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Information card for entry 7712581
Preview
| Coordinates | 7712581.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C40 H62 Cl4 O2 P2 Pd2 |
|---|---|
| Calculated formula | C40 H62 Cl4 O2 P2 Pd2 |
| Title of publication | Highly Efficient and Well-Defined Phosphinous Acid-Ligated Pd(II) Precatalysts for Hirao Cross-Coupling Reaction |
| Authors of publication | Hong, Li-Hui; Feng, Wei-Jung; Chen, Wei-Chih; Chang, Yu-Chang |
| Journal of publication | Dalton Transactions |
| Year of publication | 2023 |
| a | 11.7915 ± 0.0004 Å |
| b | 16.4016 ± 0.0005 Å |
| c | 12.2069 ± 0.0004 Å |
| α | 90° |
| β | 105.158 ± 0.0012° |
| γ | 90° |
| Cell volume | 2278.67 ± 0.13 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0281 |
| Residual factor for significantly intense reflections | 0.0245 |
| Weighted residual factors for significantly intense reflections | 0.0629 |
| Weighted residual factors for all reflections included in the refinement | 0.0668 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.032 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 281790 (current) | 2023-03-10 | cif/ Adding structures of 7712580, 7712581, 7712582 via cif-deposit CGI script. |
7712581.cif |
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Users of the data should acknowledge the original authors of the
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