Crystallography Open Database

Information card for entry 7718250

Preview

Coordinates	7718250.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C60 H72 Ge2 K2 N10 O6
Calculated formula	C60 H72 Ge2 K2 N10 O6
Title of publication	Carbon-carbon bond formation and cleavage at redox active bis(pyridylimino)isoindole (BPI) germylene compounds.
Authors of publication	Nicasio, Antonio I.; Somerville, Rosie J.; Sahagún, Pablo; Soto, Enrique; López-Serrano, Joaquín; Campos, Jesús
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2025
Journal volume	54
Journal issue	7
Pages of publication	3039 - 3046
a	10.6413 ± 0.0011 Å
b	15.2209 ± 0.0019 Å
c	20.466 ± 0.002 Å
α	106.01 ± 0.005°
β	99.137 ± 0.005°
γ	95.273 ± 0.005°
Cell volume	3113.6 ± 0.6 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1579
Residual factor for significantly intense reflections	0.0853
Weighted residual factors for significantly intense reflections	0.1787
Weighted residual factors for all reflections included in the refinement	0.2228
Goodness-of-fit parameter for all reflections included in the refinement	1.052
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
297968 (current)	2025-03-04	cif/ Adding structures of 7718243, 7718244, 7718245, 7718246, 7718247, 7718248, 7718249, 7718250, 7718251, 7718252 via cif-deposit CGI script.	7718250.cif