Crystallography Open Database

Information card for entry 7046004

Preview

Coordinates	7046004.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Glutaramidinium decavanadate
Chemical name	tris(1,5-diaminopentane-1,5-diiminium) decavanadate
Formula	C30 H106 N24 O67 V20
Calculated formula	C30 H84 N24 O67 V20
Title of publication	Interactions of vanadium(iv) with amidoxime ligands: redox reactivity.
Authors of publication	Parker, B. F.; Hohloch, S.; Pankhurst, J. R.; Zhang, Z.; Love, J. B.; Arnold, J.; Rao, L.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	16
Pages of publication	5695 - 5702
a	18.6232 ± 0.0016 Å
b	37.606 ± 0.003 Å
c	13.3441 ± 0.0011 Å
α	90°
β	90°
γ	90°
Cell volume	9345.5 ± 1.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	33
Hermann-Mauguin space group symbol	P n a 21
Hall space group symbol	P 2c -2n
Residual factor for all reflections	0.0427
Residual factor for significantly intense reflections	0.039
Weighted residual factors for significantly intense reflections	0.0952
Weighted residual factors for all reflections included in the refinement	0.0974
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
229619 (current)	2019-11-17	cif/ Updating files of 7046004 Original log message: Adding full bibliography for 7046004.cif.	7046004.cif
207287	2018-04-11	cif/ Adding structures of 7046004 via cif-deposit CGI script.	7046004.cif