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Information card for entry 7048319
Preview
Coordinates | 7048319.cif |
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Original paper (by DOI) | HTML |
Formula | C19 H15 Cl5 O W |
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Calculated formula | C19 H15 Cl5 O W |
Title of publication | Straightforward formation of carbocations from tertiary carboxylic acids via CO release at room temperature. |
Authors of publication | Bartalucci, Niccolò; Bortoluzzi, Marco; Zacchini, Stefano; Pampaloni, Guido; Marchetti, Fabio |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2019 |
Journal volume | 48 |
Journal issue | 5 |
Pages of publication | 1574 - 1577 |
a | 14.275 ± 0.002 Å |
b | 7.9205 ± 0.0011 Å |
c | 18.698 ± 0.003 Å |
α | 90° |
β | 103.08 ± 0.002° |
γ | 90° |
Cell volume | 2059.2 ± 0.5 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0441 |
Residual factor for significantly intense reflections | 0.0374 |
Weighted residual factors for significantly intense reflections | 0.0845 |
Weighted residual factors for all reflections included in the refinement | 0.0875 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.076 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
224003 (current) | 2019-11-07 | cif/ Updating files of 7048319, 7048320 Original log message: Adding full bibliography for 7048319--7048320.cif. |
7048319.cif |
212483 | 2018-12-08 | cif/ Adding structures of 7048319, 7048320 via cif-deposit CGI script. |
7048319.cif |
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Users of the data should acknowledge the original authors of the
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