Crystallography Open Database

Information card for entry 1571930

1571929 << 1571930 >> 1571931

Preview

Coordinates	1571930.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26.61 H65.22 Cl5.22 Mo10 N3 O36 U
Calculated formula	C26.609 H65.218 Cl5.218 Mo10 N3 O36 U
Title of publication	Leveraging a reduced polyoxomolybdate-alkoxide cluster for the formation of a stable U(v) sandwich complex.
Authors of publication	Shiels, Dominic; Brennessel, William W.; Crawley, Matthew R.; Matson, Ellen M.
Journal of publication	Chemical science
Year of publication	2024
Journal volume	15
Journal issue	28
Pages of publication	11072 - 11083
a	16.31 ± 0.0001 Å
b	21.2206 ± 0.0001 Å
c	18.9017 ± 0.0001 Å
α	90°
β	103.313 ± 0.001°
γ	90°
Cell volume	6366.22 ± 0.07 Å³
Cell temperature	100 ± 0.1 K
Ambient diffraction temperature	100 ± 0.1 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0404
Residual factor for significantly intense reflections	0.0389
Weighted residual factors for significantly intense reflections	0.1028
Weighted residual factors for all reflections included in the refinement	0.1038
Goodness-of-fit parameter for all reflections included in the refinement	1.093
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
293747 (current)	2024-08-05	cif/ Updating files of 1571928, 1571929, 1571930, 1571931, 1571932 Original log message: Adding full bibliography for 1571928--1571932.cif.	1571930.cif
292434	2024-06-18	cif/ Adding structures of 1571928, 1571929, 1571930, 1571931, 1571932 via cif-deposit CGI script.	1571930.cif