Crystallography Open Database

Information card for entry 7718252

Preview

Coordinates	7718252.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C64 H72 Ag2 F12 Ge2 N14 O8 S4 Si4
Calculated formula	C64 H72 Ag2 F12 Ge2 N14 O8 S4 Si4
Title of publication	Carbon-carbon bond formation and cleavage at redox active bis(pyridylimino)isoindole (BPI) germylene compounds.
Authors of publication	Nicasio, Antonio I.; Somerville, Rosie J.; Sahagún, Pablo; Soto, Enrique; López-Serrano, Joaquín; Campos, Jesús
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2025
Journal volume	54
Journal issue	7
Pages of publication	3039 - 3046
a	15.8097 ± 0.0014 Å
b	16.6796 ± 0.0015 Å
c	17.6314 ± 0.0015 Å
α	99.488 ± 0.004°
β	102.293 ± 0.004°
γ	109.977 ± 0.004°
Cell volume	4124.1 ± 0.7 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1665
Residual factor for significantly intense reflections	0.0926
Weighted residual factors for significantly intense reflections	0.2515
Weighted residual factors for all reflections included in the refinement	0.3394
Goodness-of-fit parameter for all reflections included in the refinement	1.1917
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
297968 (current)	2025-03-04	cif/ Adding structures of 7718243, 7718244, 7718245, 7718246, 7718247, 7718248, 7718249, 7718250, 7718251, 7718252 via cif-deposit CGI script.	7718252.cif