5 4 -2 0 2.9 0.9 4 2 0 2.2 0.8 4 2 0 0.1 0.6 5 -2 0 12.9 1.7 5 -2 0 15.6 1.8 5 2 0 11.5 1.4 5 2 0 11.4 1.5 6 -2 0 124.89 5.4 6 -2 0 126.59 5.3 6 2 0 126.89 5.1 7 -2 0 21.9 2.5 7 -2 0 25.6 2.7 7 2 0 22.9 2.4 7 2 0 15.4 1.8 8 -2 0 16.2 2.4 8 -2 0 14.5 2.3 8 2 0 10.5 1.7 8 2 0 14.6 2.2 9 -2 0 49.2 3.7 9 -2 0 44.3 3.7 9 2 0 47.6 3.8 9 2 0 47.9 3.6 -10 -2 0 52.79 4 10 -2 0 56.39 4.2 10 2 0 56.19 4.1 10 2 0 58.19 4.6 11 -2 0 0.3 1.5 11 2 0 0.7 1.6 11 2 0 2.6 2 12 -2 0 1.6 2 12 2 0 1.4 1.7 12 2 0 -0.9 1.8 13 -2 0 0.8 2 13 2 0 4.9 2.3 13 2 0 2 2.2 0 -3 0 0.1 0.5 1 -3 0 26.9 1.7 -1 -3 0 27 1.5 -1 3 0 27.9 1.6 -2 -3 0 25.9 1.5 2 -3 0 25.5 1.7 2 3 0 25.2 1.5 3 -3 0 5.6 1.1 -3 -3 0 8.4 1.2 3 -3 0 7.8 1 3 3 0 11.1 1.3 4 -3 0 8.5 1 4 -3 0 11.6 1.7 5 -3 0 14.7 1 5 -3 0 17.7 2.1 5 3 0 13.6 1.5 5 3 0 15.2 1.7 6 -3 0 1.6 1 6 3 0 0 0.7 6 3 0 -0.4 0.5 7 -3 0 0.5 1 7 3 0 -0.5 0.8 7 3 0 0.3 0.6 8 -3 0 22.3 2.9 8 3 0 24.8 2.7 9 -3 0 0.4 1.3 -9 -3 0 1.2 1.2 9 3 0 2.8 1.4 9 3 0 1.1 1 -10 -3 0 7 1.8 10 -3 0 6.1 2.1 10 3 0 8 2 10 3 0 6 2.1 11 -3 0 1.9 1.6 11 3 0 3.2 2.1 11 3 0 0.8 1.5 12 -3 0 0.9 1.9 12 3 0 0.8 1.7 12 3 0 0.9 2 13 -3 0 4.4 2.4 13 3 0 6.5 2.9 13 3 0 5.5 2.4 0 -4 0 778.22 22.1 0 -4 0 763.72 21.3 1 -4 0 495.25 14.2 1 -4 0 502.45 14.6 -1 -4 0 478.05 13.9 -1 4 0 480.55 13.7 2 -4 0 10.5 1.5 -2 -4 0 10.8 1.3 2 -4 0 11.2 1.6 -2 4 0 5.7 1.1 -3 -4 0 -0.5 0.4 3 -4 0 0.2 0.7 3 -4 0 0 0.5 3 4 0 -0.2 0.6 -4 -4 0 2.3 0.8 4 -4 0 1.2 0.9 4 -4 0 1.9 0.8 4 4 0 2.3 0.9 5 -4 0 7.1 1.5 -5 -4 0 6.8 1.2 5 4 0 4 1 6 -4 0 8.8 1.8 7 -4 0 7.6 1.9 7 4 0 11.1 1.8 7 4 0 6.6 1.5 -8 -4 0 -0.7 1.2 8 -4 0 -0.6 1.2 8 4 0 0 1 8 4 0 0.7 1 9 -4 0 53.59 4.2 -9 -4 0 50.19 3.9 9 4 0 51.49 3.7 10 -4 0 20.6 3.3 -10 -4 0 17.1 2.8 10 4 0 13.9 2.4 11 -4 0 1.9 1.7 -11 -4 0 0.6 1.2 11 4 0 1.8 2 12 -4 0 2.9 2.1 12 4 0 -0.6 2.1 0 -5 0 -0.3 0.7 0 -5 0 -0.3 0.6 1 -5 0 14.2 2 1 -5 0 13.3 1.7 -1 -5 0 15.1 2.3 -1 -5 0 14.2 1.7 -2 -5 0 8 1.7 -2 -5 0 10.5 1.4 2 -5 0 16 2.1 2 -5 0 15.3 2 -2 5 0 16.3 1.8 -3 -5 0 7 1.2 3 -5 0 9.7 1.6 3 -5 0 6.9 1.5 -3 5 0 11.2 1.7 4 -5 0 -0.4 0.8 -4 -5 0 0.4 0.8 -4 -5 0 1.7 0.7 4 -5 0 2.2 0.9 -4 5 0 1.5 1 4 5 0 1.2 0.8 5 -5 0 4.6 1.1 -5 -5 0 3.8 1.4 -5 -5 0 3.8 1.1 5 -5 0 4.5 1.4 5 5 0 1.7 0.7 6 -5 0 -0.3 1.1 -6 -5 0 -0.1 0.7 -6 -5 0 -0.5 0.9 6 5 0 -0.9 0.8 7 -5 0 5.5 1.8 -7 -5 0 3 1.6 7 5 0 3.4 1.6 -8 -5 0 2.8 1.7 8 -5 0 1.7 1.6 9 -5 0 0.9 1.6 -9 -5 0 1.2 1.7 -10 -5 0 -0.6 1.4 10 -5 0 2.1 2 -11 -5 0 2 1.8 11 -5 0 2.7 2.1 0 -6 0 30.5 2.4 0 -6 0 35 3.6 1 -6 0 150.38 5.9 -1 -6 0 144.79 5.7 -1 -6 0 149.69 6.8 1 -6 0 152.58 6.6 2 -6 0 3 1.3 -2 -6 0 3.3 1.3 -2 -6 0 4.4 1.5 2 -6 0 3 1.2 3 -6 0 7.6 1.7 -3 -6 0 3.1 1.3 3 -6 0 6.6 1.6 -4 -6 0 3.5 1.3 4 -6 0 4 1.4 4 -6 0 5.3 1.6 -5 -6 0 9 2.2 5 -6 0 11.8 2.2 -6 -6 0 4.6 1.6 6 -6 0 2.1 1.4 7 -6 0 3.4 1.6 -7 -6 0 -0.2 1.2 -8 -6 0 -0.2 1.3 8 -6 0 0.9 1.7 -9 -6 0 18.3 3.6 9 -6 0 16.5 3.3 10 -6 0 0.1 1.8 -10 -6 0 -0.2 1.7 0 -7 0 -0.5 0.9 1 -7 0 1.5 1.3 -1 -7 0 2 1.3 2 -7 0 15.1 2.5 -2 -7 0 9.7 2.2 -3 -7 0 1 1.2 3 -7 0 0 1.1 3 -7 0 2.2 1.4 -4 -7 0 0.9 1.3 4 -7 0 0.7 1.3 4 -7 0 0.4 1.1 5 -7 0 1.5 1.3 -5 -7 0 -0.5 1 6 -7 0 1.5 1.4 -6 -7 0 -0.3 1.2 -7 -7 0 -0.9 1.2 7 -7 0 1.4 1.6 -8 -7 0 -0.8 1.4 8 -7 0 2.7 1.9 0 -8 0 20.6 3.4 1 -8 0 40.1 4.5 -1 -8 0 30.4 3.9 2 -8 0 1 1.5 -2 -8 0 5 1.7 -3 -8 0 2.9 1.6 3 -8 0 7.3 2.2 -4 -8 0 -0.6 1 -5 -8 0 7 2.3 -6 -8 0 1.6 1.6 14 0 -1 -1.1 2 13 0 -1 7.6 2.7 12 0 -1 1.2 1.9 12 0 -1 0.6 1.6 11 0 -1 3.1 1.8 11 0 -1 4.4 2 10 0 -1 -0.8 1.3 10 0 -1 2.5 1.7 9 0 -1 60.39 4.2 9 0 -1 65.59 4.2 8 0 -1 -0.4 0.9 8 0 -1 -1.1 0.7 7 0 -1 29.6 2.5 7 0 -1 27.9 2.5 6 0 -1 0.4 0.8 6 0 -1 0.1 0.9 5 0 -1 78.79 3.6 5 0 -1 81.69 3.7 4 0 -1 -0.6 0.6 4 0 -1 0.4 0.6 4 0 -1 0.3 0.4 3 0 -1 1.8 0.6 3 0 -1 1.5 0.5 3 0 -1 1.3 0.7 2 0 -1 0.7 0.4 2 0 -1 -0.1 0.4 2 0 -1 0.3 0.3 0 0 1 -1.2 0.1 0 0 -1 -1.2 0.1 0 0 -1 -1.1 0.1 0 0 1 -1.1 0.1 0 0 -1 -1.2 0.1 -1 0 -1 25 1.1 1 0 1 27.1 1 -1 0 -1 25.2 1 2 0 1 0 0.3 -2 0 -1 0.1 0.2 2 0 1 -0.4 0.4 3 0 1 206.38 6.4 3 0 1 214.58 6.4 -3 0 -1 198.68 5.7 -4 0 -1 0.3 0.3 4 0 1 -0.2 0.5 4 0 1 0.4 0.6 -5 0 -1 7.5 0.8 5 0 1 6.8 1.2 5 0 1 7.5 1.3 6 0 1 -0.6 0.7 -6 0 -1 0 0.4 6 0 1 -0.2 0.8 7 0 1 100.89 4.6 -7 0 -1 95.99 3.3 7 0 1 92.79 4.7 8 0 1 0.1 0.8 8 0 1 0.7 1 9 0 1 149.69 6.8 9 0 1 148.99 7 10 0 1 -1.1 1.3 10 0 1 2 1.4 11 0 1 2.8 1.7 11 0 1 0.9 1.6 12 0 1 0 1.5 12 0 1 0.5 1.9 13 0 1 2.3 1.9 13 0 1 3.2 2.1 14 0 1 -1.9 2 14 0 1 1.3 2.2 14 -1 -1 -3.7 1.9 14 1 -1 1.9 2.6 14 1 -1 -2.3 2.1 13 -1 -1 8.6 2.7 13 1 -1 9.4 2.8 13 1 -1 5.5 2.7 12 -1 -1 2.5 1.7 12 1 -1 0.4 1.7 12 1 -1 1.4 1.8 11 -1 -1 -0.4 1.6 11 1 -1 1.1 1.7 11 1 -1 -1.1 1.5 10 -1 -1 2.9 1.6 10 -1 -1 0.2 1.3 10 1 -1 1.7 1.7 10 1 -1 1.2 1.4 9 -1 -1 2.5 1.4 9 -1 -1 2 1.3 9 1 -1 2.4 1.6 9 1 -1 6.3 1.8 8 -1 -1 5.8 1.5 8 1 -1 18.1 2.3 8 1 -1 19.7 2.6 7 -1 -1 -0.2 0.9 7 -1 -1 -0.3 0.5 7 1 -1 2.6 1.2 7 1 -1 0.2 0.9 6 -1 -1 24.2 2.1 6 1 -1 24.7 2.1 6 1 -1 22.6 2.3 5 -1 -1 19.8 1.8 5 -1 -1 22.5 1.1 5 1 -1 22.1 1.8 5 1 -1 24.5 2 4 -1 -1 -0.4 0.3 4 -1 -1 0.5 0.3 4 -1 -1 0.3 0.6 4 1 -1 -0.5 0.6 4 1 -1 0.2 0.6 3 -1 -1 258.87 7.2 3 -1 -1 274.07 8.1 3 1 -1 262.47 7.9 3 1 -1 267.67 7.9 2 -1 -1 0 0.3 2 -1 -1 0.2 0.5 2 1 -1 0 0.4 2 1 -1 -0.3 0.5 1 -1 -1 651.33 16.7 1 -1 -1 622.64 16.6 -1 -1 1 625.94 16.7 -1 1 1 621.24 16.6 0 -1 -1 6.7 0.7 0 -1 -1 6.9 0.6 0 -1 1 6.5 0.7 0 1 1 7.4 0.7 0 1 -1 6.8 0.7 1 -1 1 99.59 3.3 1 -1 1 102.49 3.1 1 1 1 99.39 3.2 -1 1 -1 103.49 3.1 2 -1 1 44 2 2 1 1 46 2 2 1 1 44.8 1.8 3 -1 1 326.47 9.4 3 1 1 318.07 9.1 3 1 1 308.87 9.4 4 -1 1 1.2 0.7 4 -1 1 0.8 0.8 4 1 1 1.5 0.7 4 1 1 -0.1 0.6 5 -1 1 450.05 13.5 5 -1 1 445.86 13.5 5 1 1 443.96 13.1 5 1 1 454.15 13.5 6 -1 1 10.7 1.7 6 -1 1 13.2 1.9 6 1 1 11.3 1.8 6 1 1 11.6 1.6 7 -1 1 6.3 1.5 7 -1 1 7.4 1.7 -7 -1 -1 6.1 1.1 7 1 1 6.1 1.4 7 1 1 6.2 1.4 8 -1 1 4.3 1.5 -8 -1 -1 5.1 1 8 -1 1 2.4 1.2 8 1 1 4.5 1.6 8 1 1 5.4 1.5 9 -1 1 135.39 6.6 9 -1 1 127.89 6.3 9 1 1 141.19 6.8 9 1 1 143.69 6.4 10 -1 1 6.1 2.1 10 -1 1 7.7 2 10 1 1 2.2 1.5 10 1 1 3.4 1.9 11 -1 1 -1.2 1.4 11 -1 1 1.8 1.7 11 1 1 0.8 1.5 11 1 1 0.2 1.8 12 -1 1 1.4 1.7 12 -1 1 0.4 2 12 1 1 -1.4 1.9 12 1 1 0.7 1.6 13 -1 1 4.1 2.5 13 -1 1 9.2 2.8 13 1 1 5.9 2.7 13 1 1 8.8 2.7 14 -1 1 1.1 2.3 14 1 1 1.9 2.3 14 1 1 1.1 2.3 13 -2 -1 1.1 1.9 13 2 -1 5.3 2.5 13 2 -1 2.3 2.2 12 -2 -1 -2 1.3 12 2 -1 -0.9 1.5 12 2 -1 2 2 11 -2 -1 1.2 1.5 11 2 -1 2.2 1.7 11 2 -1 4.8 2.2 10 -2 -1 6.7 2.1 10 2 -1 3.6 1.7 10 2 -1 4.9 2 9 -2 -1 25.7 3.1 9 2 -1 25.1 3 9 2 -1 20.1 2.8 8 -2 -1 25 2.9 8 2 -1 19.7 2.5 8 2 -1 20.2 2.5 7 -2 -1 27.9 3 7 2 -1 30.4 2.4 6 -2 -1 12.5 1.8 6 2 -1 9 1.4 6 2 -1 14.9 1.8 5 -2 -1 35.4 1.4 5 -2 -1 34.7 2.4 5 2 -1 34.9 2.3 5 2 -1 34.6 2.3 4 -2 -1 0.7 0.4 4 -2 -1 1.5 0.8 4 2 -1 -0.1 0.5 4 2 -1 3.7 0.9 3 -2 -1 23.7 1.3 3 -2 -1 21.8 1.6 3 2 -1 25 1.6 3 2 -1 26 1.5 2 -2 -1 67.59 2.5 2 -2 -1 60.09 2.6 -2 -2 1 66.59 2.6 2 2 -1 64.79 2.3 1 -2 -1 634.04 17.5 1 -2 -1 665.13 17.8 -1 -2 1 653.63 17.7 -1 2 1 664.33 17.7 0 -2 -1 1809.82 47.4 0 -2 -1 1887.21 48.1 0 -2 1 1827.92 47.8 0 2 1 1792.02 47.6 -1 -2 -1 322.37 9.5 -1 -2 -1 321.17 8.7 1 -2 1 321.87 9.3 1 2 1 315.87 9 2 -2 1 13.5 1.4 2 2 1 14.2 1 2 2 1 13.8 1.2 3 -2 1 99.99 3.9 3 -2 1 95.29 3.1 3 -2 1 101.69 3.8 3 2 1 97.39 3.7 3 2 1 102.09 3.5 4 -2 1 25.7 1.9 4 -2 1 29 2.1 4 2 1 28.7 2 4 2 1 30.1 1.8 5 -2 1 11.5 1.6 5 -2 1 13.2 1.7 5 2 1 11.7 1.7 6 -2 1 1.1 0.8 6 -2 1 1.3 1 6 2 1 -0.1 0.7 6 2 1 -0.4 0.7 -7 -2 -1 7 1.4 7 -2 1 9.6 1.8 7 2 1 7.1 1.5 7 2 1 4.1 1.2 8 -2 1 3.9 1.6 -8 -2 -1 6.4 1.4 8 -2 1 4.2 1.4 8 2 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8.9 1 -3 2 15.7 1.7 -1 -3 -2 10.5 1.5 1 3 2 18.2 1.7 2 -3 2 6.4 1.2 2 3 2 7.3 1.2 -3 -3 -2 62.49 3.3 3 -3 2 62.49 3.1 3 3 2 58.29 2.9 -4 -3 -2 3.7 1.1 4 -3 2 4.3 1.2 4 -3 2 2.7 0.6 4 3 2 2.4 1 4 3 2 4 0.8 -5 -3 -2 62.59 3.4 5 -3 2 60.49 3.5 5 -3 2 54.39 3.1 5 3 2 64.99 3.4 5 3 2 48 2.6 -6 -3 -2 2.8 1.1 6 -3 2 4.4 1.3 6 -3 2 3.6 1.2 6 3 2 3.1 1 6 3 2 3.6 1.2 -7 -3 -2 55.49 3.5 7 -3 2 50.69 3.5 7 -3 2 54.09 3.6 7 3 2 48.1 3 -8 -3 -2 23.6 2.8 8 -3 2 23.5 2.9 8 -3 2 20.6 2.9 8 3 2 21.8 2.4 -9 -3 -2 14.3 2.3 9 -3 2 8 2.1 9 -3 2 10.3 2.3 9 3 2 8.2 1.8 9 3 2 10.9 2.1 10 -3 2 8.2 2.2 -10 -3 -2 9.4 2 10 3 2 9.2 2 10 3 2 8.9 2.3 11 -3 2 0 1.2 11 3 2 1.8 1.6 11 3 2 -1 1.7 12 -3 2 0.6 1.6 12 3 2 0.7 2.1 13 -3 2 2.3 2.1 13 3 2 1 2.4 12 -4 -2 2.6 2.3 12 4 -2 0.5 2.4 12 4 -2 3.5 2.1 11 -4 -2 -0.3 1.7 11 4 -2 1 1.6 11 4 -2 2.7 1.7 10 -4 -2 3.6 1.9 10 4 -2 3.8 1.8 10 4 -2 1.5 1.5 9 -4 -2 6.4 1.9 9 4 -2 7.6 2 9 4 -2 5.4 1.4 8 -4 -2 1 1.2 8 4 -2 1.2 1 8 4 -2 -1.6 0.9 7 -4 -2 12.2 2.2 7 4 -2 11.2 1.8 6 -4 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0 0.4 1 0 -3 574.44 15.8 -1 0 3 594.04 15.9 1 0 -3 608.84 15.9 0 0 3 0.1 0.4 0 0 3 -0.3 0.4 0 0 -3 -0.4 0.3 0 0 -3 -0.5 0.3 -1 0 -3 48.9 1.8 1 0 3 48.5 2 1 0 3 49 1.9 2 0 3 -0.4 0.4 2 0 3 -0.3 0.5 -2 0 -3 -0.2 0.3 -3 0 -3 1.9 0.4 3 0 3 1.5 0.6 -4 0 -3 0.2 0.3 4 0 3 -0.2 0.5 4 0 3 0.4 0.4 -5 0 -3 137.59 4.2 5 0 3 130.29 5.1 6 0 3 0.1 0.8 -6 0 -3 0.4 0.4 6 0 3 0 0.5 7 0 3 14.2 2 -7 0 -3 16 1.1 8 0 3 -1.4 0.9 8 0 3 -0.3 0.6 9 0 3 78.59 4.7 9 0 3 77.79 5 10 0 3 -0.7 1.2 10 0 3 1.7 1.5 11 0 3 2.2 1.8 11 0 3 -0.9 1.4 12 0 3 -0.8 1.7 12 0 3 1 1.7 13 0 3 7 2.7 13 0 3 7.6 2.7 14 -1 -3 1.7 2.2 14 1 -3 -0.8 2 13 -1 -3 9.8 2.8 13 1 -3 9.7 2.8 12 -1 -3 0.9 1.6 12 1 -3 0.2 1.7 11 -1 -3 6.7 2.1 11 1 -3 0.7 1.6 11 1 -3 -0.2 1.6 10 -1 -3 4.8 1.8 10 1 -3 5 1.7 10 1 -3 5.1 2 9 -1 -3 147.39 6.7 9 1 -3 139.99 6.6 9 1 -3 141.99 6.6 8 -1 -3 8.5 1.1 8 1 -3 5.6 1.6 8 1 -3 10.9 2 7 -1 -3 0.9 0.5 7 -1 -3 -0.3 0.8 7 1 -3 -0.3 0.8 7 1 -3 0.1 0.9 6 -1 -3 0.8 0.9 6 -1 -3 1.2 0.5 6 1 -3 0.3 0.8 6 1 -3 0.3 0.9 5 -1 -3 341.47 10.6 5 -1 -3 339.77 9.6 5 1 -3 338.17 10.5 5 1 -3 335.37 10.5 4 -1 -3 28.5 1.5 4 -1 -3 27.1 1.9 4 1 -3 17.4 1.8 4 1 -3 25.5 1.7 4 1 -3 28.6 1.8 3 -1 -3 82.89 2.9 3 -1 -3 81.09 3.2 3 1 -3 74.89 3.1 3 1 -3 79.89 3.2 2 -1 -3 96.29 3.3 2 -1 -3 98.29 3.3 2 1 -3 98.19 3.5 2 1 -3 94.59 3.5 1 -1 -3 2743.63 71.59 1 -1 -3 2822.42 72.79 -1 1 3 2783.92 71.99 -1 1 3 2735.23 71.49 0 -1 -3 15.3 1 0 -1 3 14.3 0.9 0 1 -3 15.3 1 0 1 3 13.7 1.2 1 -1 3 250.77 7.1 -1 -1 -3 249.68 7.4 1 -1 3 251.57 7.4 1 1 3 247.08 7.4 -1 1 -3 258.67 7.1 2 -1 3 22.2 1.5 -2 -1 -3 22.6 1.4 2 -1 3 23.9 1.5 2 1 3 24.9 1.2 2 1 3 25.3 1.6 -2 1 -3 23 1 -3 -1 -3 52.89 2.4 3 -1 3 51.89 2.5 -3 1 -3 55.99 1.8 3 1 3 56.39 2.3 -4 -1 -3 2.4 0.6 4 -1 3 1.2 0.8 4 -1 3 0.9 0.8 4 1 3 1.3 0.9 4 1 3 0.3 0.6 5 -1 3 196.98 7.1 -5 -1 -3 202.68 6.6 5 -1 3 210.78 7.3 5 1 3 214.68 7.4 5 1 3 203.78 6.8 6 -1 3 2.6 1.2 -6 -1 -3 3.8 0.9 6 -1 3 5.3 1.3 6 1 3 3.3 1.2 6 1 3 5.1 1.2 -7 -1 -3 7 1.1 7 -1 3 4.6 1.4 7 -1 3 7.6 1.8 7 1 3 4.4 1.3 7 1 3 6.4 1.6 -8 -1 -3 2.9 0.9 8 -1 3 1.2 1.4 8 -1 3 1.6 1.3 8 1 3 1.3 1.2 8 1 3 2 1.4 9 -1 3 118.39 6.2 9 -1 3 111.89 5.8 9 1 3 106.79 5.5 9 1 3 104.19 6 10 -1 3 -0.6 1.7 10 -1 3 0.7 1.5 10 1 3 4.3 1.8 10 1 3 4.2 2.1 11 -1 3 -1.6 1.3 11 -1 3 1.6 2.1 11 1 3 -1.5 1.7 11 1 3 -2.1 1.3 12 -1 3 -0.1 1.8 12 -1 3 -0.7 1.8 12 1 3 0.1 2 12 1 3 2.5 2 13 -1 3 2.6 2.4 13 -1 3 5.2 2.9 13 1 3 4.7 2.5 13 1 3 2.4 2.4 14 -2 -3 4.4 2.3 14 2 -3 4.1 2.4 13 -2 -3 0.5 1.9 13 2 -3 3.7 2.3 12 -2 -3 -1.3 1.5 12 2 -3 1.2 1.7 12 2 -3 3.5 2 11 -2 -3 7.3 2.2 11 2 -3 10.5 2.6 11 2 -3 4.8 1.7 10 -2 -3 6.4 2.2 10 2 -3 7.8 2.2 10 2 -3 10.1 2.3 9 -2 -3 27.5 3.3 9 2 -3 28.8 3.2 9 2 -3 27.7 3 8 -2 -3 12.8 2.2 8 2 -3 12.8 2 8 2 -3 16.1 2.3 7 -2 -3 6.7 0.9 7 -2 -3 8.4 1.7 7 2 -3 6.3 1.4 7 2 -3 8.2 1.7 6 -2 -3 0.7 0.5 6 -2 -3 0.1 0.8 6 2 -3 -0.4 0.7 6 2 -3 1.5 1 5 -2 -3 51.19 2.9 5 -2 -3 50.79 2.2 5 2 -3 52.89 2.8 5 2 -3 47.1 2.8 4 -2 -3 1.8 0.6 4 -2 -3 2.5 0.8 4 2 -3 1.4 0.8 4 2 -3 2.3 0.8 3 -2 -3 0.7 0.6 3 -2 -3 0.3 0.4 3 2 -3 0.4 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13 2 3 3.5 2.5 13 2 3 3.8 2.8 13 -3 -3 2 2.1 13 3 -3 4.5 2.4 12 -3 -3 0.9 1.8 12 3 -3 -1.4 1.6 12 3 -3 1.1 1.6 11 -3 -3 1.6 1.7 11 3 -3 0.8 1.4 11 3 -3 -1.1 1.3 10 -3 -3 2.2 1.6 10 3 -3 0.5 1.4 10 3 -3 0.8 1.4 9 -3 -3 8.4 2.1 9 3 -3 6.4 1.6 9 3 -3 5.6 1.8 8 -3 -3 -0.7 1 8 3 -3 2.2 1.3 8 3 -3 0.3 0.9 7 -3 -3 6.1 1.6 7 3 -3 3.7 1.2 7 3 -3 4.7 1.4 6 -3 -3 -0.8 0.7 6 -3 -3 0.5 0.4 6 3 -3 0.5 0.9 6 3 -3 -1 0.6 5 3 -3 39.9 2.4 -4 -3 3 171.58 6.3 4 -3 -3 173.68 6.3 4 3 -3 178.88 5.7 3 -3 -3 2.1 0.7 3 -3 -3 2.8 0.8 -3 -3 3 2.6 0.8 -3 3 3 1.9 0.9 -2 -3 3 13.7 1.7 2 -3 -3 13 1.5 2 -3 -3 13.2 1.3 -2 3 3 7.3 1.8 -1 -3 3 144.19 5.2 1 -3 -3 143.99 5.3 1 -3 -3 146.59 4.5 0 -3 3 5.6 1.1 0 -3 -3 5.9 1.1 0 3 3 4.8 1 -1 -3 -3 44.1 2.5 1 -3 3 42.6 2.5 2 -3 3 64.79 3.2 -2 -3 -3 64.59 3.2 2 3 3 53.99 2.8 -3 -3 -3 13.8 1.8 3 -3 3 14.5 1.9 3 -3 3 16.5 1.6 3 3 3 15 1.8 4 -3 3 -0.2 0.6 4 -3 3 1.5 0.9 -4 -3 -3 0.9 0.8 4 3 3 -0.5 0.4 4 3 3 0.1 0.8 5 -3 3 30.7 2.3 -5 -3 -3 31.3 2.5 5 -3 3 30.1 2.5 5 3 3 27.3 2.3 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3.9 1 -4 -3 84.69 3.2 -1 4 3 88.29 3.8 0 -4 3 8.9 1.5 0 -4 -3 10.4 1.7 0 4 3 10.9 1.6 1 -4 3 7.4 1.4 -1 -4 -3 9.6 1.7 1 4 3 9.1 1.5 -2 -4 -3 2.1 0.9 2 -4 3 8.4 1.5 2 4 3 6.5 1.4 -3 -4 -3 1.7 1 3 -4 3 3.2 1.2 3 4 3 4.5 1.2 4 -4 3 3.1 0.8 -4 -4 -3 5.4 1.4 4 -4 3 3.3 1.3 4 4 3 4.9 1.3 5 -4 3 0.4 0.9 -5 -4 -3 0.4 0.8 5 4 3 0.2 0.9 -6 -4 -3 10 2 6 -4 3 8.1 1.9 6 4 3 9 1.4 6 4 3 11.5 1.9 7 -4 3 1.7 1.5 -7 -4 -3 2.1 1.2 7 4 3 2.1 1.1 8 -4 3 61.89 4.4 -8 -4 -3 58.59 4.1 -9 -4 -3 6.4 1.9 9 -4 3 9.7 2.5 9 4 3 2.9 1.3 -10 -4 -3 13 2.4 10 -4 3 8.9 2.6 10 4 3 13 2.5 11 -4 3 -0.9 1.6 11 4 3 0.7 1.7 12 -4 3 -2.5 1.6 12 4 3 3 2.5 11 -5 -3 1.2 1.9 10 -5 -3 5.7 2.1 9 -5 -3 1.9 1.7 -9 -5 3 1.7 1 -8 -5 3 2.3 1.3 8 -5 -3 4.5 1.8 -7 -5 3 5.8 1.6 7 -5 -3 6.9 1.9 -6 -5 3 3.1 1.2 6 -5 -3 1.6 1.2 -6 5 3 0.1 1.2 5 -5 -3 15.6 2.3 5 -5 -3 22.3 2.4 -5 -5 3 18.1 2.4 -5 5 3 20.4 2.9 4 -5 -3 76.19 3.9 4 -5 -3 79.89 3.9 -4 -5 3 77.39 4 -4 5 3 74.09 4.2 3 -5 -3 2.9 1.1 -3 -5 3 2.2 1 3 -5 -3 2.7 0.9 -3 5 3 2.1 1.2 -2 -5 3 7.1 1.5 2 -5 -3 6.3 1.1 2 -5 -3 7.1 1.6 -2 5 3 6.9 1.5 1 -5 -3 10.2 1.9 -1 -5 3 8.9 1.7 1 -5 -3 9.9 1.3 -1 5 3 8.8 1.6 0 -5 -3 43.3 3.1 0 -5 3 42 2.8 0 5 3 42.3 2.6 -1 -5 -3 26.7 3 1 -5 3 30.7 3.1 1 5 3 29.6 2.2 2 -5 3 15.4 2.3 2 5 3 20.8 2.3 -3 -5 -3 2.3 1.2 3 -5 3 3 1.1 3 -5 3 4.1 1.4 3 5 3 3.8 1.3 4 -5 3 2.2 1.3 4 -5 3 0.9 0.7 -4 -5 -3 0.4 0.9 4 5 3 4.6 1.4 -5 -5 -3 1 1.2 5 -5 3 3 1.5 5 5 3 2.3 1.1 6 -5 3 31.1 3.6 -6 -5 -3 24.6 3.2 6 5 3 24.3 2.6 -7 -5 -3 5.2 1.8 7 -5 3 2.9 1.7 7 5 3 0.8 1 8 -5 3 40.5 4.4 -8 -5 -3 39.1 4.4 -9 -5 -3 22.7 3.4 9 -5 3 19.6 3.1 10 -5 3 -0.8 1.8 -10 -5 -3 6.2 2.1 10 5 3 1.5 1.4 -11 -5 -3 -1.8 1.4 11 -5 3 1.2 2 10 -6 -3 11.9 2.9 -10 -6 3 3.5 2.1 9 -6 -3 -0.6 1.4 -9 6 3 -3 1.8 8 -6 -3 3.8 1.9 -8 6 3 2.5 2.3 7 -6 -3 5.4 1.7 -7 6 3 7.7 2.3 6 -6 -3 3.3 1.5 -6 -6 3 2.3 1.2 -6 6 3 4.2 1.8 -5 -6 3 -0.5 0.7 5 -6 -3 -0.7 0.8 5 -6 -3 0.1 1 -5 6 3 -2.2 1.4 4 -6 -3 1.5 1 4 -6 -3 3.4 1.3 -4 -6 3 1 1.1 -4 6 3 3.1 1.5 3 -6 -3 0.3 1 -3 -6 3 1.1 0.9 3 -6 -3 1 0.9 -3 6 3 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0.4 7 0 4 -0.3 0.9 7 0 4 -0.6 0.7 8 0 4 176.08 7.5 8 0 4 160.98 6.9 9 0 4 -1.6 1.2 9 0 4 -0.6 1.2 10 0 4 6.6 2 10 0 4 6.6 2.3 11 0 4 2.9 2 11 0 4 -0.8 1.5 12 0 4 -0.3 1.7 12 0 4 1 1.9 13 0 4 -2.3 2.1 13 0 4 0.6 2.1 14 -1 -4 1.5 2.2 14 1 -4 1.1 2.2 13 -1 -4 -1.7 1.7 13 1 -4 -0.7 1.8 12 -1 -4 0.7 1.7 12 1 -4 -0.1 1.7 11 -1 -4 5.5 2 11 1 -4 2.7 1.8 10 -1 -4 1.6 1.4 10 1 -4 4.3 1.6 9 -1 -4 22.9 3 9 1 -4 20.7 2.8 8 -1 -4 11.2 2 8 1 -4 10.8 2 7 -1 -4 5.3 1.4 7 -1 -4 4.9 0.9 7 1 -4 5.7 1.4 6 -1 -4 93.39 4.3 6 -1 -4 88.09 3.4 6 1 -4 87.49 3.8 6 1 -4 85.09 4.1 5 -1 -4 8.6 1.5 5 -1 -4 9.4 1.1 5 1 -4 10.7 1.4 5 1 -4 8.6 1.4 4 -1 -4 136.99 4.9 4 -1 -4 133.29 4.5 4 1 -4 129.29 5 3 -1 -4 133.29 4.7 3 -1 -4 144.69 4.6 3 1 -4 135.99 4.7 2 -1 -4 63.09 2.5 2 -1 -4 56.69 2.3 -2 1 4 58.59 2.6 2 1 -4 54.49 2.4 -1 -1 4 272.17 8.1 1 -1 -4 266.37 8 -1 -1 4 279.67 7.6 1 -1 -4 277.97 7.6 -1 1 4 262.47 8.1 0 -1 4 259.47 7.2 0 -1 4 253.37 7.7 0 1 -4 263.47 7.5 0 1 4 249.58 7.7 1 -1 4 12.3 1.3 1 -1 4 14.8 1.1 -1 -1 -4 17.1 1.2 -1 1 -4 15.1 1 1 1 4 14.1 1.4 -2 -1 -4 9.8 1.1 2 -1 4 8.1 1.2 2 -1 4 8.7 1.1 2 1 4 9.1 0.9 -2 1 -4 8.7 0.7 2 1 4 7 1.1 -3 -1 -4 13.5 1.4 3 -1 4 12.1 1.4 3 -1 4 12.7 1.4 3 1 4 13.3 1.1 3 1 4 13.1 1.6 -3 1 -4 12.5 0.8 4 -1 4 343.67 10.7 -4 -1 -4 341.87 10.2 4 -1 4 353.66 10.7 4 1 4 351.96 10.9 5 -1 4 17.9 2.1 -5 -1 -4 16.5 1.4 5 -1 4 19.7 2.1 5 1 4 16.7 1.7 5 1 4 17.8 2.2 6 -1 4 64.79 3.6 6 -1 4 67.09 3.8 -6 -1 -4 62.49 3 6 1 4 67.29 3.8 6 1 4 64.99 3.4 7 -1 4 -0.5 1.1 -7 -1 -4 0.2 0.6 7 -1 4 0.3 1 7 1 4 0.1 0.9 7 1 4 0.8 1 8 -1 4 17.1 2.6 -8 -1 -4 17.5 1.8 8 -1 4 14.7 2.5 8 1 4 14.6 2.6 8 1 4 15.6 2.3 9 -1 4 6.3 2 9 -1 4 7.3 2.3 9 1 4 8.4 2.3 9 1 4 8.1 2.1 10 -1 4 -0.2 1.4 10 -1 4 -1.1 1.5 10 1 4 0 1.5 10 1 4 -2.5 1.2 11 -1 4 -0.4 1.8 11 -1 4 -1 1.4 11 1 4 0.2 1.6 11 1 4 -1.2 1.7 12 -1 4 4.1 2.3 12 -1 4 0.8 2.2 12 1 4 4.4 2.2 13 -1 4 -0.2 2 13 -1 4 1.1 2.4 13 1 4 -0.8 2.2 13 1 4 1.1 1.9 14 -2 -4 3.2 2.4 14 2 -4 1 2.5 13 -2 -4 -0.5 1.8 13 2 -4 -0.9 1.9 12 -2 -4 0.2 1.8 12 2 -4 0.7 1.8 11 -2 -4 6.5 2.1 11 2 -4 10.8 2.5 10 -2 -4 27.7 3.6 10 2 -4 28.3 3.5 9 -2 -4 8.5 2.1 9 2 -4 12.7 2.3 9 2 -4 4.1 1.2 8 -2 -4 4.7 1.6 8 2 -4 2.3 0.9 8 2 -4 4 1.5 7 -2 -4 1.1 0.6 7 -2 -4 2.8 1.2 7 2 -4 0.8 0.7 7 2 -4 1 1.1 6 -2 -4 27 2.7 6 -2 -4 28.5 1.7 6 2 -4 27.7 2.4 6 2 -4 25.9 2.1 5 -2 -4 4.2 0.8 5 -2 -4 3.4 1.1 5 2 -4 2.7 1.1 4 -2 -4 10.4 1.2 4 -2 -4 7.8 1.3 4 2 -4 9 1.4 3 -2 -4 52.99 2.5 3 -2 -4 49.7 2.3 3 2 -4 45.3 2.6 -3 2 4 53.79 2.8 2 -2 -4 8.7 1 2 -2 -4 7.3 1.1 -2 -2 4 5.7 1 -1 -2 4 115.69 4.3 -1 2 4 121.19 4.4 1 2 -4 118.09 4.3 0 -2 4 87.89 3.6 0 2 -4 89.89 3.4 0 2 4 87.49 3.5 1 -2 4 12.3 1.5 1 2 4 18.2 1.5 2 -2 4 6.7 1 -2 -2 -4 4.8 1 2 2 4 6.2 1.2 -2 2 -4 7.4 1 3 -2 4 2.4 0.7 -3 -2 -4 2 0.8 3 2 4 3.9 1.1 4 -2 4 0.5 0.6 4 -2 4 1.2 0.8 -4 -2 -4 1.8 0.8 4 2 4 1.4 1 4 2 4 1.7 0.6 -5 -2 -4 42.5 2.6 5 -2 4 41.3 2.7 5 -2 4 42.7 2.7 5 2 4 43.2 2.8 5 2 4 28.8 2 -6 -2 -4 -0.7 0.7 6 -2 4 2.1 1.2 6 -2 4 0.1 0.6 6 2 4 0.5 0.7 6 2 4 2.9 1.3 -7 -2 -4 0.1 0.9 7 -2 4 0.4 0.8 7 -2 4 0.1 1.1 7 2 4 0.3 0.9 7 2 4 2.3 1.3 -8 -2 -4 148.79 6 8 -2 4 148.09 6.9 8 -2 4 149.69 6.8 8 2 4 147.89 6.9 8 2 4 149.49 6.2 -9 -2 -4 19.6 2.3 9 -2 4 24 3.2 9 -2 4 27.1 3.6 9 2 4 25 2.8 9 2 4 20.7 3.1 10 -2 4 8.2 2.2 10 -2 4 7.3 2.4 10 2 4 6.4 1.9 10 2 4 9.1 2.5 11 -2 4 0.3 1.8 11 -2 4 0.6 1.7 11 2 4 1.8 1.6 11 2 4 2.6 2.2 12 -2 4 -0.7 1.7 12 -2 4 0.8 2.2 12 2 4 -0.9 2.2 12 2 4 1.1 1.9 13 -2 4 2.6 2.5 13 -2 4 7.1 2.8 13 2 4 3 2.7 13 -3 -4 -0.8 1.9 13 3 -4 5.1 2.5 12 -3 -4 3.5 2.2 12 3 -4 1.7 2 11 -3 -4 3.2 2.1 11 3 -4 7.9 2.3 10 -3 -4 26.6 3.5 10 3 -4 24.9 3.2 9 -3 -4 39.5 4 9 3 -4 31.2 3.5 8 -3 -4 -0.1 1.2 8 3 -4 0.5 0.6 8 3 -4 0.1 1.2 7 -3 -4 50.69 3.5 7 3 -4 59.29 3.7 6 -3 -4 26.5 1.8 6 -3 -4 29.5 2.5 6 3 -4 28.6 2.5 5 -3 -4 20 1.6 5 -3 -4 21.3 2.3 -4 -3 4 93.69 4.2 4 -3 -4 91.99 4 4 -3 -4 92.69 3.8 -4 3 4 91.49 4.4 3 -3 -4 94.59 3.7 3 -3 -4 91.79 3.8 -3 -3 4 92.49 4.1 -3 3 4 86.79 4.1 2 -3 -4 245.38 7.9 -2 -3 4 236.28 8 2 -3 -4 243.48 7.2 -2 3 4 232.28 8 1 -3 -4 159.48 5.7 -1 -3 4 158.28 5.8 -1 3 4 156.18 5.9 0 -3 4 15.5 1.9 0 -3 -4 14 1.8 0 3 4 17.9 2.1 1 -3 4 116.79 4.8 -1 -3 -4 122.39 4.9 1 3 4 125.69 4.7 -2 -3 -4 1 0.7 2 -3 4 0.9 0.6 2 -3 4 1.6 1 2 3 4 2.2 0.9 3 -3 4 14.4 1.5 3 -3 4 11.4 1.7 -3 -3 -4 10.2 1.7 3 3 4 15.4 1.9 -4 -3 -4 84.59 4.2 4 -3 4 84.09 3.7 4 -3 4 82.29 4.1 4 3 4 88.49 4.1 5 -3 4 30.9 2.4 5 -3 4 35.3 2.8 -5 -3 -4 33.7 2.6 5 3 4 35.3 2.7 6 -3 4 14.5 2.1 -6 -3 -4 18.1 2.4 6 -3 4 14.2 2.3 6 3 4 13.4 2.1 6 3 4 13.5 1.6 7 -3 4 7.7 1.9 -7 -3 -4 6.2 1.7 7 -3 4 6.6 1.7 7 3 4 6 1.3 7 3 4 5.2 1.6 8 -3 4 18.7 2.9 -8 -3 -4 16.6 2.5 8 -3 4 17.1 2.7 8 3 4 13.9 2 8 3 4 16.1 2.6 -9 -3 -4 11.9 2.1 9 -3 4 7.1 1.9 9 -3 4 13.5 2.7 9 3 4 6.7 1.9 9 3 4 12.7 2.1 10 -3 4 4.8 2.1 10 -3 4 1.1 1.7 10 3 4 4.2 2 11 -3 4 -1.4 1.5 11 -3 4 0.9 1.8 11 3 4 1.1 1.9 12 -3 4 2.5 2.2 12 -3 4 3.4 2 12 3 4 3 2.5 12 -4 -4 0.4 1.9 12 4 -4 0.8 2.1 11 -4 -4 41.6 4.8 11 4 -4 33.9 4.1 10 -4 -4 0.5 1.7 10 4 -4 1.3 1.5 10 4 -4 0.9 1.6 9 -4 -4 -1.2 1.2 9 4 -4 -0.4 0.9 9 4 -4 -0.2 1.2 8 -4 -4 5.3 1.8 8 4 -4 4.6 1.3 7 -4 -4 1.8 1.2 7 4 -4 1.1 1 6 -4 -4 11.8 2 6 -4 -4 10.5 1.5 -6 -4 4 10 1.8 5 -4 -4 2.1 1 5 -4 -4 2.1 0.9 -5 -4 4 3.4 1.1 -5 4 4 2.3 1.1 4 -4 -4 25.5 2.5 4 -4 -4 25.2 2 -4 -4 4 25.3 2.7 -4 4 4 25 2.8 3 -4 -4 3.6 1.1 -3 -4 4 3.4 1.1 3 -4 -4 3.8 0.9 2 -4 -4 16.7 2.1 2 -4 -4 14.2 1.5 -2 -4 4 15.5 2.1 -2 4 4 13.6 1.9 -1 -4 4 239.38 8.3 1 -4 -4 253.67 8.5 -1 4 4 238.08 8.1 0 -4 4 20.3 2.2 0 -4 -4 20.2 2.3 0 4 4 20.2 2.1 -1 -4 -4 2.4 0.9 1 -4 4 1.4 1 1 4 4 2.1 1.1 2 -4 4 8.3 1.7 -2 -4 -4 9 1.7 2 4 4 12.7 1.8 -3 -4 -4 0.4 0.8 3 -4 4 2.2 1.2 3 4 4 2.4 1.1 -4 -4 -4 6 1.5 4 -4 4 9.4 1.9 4 4 4 9.8 1.8 5 -4 4 1.2 1.2 -5 -4 -4 -0.8 0.8 5 4 4 -0.5 0.9 6 -4 4 1.4 1.3 -6 -4 -4 -1 0.9 6 4 4 0.9 1.2 -7 -4 -4 10.1 2.1 7 -4 4 11 2.3 7 4 4 8.5 1.9 8 -4 4 36.1 4 -8 -4 -4 29.6 3.4 8 4 4 29.6 3.3 -9 -4 -4 17.2 2.8 9 -4 4 16.9 2.9 9 4 4 12.6 2.1 -10 -4 -4 0.2 1.2 10 -4 4 -0.5 1.6 10 4 4 1.4 1.7 11 -4 4 0.5 1.7 11 4 4 2.2 2.1 12 -4 4 -0.9 1.9 12 4 4 3.1 2.4 11 -5 -4 -0.3 1.7 10 -5 -4 7.9 2.4 -9 -5 4 7.9 2 9 -5 -4 10.7 2.5 -8 -5 4 10.6 2.2 8 -5 -4 12.7 2.5 7 -5 -4 45.1 3.6 -7 -5 4 47.2 3.6 -7 5 4 49.3 4.9 -6 -5 4 12.2 2.2 6 -5 -4 13.5 2.2 6 -5 -4 10 1.7 -6 5 4 12.3 2.5 -5 -5 4 18.5 2.5 5 -5 -4 21.3 2.4 5 -5 -4 19.1 2.4 -5 5 4 15 2.8 4 -5 -4 0.4 0.8 4 -5 -4 0 0.7 -4 -5 4 0 0.8 -4 5 4 0.1 1 3 -5 -4 13.1 2.1 -3 -5 4 11.1 1.9 3 -5 -4 14 1.8 -3 5 4 13.6 2.2 2 -5 -4 20.4 2.6 2 -5 -4 21.3 2 -2 -5 4 20.7 2.6 -2 5 4 23 2.6 -1 -5 4 10 1.8 1 -5 -4 15.6 2.3 -1 5 4 14.5 2.1 0 -5 -4 12.8 2.1 0 -5 4 12.7 2 0 5 4 13 2 -1 -5 -4 38.6 3.1 1 -5 4 44.7 3.2 1 5 4 46.3 2.9 2 -5 4 11.8 2.1 2 5 4 13.6 2.1 3 -5 4 6.7 1.8 -3 -5 -4 4.5 1.5 3 5 4 2 1.2 -4 -5 -4 7.4 1.9 4 -5 4 8 1.4 4 -5 4 8.6 2 4 5 4 6.7 1.7 -5 -5 -4 25.6 3.3 5 -5 4 29 3.5 5 5 4 31.4 2.8 -6 -5 -4 2.4 1.5 6 -5 4 0.7 1.5 6 5 4 1.3 1.3 7 -5 4 6.2 2.2 -7 -5 -4 4.2 1.9 7 5 4 3.5 1.6 8 -5 4 -1.1 1.5 -8 -5 -4 1.4 1.5 8 5 4 1.8 1.4 9 -5 4 4.6 2.2 -9 -5 -4 -0.7 1.4 9 5 4 4.2 1.6 10 -5 4 4.4 2.1 -10 -5 -4 -0.3 1.5 10 5 4 0 1.6 11 -5 4 1.6 2.3 11 5 4 1.3 2.4 10 -6 -4 -1.2 1.8 -10 6 4 1.5 2.5 9 -6 -4 0.9 1.4 -9 6 4 -0.4 1.9 8 -6 -4 -0.6 1.3 -8 6 4 -0.5 1.9 -7 -6 4 1.8 1.1 7 -6 -4 1.3 1.4 -7 6 4 0.4 1.6 -6 -6 4 1.3 1.1 6 -6 -4 0.6 1.3 -6 6 4 1.6 1.5 5 -6 -4 -1.4 0.9 -5 -6 4 -0.7 0.9 5 -6 -4 -0.9 0.8 -5 6 4 -1.5 1.4 4 -6 -4 14.6 2.2 -4 -6 4 10.8 2.1 4 -6 -4 8.4 1.9 -4 6 4 14.3 2.5 -3 -6 4 1.5 1.2 3 -6 -4 1.2 1.1 -3 6 4 2 1.6 -2 -6 4 20.8 2.7 2 -6 -4 21.9 2.9 -2 6 4 34.6 3.4 -1 -6 4 18.7 2.5 1 -6 -4 25 3.2 -1 6 4 22.3 2.6 0 -6 -4 0.6 1 0 -6 4 -0.7 1 0 6 4 -0.1 1.2 -1 -6 -4 1.6 1.2 1 -6 4 2 1.5 1 6 4 2.3 1.3 2 -6 4 0.7 1.3 -2 -6 -4 -0.5 0.8 2 6 4 0.2 1.2 3 -6 4 2 1.1 3 -6 4 4.7 1.6 -3 -6 -4 2 1.2 -4 -6 -4 5.8 1.9 4 -6 4 5.4 1.8 5 -6 4 0.8 1.4 -5 -6 -4 0.5 1 6 -6 4 27.6 3.8 -6 -6 -4 20.9 3.3 -7 -6 -4 -1.1 1.2 7 -6 4 0.3 1.7 8 -6 4 1 1.9 -8 -6 -4 -0.3 1.5 -9 -6 -4 24.4 4 9 -6 4 21 3.5 4 -7 -4 1.5 1.4 -3 -7 4 16.4 3.8 3 -7 -4 20.5 3.1 -2 -7 4 3.3 1.6 2 -7 -4 0.7 1.2 1 -7 -4 12.2 2.5 -1 -7 4 12 2.4 0 -7 4 0 1.1 0 -7 4 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330.97 9.5 1 0 -5 304.57 9.4 -1 0 5 345.67 9.4 0 0 5 -0.3 0.6 0 0 5 0 0.5 0 0 -5 -0.1 0.4 1 0 5 18.7 1.4 1 0 5 20.7 1.5 -1 0 -5 22.5 1.4 -2 0 -5 -0.3 0.4 2 0 5 0.2 0.6 2 0 5 -0.2 0.6 3 0 5 168.18 5.9 -3 0 -5 162.58 5.2 4 0 5 0 0.7 4 0 5 -0.1 0.7 -4 0 -5 -0.4 0.3 -5 0 -5 48.5 2.1 5 0 5 56.69 3 5 0 5 50.69 3.1 -6 0 -5 0 0.4 6 0 5 -1.3 0.7 6 0 5 0.3 0.8 -7 0 -5 100.59 3.6 7 0 5 103.69 5 7 0 5 103.99 5.2 8 0 5 -1.8 1 8 0 5 -1.8 1.1 9 0 5 25.2 3.1 9 0 5 24.7 3.4 10 0 5 1.3 1.5 10 0 5 1.2 1.6 11 0 5 0.8 1.9 11 0 5 1.1 1.8 12 0 5 2.3 2.1 12 0 5 1.8 2.1 13 0 5 -0.3 2 13 0 5 -4.9 1.8 14 -1 -5 2.4 2.3 14 1 -5 2.9 2.3 13 -1 -5 2.1 1.8 13 1 -5 1.8 2.2 12 -1 -5 2 1.7 12 1 -5 0 1.6 11 -1 -5 6.1 2.1 11 1 -5 7.3 2.3 10 -1 -5 2.5 1.7 10 1 -5 2 1.5 9 -1 -5 121.09 6 9 1 -5 120.89 6 8 -1 -5 2 0.9 8 -1 -5 3.2 1.4 8 1 -5 1.4 1.1 7 -1 -5 58.59 2.8 7 -1 -5 68.99 3.8 7 1 -5 61.99 3.7 7 1 -5 62.29 3.3 6 -1 -5 8.7 1.6 6 1 -5 6.6 1.4 6 1 -5 7.5 1.4 5 -1 -5 22.9 2.2 5 1 -5 21.2 2.2 5 1 -5 21.3 1.8 4 -1 -5 47.4 2.6 4 -1 -5 49.9 2.4 4 1 -5 48.7 2.7 4 1 -5 49.5 2.6 2 -1 -5 184.88 6 2 -1 -5 187.88 5.8 -2 -1 5 187.08 5.7 -1 -1 5 229.98 6.6 -1 -1 5 230.08 7.1 1 -1 -5 229.48 6.5 1 -1 -5 221.78 7 -1 1 5 212.78 7.1 1 1 -5 230.88 7 0 -1 5 56.19 2.2 0 -1 5 54.89 2.5 0 1 -5 57.19 2.4 0 1 5 54.49 2.6 -1 -1 -5 199.58 6.3 1 -1 5 189.48 6.3 1 -1 5 194.88 6 1 1 5 198.58 5.6 -1 1 -5 192.18 5.9 2 -1 5 1.2 0.7 -2 -1 -5 1.7 0.6 2 -1 5 -0.5 0.5 2 1 5 0.8 0.5 2 1 5 1 0.7 -2 1 -5 2.2 0.5 3 -1 5 28.1 2.1 3 -1 5 31.1 2 -3 -1 -5 28.8 1.8 3 1 5 27.7 2.1 -3 1 -5 29.5 1.4 3 1 5 31.6 1.7 4 -1 5 14.3 1.8 -4 -1 -5 13.5 1.5 4 -1 5 15.1 1.8 -4 1 -5 14.4 0.9 4 1 5 10.7 1.6 5 -1 5 3.6 1.2 5 -1 5 6.3 1.4 -5 -1 -5 3.7 0.9 5 1 5 4.5 1.1 5 1 5 4.3 1.1 6 -1 5 0.9 0.9 -6 -1 -5 0.8 0.6 6 -1 5 1.6 1.1 6 1 5 -0.5 0.7 6 1 5 -0.9 0.8 -7 -1 -5 0.3 0.6 7 -1 5 -0.5 0.9 7 -1 5 1.5 1.2 7 1 5 1.7 1.1 7 1 5 1.3 1 8 -1 5 0.6 1.3 8 -1 5 1.5 1.7 8 1 5 4.1 1.7 8 1 5 2 1.3 9 -1 5 11.5 2.3 9 -1 5 13.1 2.8 9 1 5 11.5 2.6 9 1 5 6.6 1.9 10 -1 5 -0.6 1.5 10 -1 5 0.4 1.9 10 1 5 0.4 1.7 10 1 5 1.9 1.5 11 -1 5 1.5 2 11 -1 5 0.6 1.6 11 1 5 2.3 2 11 1 5 -0.5 1.5 12 -1 5 -1.1 1.6 12 -1 5 -1.9 2 12 1 5 -0.9 1.6 12 1 5 -0.2 2.2 13 -1 5 1.2 2.5 13 -1 5 -2.7 1.7 13 1 5 -0.4 2.2 13 1 5 2.1 2.3 14 -2 -5 3 2.3 14 2 -5 -0.1 2.1 13 -2 -5 1.4 2 13 2 -5 3.3 2.4 12 -2 -5 2.2 1.8 12 2 -5 -1.1 1.7 11 -2 -5 1.8 1.7 11 2 -5 1.5 1.9 10 -2 -5 55.39 4.5 10 2 -5 64.49 4.6 9 -2 -5 5 1.8 9 2 -5 4.6 1.8 8 -2 -5 5 1 8 -2 -5 3 1.3 8 2 -5 4.6 1.5 7 -2 -5 2.8 1.2 7 -2 -5 0.5 0.6 7 2 -5 0.8 1 6 -2 -5 3.5 1.2 6 -2 -5 1.5 0.7 6 2 -5 2 1.1 5 -2 -5 31.7 2.4 5 2 -5 32.2 2.4 5 2 -5 27.4 2.6 4 -2 -5 15.6 1.7 4 2 -5 16.7 2 3 -2 -5 95.39 3.7 -3 -2 5 96.69 4.1 -3 2 5 99.89 4.2 3 2 -5 94.39 4 2 -2 -5 48.9 2.4 1 -2 -5 288.27 9.4 -1 -2 5 321.87 9.6 1 2 -5 322.37 9.5 0 -2 -5 78.89 3.6 0 2 -5 102.09 3.6 -1 -2 -5 6.5 1.1 1 -2 5 7.2 0.9 1 2 5 6 1.2 -1 2 -5 9.2 1.1 -2 -2 -5 24.2 1.8 2 -2 5 21.2 1.5 2 -2 5 18.9 2 -2 2 -5 20.1 1.3 2 2 5 22.2 2.2 -3 -2 -5 41.3 2.5 3 -2 5 38.3 2.2 3 -2 5 42.8 2.7 3 2 5 42.8 2.6 -3 2 -5 38.5 1.8 -4 -2 -5 64.59 3.3 4 -2 5 66.39 3.5 4 -2 5 71.19 3.4 4 2 5 66.79 2.8 4 2 5 69.09 3.6 -4 2 -5 71.59 2.5 5 -2 5 3.6 1.2 -5 -2 -5 1 0.8 5 -2 5 3.2 1.1 5 2 5 4.2 1.3 5 2 5 1.5 0.7 6 -2 5 16.2 2.2 -6 -2 -5 16.4 2 6 2 5 17 1.8 6 2 5 19.7 2.6 7 -2 5 39 3.2 -7 -2 -5 42.6 2.8 7 -2 5 38.5 3.3 7 2 5 45 2.9 7 2 5 41.2 3.4 8 -2 5 9.7 2.3 -8 -2 -5 11.5 1.8 8 -2 5 12.7 2.3 8 2 5 12.7 2.1 8 2 5 9.7 2.3 9 -2 5 2 1.6 9 -2 5 5.4 2.2 9 2 5 4.2 1.6 9 2 5 3.4 1.7 10 -2 5 2.7 2.2 10 -2 5 1 1.7 10 2 5 2.5 2 10 2 5 -0.4 1.3 11 -2 5 -2.1 1.4 11 -2 5 -0.8 2 11 2 5 -1.6 1.3 11 2 5 2.9 2.2 12 -2 5 2.7 2.2 12 -2 5 3.7 2.6 12 2 5 0.9 2.4 12 2 5 0.8 2.2 13 -3 -5 0.2 1.8 13 3 -5 3.5 2.3 12 -3 -5 3.2 2.1 12 3 -5 5.2 2.4 11 -3 -5 0.5 1.5 11 3 -5 1.7 1.8 10 -3 -5 1.6 1.8 10 3 -5 6.1 2.1 9 -3 -5 12.6 2.5 9 3 -5 12.7 2.5 8 -3 -5 34.7 3.7 8 3 -5 36.8 3.6 7 -3 -5 24.7 1.8 7 3 -5 34.2 3.4 6 -3 -5 20.5 1.7 6 -3 -5 19.6 2.5 6 3 -5 25.2 2.7 5 -3 -5 0.7 0.8 5 -3 -5 -0.2 0.5 -4 -3 5 18.5 2.2 4 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6.3 3 12 -4 -5 10.3 2.8 12 4 -5 10.2 2.7 11 -4 -5 2.1 2 11 4 -5 1.8 1.9 10 -4 -5 28 3.8 10 4 -5 25.6 3.5 9 -4 -5 1.9 1.5 8 -4 -5 20.4 3 7 -4 -5 2.8 1.4 7 -4 -5 4.2 1.4 -6 -4 5 1.1 1.1 6 -4 -5 0.8 0.8 6 -4 -5 -0.7 0.8 -6 4 5 -0.4 1.1 5 -4 -5 2.9 1.1 -5 -4 5 2.2 1.1 5 -4 -5 3 1 -5 4 5 3.5 1.4 -4 -4 5 0.6 1 4 -4 -5 1.8 0.9 4 -4 -5 1.6 0.8 -4 4 5 0.3 1 3 -4 -5 22 1.7 3 -4 -5 24.9 2.5 -3 -4 5 23.6 2.6 -3 4 5 23.1 2.6 2 -4 -5 119.79 4.1 2 -4 -5 108.79 4.9 -2 -4 5 112.59 5 -2 4 5 113.29 5 -1 -4 5 0.3 0.8 1 -4 -5 0.8 0.8 -1 4 5 1.7 1 0 -4 -5 11.7 1.8 0 -4 5 7.2 1.5 0 4 5 11.5 1.8 1 -4 5 8.9 1.7 1 4 5 8.6 1.6 2 -4 5 4.5 1.5 -2 -4 -5 1.4 0.9 2 4 5 4.8 1.3 -3 -4 -5 23.1 2.7 3 -4 5 24 2.8 3 4 5 27.4 2.8 4 -4 5 5.7 1.6 4 -4 5 7.3 1.3 -4 -4 -5 5.5 1.5 4 4 5 7 1.6 5 -4 5 6.4 1.8 5 -4 5 9.7 1.6 -5 -4 -5 7 1.8 5 4 5 4.3 1.5 6 -4 5 86.69 4.4 6 -4 5 89.09 5.1 -6 -4 -5 86.29 5 6 4 5 92.49 4.9 -7 -4 -5 36.4 3.9 7 -4 5 40.6 3.2 7 -4 5 40.5 4.2 7 4 5 34.8 3.7 8 -4 5 61.79 4.7 8 -4 5 72.59 4.5 -8 -4 -5 62.09 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6 1 -6 138.79 5.5 5 -1 -6 60.49 3.2 5 -1 -6 56.79 2.8 5 1 -6 54.49 3.1 5 1 -6 56.69 3 4 -1 -6 152.28 5.7 4 -1 -6 158.28 5.6 4 1 -6 161.78 5.9 4 1 -6 167.18 5.8 3 -1 -6 14.9 1.5 -3 -1 6 14.8 1.5 3 1 -6 15.4 1.6 -2 -1 6 10.3 1.3 1 -1 6 2.5 0.8 1 -1 6 -0.7 0.5 -1 -1 -6 1.4 0.6 1 1 6 1.6 0.6 1 1 6 -0.6 0.5 -1 1 -6 3.2 0.8 2 -1 6 16 1.7 2 -1 6 15.1 1.6 -2 -1 -6 10.6 1.3 2 1 6 14.1 1.2 -2 1 -6 15.5 1.2 2 1 6 16.8 1.9 -3 -1 -6 2.1 0.8 3 -1 6 2.1 0.9 3 -1 6 2.1 0.9 3 1 6 2 0.7 -3 1 -6 3.1 0.6 3 1 6 1.5 0.9 -4 -1 -6 246.88 7.9 4 -1 6 242.38 8.2 4 -1 6 248.68 8.4 -4 1 -6 241.08 7.1 4 1 6 245.68 8.5 -5 -1 -6 -0.8 0.5 5 -1 6 1 1 5 -1 6 1.4 0.9 5 1 6 -0.4 0.7 5 1 6 0.5 0.8 -5 1 -6 0 0.3 6 -1 6 1.3 1.2 -6 -1 -6 2 0.8 6 -1 6 1.2 0.9 6 1 6 1.1 1 6 1 6 0.5 0.8 7 -1 6 4.6 1.8 7 -1 6 4.1 1.5 -7 -1 -6 4.5 1.1 7 1 6 0 1 7 1 6 5.7 1.4 8 -1 6 -0.3 1.2 8 -1 6 0.5 1.2 8 1 6 -0.6 1 8 1 6 0.1 1.2 9 -1 6 1.2 1.5 9 -1 6 -0.8 1.5 9 1 6 -0.4 1.4 9 1 6 1.6 1.3 10 -1 6 3.4 2 10 -1 6 -0.7 1.5 10 1 6 2 1.7 10 1 6 -0.6 1.4 11 -1 6 -1.4 1.4 11 -1 6 -0.7 2.1 11 1 6 -1.9 1.3 11 1 6 2.6 2.1 12 -1 6 -2.4 2 12 -1 6 -1.6 1.6 12 1 6 -0.6 1.8 12 1 6 2 2.4 13 -1 6 -0.3 2 13 -1 6 2.4 2.7 13 1 6 -0.9 2 13 1 6 1.9 2.4 14 -2 -6 0.8 2.1 14 2 -6 2.2 2.3 13 -2 -6 0.5 1.9 13 2 -6 -1.6 2 12 -2 -6 6.9 2.4 12 2 -6 8.6 2.6 11 -2 -6 0.5 1.6 11 2 -6 0.1 1.6 10 -2 -6 181.38 8.4 10 2 -6 188.18 8.5 9 -2 -6 2 1.4 9 2 -6 2.8 1.6 8 -2 -6 16.3 2.5 8 -2 -6 14.8 1.8 8 2 -6 18.7 2.7 7 -2 -6 13.1 1.6 7 -2 -6 13.7 2.2 7 2 -6 15.1 2.4 6 -2 -6 97.29 4.1 6 -2 -6 103.39 4.7 6 2 -6 101.59 4.9 6 2 -6 100.69 4.7 5 -2 -6 5.3 1 5 -2 -6 4.3 1.1 5 2 -6 2.8 1.1 5 2 -6 5.5 1.4 4 -2 -6 68.69 3.2 4 -2 -6 66.29 3.1 -4 2 6 64.89 3.6 4 2 -6 70.59 3.5 -3 -2 6 27 2.2 3 -2 -6 33.7 2.1 3 -2 -6 30.7 1.8 -3 -2 6 29.7 1.7 -3 2 6 29.7 2.5 3 2 -6 29.7 2.1 2 -2 -6 192.88 5.7 2 -2 -6 196.88 6.4 -2 -2 6 193.88 6.6 -2 2 6 179.18 6.5 2 2 -6 163.08 6.3 1 -2 -6 39.2 2.3 1 2 -6 41.8 2.3 -1 2 6 42.1 2.5 0 -2 -6 78.89 3.5 0 2 6 83.19 3.6 0 2 -6 76.79 3.3 -1 -2 -6 71.89 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11.7 2.5 8 -3 -6 41.8 3.5 8 3 -6 47.8 3.7 7 -3 -6 0.8 0.8 7 -3 -6 1 1.2 7 3 -6 1 1.2 6 -3 -6 37.3 2.8 6 -3 -6 36.5 2.4 5 -3 -6 77.69 3.9 -5 -3 6 87.99 4.4 5 -3 -6 73.79 3.6 -5 3 6 84.89 4.5 4 -3 -6 0.6 0.6 4 -3 -6 0.9 0.7 -4 -3 6 2.4 1 -4 3 6 -0.3 1 3 -3 -6 29.1 1.9 -3 -3 6 28.3 2.4 3 -3 -6 31.8 2.2 -3 3 6 34.4 2.6 2 -3 -6 23.6 2 -2 -3 6 25.2 2.5 2 -3 -6 24.3 1.4 2 3 -6 25.8 2.5 -2 3 6 28.1 2.7 1 -3 -6 8.5 1.4 -1 -3 6 8.8 1.6 -1 3 6 7.5 1.6 1 3 -6 8.5 1.5 0 -3 6 80.49 4 0 -3 -6 86.79 4 0 3 6 73.49 3.7 0 3 -6 78.19 3.6 -1 -3 -6 3.5 1 1 -3 6 3.7 1.3 1 3 6 5.5 1.4 -1 3 -6 6.9 1.2 -2 -3 -6 -0.1 0.6 2 -3 6 0.2 0.9 2 -3 6 0.6 0.5 2 3 6 0.8 0.9 3 -3 6 0.4 0.6 -3 -3 -6 0.4 0.8 3 -3 6 0.5 0.9 3 3 6 0.4 0.9 4 -3 6 35.1 2.8 4 -3 6 33.8 2.4 -4 -3 -6 34.2 2.7 4 3 6 37 2.9 -5 -3 -6 9.6 1.8 5 -3 6 9.4 1.7 5 3 6 12.3 2.1 -6 -3 -6 1.1 1.1 6 -3 6 0.6 1.1 6 -3 6 1.6 1.2 6 3 6 0.6 0.8 6 3 6 0.9 1.3 -7 -3 -6 17.1 2.5 7 -3 6 17.9 2.8 7 -3 6 19.5 2.7 7 3 6 18.1 2.3 7 3 6 17.1 2.8 8 -3 6 9.4 2.3 -8 -3 -6 8.2 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1.4 2.1 12 0 -7 0 1.5 11 0 -7 2.7 1.6 10 0 -7 1.6 1.3 10 0 -7 -1.5 1.1 9 0 -7 9.2 2.1 9 0 -7 9.2 1.8 8 0 -7 0.5 0.8 8 0 -7 -0.4 1 7 0 -7 82.09 3.9 7 0 -7 77.59 4.3 6 0 -7 0.2 0.7 6 0 -7 -1 0.6 5 0 -7 4.7 1.2 5 0 -7 4.8 1.1 -4 0 7 -0.4 0.8 4 0 -7 0.3 0.8 4 0 -7 -0.3 0.6 3 0 -7 142.69 5.3 3 0 -7 150.58 5.3 -3 0 7 144.09 5.3 -2 0 7 -0.4 0.7 -2 0 7 0.4 0.5 2 0 -7 -0.6 0.4 -1 0 7 5.2 1 -1 0 7 5.1 1.1 0 0 7 0.2 0.8 0 0 -7 -0.4 0.5 0 0 7 -1.3 0.5 -1 0 -7 246.28 7.7 1 0 7 252.57 7.9 1 0 7 241.88 7.6 2 0 7 -0.5 0.6 2 0 7 -0.2 0.7 -2 0 -7 -0.1 0.5 3 0 7 41.9 2.5 -3 0 -7 44.2 2.2 3 0 7 41.7 2.7 4 0 7 -0.1 0.9 -4 0 -7 0 0.4 4 0 7 -0.3 0.7 5 0 7 81.79 4 5 0 7 83.79 4.3 -5 0 -7 81.99 3.3 6 0 7 -0.7 0.8 6 0 7 -0.5 1 -6 0 -7 -0.5 0.4 7 0 7 13.2 2.4 7 0 7 11.6 2 8 0 7 2.6 1.6 8 0 7 1.3 1.2 9 0 7 65.59 5 9 0 7 63.49 4.4 10 0 7 -1.7 1.5 10 0 7 2 1.7 11 0 7 4.8 2 11 0 7 2.7 2.3 12 0 7 -1.4 2.2 12 0 7 1 2 14 -1 -7 0.8 2.1 14 1 -7 -1.3 2 13 -1 -7 4.6 2.1 13 1 -7 4.3 2.4 12 -1 -7 1 1.8 12 1 -7 0.6 1.7 11 -1 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41.9 2.5 4 -1 7 43.9 2.9 4 1 7 49.3 2.5 -4 1 -7 45.2 2.1 5 -1 7 1.6 1.1 5 -1 7 2.7 1.2 -5 -1 -7 2.8 0.8 -5 1 -7 1.4 0.5 5 1 7 4 1.1 5 1 7 -0.1 0.6 -6 -1 -7 3.4 1 6 -1 7 4.5 1.4 6 -1 7 2.6 1.4 6 1 7 -0.2 0.7 6 1 7 6.4 1.5 7 -1 7 32.3 3.5 -7 -1 -7 29.7 2.2 7 -1 7 28.9 3.1 7 1 7 28.8 2.8 7 1 7 30 3.5 8 -1 7 0.7 1.3 8 -1 7 1.3 1.6 8 1 7 1.3 1.2 8 1 7 0.3 1.3 9 -1 7 3 1.7 9 -1 7 8.9 2.5 9 1 7 10.7 2.5 9 1 7 3.8 1.7 10 -1 7 2.6 2.2 10 -1 7 2.5 1.7 10 1 7 -0.7 1.4 10 1 7 3.7 2.2 11 -1 7 -1.4 2 11 -1 7 3.5 1.8 11 1 7 1.7 2.1 11 1 7 -1.2 1.7 12 -1 7 0.1 2.2 12 -1 7 2.7 2.1 12 1 7 1.6 2 12 1 7 -0.4 2.1 13 -2 -7 2.5 2.4 13 2 -7 6 2.7 12 -2 -7 4.2 2.1 12 2 -7 7.3 2.6 11 -2 -7 11 2.7 11 2 -7 12.5 2.7 10 -2 -7 43.5 4.5 10 2 -7 51.99 4.3 9 -2 -7 18.1 2.9 9 2 -7 21.2 3 8 -2 -7 4.8 1.2 8 -2 -7 5.3 1.6 8 2 -7 4.1 1.5 7 -2 -7 64.09 3.8 7 -2 -7 62.59 3.1 7 2 -7 52.69 3.7 7 2 -7 56.19 3.6 6 -2 -7 25.5 2.6 6 -2 -7 20.8 2.2 6 2 -7 22.4 2.7 6 2 -7 17.9 2.3 5 -2 -7 1.6 0.9 5 -2 -7 1.7 0.7 5 2 -7 1.1 0.8 -5 2 7 1.6 1 -4 -2 7 2.6 1.1 4 -2 -7 2.8 1 4 -2 -7 2.1 0.9 4 2 -7 2 0.9 -4 2 7 1.1 1.1 -3 -2 7 28.7 2.3 -3 -2 7 32.2 1.8 3 -2 -7 32.1 1.9 3 -2 -7 28.6 2.1 -3 2 7 29.7 2.4 3 2 -7 25.8 2 -2 -2 7 8.5 1.4 2 -2 -7 11.4 1.5 2 -2 -7 9.6 1.1 2 2 -7 13 1.7 -2 2 7 6.1 1.8 1 -2 -7 38.9 2.4 -1 2 7 35.1 2.9 1 2 -7 36.7 2.3 0 -2 7 37.8 1.9 0 -2 7 38.4 2.7 0 2 -7 38.2 2.3 0 2 7 45.9 3.1 -1 -2 -7 65.59 3.4 1 -2 7 69.59 2.9 1 -2 7 71.69 3.6 1 2 7 72.69 3.6 -1 2 -7 75.89 3.2 2 -2 7 6 1.1 -2 -2 -7 4.7 1.2 2 -2 7 5.7 1.4 2 2 7 3.9 1.3 -2 2 -7 6.4 1.1 -3 -2 -7 76.89 3.7 3 -2 7 72.39 3.5 3 -2 7 75.49 3.9 3 2 7 68.19 3.8 -3 2 -7 72.39 3 -4 -2 -7 20.1 2.3 4 -2 7 19.7 2.4 4 -2 7 19.7 2.2 4 2 7 19.4 1.4 -4 2 -7 17.5 1.3 4 2 7 25.3 2.7 5 -2 7 114.29 5.1 5 -2 7 112.19 5.3 -5 -2 -7 116.69 5 -5 2 -7 113.79 3.8 5 2 7 101.89 4.2 5 2 7 113.19 5.4 6 -2 7 12.7 2.2 6 -2 7 12.5 2.2 -6 -2 -7 8.9 1.6 6 2 7 13 1.7 6 2 7 10.8 2 -7 -2 -7 39.2 2.8 7 -2 7 47 3.7 7 -2 7 39.1 3.4 7 2 7 41.4 3.6 7 2 7 36.6 2.8 8 -2 7 3.5 1.6 -8 -2 -7 5 1.4 8 -2 7 3.6 1.8 8 2 7 3.3 1.8 8 2 7 3.7 1.5 9 -2 7 20.8 3.2 9 -2 7 24.1 3.6 9 2 7 24 3.7 9 2 7 24.7 3 10 -2 7 0.8 1.7 10 -2 7 0.6 2.2 10 2 7 -1 1.6 10 2 7 1.5 2.2 11 -2 7 1.2 2.4 11 -2 7 1 1.9 11 2 7 0.8 2 12 -2 7 3.4 2.8 12 -2 7 -1.1 1.8 12 2 7 2.9 2.5 13 -3 -7 -1.8 1.6 13 3 -7 1.1 2.2 12 -3 -7 0.1 1.7 12 3 -7 -2.8 1.8 11 -3 -7 14.5 3 11 3 -7 18.4 3.3 10 -3 -7 1.3 1.5 10 3 -7 -0.2 1.6 9 -3 -7 -0.3 1.2 9 3 -7 2 1.6 8 -3 -7 15.9 2.6 8 -3 -7 14.4 1.9 8 3 -7 13.5 2.5 7 -3 -7 1.1 0.8 7 -3 -7 1.1 1.2 6 -3 -7 25.7 2.1 6 -3 -7 24 2.6 -6 3 7 28.3 3.3 5 -3 -7 80.99 3.8 5 -3 -7 74.39 3.8 -5 -3 7 72.09 4.2 -5 3 7 83.79 4.5 4 -3 -7 17.6 1.9 4 -3 -7 15.2 1.9 -4 -3 7 12.9 2 -4 3 7 13 2.1 3 -3 -7 47.6 2.9 3 -3 -7 50.59 2.5 -3 -3 7 51.79 3.2 3 3 -7 54.49 3.2 -3 3 7 51.49 3.3 -2 -3 7 14 2 2 -3 -7 12.5 1.8 2 3 -7 11.9 1.8 -2 3 7 11.1 1.8 1 -3 -7 137.59 5.5 -1 -3 7 130.19 5.5 1 3 -7 131.19 5.3 -1 3 7 132.49 5.5 0 -3 -7 34.3 2.5 0 -3 7 35.7 2.7 0 3 -7 36.5 2.4 0 3 7 34.6 2.6 1 -3 7 26.1 2.7 -1 -3 -7 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