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Information card for entry 7250679
Preview
| Coordinates | 7250679.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C30 H34 Cl2 Hg N4 O S3 |
|---|---|
| Calculated formula | C30 H34 Cl2 Hg N4 O S3 |
| Title of publication | Beckmann rearrangement of ketoximes for accessing amides and lactams promoted by a perimidine-2-thione supported Hg(ii) complex: a mechanistic perception |
| Authors of publication | Velmurugan, Priyanka; Kanniyappan, Poovarasan; Ghatak, Tapas |
| Journal of publication | RSC Advances |
| Year of publication | 2025 |
| Journal volume | 15 |
| Journal issue | 30 |
| Pages of publication | 24317 - 24330 |
| a | 9.2166 ± 0.0007 Å |
| b | 13.6839 ± 0.0009 Å |
| c | 13.696 ± 0.0009 Å |
| α | 74.558 ± 0.002° |
| β | 76.599 ± 0.002° |
| γ | 79.748 ± 0.002° |
| Cell volume | 1607.14 ± 0.19 Å3 |
| Cell temperature | 300 ± 2 K |
| Ambient diffraction temperature | 300 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1196 |
| Residual factor for significantly intense reflections | 0.0602 |
| Weighted residual factors for significantly intense reflections | 0.1538 |
| Weighted residual factors for all reflections included in the refinement | 0.1822 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 301243 (current) | 2025-07-12 | cif/ Adding structures of 7250679 via cif-deposit CGI script. |
7250679.cif |
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Users of the data should acknowledge the original authors of the
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