Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7048320
Preview
Coordinates | 7048320.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H24 |
---|---|
Calculated formula | C28 H24 |
Title of publication | Straightforward formation of carbocations from tertiary carboxylic acids via CO release at room temperature. |
Authors of publication | Bartalucci, Niccolò; Bortoluzzi, Marco; Zacchini, Stefano; Pampaloni, Guido; Marchetti, Fabio |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2019 |
Journal volume | 48 |
Journal issue | 5 |
Pages of publication | 1574 - 1577 |
a | 11.0309 ± 0.0003 Å |
b | 17.4337 ± 0.0005 Å |
c | 11.3811 ± 0.0003 Å |
α | 90° |
β | 111.847 ± 0.002° |
γ | 90° |
Cell volume | 2031.5 ± 0.1 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 2 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0592 |
Residual factor for significantly intense reflections | 0.0406 |
Weighted residual factors for significantly intense reflections | 0.0974 |
Weighted residual factors for all reflections included in the refinement | 0.1099 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.024 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
224003 (current) | 2019-11-07 | cif/ Updating files of 7048319, 7048320 Original log message: Adding full bibliography for 7048319--7048320.cif. |
7048320.cif |
212483 | 2018-12-08 | cif/ Adding structures of 7048319, 7048320 via cif-deposit CGI script. |
7048320.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.