Crystallography Open Database

Information card for entry 1557457

Preview

Coordinates	1557457.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H72 Ag2 Li2 N4
Calculated formula	C36 H72 Ag2 Li2 N4
Title of publication	Lipshutz-type bis(amido)argentates for directed ortho argentation
Authors of publication	Tezuka, Noriyuki; Hirano, Keiichi; Peel, Andrew J.; Wheatley, Andrew E. H.; Miyamoto, Kazunori; Uchiyama, Masanobu
Journal of publication	Chemical Science
Year of publication	2020
Journal volume	11
Journal issue	7
Pages of publication	1855 - 1861
a	22.1326 ± 0.0005 Å
b	8.3936 ± 0.0002 Å
c	22.8868 ± 0.0006 Å
α	90°
β	109.561 ± 0.001°
γ	90°
Cell volume	4006.34 ± 0.17 Å³
Cell temperature	180 ± 2 K
Ambient diffraction temperature	180 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0345
Residual factor for significantly intense reflections	0.0257
Weighted residual factors for significantly intense reflections	0.0517
Weighted residual factors for all reflections included in the refinement	0.0537
Goodness-of-fit parameter for all reflections included in the refinement	1.128
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
257366 (current)	2020-10-06	cif/ Updating files of 1557456, 1557457, 1557458, 1557459 Original log message: Adding full bibliography for 1557456--1557459.cif.	1557457.cif
248753	2020-03-04	cif/ Adding structures of 1557456, 1557457, 1557458, 1557459 via cif-deposit CGI script.	1557457.cif