Crystallography Open Database

Information card for entry 1557456

Preview

Coordinates	1557456.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H88 Ag2 Li4 N6 O2
Calculated formula	C46 H88 Ag2 Li4 N6 O2
Title of publication	Lipshutz-type bis(amido)argentates for directed ortho argentation
Authors of publication	Tezuka, Noriyuki; Hirano, Keiichi; Peel, Andrew J.; Wheatley, Andrew E. H.; Miyamoto, Kazunori; Uchiyama, Masanobu
Journal of publication	Chemical Science
Year of publication	2020
Journal volume	11
Journal issue	7
Pages of publication	1855 - 1861
a	8.3861 ± 0.0003 Å
b	11.5994 ± 0.0004 Å
c	14.05 ± 0.0005 Å
α	86.881 ± 0.002°
β	79.282 ± 0.002°
γ	83.876 ± 0.002°
Cell volume	1334.35 ± 0.08 Å³
Cell temperature	180 ± 2 K
Ambient diffraction temperature	180 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.033
Residual factor for significantly intense reflections	0.0272
Weighted residual factors for significantly intense reflections	0.0633
Weighted residual factors for all reflections included in the refinement	0.0673
Goodness-of-fit parameter for all reflections included in the refinement	1.077
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
257366 (current)	2020-10-06	cif/ Updating files of 1557456, 1557457, 1557458, 1557459 Original log message: Adding full bibliography for 1557456--1557459.cif.	1557456.cif
248753	2020-03-04	cif/ Adding structures of 1557456, 1557457, 1557458, 1557459 via cif-deposit CGI script.	1557456.cif