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Information card for entry 7712582
Preview
| Coordinates | 7712582.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C26 H23 O P |
|---|---|
| Calculated formula | C26 H23 O P |
| Title of publication | Highly Efficient and Well-Defined Phosphinous Acid-Ligated Pd(II) Precatalysts for Hirao Cross-Coupling Reaction |
| Authors of publication | Hong, Li-Hui; Feng, Wei-Jung; Chen, Wei-Chih; Chang, Yu-Chang |
| Journal of publication | Dalton Transactions |
| Year of publication | 2023 |
| a | 9.3661 ± 0.0005 Å |
| b | 9.7124 ± 0.0005 Å |
| c | 11.4886 ± 0.0005 Å |
| α | 77.95 ± 0.002° |
| β | 88.078 ± 0.0019° |
| γ | 79.4227 ± 0.0018° |
| Cell volume | 1004.68 ± 0.09 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0753 |
| Residual factor for significantly intense reflections | 0.0628 |
| Weighted residual factors for significantly intense reflections | 0.1662 |
| Weighted residual factors for all reflections included in the refinement | 0.1795 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.046 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 281790 (current) | 2023-03-10 | cif/ Adding structures of 7712580, 7712581, 7712582 via cif-deposit CGI script. |
7712582.cif |
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Users of the data should acknowledge the original authors of the
structural data.