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Information card for entry 7032847
Preview
| Coordinates | 7032847.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C20 H16 N12 O8 Pb2 |
|---|---|
| Calculated formula | C20 H16 N12 O8 Pb2 |
| SMILES | c1([n]2ccnc1N)C(=O)[O]1[Pb]23([n]4c(c(ncc4)N)C(=O)O3)[O]2C(=O)c3c(ncc[n]3[Pb]312[n]1c(C(=O)O3)c(ncc1)N)N |
| Title of publication | Synthesis, structure and catalytic application of lead(II) complexes in cyanosilylation reactions. |
| Authors of publication | Karmakar, Anirban; Hazra, Susanta; Guedes da Silva, M Fátima C; Pombeiro, Armando J. L. |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2015 |
| Journal volume | 44 |
| Journal issue | 1 |
| Pages of publication | 268 - 280 |
| a | 7.752 ± 0.0003 Å |
| b | 7.8081 ± 0.0003 Å |
| c | 11.2756 ± 0.0005 Å |
| α | 85.184 ± 0.002° |
| β | 86.853 ± 0.002° |
| γ | 67.114 ± 0.001° |
| Cell volume | 626.36 ± 0.04 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.022 |
| Residual factor for significantly intense reflections | 0.0214 |
| Weighted residual factors for significantly intense reflections | 0.054 |
| Weighted residual factors for all reflections included in the refinement | 0.0544 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.166 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 180034 (current) | 2016-03-25 | cif/7/03/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/03/28. |
7032847.cif |
| 131065 | 2015-02-04 | cif/ Updating files of 7032845, 7032846, 7032847, 7032848, 7032849, 7032850 Original log message: Adding full bibliography for 7032845--7032850.cif. |
7032847.cif |
| 125575 | 2014-10-21 | cif/ Adding structures of 7032845, 7032846, 7032847, 7032848, 7032849, 7032850 via cif-deposit CGI script. |
7032847.cif |
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Users of the data should acknowledge the original authors of the
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