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Information card for entry 7250678
Preview
| Coordinates | 7250678.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H22 N O2 P |
|---|---|
| Calculated formula | C24 H22 N O2 P |
| Title of publication | Photoinduced cobaloxime catalysis enabled dehydrogenative C2-phosphinylation of bicyclo[1.1.0]butanes to access phosphorylated cyclobutenes |
| Authors of publication | Chang, Yunong; Bian, Fangyu; Guo, Jiefei; Li, Miao-Miao; Ding, Wei |
| Journal of publication | RSC Advances |
| Year of publication | 2025 |
| Journal volume | 15 |
| Journal issue | 29 |
| Pages of publication | 24053 - 24057 |
| a | 11.5363 ± 0.0001 Å |
| b | 12.0675 ± 0.0001 Å |
| c | 14.5536 ± 0.0001 Å |
| α | 90° |
| β | 102.115 ± 0.001° |
| γ | 90° |
| Cell volume | 1980.95 ± 0.03 Å3 |
| Cell temperature | 100 ± 0.1 K |
| Ambient diffraction temperature | 100 ± 0.1 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0351 |
| Residual factor for significantly intense reflections | 0.033 |
| Weighted residual factors for significantly intense reflections | 0.0857 |
| Weighted residual factors for all reflections included in the refinement | 0.0874 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.036 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 301233 (current) | 2025-07-11 | cif/ Adding structures of 7250678 via cif-deposit CGI script. |
7250678.cif |
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