Crystallography Open Database

Information card for entry 1571929

1571928 << 1571929 >> 1571930

Preview

Coordinates	1571929.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H99 Mo10 N5 O36 Th
Calculated formula	C42 H99 Mo10 N5 O36 Th
Title of publication	Leveraging a reduced polyoxomolybdate-alkoxide cluster for the formation of a stable U(v) sandwich complex.
Authors of publication	Shiels, Dominic; Brennessel, William W.; Crawley, Matthew R.; Matson, Ellen M.
Journal of publication	Chemical science
Year of publication	2024
Journal volume	15
Journal issue	28
Pages of publication	11072 - 11083
a	12.8161 ± 0.0002 Å
b	15.4649 ± 0.0002 Å
c	19.9194 ± 0.0003 Å
α	87.176 ± 0.001°
β	84.075 ± 0.001°
γ	73.714 ± 0.001°
Cell volume	3768.5 ± 0.1 Å³
Cell temperature	100.01 ± 0.16 K
Ambient diffraction temperature	100.01 ± 0.16 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0372
Residual factor for significantly intense reflections	0.0252
Weighted residual factors for significantly intense reflections	0.0507
Weighted residual factors for all reflections included in the refinement	0.053
Goodness-of-fit parameter for all reflections included in the refinement	1.04
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.56087 Å
Diffraction radiation type	AgKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
293747 (current)	2024-08-05	cif/ Updating files of 1571928, 1571929, 1571930, 1571931, 1571932 Original log message: Adding full bibliography for 1571928--1571932.cif.	1571929.cif
292434	2024-06-18	cif/ Adding structures of 1571928, 1571929, 1571930, 1571931, 1571932 via cif-deposit CGI script.	1571929.cif