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Information card for entry 7046003
Preview
| Coordinates | 7046003.cif |
|---|---|
| Original paper (by DOI) | HTML |
| External links | PubChem |
| Formula | C30 H72 Mg N2 Si4 |
|---|---|
| Calculated formula | C30 H72 Mg N2 Si4 |
| Title of publication | Salt metathesis routes to homoleptic near-linear Mg(ii) and Ca(ii) bulky bis(silyl)amide complexes. |
| Authors of publication | Leng, Ji-Dong; Goodwin, Conrad A. P.; Vitorica-Yrezabal, Iñigo J; Mills, David P. |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2018 |
| Journal volume | 47 |
| Journal issue | 36 |
| Pages of publication | 12526 - 12533 |
| a | 12.0018 ± 0.0005 Å |
| b | 17.341 ± 0.0007 Å |
| c | 20.7079 ± 0.0008 Å |
| α | 68.97 ± 0.004° |
| β | 80.84 ± 0.003° |
| γ | 73.015 ± 0.004° |
| Cell volume | 3840.1 ± 0.3 Å3 |
| Cell temperature | 150.01 ± 0.1 K |
| Ambient diffraction temperature | 150.01 ± 0.1 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0764 |
| Residual factor for significantly intense reflections | 0.0509 |
| Weighted residual factors for significantly intense reflections | 0.107 |
| Weighted residual factors for all reflections included in the refinement | 0.1226 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.026 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 301850 (current) | 2025-08-21 | Add cross-references to PubChem compounds in COD range 7/04/ Each referenced PubChem compound corresponds to the full crystal structure. |
7046003.cif |
| 229921 | 2019-11-17 | cif/ Updating files of 7045998, 7045999, 7046000, 7046001, 7046002, 7046003 Original log message: Adding full bibliography for 7045998--7046003.cif. |
7046003.cif |
| 207286 | 2018-04-11 | cif/ Adding structures of 7045998, 7045999, 7046000, 7046001, 7046002, 7046003 via cif-deposit CGI script. |
7046003.cif |
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Users of the data should acknowledge the original authors of the
structural data.