Crystallography Open Database

Information card for entry 7718251

Preview

Coordinates	7718251.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H55 Ge2 K2 N10 O3
Calculated formula	C52 H55 Ge2 K2 N10 O3
Title of publication	Carbon-carbon bond formation and cleavage at redox active bis(pyridylimino)isoindole (BPI) germylene compounds.
Authors of publication	Nicasio, Antonio I.; Somerville, Rosie J.; Sahagún, Pablo; Soto, Enrique; López-Serrano, Joaquín; Campos, Jesús
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2025
Journal volume	54
Journal issue	7
Pages of publication	3039 - 3046
a	14.168 ± 0.0005 Å
b	16.0363 ± 0.0007 Å
c	23.4696 ± 0.0009 Å
α	90°
β	94.698 ± 0.001°
γ	90°
Cell volume	5314.4 ± 0.4 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0827
Residual factor for significantly intense reflections	0.0478
Weighted residual factors for significantly intense reflections	0.1344
Weighted residual factors for all reflections included in the refinement	0.1652
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
297968 (current)	2025-03-04	cif/ Adding structures of 7718243, 7718244, 7718245, 7718246, 7718247, 7718248, 7718249, 7718250, 7718251, 7718252 via cif-deposit CGI script.	7718251.cif